#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/28/2222825.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2222825_Fobs loop_ _publ_author_name 'Fun, Hoong-Kun' 'Loh, Wan-Sin' 'Rai, Sankappa' 'Shetty, Prakash' 'Isloor, Arun M.' _publ_section_title ; 5-Azido-4-benzyloxy-2-methoxy-6-methylperhydropyran-3-ol ; _journal_coeditor_code NG2616 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1972 _journal_volume 65 _journal_year 2009 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 4.6662 _cell_length_b 15.3356 _cell_length_c 20.9273 _exptl_crystal_F_000 624.00 _reflns_d_resolution_high 0.8107 _[local]_cod_data_source_file ng2616Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' sr2_0m in P2(1)2(1)2(1) (100K)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 149.88 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 13.56 13.42 12.91 o 4 0 0 678.25 646.66 26.53 o 1 1 0 22463.57 21546.44 258.22 o 2 1 0 458.83 454.77 16.18 o 3 1 0 263.45 261.29 13.40 o 4 1 0 43.18 47.30 10.83 o 5 1 0 332.86 343.84 13.97 o 0 2 0 1632.76 1720.36 58.25 o 1 2 0 8315.07 8023.54 82.60 o 2 2 0 83.87 102.83 7.24 o 3 2 0 75.40 68.15 9.36 o 4 2 0 9.84 -8.24 5.75 o 5 2 0 24.18 52.60 9.79 o 1 3 0 0.14 -5.56 4.24 o 2 3 0 14.84 17.59 5.53 o 3 3 0 1.51 -2.60 5.83 o 4 3 0 154.96 151.47 11.53 o 5 3 0 153.63 163.61 12.50 o 0 4 0 3740.14 3610.31 55.05 o 1 4 0 330.90 342.90 13.13 o 2 4 0 35.76 34.61 5.81 o 3 4 0 0.82 -5.47 5.26 o 4 4 0 1.40 5.39 7.05 o 5 4 0 0.52 0.95 10.79 o 1 5 0 1803.40 1673.53 28.05 o 2 5 0 2712.48 2725.59 34.63 o 3 5 0 147.43 153.73 10.63 o 4 5 0 6.00 7.56 7.46 o 5 5 0 1.88 15.72 15.51 o 0 6 0 4633.02 4581.68 70.98 o 1 6 0 139.55 124.93 7.10 o 2 6 0 268.58 266.22 12.45 o 3 6 0 373.22 367.64 14.69 o 4 6 0 215.40 242.04 15.46 o 5 6 0 53.49 69.52 14.39 o 1 7 0 1746.14 1724.83 24.62 o 2 7 0 1.02 -11.74 7.03 o 3 7 0 241.99 249.60 15.22 o 4 7 0 65.86 75.15 13.37 o 5 7 0 44.79 44.09 14.50 o 0 8 0 431.57 408.52 18.51 o 1 8 0 1608.59 1601.48 27.83 o 2 8 0 715.69 693.01 21.59 o 3 8 0 10.69 7.49 10.68 o 4 8 0 349.98 362.58 21.10 o 5 8 0 51.27 73.66 16.92 o 1 9 0 534.08 548.48 15.12 o 2 9 0 1404.17 1231.30 29.16 o 3 9 0 0.29 -2.09 10.20 o 4 9 0 