#------------------------------------------------------------------------------ #$Date: 2016-04-03 04:09:52 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181148 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/27/2222785.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2222785_Fobs loop_ _publ_author_name 'Mahmoudi, Ali' 'Dehghanpour, Saeed' 'Khalaj, Mehdi' 'Pakravan, Shabnam' _publ_section_title ; Di-\m-chlorido-bis({2-[(4-bromophenyl)iminomethyl]pyridine-\k^2^N,N'}chloridomercury(II)) ; _journal_coeditor_code LH2844 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m889 _journal_volume 65 _journal_year 2009 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 96.738 _cell_angle_gamma 90.000 _cell_length_a 7.6697 _cell_length_b 15.0247 _cell_length_c 12.2129 _exptl_crystal_F_000 976.00 _reflns_d_resolution_high 0.7108 _cod_data_source_file lh2844Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' s3 in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 351.34 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 8986.84 9042.83 193.98 o 4 0 0 22909.03 22419.60 405.58 o 6 0 0 21979.11 21989.69 408.93 o 8 0 0 4172.42 4392.92 171.10 o 10 0 0 931.51 845.28 114.80 o 2 1 0 1598.54 1732.01 44.95 o 3 1 0 22872.09 22113.25 279.61 o 4 1 0 4319.29 4373.25 70.33 o 5 1 0 26722.39 26427.14 338.76 o 6 1 0 5100.72 5011.57 89.09 o 7 1 0 1233.76 1342.78 47.82 o 8 1 0 1719.33 1777.85 56.65 o 9 1 0 10518.06 10443.37 205.81 o 10 1 0 1254.78 1326.92 65.90 o 0 2 0 37064.13 39088.96 580.44 o 1 2 0 46049.48 46925.97 700.81 o 2 2 0 4854.54 5164.87 79.75 o 3 2 0 2588.16 2600.80 46.15 o 4 2 0 9263.18 9200.28 129.30 o 5 2 0 15403.33 15606.31 209.76 o 6 2 0 11559.71 11390.58 161.68 o 7 2 0 6114.01 6008.48 99.23 o 8 2 0 6431.10 6645.41 124.61 o 9 2 0 147.62 199.45 37.65 o 10 2 0 343.91 282.98 43.52 o 1 3 0 257.28 241.66 11.90 o 2 3 0 18006.85 18734.15 238.45 o 3 3 0 30105.10 30486.47 383.24 o 4 3 0 6638.55 6310.85 96.26 o 5 3 0 4021.79 3957.64 69.63 o 6 3 0 6626.52 6482.75 103.42 o 7 3 0 2147.74 2137.68 52.32 o 8 3 0 1725.28 1737.29 56.83 o 9 3 0 1174.13 1092.94 57.84 o 10 3 0 4998.93 5186.20 130.65 o 0 4 0 1028.10 1031.95 48.69 o 1 4 0 59999.81 60641.67 740.08 o 2 4 0 5440.00 5646.97 89.46 o 3 4 0 88.14 171.19 34.00 o 4 4 0 14.92 47.51 15.89 o 5 4 0 23409.40 22831.79 298.68 o 6 4 0 487.68 556.51 27.59 o 7 4 0 14870.17 14727.80 206.76 o 8 4 0 581.49 649.62 51.66 o 9 4 0 31.29 21.73 35.21 o 10 4 0 