#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/28/2222826.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2222826_Fobs loop_ _publ_author_name 'Zhi, Y.-X.' 'Long, J.' 'Chen, J.-Y.' 'Ren, Y.-T.' _publ_section_title ; 3,3'-(2,2'-Bi-1H-imidazole-1,1'-diyl)dipropanamide ; _journal_coeditor_code NG2617 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2008 _journal_volume 65 _journal_year 2009 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 93.377 _cell_angle_gamma 90.000 _cell_length_a 18.4450 _cell_length_b 4.8622 _cell_length_c 13.4457 _exptl_crystal_F_000 584.00 _reflns_d_resolution_high 0.7703 _[local]_cod_data_source_file ng2617Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' C12H16N6O2 in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 252.45 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 7702.67 7920.01 63.79 o 6 0 0 5331.46 5416.10 54.28 o 8 0 0 2760.44 3060.57 25.73 o 10 0 0 2975.00 3164.21 29.88 o 12 0 0 254.77 366.55 5.14 o 14 0 0 2829.85 2913.49 23.84 o 16 0 0 7796.00 7681.61 62.84 o 18 0 0 181.14 161.04 6.71 o 20 0 0 1070.73 1106.96 11.78 o 22 0 0 1598.02 1775.95 16.87 o 1 1 0 3760.90 3340.13 38.66 o 3 1 0 1827.05 1650.68 8.76 o 5 1 0 727.29 803.65 4.44 o 7 1 0 0.02 1.90 1.13 o 9 1 0 489.03 565.19 4.26 o 11 1 0 16.52 9.70 1.97 o 13 1 0 316.76 292.66 4.12 o 15 1 0 942.81 861.25 7.59 o 17 1 0 222.30 230.21 4.62 o 19 1 0 339.90 349.63 4.65 o 21 1 0 31.67 28.48 4.04 o 23 1 0 336.10 371.28 6.28 o 0 2 0 1627.12 1807.91 20.70 o 2 2 0 690.69 787.72 5.54 o 4 2 0 189.78 203.49 2.38 o 6 2 0 1599.86 1678.85 8.81 o 8 2 0 1295.16 1298.01 7.99 o 10 2 0 104.87 127.47 2.73 o 12 2 0 407.58 412.83 4.68 o 14 2 0 61.19 48.50 3.51 o 16 2 0 44.69 23.71 2.79 o 18 2 0 183.45 188.83 4.38 o 20 2 0 120.53 141.43 4.44 o 22 2 0 114.51 100.24 5.64 o 1 3 0 981.79 1156.33 7.61 o 3 3 0 490.50 522.64 4.48 o 5 3 0 485.37 521.58 4.66 o 7 3 0 1007.83 1033.58 6.63 o 9 3 0 3066.80 3184.81 17.95 o 11 3 0 515.04 524.77 4.47 o 13 3 0 0.32 -0.11 1.47 o 15 3 0 664.38 661.54 8.43 o 17 3 0 176.04 226.86 8.55 o 19 3 0 752.22 750.72 9.76 o 21 3 0 53.56 59.56 13.20 o 0 4 0 151.34 130.34 4.01 o 2 4 0 724.25 663.43 5.58 o 4 4 0 859.10 839.04 7.71 o 6 4 0 333.07 353.46 4.59 o 8 4 0 60.67 66.26 2.88 o 10 4 0 10.49 10.35 2.19 o 12 4 0 831.09 857.10 6.90 o 14 4 0 25.85 31.05 2.59 o 16 4 0 583.12 719.15 7.98 o 18 4 0 403.50 461.97 24.73 o 1 5 0 0.47 0.52 1.96 o 3 5 0 136.63 133.13 3.10 o 5 5 0 19.96 25.32 2.78 o 7 