6.47 25.81 12.07 o 5 9 0 13.09 -1.53 12.96 o 0 10 0 103.93 102.16 14.86 o 1 10 0 16.13 3.26 8.21 o 2 10 0 653.91 595.86 22.55 o 3 10 0 965.63 849.82 26.71 o 4 10 0 5.77 5.91 21.09 o 1 11 0 202.94 181.13 21.86 o 2 11 0 690.79 652.99 24.48 o 3 11 0 6.57 5.78 15.56 o 4 11 0 250.06 281.92 22.94 o 0 12 0 20.73 -1.50 13.49 o 1 12 0 27.83 9.80 11.85 o 2 12 0 143.88 165.64 16.59 o 3 12 0 302.62 307.17 22.25 o 4 12 0 23.16 84.20 29.60 o 1 13 0 9.89 13.85 12.53 o 2 13 0 0.04 4.50 11.77 o 3 13 0 0.30 5.02 13.02 o 4 13 0 22.70 14.20 16.06 o 0 14 0 177.09 136.90 28.81 o 1 14 0 133.02 134.86 16.15 o 2 14 0 136.99 158.43 25.55 o 3 14 0 14.25 29.82 18.97 o 1 15 0 27.53 40.40 13.51 o 2 15 0 3.06 21.71 14.34 o 3 15 0 13.45 29.31 28.02 o 0 16 0 32.92 4.81 24.03 o 1 16 0 11.72 32.42 17.39 o 2 16 0 0.00 35.12 14.66 o 3 16 0 53.37 66.82 19.28 o 1 17 0 5.28 17.49 17.00 o 2 17 0 4.68 39.76 57.41 o 0 18 0 97.25 64.94 27.95 o 1 18 0 12.64 45.87 19.28 o 1 0 1 4327.16 4265.45 56.53 o 2 0 1 689.01 672.06 17.55 o 3 0 1 276.18 314.27 12.52 o 4 0 1 302.44 321.61 15.57 o 5 0 1 9.61 14.46 9.70 o 1 1 1 5208.60 5028.46 48.53 o 2 1 1 244.63 249.27 7.35 o 3 1 1 640.88 574.18 12.06 o 4 1 1 53.64 63.23 6.91 o 5 1 1 24.79 30.12 7.68 o 1 2 1 4147.60 4021.05 30.87 o 2 2 1 551.77 555.82 10.27 o 3 2 1 147.93 168.37 7.70 o 4 2 1 168.78 171.89 7.85 o 5 2 1 46.93 53.24 6.46 o 0 3 1 1104.59 1034.63 33.02 o 1 3 1 6522.83 6340.06 46.53 o 2 3 1 67.49 69.63 4.75 o 3 3 1 18.20 17.44 4.72 o 4 3 1 186.66 180.79 8.09 o 5 3 1 169.73 184.83 9.25 o 0 4 1 8267.84 8028.28 79.16 o 1 4 1 1360.12 1289.20 15.03 o 2 4 1 212.80 228.37 7.02 o 3 4 1 61.88 59.05 5.79 o 4 4 1 380.38 387.68 10.48 o 5 4 1 31.97 23.72 7.26 o 0 5 1 1450.75 1348.43 19.46 o 1 5 1 670.17 612.01 11.14 o 2 5 1 161.99 171.15 7.20 o 3 5 1 421.10 406.86 10.21 o 4 5 1 0.80 2.69 4.92 o 5 5 1 18.16 25.21 7.13 o 0 6 1 2131.51 2088.29 27.46 o 1 6 1 919.53 823.09 12.30 o 2 6 1 155.59 158.67 7.62 o 3 6 1 106.76 94.10 7.39 o 4 6 1 235.64 226.78 10.27 o 5 6 1 88.13 109.12 11.42 o 0 7 1 6518.02 6673.55 70.58 o 1 7 1 496.64 492.40 12.25 o 2 7 1 160.44 168.56 8.35 o 3 7 1 137.63 142.10 9.45 o 4 7 1 67.74 71.69 9.01 o 5 7 1 9.45 18.20 8.82 o 0 8 1 49.32 