15.48 22.75 40.46 o 2 5 0 58318.71 57986.89 712.58 o 3 5 0 7243.55 7595.87 123.36 o 4 5 0 21166.83 21002.35 276.05 o 5 5 0 1805.33 1820.07 46.09 o 6 5 0 397.19 421.29 37.82 o 7 5 0 1842.66 1877.37 51.14 o 8 5 0 4422.13 4352.30 95.65 o 9 5 0 1143.81 1167.89 59.69 o 10 5 0 6076.89 6153.27 164.62 o 0 6 0 62128.34 64641.04 1123.40 o 1 6 0 15235.82 15831.89 209.22 o 2 6 0 2010.75 2131.46 44.09 o 3 6 0 14042.15 14184.21 192.51 o 4 6 0 7277.23 7420.54 113.52 o 5 6 0 14847.97 14650.35 203.90 o 6 6 0 6133.49 6140.86 103.21 o 7 6 0 12142.85 12209.90 178.51 o 8 6 0 443.02 550.51 44.21 o 9 6 0 399.30 372.33 58.28 o 10 6 0 388.96 382.81 77.55 o 1 7 0 4124.02 4216.16 95.64 o 2 7 0 50414.96 49994.01 622.05 o 3 7 0 15650.46 15829.16 214.31 o 4 7 0 12549.57 12790.13 180.05 o 5 7 0 4420.60 4410.81 80.86 o 6 7 0 1957.18 2063.73 54.01 o 7 7 0 584.87 677.01 34.75 o 8 7 0 1295.50 1344.46 61.28 o 9 7 0 2828.89 2848.95 104.48 o 10 7 0 1776.55 1849.78 238.22 o 0 8 0 19017.17 19212.81 359.85 o 1 8 0 573.99 671.20 38.17 o 2 8 0 15955.36 16050.03 218.62 o 3 8 0 7940.61 7969.03 121.57 o 4 8 0 308.04 321.54 24.14 o 5 8 0 3957.87 4199.04 87.34 o 6 8 0 13603.96 13663.98 227.83 o 7 8 0 3704.18 3676.51 76.99 o 8 8 0 4289.83 4494.28 113.91 o 9 8 0 147.13 149.07 65.36 o 1 9 0 8236.34 8244.35 126.08 o 2 9 0 3856.70 4064.73 76.37 o 3 9 0 67657.51 65109.12 809.96 o 4 9 0 1857.19 1901.96 94.69 o 5 9 0 6075.66 6092.83 111.16 o 6 9 0 251.49 258.49 27.20 o 7 9 0 4048.86 4207.07 119.41 o 8 9 0 513.36 487.20 61.09 o 9 9 0 3287.27 2940.23 346.67 o 0 10 0 12686.14 12898.10 260.39 o 1 10 0 980.31 1015.21 36.93 o 2 10 0 12513.77 12415.20 179.27 o 3 10 0 6.31 41.37 21.46 o 4 10 0 7115.43 7121.77 150.88 o 5 10 0 221.00 237.98 27.00 o 6 10 0 10735.69 10821.11 181.43 o 7 10 0 771.03 850.76 52.39 o 8 10 0 6573.60 6858.23 239.07 o 9 10 0 300.65 378.68 80.00 o 1 11 0 3775.82 3984.58 78.57 o 2 11 0 6767.94 6600.95 110.69 o 3 11 0 36894.13 36621.15 473.08 o 4 11 0 11178.64 11247.35 169.69 o 5 11 0 4624.15 4699.09 100.24 o 6 11 0 718.88 793.77 77.53 o 7 11 0 3793.33 3926.93 157.91 o 8 11 0 1226.20 1300.12 86.73 o 9 11 0 2471.74 2594.68 148.76 o 0 12 0 17966.50 17647.69 347.20 o 1 12 0 5125.93 5358.20 97.57 o 2 12 0 761.43 774.28 37.02 o 3 12 0 4603.07 4585.07 92.55 o 4 12 0 257.04 302.63 30.95 o 5 12 0 2804.48 2771.83 88.04 o 6 12 0 1607.25 1632.46 93.46 o 7 12 0 5002.42 4905.50 125.33 o 8 12 0 989.85 989.66 133.98 o 1 13 0 9.43 47.71 24.81 o 2 13 0 