5 0 78.03 74.12 3.11 o 9 5 0 225.44 246.91 3.64 o 11 5 0 2.02 3.09 2.46 o 13 5 0 2.83 8.20 4.88 o 0 6 0 0.29 3.08 3.16 o 2 6 0 86.26 93.89 4.14 o 4 6 0 9.94 6.91 3.41 o 6 6 0 327.18 332.64 5.48 o -23 1 1 51.69 98.44 4.87 o -21 1 1 18.87 17.54 3.31 o -19 1 1 4.45 5.11 3.22 o -17 1 1 54.44 64.57 3.53 o -15 1 1 2264.95 2211.84 14.21 o -13 1 1 13.28 11.79 2.22 o -11 1 1 1557.67 1520.97 9.58 o -9 1 1 5666.91 5692.62 30.93 o -7 1 1 171.30 634.29 4.42 o -5 1 1 138.15 335.60 3.16 o -3 1 1 2266.99 2152.71 12.51 o -1 1 1 4355.06 4548.26 27.14 o 1 1 1 837.37 805.66 5.27 o 3 1 1 599.11 635.30 4.60 o 5 1 1 3688.51 3762.13 26.76 o 7 1 1 7797.20 7966.84 53.75 o 9 1 1 121.35 472.32 4.17 o 11 1 1 1292.45 1378.18 8.43 o 13 1 1 127.40 120.01 3.11 o 15 1 1 179.75 253.41 4.15 o 17 1 1 43.89 36.18 3.19 o 19 1 1 300.86 280.94 4.80 o 21 1 1 57.43 66.30 3.72 o 23 1 1 453.81 526.66 6.28 o -22 2 1 35.68 43.75 5.03 o -20 2 1 78.21 85.45 4.52 o -18 2 1 33.23 66.76 3.99 o -16 2 1 494.63 450.37 12.26 o -14 2 1 185.45 268.47 5.49 o -12 2 1 252.70 270.92 4.66 o -10 2 1 41.45 30.01 3.12 o -8 2 1 1931.30 1923.30 11.00 o -6 2 1 737.15 732.40 4.56 o -4 2 1 1207.98 1126.15 7.10 o -2 2 1 5370.61 5316.43 30.95 o 0 2 1 532.34 593.24 4.23 o 2 2 1 440.47 761.47 4.33 o 4 2 1 293.12 402.66 3.62 o 6 2 1 169.79 216.54 2.33 o 8 2 1 69.45 196.19 3.28 o 10 2 1 3.20 4.58 2.38 o 12 2 1 798.98 810.36 6.22 o 14 2 1 1999.34 2019.57 12.41 o 16 2 1 270.21 257.29 4.32 o 18 2 1 343.02 337.89 4.96 o 20 2 1 31.79 51.84 3.59 o 22 2 1 137.44 154.83 4.65 o -21 3 1 732.58 843.88 11.56 o -19 3 1 319.57 339.85 6.26 o -17 3 1 0.25 4.89 3.61 o -15 3 1 305.66 244.85 5.27 o -13 3 1 336.00 322.35 4.21 o -11 3 1 381.27 402.02 4.09 o -9 3 1 1981.62 1860.70 11.85 o -7 3 1 554.66 611.62 5.19 o -5 3 1 1014.73 1134.66 8.27 o -3 3 1 424.24 402.44 3.85 o -1 3 1 1037.47 1139.88 7.85 o 1 3 1 1789.46 1988.64 12.67 o 3 3 1 7.80 29.20 1.72 o 5 3 1 862.12 808.54 6.08 o 7 3 1 2478.39 2432.00 13.38 o 9 3 1 243.73 318.80 3.78 o 11 3 1 2.20 22.85 5.60 o 13 3 1 782.41 747.17 5.66 o 15 3 1 23.25 48.81 3.25 o 17 3 1 115.08 108.08 4.22 o 19 3 1 0.83 4.73 3.44 o -18 4 1 6.05 3.46 3.57 o -16 4 1 71.92 125.47 4.65 o -14 4 1 0.71 5.68 3.43 o -12 4 1 264.09 250.54 4.14 o -10 4 1 141.00 155.48 3.61 o -8 4 1 529.33 558.86 5.47 o -6 4 1 842.09 763.73 6.98 o -4 4 1 36.56 133.22 3.41 o -2 4 1 72.28 97.22 2.82 o 0 4 1 70.40 47.71 2.76 o 2 4 1 361.80 335.71 3.93 o 4 4 1 1644.61 1650.72 11.84 o 6 4 1 29.79 79.41 