49.10 6.86 o 1 8 1 2781.88 2629.61 26.68 o 2 8 1 271.58 266.31 10.79 o 3 8 1 943.77 878.29 17.93 o 4 8 1 32.63 29.11 8.88 o 5 8 1 6.03 9.37 9.29 o 0 9 1 1159.68 1272.24 22.90 o 1 9 1 1056.56 1034.50 16.79 o 2 9 1 189.58 189.95 10.46 o 3 9 1 277.11 255.27 13.03 o 4 9 1 176.83 197.28 16.53 o 5 9 1 60.03 73.60 13.40 o 0 10 1 34.90 42.58 8.58 o 1 10 1 379.99 332.56 11.39 o 2 10 1 118.10 121.88 10.12 o 3 10 1 142.76 148.24 11.50 o 4 10 1 141.19 152.63 15.67 o 0 11 1 760.66 772.89 20.00 o 1 11 1 85.25 72.99 9.81 o 2 11 1 946.24 829.86 18.80 o 3 11 1 120.08 119.22 11.16 o 4 11 1 21.20 36.98 13.34 o 0 12 1 160.34 198.43 22.15 o 1 12 1 161.80 154.76 12.31 o 2 12 1 82.38 74.92 9.99 o 3 12 1 101.31 105.65 15.18 o 4 12 1 78.74 128.37 21.95 o 0 13 1 370.55 362.61 20.26 o 1 13 1 577.46 543.98 16.26 o 2 13 1 101.50 93.01 10.57 o 3 13 1 33.50 45.23 10.88 o 4 13 1 62.07 90.54 19.89 o 0 14 1 0.60 5.57 15.52 o 1 14 1 255.26 242.91 15.03 o 2 14 1 85.10 87.56 11.28 o 3 14 1 83.84 109.80 20.76 o 0 15 1 27.97 10.69 16.27 o 1 15 1 4.31 27.46 11.04 o 2 15 1 204.64 218.60 17.91 o 3 15 1 74.07 114.03 24.62 o 0 16 1 2.04 15.46 17.13 o 1 16 1 47.82 42.46 13.41 o 2 16 1 197.19 258.89 25.78 o 3 16 1 29.43 86.53 28.31 o 0 17 1 111.40 145.28 22.18 o 1 17 1 26.55 49.69 13.82 o 2 17 1 35.81 72.64 28.83 o 0 18 1 22.65 15.05 22.83 o 1 18 1 33.78 45.21 14.17 o 0 0 2 3616.96 3757.18 67.24 o 1 0 2 5271.47 5271.81 63.29 o 2 0 2 1545.79 1538.74 23.43 o 3 0 2 671.89 667.76 17.32 o 4 0 2 14.92 0.24 6.69 o 5 0 2 1.23 -9.16 9.17 o 0 1 2 1832.18 1974.64 29.09 o 1 1 2 1869.34 1784.63 17.55 o 2 1 2 237.28 243.74 7.09 o 3 1 2 225.19 250.83 8.26 o 4 1 2 473.72 466.79 12.20 o 5 1 2 19.71 24.87 5.63 o 0 2 2 5862.18 6001.98 153.53 o 1 2 2 1456.49 1459.57 15.37 o 2 2 2 6281.92 6243.59 47.90 o 3 2 2 893.93 897.30 13.97 o 4 2 2 143.25 134.56 7.43 o 5 2 2 101.43 108.06 9.91 o 0 3 2 446.03 438.65 18.15 o 1 3 2 4616.36 4520.33 43.37 o 2 3 2 357.86 342.14 7.22 o 3 3 2 1708.44 1663.00 19.10 o 4 3 2 230.69 221.74 8.92 o 5 3 2 102.06 118.81 9.06 o 0 4 2 1.26 -5.10 9.86 o 1 4 2 135.25 140.20 7.14 o 2 4 2 1056.74 987.56 12.45 o 3 4 2 71.47 73.48 5.70 o 4 4 2 232.98 249.02 9.28 o 5 4 2 6.25 35.98 8.41 