17961.67 18425.40 257.19 o 3 13 0 117.50 152.60 27.88 o 4 13 0 14453.54 13725.03 253.47 o 5 13 0 4075.85 4103.62 111.45 o 6 13 0 362.26 418.12 46.50 o 7 13 0 635.08 664.45 53.85 o 8 13 0 2537.71 2592.36 214.61 o 0 14 0 11539.56 11516.33 248.91 o 1 14 0 12773.40 12777.33 191.30 o 2 14 0 1017.85 1113.50 48.50 o 3 14 0 157.78 203.69 33.37 o 4 14 0 1548.43 1687.89 73.12 o 5 14 0 6596.38 6538.65 150.16 o 6 14 0 49.20 -11.96 47.33 o 7 14 0 3995.73 4084.16 117.40 o 8 14 0 7.87 9.64 55.37 o 1 15 0 732.61 898.92 42.96 o 2 15 0 11944.10 11821.21 216.93 o 3 15 0 4810.40 4816.63 124.12 o 4 15 0 10716.78 10445.25 209.94 o 5 15 0 20.63 15.94 36.99 o 6 15 0 875.87 989.48 63.59 o 7 15 0 171.82 211.05 47.64 o 0 16 0 1957.82 2172.03 91.85 o 1 16 0 10584.42 11030.70 194.69 o 2 16 0 2564.56 2627.50 91.62 o 3 16 0 238.33 298.47 52.26 o 4 16 0 171.73 224.82 44.80 o 5 16 0 4882.91 4860.58 129.47 o 6 16 0 3298.71 3281.05 106.16 o 7 16 0 4197.15 4232.60 123.70 o 1 17 0 4015.51 3939.45 100.23 o 2 17 0 3132.03 3266.53 138.05 o 3 17 0 7425.67 7089.37 162.55 o 4 17 0 653.99 717.14 59.10 o 5 17 0 2589.35 2620.83 97.26 o 6 17 0 1094.73 1131.12 69.97 o 0 18 0 14082.57 14275.12 390.79 o 1 18 0 1933.08 1990.42 98.52 o 2 18 0 2075.84 2072.53 83.61 o 3 18 0 5.43 31.62 41.89 o 4 18 0 1397.61 1493.44 76.29 o 5 18 0 1252.80 1246.35 71.94 o 1 19 0 2625.16 2759.69 116.33 o 2 19 0 117.65 210.11 58.60 o 3 19 0 4069.51 4179.39 122.37 o 4 19 0 416.34 505.53 57.13 o 0 20 0 18032.38 19032.18 689.31 o 1 20 0 2251.46 2232.43 127.35 o 2 20 0 1237.74 1329.62 89.10 o 3 20 0 335.26 391.78 90.04 o 1 21 0 1102.11 1191.98 167.02 o -9 0 1 9233.46 9208.37 321.15 o -7 0 1 14060.66 14228.08 289.10 o -5 0 1 1168.62 1152.10 44.43 o -3 0 1 52013.14 51131.07 1077.65 o -1 0 1 86548.05 83688.16 2073.19 o 3 0 1 57415.20 56730.86 1321.06 o 5 0 1 30242.52 30284.10 544.22 o 7 0 1 319.66 333.25 36.29 o 9 0 1 1159.47 1137.55 81.68 o -10 1 1 2573.27 2744.89 91.81 o -9 1 1 44.11 62.73 35.24 o -8 1 1 1962.16 2096.57 74.34 o -7 1 1 63.71 80.72 18.28 o -6 1 1 9340.34 9238.79 151.31 o -5 1 1 164.11 168.78 24.29 o -4 1 1 23437.28 22977.41 293.71 o -3 1 1 151.71 206.69 27.28 o -2 1 1 400.23 416.55 15.55 o -1 1 1 79.68 110.03 7.05 o 0 1 1 26582.63 27676.17 280.59 o 1 1 1 4530.20 4736.71 59.68 o 2 1 1 15909.42 15451.03 196.89 o 3 1 1 6178.48 6195.02 89.15 o 4 1 1 24863.21 24560.01 313.42 o 5 1 1 1011.37 1064.24 37.71 o 6 1 1 8252.62 7943.14 120.36 o 7 1 1 2766.74 2887.35 62.51 