#------------------------------------------------------------------------------ #$Date: 2016-04-03 04:10:29 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181149 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/28/2222828.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2222828_Fobs loop_ _publ_author_name 'Raza, Abdul Rauf' 'Tahir, M. Nawaz' 'Saddiqa, Aisha' 'Danish, Muhammad' 'Iqbal, M. Saeed' _publ_section_title ; (2R)-2-(1,3-Dioxoisoindolin-2-yl)-4-(methylsulfanyl)butanoic acid ; _journal_coeditor_code PB2001 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2002 _journal_volume 65 _journal_year 2009 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 6.7923 _cell_length_b 9.9581 _cell_length_c 20.0970 _exptl_crystal_F_000 584.00 _reflns_d_resolution_high 0.7582 _cod_data_source_file pb2001Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' AS621_0m in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 121.61 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1071.44 1024.90 13.03 o 4 0 0 3644.74 3645.62 64.48 o 6 0 0 8.26 6.08 1.81 o 8 0 0 12.53 20.52 2.20 o 1 1 0 455.41 464.97 5.56 o 2 1 0 988.99 1018.73 9.12 o 3 1 0 383.13 391.65 4.77 o 4 1 0 0.45 2.22 0.65 o 5 1 0 12.41 7.02 0.81 o 6 1 0 94.56 96.96 2.29 o 7 1 0 150.94 160.58 3.31 o 8 1 0 26.91 28.70 2.01 o 0 2 0 2069.40 2037.38 65.13 o 1 2 0 46.24 46.01 1.31 o 2 2 0 1117.47 1152.92 11.00 o 3 2 0 1302.26 1415.75 17.10 o 4 2 0 34.58 36.89 1.13 o 5 2 0 161.55 148.35 2.72 o 6 2 0 194.27 197.95 3.55 o 7 2 0 53.40 53.90 1.93 o 8 2 0 9.75 12.36 1.92 o 1 3 0 966.29 974.81 12.54 o 2 3 0 3139.26 3244.08 40.40 o 3 3 0 206.62 202.87 2.70 o 4 3 0 34.21 33.55 1.14 o 5 3 0 27.31 26.95 1.18 o 6 3 0 72.04 68.30 2.20 o 7 3 0 18.63 19.90 1.63 o 8 3 0 1.46 -1.30 2.62 o 0 4 0 249.76 257.08 4.84 o 1 4 0 1291.59 1367.06 17.25 o 2 4 0 28.21 29.61 1.45 o 3 4 0 268.87 235.79 3.46 o 4 4 0 21.83 18.60 0.88 o 5 4 0 113.51 123.31 2.41 o 6 4 0 34.52 28.69 1.65 o 7 4 0 1.73 2.06 1.14 o 8 4 0 0.09 -1.48 3.59 o 1 5 0 524.48 520.34 6.70 o 2 5 0 23.03 23.81 0.60 o 3 5 0 0.46 0.93 0.41 o 4 5 0 271.00 277.66 4.80 o 5 5 0 176.69 173.80 3.56 o 6 5 0 0.88 -1.64 1.64 o 7 5 0 39.45 40.53 2.48 o 8 5 0 30.56 30.61 2.52 o 0 6 0 1092.87 1112.60 19.97 o 1 6 0 10.99 12.78 0.57 o 2 6 0 424.27 416.06 5.53 o 3 6 0 116.49 116.35 1.97 o 4 6 0 94.90 84.19 2.13 o 5 6 0 0.01 -1.52 1.52 o 6 6 0 50.04 44.57 2.33 o 7 6 0 8.77 7.56 