o 0 5 2 0.37 -4.84 3.68 o 1 5 2 262.89 249.45 7.39 o 2 5 2 603.09 544.81 10.85 o 3 5 2 309.95 318.03 9.03 o 4 5 2 68.61 65.66 7.20 o 5 5 2 19.67 16.22 8.03 o 0 6 2 141.35 157.03 8.62 o 1 6 2 34.89 33.14 4.79 o 2 6 2 191.12 183.90 7.05 o 3 6 2 93.50 101.58 6.77 o 4 6 2 51.68 56.92 7.37 o 5 6 2 77.95 72.42 11.53 o 0 7 2 2297.97 2329.96 31.02 o 1 7 2 239.53 232.89 7.77 o 2 7 2 323.21 323.47 10.32 o 3 7 2 82.86 78.53 8.40 o 4 7 2 156.02 168.34 10.67 o 5 7 2 20.93 43.71 13.47 o 0 8 2 596.84 618.84 15.07 o 1 8 2 1966.87 1945.06 23.17 o 2 8 2 1399.90 1285.39 25.73 o 3 8 2 132.58 141.81 10.39 o 4 8 2 12.38 17.31 8.21 o 5 8 2 78.24 55.16 12.02 o 0 9 2 1457.22 1395.25 27.02 o 1 9 2 1022.55 958.12 16.52 o 2 9 2 266.40 259.91 11.32 o 3 9 2 822.86 729.63 18.97 o 4 9 2 11.29 -0.37 8.09 o 5 9 2 0.64 10.48 11.35 o 0 10 2 751.45 754.79 25.48 o 1 10 2 117.57 130.78 8.03 o 2 10 2 31.91 22.25 8.26 o 3 10 2 119.88 122.44 11.02 o 4 10 2 158.86 162.12 20.98 o 0 11 2 26.80 12.32 8.90 o 1 11 2 322.43 301.03 11.28 o 2 11 2 118.75 115.19 10.43 o 3 11 2 187.56 184.29 12.57 o 4 11 2 85.00 103.28 16.02 o 0 12 2 59.87 48.36 10.43 o 1 12 2 61.77 37.36 7.43 o 2 12 2 340.28 321.52 16.61 o 3 12 2 108.19 111.20 12.37 o 4 12 2 9.08 31.45 14.39 o 0 13 2 208.95 196.41 17.29 o 1 13 2 0.31 -4.71 8.95 o 2 13 2 315.27 324.14 15.66 o 3 13 2 32.25 56.72 14.19 o 4 13 2 20.06 42.12 17.65 o 0 14 2 353.96 332.04 24.80 o 1 14 2 386.31 385.29 15.12 o 2 14 2 94.83 106.41 11.41 o 3 14 2 52.11 68.16 19.82 o 0 15 2 8.44 14.14 16.17 o 1 15 2 46.62 50.18 11.33 o 2 15 2 222.30 251.75 27.85 o 3 15 2 5.08 27.18 24.23 o 0 16 2 111.21 185.67 26.40 o 1 16 2 32.00 19.51 16.35 o 2 16 2 28.70 50.67 16.56 o 3 16 2 10.52 66.00 19.75 o 0 17 2 30.55 39.87 18.63 o 1 17 2 41.78 28.06 13.33 o 2 17 2 0.60 18.22 12.06 o 0 18 2 0.38 50.16 19.25 o 1 18 2 2.04 3.51 19.04 o 1 0 3 2.74 -1.59 4.30 o 2 0 3 2102.01 2009.24 28.17 o 3 0 3 656.74 653.44 17.18 o 4 0 3 102.30 87.32 10.19 o 5 0 3 0.00 6.03 10.67 o 0 1 3 3728.35 3851.79 77.86 o 1 1 3 9238.49 8803.65 67.63 o 2 1 3 1698.37 1761.46 18.20 o 3 1 3 291.89 294.77 8.79 o 4 1 3 58.34 56.16 6.50 o 5 1 3 118.53 121.85 18.58 o 0 2 3 1947.89 2074.39 29.62 o 1 2 3 2645.22 