o 8 1 1 15542.96 15446.15 265.99 o 9 1 1 819.49 852.45 52.82 o 10 1 1 296.40 251.48 43.84 o -10 2 1 311.57 350.84 46.14 o -9 2 1 5651.90 5753.50 136.94 o -8 2 1 3839.07 3853.24 102.80 o -7 2 1 10495.39 10184.33 149.27 o -6 2 1 11145.38 11096.65 157.99 o -5 2 1 195.01 234.63 17.73 o -3 2 1 25355.56 25549.20 382.92 o -2 2 1 117591.69 112407.87 2183.02 o -1 2 1 65375.80 63503.61 774.41 o 0 2 1 21006.11 21936.61 236.90 o 2 2 1 18146.96 18550.31 303.58 o 3 2 1 38836.29 38964.63 482.92 o 4 2 1 4360.12 4108.35 69.04 o 5 2 1 17754.64 17234.82 229.31 o 6 2 1 3900.97 3838.88 79.87 o 7 2 1 90.63 91.10 21.91 o 8 2 1 1404.87 1299.25 44.41 o 9 2 1 1050.19 1123.05 58.53 o 10 2 1 838.41 858.10 69.21 o -10 3 1 350.80 356.29 46.66 o -9 3 1 542.95 599.31 102.39 o -8 3 1 298.63 323.95 49.89 o -7 3 1 12360.34 12107.53 173.72 o -6 3 1 3798.11 3786.97 69.20 o -5 3 1 8367.29 8296.64 122.28 o -4 3 1 27544.46 27525.07 351.10 o -3 3 1 2686.55 2671.29 48.41 o -1 3 1 187.31 210.89 32.99 o 0 3 1 39048.11 40025.13 452.98 o 1 3 1 20083.12 21040.97 285.39 o 2 3 1 13867.08 14549.44 188.65 o 3 3 1 32299.68 32066.25 401.72 o 4 3 1 118.20 180.03 18.88 o 5 3 1 89.59 139.10 24.85 o 6 3 1 1892.95 1829.99 51.74 o 7 3 1 17434.39 16816.70 231.35 o 8 3 1 4778.37 4607.74 85.92 o 9 3 1 4561.18 4607.02 116.84 o 10 3 1 177.46 311.11 49.34 o -10 4 1 2128.25 2268.12 84.19 o -9 4 1 557.30 624.51 49.85 o -8 4 1 12553.52 12345.30 285.31 o -7 4 1 539.61 585.92 28.94 o -6 4 1 12059.21 11765.35 167.88 o -5 4 1 4209.31 4173.14 73.43 o -4 4 1 4682.63 4893.40 80.67 o -3 4 1 534.38 535.37 22.86 o -2 4 1 123437.71 117677.66 1426.05 o -1 4 1 608.19 681.84 21.14 o 0 4 1 11879.12 12157.60 158.99 o 1 4 1 29499.47 30672.41 351.55 o 2 4 1 13111.38 13969.67 183.55 o 3 4 1 539.55 512.50 26.68 o 4 4 1 45724.98 46386.41 578.18 o 5 4 1 1776.92 1811.82 44.67 o 6 4 1 15319.62 15325.41 211.11 o 7 4 1 1084.39 1077.06 38.61 o 8 4 1 300.15 301.19 32.82 o 9 4 1 257.10 271.32 42.70 o 10 4 1 3912.47 4325.46 209.79 o -10 5 1 135.64 154.04 45.62 o -9 5 1 2396.78 2638.91 88.88 o -8 5 1 3002.79 2839.72 88.70 o -7 5 1 4754.03 4882.83 87.67 o -6 5 1 32.73 28.82 23.98 o -5 5 1 28252.21 27958.37 362.15 o -4 5 1 1347.40 1303.20 36.81 o -3 5 1 20984.43 21694.22 281.11 o -2 5 1 115.86 129.42 13.99 o -1 5 1 2273.54 2353.70 44.67 o 1 5 1 92804.09 90445.68 1215.96 o 2 5 1 291.76 344.13 17.55 o 3 5 1 31715.23 32552.62 411.41 o 4 5 1 7930.76 7822.19 117.14 o 5 5 1 4843.69 4860.28 83.33 