3.97 o 8 4 1 426.79 444.45 4.19 o 10 4 1 219.13 237.48 3.44 o 12 4 1 22.58 34.78 4.03 o 14 4 1 39.35 27.15 2.23 o 16 4 1 694.12 773.28 10.85 o 18 4 1 2.17 -0.01 5.63 o -13 5 1 1055.40 1148.44 12.35 o -11 5 1 96.18 95.32 4.00 o -9 5 1 127.96 118.51 3.48 o -7 5 1 417.43 449.12 5.82 o -5 5 1 1143.31 1139.81 10.23 o -3 5 1 9.20 137.40 3.29 o -1 5 1 30.80 83.43 2.96 o 1 5 1 984.49 895.41 6.74 o 3 5 1 2180.06 2095.17 23.73 o 5 5 1 902.59 954.11 9.23 o 7 5 1 863.91 853.38 7.96 o 9 5 1 26.80 25.54 2.48 o 11 5 1 24.02 17.06 4.91 o 13 5 1 92.71 156.10 7.82 o -6 6 1 747.01 735.72 7.77 o -4 6 1 289.34 308.37 5.28 o -2 6 1 2.06 1.67 2.91 o 0 6 1 456.24 477.79 5.28 o 2 6 1 26.56 33.78 5.96 o 4 6 1 1.23 6.54 3.90 o 6 6 1 101.99 154.84 6.75 o -22 0 2 164.73 156.61 7.37 o -20 0 2 1293.84 1206.41 13.42 o -18 0 2 102.56 93.64 5.44 o -16 0 2 727.22 643.16 8.67 o -14 0 2 361.37 361.58 8.69 o -12 0 2 4835.24 4546.12 40.07 o -10 0 2 50.67 275.01 5.53 o -8 0 2 68.40 55.35 3.14 o -6 0 2 11.79 3.49 2.36 o -4 0 2 13686.53 13892.20 117.74 o -2 0 2 590.20 660.34 59.09 o 0 0 2 4684.07 4726.57 28.83 o 2 0 2 2593.57 2348.04 12.63 o 4 0 2 3888.79 4884.56 55.43 o 6 0 2 120.23 131.31 3.73 o 8 0 2 125.47 180.36 3.00 o 10 0 2 4727.69 4783.29 33.03 o 12 0 2 7.88 236.76 9.49 o 14 0 2 436.39 397.28 6.41 o 16 0 2 503.03 487.50 10.69 o 18 0 2 15.05 6.80 4.73 o 20 0 2 154.32 197.24 6.97 o 22 0 2 37.11 55.01 5.10 o -23 1 2 5.56 2.77 3.46 o -21 1 2 60.84 87.30 4.53 o -19 1 2 99.49 88.39 3.80 o -17 1 2 2318.62 2227.86 14.35 o -15 1 2 247.80 221.70 3.95 o -13 1 2 37.13 47.37 3.09 o -11 1 2 1714.24 1742.88 10.81 o -9 1 2 130.85 139.65 2.37 o -7 1 2 4266.93 4527.23 42.31 o -5 1 2 252.86 330.84 13.58 o -3 1 2 5236.10 5166.34 29.02 o -1 1 2 24603.54 23466.67 428.68 o 1 1 2 11361.76 10917.50 56.22 o 3 1 2 191.52 481.68 5.76 o 5 1 2 2482.58 2385.93 11.74 o 7 1 2 4940.19 5215.73 30.13 o 9 1 2 21.66 28.01 2.77 o 11 1 2 727.92 832.80 6.76 o 13 1 2 259.57 244.29 3.62 o 15 1 2 0.24 2.67 2.97 o 17 1 2 1273.04 1230.82 8.57 o 19 1 2 43.36 55.52 3.43 o 21 1 2 378.31 395.67 5.21 o 23 1 2 12.02 9.28 3.50 o -22 2 2 238.27 248.08 7.63 o -20 2 2 40.58 33.78 4.70 o -18 2 2 3.40 23.92 10.76 o -16 2 2 974.42 1010.93 9.15 o -14 2 2 88.01 74.57 3.96 o -12 2 2 443.05 469.97 6.07 o -10 2 2 162.93 135.09 3.51 o -8 2 2 1552.79 1688.73 10.42 o -6 2 2 960.81 974.54 5.30 o -4 2 2 1.98 101.10 7.91 o -2 2 2 1066.28 1147.37 7.68 o 0 2 2 1354.80 1468.95 8.80 o 2 2 2 0.81 66.20 3.38 o 4 