2473.18 22.25 o 2 2 3 148.23 163.79 5.73 o 3 2 3 692.89 701.13 12.20 o 4 2 3 192.62 191.31 8.40 o 5 2 3 3.71 6.43 6.74 o 0 3 3 1214.49 1211.34 23.07 o 1 3 3 258.25 271.65 7.87 o 2 3 3 161.54 175.19 5.78 o 3 3 3 62.48 71.56 5.47 o 4 3 3 163.29 151.57 8.09 o 5 3 3 52.75 49.80 11.31 o 0 4 3 635.90 617.44 13.62 o 1 4 3 1023.32 1011.64 12.22 o 2 4 3 678.61 664.64 10.65 o 3 4 3 16.54 6.88 4.13 o 4 4 3 29.00 25.30 5.66 o 5 4 3 168.18 175.04 12.07 o 0 5 3 3042.53 2986.11 52.05 o 1 5 3 217.76 211.79 6.98 o 2 5 3 375.01 377.33 8.46 o 3 5 3 67.41 68.91 5.97 o 4 5 3 152.73 172.75 9.71 o 5 5 3 80.50 114.69 15.41 o 0 6 3 756.63 784.74 24.84 o 1 6 3 684.41 660.89 11.60 o 2 6 3 479.17 470.86 10.75 o 3 6 3 190.64 195.16 8.60 o 4 6 3 49.69 43.08 7.31 o 5 6 3 6.61 22.55 10.89 o 0 7 3 1024.23 1198.46 21.55 o 1 7 3 64.16 66.89 6.03 o 2 7 3 118.96 116.92 7.48 o 3 7 3 478.43 444.31 14.08 o 4 7 3 74.85 92.19 10.53 o 5 7 3 34.20 41.98 16.77 o 0 8 3 179.91 211.90 9.98 o 1 8 3 357.31 391.60 10.98 o 2 8 3 405.18 401.19 10.90 o 3 8 3 234.39 232.49 11.87 o 4 8 3 117.27 124.54 10.88 o 5 8 3 13.70 12.32 9.88 o 0 9 3 12.30 3.79 6.32 o 1 9 3 69.65 83.63 7.63 o 2 9 3 825.22 804.16 17.62 o 3 9 3 657.34 590.79 16.36 o 4 9 3 3.42 13.18 8.10 o 5 9 3 4.08 0.44 16.78 o 0 10 3 0.00 -1.12 7.75 o 1 10 3 109.46 107.80 8.11 o 2 10 3 528.24 487.60 14.88 o 3 10 3 446.43 455.23 15.64 o 4 10 3 5.83 13.84 8.98 o 0 11 3 10.73 -0.76 8.26 o 1 11 3 395.22 375.11 12.19 o 2 11 3 41.50 34.79 8.83 o 3 11 3 139.47 136.43 11.74 o 4 11 3 85.95 79.69 11.65 o 0 12 3 652.94 591.08 23.93 o 1 12 3 218.71 215.58 12.16 o 2 12 3 22.93 21.00 8.83 o 3 12 3 57.03 58.75 10.40 o 4 12 3 35.19 69.79 20.35 o 0 13 3 859.20 796.51 26.86 o 1 13 3 339.91 338.81 15.47 o 2 13 3 19.13 29.13 9.21 o 3 13 3 10.77 11.43 14.26 o 4 13 3 60.14 113.07 23.38 o 0 14 3 0.75 9.73 16.31 o 1 14 3 97.26 103.78 11.68 o 2 14 3 127.57 116.01 12.56 o 3 14 3 7.10 18.41 14.80 o 0 15 3 4.58 18.33 15.79 o 1 15 3 470.89 436.24 22.61 o 2 15 3 27.12 54.17 14.07 o 3 15 3 45.12 59.80 20.24 o 0 16 3 18.28 53.10 18.87 o 1 16 3 165.64 177.27 19.54 o 2 16 3 9.18 19.72 11.26 o 0 17 3 102.98 93.07 20.18 o 1 17 3 11.89 41.62 14.54 o 2 17 3 32.41 52.37 13.60 o 