o 6 5 1 134.80 156.21 22.26 o 7 5 1 9065.37 8942.31 137.89 o 8 5 1 302.71 357.24 29.34 o 9 5 1 4609.68 4605.37 133.53 o 10 5 1 65.33 -0.24 57.43 o -10 6 1 1929.51 2066.26 92.93 o -9 6 1 1343.55 1366.73 91.45 o -8 6 1 5792.01 6054.80 143.32 o -7 6 1 2342.14 2329.08 57.26 o -6 6 1 2965.20 3074.82 65.16 o -5 6 1 766.26 688.77 38.05 o -4 6 1 9695.45 9586.29 140.24 o -3 6 1 15917.36 16417.88 219.17 o -2 6 1 32367.91 32948.56 415.14 o -1 6 1 23386.70 24027.25 308.03 o 1 6 1 3959.99 4189.17 68.82 o 2 6 1 15.36 116.73 33.12 o 3 6 1 5237.36 5584.87 161.63 o 4 6 1 19083.84 18816.74 268.20 o 5 6 1 5378.24 5262.30 98.35 o 6 6 1 17761.85 17951.81 245.47 o 7 6 1 4.48 44.49 24.39 o 8 6 1 498.09 511.42 34.99 o 9 6 1 727.80 784.32 87.77 o 10 6 1 6039.24 6437.11 227.48 o -10 7 1 872.39 945.25 96.03 o -9 7 1 2666.34 2676.60 101.56 o -8 7 1 100.49 135.66 36.49 o -7 7 1 1611.49 1642.51 49.25 o -6 7 1 5726.05 5595.30 98.89 o -5 7 1 28070.48 27347.66 358.18 o -4 7 1 10067.00 9846.42 144.93 o -3 7 1 6523.66 6492.35 102.24 o -2 7 1 135.15 169.01 19.20 o -1 7 1 3847.73 3907.15 68.89 o 0 7 1 21805.21 22761.59 294.19 o 1 7 1 61714.81 61840.62 762.52 o 2 7 1 14074.09 14014.25 191.17 o 3 7 1 7969.81 8166.48 121.60 o 4 7 1 1960.24 1913.28 46.30 o 5 7 1 9877.22 9975.25 148.38 o 6 7 1 2142.94 2149.71 55.09 o 7 7 1 1345.41 1384.59 46.25 o 8 7 1 5492.27 5426.71 108.45 o 9 7 1 1149.92 1356.61 128.60 o 10 7 1 373.59 377.12 79.50 o -9 8 1 5363.09 5578.06 156.00 o -8 8 1 403.45 474.90 71.61 o -7 8 1 7269.73 7207.12 121.62 o -6 8 1 715.68 780.07 41.12 o -5 8 1 1204.93 1330.03 42.61 o -4 8 1 688.52 712.93 31.09 o -3 8 1 17282.76 17184.38 232.95 o -2 8 1 640.37 724.84 47.91 o -1 8 1 19191.46 19823.38 263.18 o 0 8 1 105.10 178.62 19.31 o 1 8 1 5221.21 5100.15 85.65 o 2 8 1 885.51 1013.47 34.91 o 3 8 1 17996.34 18088.46 243.45 o 4 8 1 3427.45 3563.47 68.89 o 5 8 1 15639.87 15741.32 219.70 o 6 8 1 5451.85 5364.10 95.90 o 7 8 1 1670.38 1644.90 55.78 o 8 8 1 364.38 283.01 39.19 o 9 8 1 1952.05 2005.57 124.53 o -9 9 1 573.97 637.04 124.51 o -8 9 1 836.80 1001.36 64.56 o -7 9 1 256.53 295.43 29.73 o -6 9 1 12341.68 12584.30 202.26 o -5 9 1 1854.39 1722.38 60.28 o -4 9 1 36840.38 36187.74 465.64 o -3 9 1 763.47 804.51 35.20 o -2 9 1 37.46 75.41 24.61 o -1 9 1 86.05 95.54 26.17 o 0 9 1 39559.22 39565.28 501.26 o 1 9 1 3005.25 3082.34 70.19 o 2 9 1 37289.09 37251.70 474.55 o 3 9 1 270.66 480.05 92.81 o 4 9 1 1224.39 1166.66 39.39 o 5 9 1 2868.22 