1.77 o 1 7 0 0.02 -0.52 0.61 o 2 7 0 209.21 192.64 2.78 o 3 7 0 17.19 14.48 1.11 o 4 7 0 23.31 22.54 2.36 o 5 7 0 30.21 22.91 1.67 o 6 7 0 37.73 33.67 2.16 o 7 7 0 0.89 1.94 1.58 o 0 8 0 274.61 273.84 6.40 o 1 8 0 104.13 107.76 1.64 o 2 8 0 13.00 8.85 2.66 o 3 8 0 201.78 200.46 5.59 o 4 8 0 98.71 96.64 2.89 o 5 8 0 0.29 0.10 1.21 o 6 8 0 22.35 23.28 1.98 o 7 8 0 0.01 -1.96 1.96 o 1 9 0 47.98 48.41 2.17 o 2 9 0 37.32 36.78 1.40 o 3 9 0 84.64 77.02 2.29 o 4 9 0 10.58 9.83 1.29 o 5 9 0 0.15 -0.78 1.15 o 6 9 0 0.01 -0.62 1.32 o 0 10 0 0.10 -0.49 0.57 o 1 10 0 80.39 83.10 3.01 o 2 10 0 2.61 1.51 0.69 o 3 10 0 20.33 19.91 1.34 o 4 10 0 32.54 34.47 2.73 o 5 10 0 0.93 -0.38 1.26 o 1 11 0 49.74 53.96 2.33 o 2 11 0 38.16 34.21 2.46 o 3 11 0 25.54 22.21 1.80 o 4 11 0 4.35 5.22 1.20 o 1 12 0 1.82 1.76 0.95 o 2 12 0 0.32 -1.09 1.27 o 3 12 0 34.12 35.37 2.85 o 1 0 1 5951.41 4996.33 51.19 o 2 0 1 868.75 927.82 8.90 o 3 0 1 131.35 131.77 1.91 o 4 0 1 1629.03 1666.87 21.22 o 5 0 1 1.09 -0.69 0.69 o 6 0 1 22.19 22.44 1.43 o 7 0 1 120.56 120.52 2.82 o 8 0 1 6.51 10.36 2.11 o 0 1 1 0.13 -0.18 0.18 o 1 1 1 3224.42 3011.22 22.76 o 2 1 1 401.65 415.52 2.92 o 3 1 1 896.04 945.92 8.11 o 4 1 1 100.73 82.83 1.24 o 5 1 1 154.12 152.75 1.94 o 6 1 1 95.52 94.28 1.57 o 7 1 1 14.65 16.61 0.94 o 8 1 1 35.08 41.45 1.60 o 0 2 1 309.33 328.55 8.03 o 1 2 1 14788.00 11036.50 192.22 o 2 2 1 2017.87 2035.11 15.36 o 3 2 1 376.56 418.41 3.42 o 4 2 1 58.87 57.54 1.23 o 5 2 1 127.59 116.79 1.63 o 6 2 1 303.89 318.68 3.56 o 7 2 1 40.74 44.78 1.30 o 8 2 1 14.16 13.15 1.21 o 0 3 1 1466.31 1457.24 21.93 o 1 3 1 2452.75 2510.45 19.02 o 2 3 1 387.04 412.67 3.64 o 3 3 1 311.53 334.84 2.80 o 4 3 1 247.08 251.75 2.52 o 5 3 1 168.16 148.61 1.91 o 6 3 1 104.50 105.80 1.70 o 7 3 1 57.84 54.84 1.63 o 8 3 1 25.60 28.36 1.56 o 0 4 1 330.62 380.19 6.96 o 1 4 1 1227.64 1191.33 10.05 o 2 4 1 1188.19 1322.86 10.55 o 3 4 1 350.95 393.75 3.59 o 4 4 1 8.99 8.08 0.49 o 5 4 1 43.84 35.13 0.97 o 6 4 1 17.98 17.81 0.98 o 7 4 1 15.54 18.02 1.22 o 8 4 1 38.84 42.76 1.96 o 0 5 1 16.30 20.22 0.70 o 1 5 1 16.41 13.11 0.34 o 2 5 1 383.46 413.18 3.86 o 3 5 1 74.20 77.63 0.94 o 4 5 1 48.52 41.67 0.98 o 5 5 1 34.24 32.33 1.09 o 6 5 1 47.43 46.79 1.66 o 7 5 1 0.28 -0.11 1.01 o 8 5 1 1.35 1.91 1.23 o 0 6 1 448.23 436.44 6.54 o 1 6 1 101.68 91.11 1.46 o 2 6 1 359.66 365.52 3.47 o 3 6 1 292.70 296.03 2.95 o 4 6 1 231.15 208.14 2.73 o 5 6 