0 18 3 90.60 107.30 21.52 o 1 18 3 37.27 60.17 14.86 o 0 0 4 1532.90 1424.10 31.76 o 1 0 4 876.06 800.15 19.18 o 2 0 4 777.56 723.34 14.92 o 3 0 4 36.55 32.26 6.74 o 4 0 4 170.05 189.47 12.55 o 5 0 4 16.95 12.42 12.75 o 0 1 4 1408.51 1397.40 22.49 o 1 1 4 2048.62 2014.98 19.04 o 2 1 4 243.83 254.12 6.69 o 3 1 4 246.01 245.15 8.12 o 4 1 4 93.67 98.43 7.28 o 5 1 4 9.02 17.39 8.60 o 0 2 4 841.92 847.12 14.96 o 1 2 4 130.17 119.77 5.53 o 2 2 4 199.16 189.53 5.82 o 3 2 4 226.83 248.08 7.73 o 4 2 4 222.69 202.93 9.25 o 5 2 4 64.37 48.11 9.31 o 0 3 4 1.09 -1.07 4.37 o 1 3 4 1134.44 1020.73 16.16 o 2 3 4 2944.55 2947.25 25.58 o 3 3 4 377.41 370.83 9.00 o 4 3 4 84.59 99.40 7.25 o 5 3 4 187.68 180.47 19.58 o 0 4 4 703.77 689.76 14.62 o 1 4 4 4181.80 4179.25 51.82 o 2 4 4 506.95 497.75 8.74 o 3 4 4 478.48 454.91 10.15 o 4 4 4 151.64 158.78 8.37 o 5 4 4 7.79 17.25 10.41 o 0 5 4 7.17 -2.67 5.66 o 1 5 4 2422.04 2394.99 24.65 o 2 5 4 62.66 74.11 4.87 o 3 5 4 641.53 587.24 12.20 o 4 5 4 244.15 240.25 10.68 o 5 5 4 40.55 35.16 10.39 o 0 6 4 1614.45 1738.37 28.76 o 1 6 4 193.59 231.16 7.99 o 2 6 4 345.26 345.70 9.29 o 3 6 4 101.44 95.16 8.55 o 4 6 4 294.34 315.52 13.61 o 5 6 4 188.72 219.49 26.40 o 0 7 4 29.81 25.22 6.11 o 1 7 4 468.86 463.61 10.81 o 2 7 4 61.41 63.34 6.73 o 3 7 4 423.66 386.06 13.30 o 4 7 4 191.03 212.53 11.33 o 5 7 4 101.01 118.47 16.71 o 0 8 4 591.44 497.06 37.11 o 1 8 4 37.30 36.17 6.11 o 2 8 4 270.23 289.66 10.55 o 3 8 4 64.82 65.83 10.11 o 4 8 4 298.65 296.09 14.87 o 5 8 4 8.27 10.92 10.97 o 0 9 4 14.77 3.23 6.69 o 1 9 4 171.31 184.75 8.23 o 2 9 4 63.95 54.99 7.94 o 3 9 4 32.60 28.60 8.56 o 4 9 4 55.47 55.50 9.59 o 0 10 4 465.33 445.85 16.15 o 1 10 4 240.89 260.43 11.20 o 2 10 4 53.31 42.71 8.69 o 3 10 4 21.93 14.38 7.48 o 4 10 4 50.82 68.20 14.02 o 0 11 4 324.18 336.56 14.55 o 1 11 4 283.66 298.99 11.61 o 2 11 4 332.62 341.87 14.71 o 3 11 4 134.64 131.62 14.51 o 4 11 4 75.24 85.34 16.87 o 0 12 4 220.57 203.04 17.86 o 1 12 4 117.46 119.17 10.78 o 2 12 4 8.57 13.96 8.60 o 3 12 4 117.77 131.43 12.29 o 4 12 4 31.69 58.66 22.27 o 0 13 4 9.44 -0.27 13.12 o 1 13 4 357.06 335.34 14.09 o 2 13 4 177.18 164.71 12.51 o 3 13 4 39.70 62.60 10.81 