2 2 1882.98 1832.01 9.58 o 6 2 2 161.99 208.04 5.85 o 8 2 2 2198.45 2429.05 13.45 o 10 2 2 50.72 45.94 2.19 o 12 2 2 17.70 20.42 6.03 o 14 2 2 52.58 45.75 2.34 o 16 2 2 2490.59 2466.84 15.91 o 18 2 2 691.98 724.67 7.89 o 20 2 2 85.00 72.37 3.68 o 22 2 2 46.35 55.33 3.60 o -21 3 2 473.64 542.72 11.25 o -19 3 2 483.84 490.53 7.15 o -17 3 2 283.87 351.48 5.76 o -15 3 2 369.11 363.24 6.68 o -13 3 2 441.05 427.00 4.77 o -11 3 2 0.11 24.76 7.73 o -9 3 2 609.58 570.42 4.80 o -7 3 2 1101.30 1125.95 7.21 o -5 3 2 271.25 312.13 4.60 o -3 3 2 156.34 167.96 2.73 o -1 3 2 7.54 14.07 1.61 o 1 3 2 9.64 13.87 1.42 o 3 3 2 82.00 100.00 1.81 o 5 3 2 24.76 34.39 3.41 o 7 3 2 136.90 180.38 2.66 o 9 3 2 9.00 35.68 8.60 o 11 3 2 622.81 587.39 7.05 o 13 3 2 0.28 -1.62 1.62 o 15 3 2 5.19 1.37 1.93 o 17 3 2 48.74 35.42 4.29 o 19 3 2 46.39 84.78 6.43 o -18 4 2 67.69 77.46 4.63 o -16 4 2 33.39 36.07 4.42 o -14 4 2 285.06 261.84 4.30 o -12 4 2 438.36 470.80 5.27 o -10 4 2 120.07 115.06 2.97 o -8 4 2 4902.79 4923.65 28.77 o -6 4 2 403.31 418.09 6.74 o -4 4 2 15.40 15.16 2.42 o -2 4 2 681.79 600.73 4.79 o 0 4 2 61.26 57.23 3.55 o 2 4 2 73.47 81.70 7.18 o 4 4 2 224.33 216.38 3.35 o 6 4 2 211.24 216.24 3.06 o 8 4 2 4509.01 4559.38 25.63 o 10 4 2 32.76 34.70 1.63 o 12 4 2 330.04 356.79 6.13 o 14 4 2 406.46 387.93 8.84 o 16 4 2 16.23 12.21 7.11 o 18 4 2 2.38 -0.61 16.58 o -13 5 2 143.77 152.15 4.03 o -11 5 2 1.01 2.62 2.62 o -9 5 2 0.06 1.89 2.83 o -7 5 2 35.26 60.18 3.63 o -5 5 2 41.88 55.79 3.60 o -3 5 2 39.86 57.82 4.04 o -1 5 2 31.77 25.06 3.49 o 1 5 2 139.02 135.35 3.44 o 3 5 2 39.54 46.53 3.15 o 5 5 2 110.87 105.91 3.21 o 7 5 2 383.99 390.51 4.74 o 9 5 2 151.31 149.58 5.78 o 11 5 2 164.01 156.91 9.26 o 13 5 2 583.64 586.76 12.40 o -6 6 2 10.79 15.75 4.39 o -4 6 2 31.13 57.84 7.27 o -2 6 2 123.55 164.90 17.33 o 0 6 2 151.19 151.72 4.14 o 2 6 2 1205.78 1187.06 11.63 o 4 6 2 355.14 364.97 7.44 o 6 6 2 72.12 53.77 5.89 o -23 1 3 21.21 32.89 4.53 o -21 1 3 1010.40 1060.67 10.36 o -19 1 3 0.68 0.28 2.33 o -17 1 3 53.16 66.51 4.17 o -15 1 3 1108.78 1079.60 9.07 o -13 1 3 978.70 953.99 7.47 o -11 1 3 410.58 407.08 9.44 o -9 1 3 68.97 68.06 3.57 o -7 1 3 1590.31 1545.74 10.16 o -5 1 3 18731.90 19106.88 145.78 o -3 1 3 6592.51 6494.29 54.37 o -1 1 3 9593.48 9618.58 56.45 o 1 1 3 608.53 594.75 4.62 o 3 1 3 1058.29 928.48 7.18 o 5 1 3 86.02 82.31 2.04 o 7 1 3 21.99 12.92 1.50 o 9 1 3 3750.86 3883.90 18.96 o 11 1 3 1792.73 1693.76 9.98 o 13 1 3 