1 216.41 220.76 3.70 o 6 6 1 4.27 4.22 0.96 o 7 6 1 10.95 8.96 1.30 o 0 7 1 267.00 264.21 3.51 o 1 7 1 16.55 18.08 1.16 o 2 7 1 71.55 65.14 0.90 o 3 7 1 1.74 -0.67 0.67 o 4 7 1 7.03 5.43 0.78 o 5 7 1 15.24 13.61 1.06 o 6 7 1 40.95 39.97 1.89 o 7 7 1 10.18 15.31 1.38 o 0 8 1 82.90 87.68 1.57 o 1 8 1 195.71 188.53 2.18 o 2 8 1 225.20 209.72 3.04 o 3 8 1 14.24 14.15 0.80 o 4 8 1 72.35 74.41 1.93 o 5 8 1 12.76 9.77 0.99 o 6 8 1 10.51 7.38 1.12 o 7 8 1 18.00 21.71 2.03 o 0 9 1 24.49 24.23 0.99 o 1 9 1 121.17 115.20 1.95 o 2 9 1 146.33 142.10 2.22 o 3 9 1 81.91 79.91 1.67 o 4 9 1 65.77 62.18 1.64 o 5 9 1 23.27 25.67 1.32 o 6 9 1 0.09 -0.90 0.95 o 0 10 1 23.63 26.45 1.47 o 1 10 1 17.57 18.05 0.83 o 2 10 1 67.61 63.49 1.57 o 3 10 1 12.95 10.33 0.78 o 4 10 1 7.46 7.90 0.89 o 5 10 1 29.51 29.55 1.43 o 0 11 1 14.70 12.77 1.13 o 1 11 1 6.77 9.34 0.82 o 2 11 1 81.36 80.94 1.89 o 3 11 1 13.31 16.96 0.92 o 4 11 1 6.90 9.05 0.91 o 1 12 1 19.20 17.46 1.63 o 2 12 1 6.58 7.21 1.07 o 3 12 1 1.58 1.18 2.22 o 1 0 2 615.07 592.05 6.16 o 2 0 2 387.09 425.98 4.56 o 3 0 2 741.05 695.75 8.13 o 4 0 2 25.35 26.83 2.20 o 5 0 2 522.88 521.78 7.30 o 6 0 2 119.42 116.46 2.49 o 7 0 2 6.45 11.61 1.30 o 8 0 2 0.06 1.25 1.18 o 0 1 2 204.28 220.99 7.20 o 1 1 2 3173.85 3108.73 22.41 o 2 1 2 791.78 790.90 5.83 o 3 1 2 2285.44 2322.83 19.42 o 4 1 2 1067.41 1032.31 9.48 o 5 1 2 135.40 128.25 1.74 o 6 1 2 79.84 73.02 1.39 o 7 1 2 12.84 10.22 0.85 o 8 1 2 7.43 9.18 1.32 o 0 2 2 897.04 927.96 10.76 o 1 2 2 6539.35 5819.27 43.92 o 2 2 2 2050.90 2220.14 16.74 o 3 2 2 1409.97 1549.40 11.82 o 4 2 2 421.52 409.85 3.82 o 5 2 2 129.11 132.40 1.78 o 6 2 2 58.06 57.24 1.27 o 7 2 2 47.05 48.12 1.37 o 8 2 2 4.08 2.72 0.97 o 0 3 2 5114.26 4676.24 128.67 o 1 3 2 1290.01 1358.96 11.41 o 2 3 2 1432.50 1461.03 13.92 o 3 3 2 263.65 285.79 2.43 o 4 3 2 299.56 305.25 2.97 o 5 3 2 62.57 63.95 1.19 o 6 3 2 114.01 119.93 1.82 o 7 3 2 18.85 25.68 1.50 o 8 3 2 0.46 1.18 1.11 o 0 4 2 750.14 761.59 11.18 o 1 4 2 626.11 689.55 5.56 o 2 4 2 385.07 433.98 3.62 o 3 4 2 279.99 268.40 2.44 o 4 4 2 318.92 313.32 3.03 o 5 4 2 385.39 370.24 3.85 o 6 4 2 51.48 51.69 1.41 o 7 4 2 63.07 66.37 1.87 o 8 4 2 6.72 6.23 1.33 o 0 5 2 1116.45 1110.42 19.82 o 1 5 2 201.36 194.75 1.89 o 2 5 2 103.33 97.99 1.07 o 3 5 2 162.19 169.37 1.58 o 4 5 2 66.39 54.94 1.22 o 5 5 2 14.60 11.00 0.78 o 6 5 2 4.77 2.00 0.81 o 7 5 2 1.76 2.18 1.13 o 8 5 2 8.09 10.50 