o 4 13 4 197.88 189.83 19.89 o 0 14 4 0.07 7.24 12.39 o 1 14 4 52.62 53.26 7.62 o 2 14 4 133.25 135.31 12.47 o 3 14 4 120.63 129.83 19.84 o 0 15 4 124.80 113.81 30.23 o 1 15 4 2.81 16.74 8.91 o 2 15 4 44.99 57.57 9.80 o 3 15 4 16.76 25.74 12.05 o 0 16 4 190.22 186.07 25.37 o 1 16 4 11.35 31.73 11.92 o 2 16 4 7.00 12.48 10.79 o 0 17 4 255.62 259.16 25.75 o 1 17 4 0.31 17.94 14.96 o 2 17 4 28.57 39.56 14.18 o 0 18 4 0.17 2.97 17.57 o 1 18 4 151.64 182.79 20.77 o 1 0 5 451.44 412.42 11.59 o 2 0 5 516.23 551.05 13.76 o 3 0 5 869.87 908.83 19.96 o 4 0 5 12.68 21.11 7.38 o 5 0 5 78.38 109.86 17.30 o 0 1 5 904.08 870.27 18.64 o 1 1 5 568.38 571.80 8.78 o 2 1 5 600.75 633.70 9.53 o 3 1 5 63.95 66.95 5.47 o 4 1 5 323.37 332.45 10.25 o 5 1 5 55.54 68.97 11.14 o 0 2 5 10.84 8.74 5.15 o 1 2 5 548.54 537.99 10.00 o 2 2 5 107.39 105.16 4.51 o 3 2 5 370.49 374.28 9.09 o 4 2 5 68.22 73.42 8.05 o 5 2 5 17.59 26.86 8.72 o 0 3 5 3779.78 3846.83 59.50 o 1 3 5 972.69 994.50 12.83 o 2 3 5 88.07 85.35 5.79 o 3 3 5 295.83 301.19 8.24 o 4 3 5 163.53 169.92 9.71 o 5 3 5 213.89 231.13 17.09 o 0 4 5 41.67 45.76 5.44 o 1 4 5 2037.56 2095.10 25.80 o 2 4 5 981.92 997.38 14.29 o 3 4 5 253.09 249.42 7.82 o 4 4 5 57.95 65.67 7.62 o 5 4 5 216.85 215.70 19.92 o 0 5 5 196.45 213.82 10.09 o 1 5 5 737.66 737.07 14.16 o 2 5 5 1983.02 1905.11 19.92 o 3 5 5 136.18 143.07 8.06 o 4 5 5 680.10 698.74 18.58 o 5 5 5 76.90 101.08 21.64 o 0 6 5 324.77 332.19 12.17 o 1 6 5 17.23 12.62 4.86 o 2 6 5 326.43 308.56 9.79 o 3 6 5 83.89 84.01 8.43 o 4 6 5 120.48 120.81 10.74 o 5 6 5 128.65 149.24 18.99 o 0 7 5 523.19 552.71 17.44 o 1 7 5 125.46 130.99 7.33 o 2 7 5 121.74 122.75 7.89 o 3 7 5 579.68 502.87 14.73 o 4 7 5 22.08 24.18 8.25 o 5 7 5 24.35 24.50 10.88 o 0 8 5 8.63 18.93 8.60 o 1 8 5 109.68 125.51 7.79 o 2 8 5 180.60 197.00 9.54 o 3 8 5 110.81 119.49 10.84 o 4 8 5 13.68 17.51 8.00 o 5 8 5 20.86 12.01 14.33 o 0 9 5 110.12 104.44 10.84 o 1 9 5 135.02 144.88 9.31 o 2 9 5 18.52 13.24 7.37 o 3 9 5 6.47 -10.63 7.65 o 4 9 5 38.24 47.34 10.12 o 0 10 5 35.53 49.70 9.00 o 1 10 5 482.63 439.89 12.45 o 2 10 5 304.30 295.99 12.09 o 3 10 5 179.63 138.59 11.07 o 4 10 5 144.56 141.43 18.21 o 0 11 5 72.24 