2810.94 63.00 o 6 9 1 5229.87 5091.82 102.80 o 7 9 1 14.86 9.59 34.34 o 8 9 1 6145.80 5970.52 138.28 o 9 9 1 0.54 31.32 61.95 o -9 10 1 4721.56 4901.35 421.84 o -8 10 1 1133.17 1144.89 186.80 o -7 10 1 7388.21 7616.87 150.39 o -6 10 1 67.97 74.87 24.62 o -5 10 1 3043.29 3163.11 71.07 o -4 10 1 669.76 740.60 35.07 o -3 10 1 3654.14 3682.31 75.03 o -2 10 1 83.90 68.66 21.78 o -1 10 1 12123.46 12142.58 175.19 o 0 10 1 1315.07 1288.71 40.83 o 1 10 1 18820.39 19211.85 259.35 o 2 10 1 127.93 134.31 21.92 o 3 10 1 12226.08 12189.64 177.18 o 4 10 1 2435.20 2559.86 60.25 o 5 10 1 17108.88 17260.69 263.75 o 6 10 1 265.06 285.82 39.94 o 7 10 1 2138.56 2175.00 79.19 o 8 10 1 10.10 -8.69 49.28 o 9 10 1 1361.40 1311.93 110.35 o -9 11 1 329.16 452.11 85.29 o -8 11 1 470.33 493.74 79.14 o -7 11 1 16.17 19.88 32.85 o -6 11 1 9474.65 9701.67 168.61 o -5 11 1 9668.92 9860.85 155.06 o -4 11 1 22638.54 22076.57 326.61 o -3 11 1 11395.76 11309.20 170.11 o -2 11 1 117.15 138.97 24.42 o -1 11 1 3645.57 3595.65 73.95 o 0 11 1 25542.41 26044.00 343.99 o 1 11 1 10847.64 10841.25 160.64 o 2 11 1 23835.39 23995.15 319.47 o 3 11 1 754.43 801.48 39.92 o 4 11 1 219.89 295.12 38.79 o 5 11 1 474.47 588.75 47.00 o 6 11 1 5477.52 5293.25 129.46 o 7 11 1 508.13 466.31 56.22 o 8 11 1 5826.29 5623.95 172.75 o 9 11 1 1055.10 1105.35 192.36 o -8 12 1 3472.91 3673.30 396.32 o -7 12 1 2485.43 2447.62 85.44 o -6 12 1 498.48 480.78 45.80 o -5 12 1 7.35 24.13 25.33 o -4 12 1 2487.88 2564.34 66.31 o -3 12 1 6557.52 6631.68 123.85 o -2 12 1 3478.61 3665.23 78.22 o -1 12 1 11186.23 10982.60 165.97 o 0 12 1 7249.21 7473.70 122.75 o 1 12 1 1581.89 1691.09 53.76 o 2 12 1 48.13 53.14 22.38 o 3 12 1 7941.02 7752.99 141.65 o 4 12 1 15234.54 14880.20 270.56 o 5 12 1 4498.80 4556.40 130.61 o 6 12 1 5388.94 5185.49 165.74 o 7 12 1 65.22 79.34 38.65 o 8 12 1 335.61 389.50 65.66 o -8 13 1 146.22 177.07 70.44 o -7 13 1 1754.80 1840.90 75.82 o -6 13 1 563.30 651.01 51.28 o -5 13 1 22722.19 21859.02 374.91 o -4 13 1 3731.70 3680.52 81.66 o -3 13 1 4941.37 4907.16 95.35 o -2 13 1 20.51 72.19 29.99 o -1 13 1 5809.82 5860.66 105.97 o 0 13 1 2410.43 2356.48 62.37 o 1 13 1 32212.04 32081.80 492.79 o 2 13 1 282.35 342.09 29.67 o 3 13 1 8965.66 8764.36 180.72 o 4 13 1 3361.08 3385.62 101.21 o 5 13 1 3124.61 2972.50 104.22 o 6 13 1 1019.85 917.11 58.81 o 7 13 1 4301.18 4116.52 157.47 o 8 13 1 1925.83 2177.14 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