1.46 o 0 6 2 395.01 371.33 6.89 o 1 6 2 29.68 26.04 1.81 o 2 6 2 30.01 35.42 0.71 o 3 6 2 88.92 71.66 1.06 o 4 6 2 413.48 394.22 4.59 o 5 6 2 52.40 51.83 1.62 o 6 6 2 20.40 19.45 1.57 o 7 6 2 13.89 17.36 1.55 o 0 7 2 56.93 62.60 2.38 o 1 7 2 307.14 309.25 3.73 o 2 7 2 70.47 70.46 1.01 o 3 7 2 396.70 376.96 5.25 o 4 7 2 140.98 136.45 2.50 o 5 7 2 20.53 17.26 1.12 o 6 7 2 26.55 25.91 1.39 o 7 7 2 9.70 10.13 1.28 o 0 8 2 11.20 12.75 0.88 o 1 8 2 58.12 53.37 0.88 o 2 8 2 165.72 162.82 2.48 o 3 8 2 141.68 130.94 2.25 o 4 8 2 35.20 37.10 1.31 o 5 8 2 33.97 32.32 1.39 o 6 8 2 4.01 5.72 1.11 o 7 8 2 4.51 3.89 1.24 o 0 9 2 112.56 111.33 2.49 o 1 9 2 108.31 104.40 1.52 o 2 9 2 73.80 76.50 2.50 o 3 9 2 137.16 132.91 2.31 o 4 9 2 2.01 -0.18 0.74 o 5 9 2 16.04 15.80 1.11 o 6 9 2 22.45 25.91 1.44 o 0 10 2 0.16 1.20 0.88 o 1 10 2 115.96 112.95 2.11 o 2 10 2 7.01 6.26 0.75 o 3 10 2 63.27 62.75 1.46 o 4 10 2 33.56 36.28 1.37 o 5 10 2 7.59 6.69 1.00 o 0 11 2 56.80 57.28 2.29 o 1 11 2 24.17 23.18 0.90 o 2 11 2 16.20 14.39 1.19 o 3 11 2 19.87 19.85 0.93 o 4 11 2 5.04 4.36 0.84 o 0 12 2 4.94 8.14 1.02 o 1 12 2 7.71 7.69 1.29 o 2 12 2 8.15 11.59 1.17 o 3 12 2 16.39 15.20 1.50 o 1 0 3 1964.87 2011.42 20.56 o 2 0 3 42.90 51.92 0.89 o 3 0 3 4024.51 3982.70 49.61 o 4 0 3 544.07 622.14 8.38 o 5 0 3 143.90 130.15 2.49 o 6 0 3 9.02 6.71 0.96 o 7 0 3 294.70 304.34 5.10 o 8 0 3 1.94 2.74 1.19 o 0 1 3 482.92 529.66 5.55 o 1 1 3 1157.92 1253.20 9.10 o 2 1 3 436.83 464.23 3.51 o 3 1 3 101.15 117.96 1.50 o 4 1 3 72.87 68.48 1.13 o 5 1 3 174.21 176.85 2.17 o 6 1 3 10.86 9.62 0.72 o 7 1 3 18.74 22.58 1.05 o 8 1 3 2.66 1.70 1.00 o 0 2 3 11478.54 8791.31 191.22 o 1 2 3 4215.54 4017.97 44.41 o 2 2 3 404.58 387.94 3.43 o 3 2 3 432.89 449.42 4.17 o 4 2 3 207.15 206.57 2.17 o 5 2 3 207.49 193.69 2.32 o 6 2 3 21.49 18.64 0.85 o 7 2 3 19.36 21.57 1.06 o 8 2 3 15.20 20.53 1.29 o 0 3 3 1110.31 1128.01 14.26 o 1 3 3 80.32 74.33 0.70 o 2 3 3 466.62 474.74 4.41 o 3 3 3 179.01 181.22 1.67 o 4 3 3 39.40 33.93 0.76 o 5 3 3 42.90 44.08 1.01 o 6 3 3 117.24 116.12 1.80 o 7 3 3 11.55 12.64 1.03 o 8 3 3 27.25 25.77 1.49 o 0 4 3 1059.44 1062.13 15.59 o 1 4 3 552.91 579.05 5.62 o 2 4 3 1217.91 1166.84 10.45 o 3 4 3 404.15 453.93 3.89 o 4 4 3 124.06 137.40 1.73 o 5 4 3 79.57 76.97 1.33 o 6 4 3 169.76 164.27 2.58 o 7 4 3 6.24 7.13 1.08 o 8 4 3 7.86 4.88 1.28 o 0 5 3 32.02 36.54 0.83 o 1 5 3 418.66 435.51 4.29 o 2 5 