67.03 10.50 o 1 11 5 349.50 312.02 11.74 o 2 11 5 126.92 130.55 11.42 o 3 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14.10 o 2 9 20 84.07 78.04 14.73 o 0 10 20 0.49 -7.10 20.95 o 1 10 20 44.09 32.79 18.12 o 0 11 20 3.02 1.21 22.07 o 1 11 20 59.33 26.23 18.43 o 1 0 21 137.77 142.62 14.03 o 2 0 21 62.33 67.24 13.69 o 3 0 21 168.01 170.28 17.52 o 0 1 21 166.09 131.02 19.13 o 1 1 21 62.48 53.61 8.18 o 2 1 21 80.70 81.40 9.88 o 3 1 21 5.47 17.34 10.03 o 0 2 21 72.13 66.68 17.21 o 1 2 21 20.07 11.22 7.61 o 2 2 21 15.70 8.34 8.57 o 3 2 21 111.62 108.03 14.23 o 0 3 21 6.60 -12.66 16.23 o 1 3 21 118.02 116.57 10.42 o 2 3 21 35.59 31.43 9.17 o 3 3 21 90.28 78.60 13.65 o 0 4 21 16.53 32.10 17.50 o 1 4 21 66.24 58.40 10.63 o 2 4 21 37.31 22.42 9.85 o 3 4 21 15.11 14.59 11.71 o 0 5 21 9.85 22.61 18.10 o 1 5 21 67.08 55.59 11.94 o 2 5 21 50.56 39.91 11.77 o 0 6 21 0.17 30.20 23.37 o 1 6 21 45.51 34.40 12.89 o 2 6 21 14.22 20.77 10.85 o 0 7 21 43.90 36.89 18.21 o 1 7 21 6.78 -22.15 11.59 o 2 7 21 81.23 81.76 14.63 o 0 8 21 1.09 -23.62 23.12 o 1 8 21 31.80 61.08 17.98 o 2 8 21 11.15 -2.37 11.71 o 0 9 21 10.09 3.78 25.29 o 1 9 21 42.74 49.35 18.07 o 0 10 21 3.86 -30.89 43.49 o 1 10 21 28.29 31.29 18.52 o 0 11 21 12.22 -20.06 27.05 o 0 0 22 12.14 12.54 22.22 o 1 0 22 34.07 39.12 18.40 o 2 0 22 38.61 59.78 14.03 o 3 0 22 47.29 55.44 14.32 o 0 1 22 47.04 50.33 16.82 o 1 1 22 41.35 53.35 13.56 o 2 1 22 0.55 -11.84 7.73 o 0 2 22 1.11 0.80 17.38 o 1 2 22 14.38 9.06 9.69 o 2 2 22 95.19 97.86 11.40 o 0 3 22 67.72 39.93 19.11 o 1 3 22 3.58 1.36 9.17 o 2 3 22 6.82 2.13 8.62 o 0 4 22 8.11 20.95 18.53 o 1 4 22 11.06 5.06 10.66 o 2 4 22 14.28 13.89 10.04 o 0 5 22 0.95 -20.74 16.04 o 1 5 22 14.41 6.36 11.02 o 2 5 22 43.17 34.82 11.74 o 0 6 22 0.51 -22.86 18.92 o 1 6 22 39.24 25.69 13.80 o 2 6 22 4.51 1.94 12.29 o 0 7 22 8.20 10.49 17.53 o 1 7 22 10.03 7.50 13.23 o 2 7 22 20.90 7.87 12.75 o 0 8 22 0.30 1.56 26.29 o 1 8 22 2.00 -3.81 15.66 o 0 9 22 2.03 3.14 26.69 o 1 9 22 11.90 -8.27 16.93 o 1 0 23 4.72 -8.07 16.67 o 2 0 23 34.37 41.50 12.95 o 0 1 23 2.93 18.00 17.59 o 1 1 23 26.08 23.11 12.84 o 2 1 23 5.32 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