263.48 270.01 4.95 o 15 1 3 3386.26 3234.04 17.99 o 17 1 3 68.14 47.99 3.46 o 19 1 3 57.57 54.45 3.37 o 21 1 3 0.35 -0.53 2.79 o 23 1 3 12.51 12.76 5.22 o -22 2 3 26.09 27.66 4.77 o -20 2 3 11.93 7.52 3.61 o -18 2 3 60.74 51.75 5.00 o -16 2 3 52.13 67.41 4.21 o -14 2 3 23.90 31.28 3.14 o -12 2 3 225.83 196.77 4.34 o -10 2 3 1274.35 1229.39 9.79 o -8 2 3 476.66 553.98 16.88 o -6 2 3 399.73 451.25 3.90 o -4 2 3 185.43 175.48 6.30 o -2 2 3 1549.95 1564.18 10.29 o 0 2 3 446.55 366.30 4.70 o 2 2 3 487.92 534.01 16.47 o 4 2 3 1609.62 1736.01 13.36 o 6 2 3 491.65 515.62 4.78 o 8 2 3 2269.88 2294.48 13.87 o 10 2 3 40.01 30.66 5.69 o 12 2 3 64.14 47.74 1.98 o 14 2 3 44.51 62.13 2.50 o 16 2 3 2.69 1.02 2.00 o 18 2 3 219.00 221.35 3.88 o 20 2 3 228.62 251.88 5.15 o 22 2 3 3.21 3.11 4.18 o -19 3 3 84.14 72.34 4.45 o -17 3 3 1.30 1.53 2.91 o -15 3 3 178.96 214.14 4.34 o -13 3 3 1.36 3.21 2.09 o -11 3 3 196.12 233.04 17.69 o -9 3 3 375.33 328.94 3.89 o -7 3 3 271.40 306.33 15.34 o -5 3 3 1803.29 1667.91 15.53 o -3 3 3 244.91 234.97 5.50 o -1 3 3 8.47 4.06 1.68 o 1 3 3 8.73 4.55 1.44 o 3 3 3 661.70 616.06 4.60 o 5 3 3 1482.89 1493.27 8.45 o 7 3 3 1035.56 1008.77 8.96 o 9 3 3 14.12 10.24 1.03 o 11 3 3 2493.73 2443.67 26.78 o 13 3 3 3.94 3.44 1.90 o 15 3 3 53.46 34.71 2.65 o 17 3 3 164.28 143.30 14.43 o 19 3 3 128.54 143.32 7.12 o -18 4 3 24.84 21.06 3.97 o -16 4 3 59.24 80.58 4.78 o -14 4 3 699.63 691.12 9.54 o -12 4 3 27.95 36.02 4.40 o -10 4 3 0.45 0.79 2.24 o -8 4 3 1236.42 1162.15 8.42 o -6 4 3 63.74 79.20 11.17 o -4 4 3 283.00 287.41 9.98 o -2 4 3 127.99 144.22 16.33 o 0 4 3 48.36 77.51 4.34 o 2 4 3 1242.14 1262.71 9.62 o 4 4 3 535.19 518.53 5.58 o 6 4 3 1013.74 948.51 6.62 o 8 4 3 311.37 335.17 5.92 o 10 4 3 465.42 456.60 6.76 o 12 4 3 133.80 144.98 4.48 o 14 4 3 519.49 491.03 9.95 o 16 4 3 62.85 67.62 7.44 o -13 5 3 134.44 146.91 4.27 o -11 5 3 0.09 2.08 2.69 o -9 5 3 117.26 108.26 3.30 o -7 5 3 126.26 130.20 4.13 o -5 5 3 1.28 1.63 2.45 o -3 5 3 585.22 531.43 5.88 o -1 5 3 1706.47 1593.38 10.50 o 1 5 3 59.85 52.90 2.79 o 3 5 3 149.69 142.24 3.62 o 5 5 3 63.77 68.50 3.75 o 7 5 3 96.40 96.88 6.90 o 9 5 3 8.09 9.68 4.87 o 11 5 3 0.89 3.23 4.33 o 13 5 3 316.76 307.25 8.20 o -6 6 3 0.18 16.29 9.04 o -4 6 3 10.59 17.50 3.43 o -2 6 3 0.48 -1.66 2.26 o 0 6 3 172.17 179.07 4.32 o 2 6 3 144.08 132.96 7.16 o 4 6 3 396.75 420.47 8.15 o -22 0 4 1407.93 1442.82 19.47 o -20 0 4 1142.76 1148.68 14.82 o -18 0 4 125.06 122.11 5.00 o -16 0 4 4469.49 4287.61 40.47 o -14 0 4 3586.55 3447.61 32.45 o -12 0 4 205.61 212.94 5.95 o -10 0 4 792.89 694.34 8.69 o -8 0 4 791.86 709.99 8.16 o -6 0 4 2923.20 2802.46 23.47 o -4 0 4 7466.65 7183.07 59.25 o -2 0 4 1950.45 1887.08 22.01 o 0 0 4 63731.13 64112.59 624.71 o 2 0 4 13362.77 13163.96 95.37 o 4 0 4 362.04 322.78 3.07 o 6 0 4 4177.60 4483.02 30.07 o 8 0 4 134.65 86.04 2.43 o 10 0 4 31.38 20.54 2.53 o 12 0 4 642.12 593.06 6.93 o 14 0 4 1545.92 1363.08 13.46 o 16 0 4 2656.61 2519.47 21.72 o 18 0 4 1024.16 1009.37 11.29 o 20 0 4 50.86 58.27 4.87 o 22 0 4 1277.12 1365.84 14.02 o -23 1 4 611.85 604.29 8.12 o -21 1 4 205.25 200.07 5.39 o -19 1 4 355.18 341.43 5.94 o -17 1 4 76.80 69.24 3.88 o -15 1 4 215.30 183.89 3.99 o -13 1 4 812.69 756.36 7.28 o -11 1 4 313.42 292.22 4.15 o -9 1 4 495.95 447.04 4.70 o -7 1 4 39.78 37.58 3.91 o -5 1 4 1252.17 1215.93 7.52 o -3 1 4 3078.77 3025.12 20.52 o -1 1 4 1613.81 1506.48 17.30 o 1 1 4 2971.84 2693.83 16.41 o 3 1 4 56.06 91.43 1.90 o 5 1 4 188.60 196.20 1.94 o 7 1 4 1076.33 1141.72 6.27 o 9 1 4 1615.39 1770.85 9.04 o 11 1 4 668.00 718.05 4.99 o 13 1 4 21.58 24.62 2.18 o 15 1 4 2149.54 2020.27 11.74 o 17 1 4 249.61 251.82 3.87 o 19 1 4 134.45 145.48 4.21 o 21 1 4 15.22 11.43 3.27 o -22 2 4 128.21 138.22 5.55 o -20 2 4 16.87 40.04 4.45 o -18 2 4 118.55 131.83 4.47 o -16 2 4 112.79 119.01 4.17 o -14 2 4 1519.40 1327.18 10.00 o -12 2 4 306.94 298.41 4.90 o -10 2 4 5.56 14.85 3.19 o -8 2 4 846.13 912.60 7.41 o -6 2 4 1775.26 1864.39 11.59 o -4 2 4 3610.55 3832.00 22.10 o -2 2 4 979.02 1017.28 7.56 o 0 2 4 3486.31 3646.80 45.34 o 2 2 4 720.18 768.35 4.53 o 4 2 4 236.77 419.99 6.38 o 6 2 4 335.97 362.59 23.28 o 8 2 4 869.70 880.44 5.80 o 10 2 4 8.09 3.56 1.73 o 12 2 4 893.89 763.98 5.23 o 14 2 4 260.04 242.49 3.34 o 16 2 4 1054.68 908.38 8.15 o 18 2 4 10.84 13.49 2.66 o 20 2 4 0.23 0.13 2.35 o -19 3 4 1.54 2.13 3.41 o -17 3 4 256.66 240.02 6.59 o -15 3 4 68.47 60.84 4.36 o -13 3 4 0.18 0.98 3.11 o -11 3 4 317.34 280.91 5.01 o -9 3 4 960.67 833.99 6.38 o -7 3 4 160.83 171.08 2.87 o -5 3 4 282.18 236.80 3.30 o -3 3 4 661.59 637.67 4.47 o -1 3 4 2372.31 2540.06 15.34 o 1 3 4 190.58 177.36 2.79 o 3 3 4 47.21 62.41 4.68 o 5 3 4 654.76 660.71 8.20 o 7 3 4 231.81 237.63 5.30 o 9 3 4 225.82 212.84 6.51 o 11 3 4 282.48 301.27 5.89 o 13 3 4 672.31 660.93 13.08 o 15 3 4 263.58 250.32 5.04 o 17 3 4 88.03 98.25 7.97 o 19 3 4 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