3 803.76 784.87 6.71 o 3 5 3 132.19 131.57 1.38 o 4 5 3 402.49 381.50 4.40 o 5 5 3 24.32 21.18 0.92 o 6 5 3 2.37 2.56 0.79 o 7 5 3 38.14 42.85 1.84 o 8 5 3 18.17 18.60 1.58 o 0 6 3 348.15 367.31 6.90 o 1 6 3 573.44 617.18 7.12 o 2 6 3 93.81 97.98 1.03 o 3 6 3 84.41 80.24 1.08 o 4 6 3 7.15 4.28 0.67 o 5 6 3 23.39 21.73 1.16 o 6 6 3 5.08 6.93 1.32 o 7 6 3 2.26 4.21 1.17 o 0 7 3 108.63 112.59 2.52 o 1 7 3 989.85 998.96 12.49 o 2 7 3 2.88 3.39 0.38 o 3 7 3 0.87 0.46 0.66 o 4 7 3 20.76 19.49 1.05 o 5 7 3 128.59 122.17 2.49 o 6 7 3 3.66 3.25 1.05 o 7 7 3 2.45 1.91 1.15 o 0 8 3 8.49 6.35 0.85 o 1 8 3 34.00 37.67 0.76 o 2 8 3 407.21 389.19 5.28 o 3 8 3 85.95 84.57 1.73 o 4 8 3 49.35 45.06 1.42 o 5 8 3 5.77 6.53 0.93 o 6 8 3 74.99 77.41 2.15 o 7 8 3 16.22 20.36 1.50 o 0 9 3 2.73 3.68 0.96 o 1 9 3 51.34 53.09 1.11 o 2 9 3 19.52 18.21 1.02 o 3 9 3 49.41 43.15 1.28 o 4 9 3 14.75 12.02 1.15 o 5 9 3 22.35 24.44 1.29 o 6 9 3 5.19 5.37 1.11 o 0 10 3 251.95 240.95 6.87 o 1 10 3 11.37 12.21 0.73 o 2 10 3 41.86 43.32 1.37 o 3 10 3 19.11 16.56 0.93 o 4 10 3 32.89 31.35 1.50 o 5 10 3 5.81 7.54 1.02 o 0 11 3 28.44 26.39 1.79 o 1 11 3 23.76 25.20 0.97 o 2 11 3 52.18 52.79 1.52 o 3 11 3 10.82 10.98 1.04 o 4 11 3 11.33 11.79 1.01 o 0 12 3 2.10 0.61 0.98 o 1 12 3 19.63 19.95 1.19 o 2 12 3 10.99 13.69 1.16 o 3 12 3 1.96 1.51 0.87 o 0 0 4 837.56 848.03 12.40 o 1 0 4 7025.66 6302.93 64.14 o 2 0 4 150.61 177.95 2.11 o 3 0 4 98.86 125.27 4.05 o 4 0 4 1.82 1.76 0.63 o 5 0 4 0.62 -0.69 0.69 o 6 0 4 33.12 37.24 1.84 o 7 0 4 29.36 33.68 1.79 o 8 0 4 0.71 2.59 1.22 o 0 1 4 45.12 59.33 0.81 o 1 1 4 1027.26 996.28 7.27 o 2 1 4 73.86 72.47 0.81 o 3 1 4 111.33 144.98 2.57 o 4 1 4 669.14 671.15 6.36 o 5 1 4 46.24 46.98 1.05 o 6 1 4 15.24 12.88 0.79 o 7 1 4 81.92 75.99 1.59 o 8 1 4 13.30 18.17 1.26 o 0 2 4 79.25 91.56 1.42 o 1 2 4 9598.97 8430.46 73.92 o 2 2 4 57.66 56.85 1.40 o 3 2 4 1265.85 1409.80 12.66 o 4 2 4 460.03 462.16 4.28 o 5 2 4 219.29 224.75 2.60 o 6 2 4 71.16 69.11 1.37 o 7 2 4 8.15 11.20 0.93 o 8 2 4 23.68 23.67 1.37 o 0 3 4 368.23 364.85 3.89 o 1 3 4 1566.83 1682.51 14.08 o 2 3 4 1293.67 1347.80 12.04 o 3 3 4 42.39 53.43 0.78 o 4 3 4 101.30 99.08 1.30 o 5 3 4 26.77 26.95 0.86 o 6 3 4 133.47 128.88 1.90 o 7 3 4 6.43 8.49 0.98 o 8 3 4 10.22 12.01 1.36 o 0 4 4 401.30 474.33 7.10 o 1 4 4 1855.91 2029.74 19.22 o 2 4 4 1511.15 1542.83 13.74 o 3 4 4 1.26 0.01 0.33 o 4 4 4 93.18 71.79 1.09 o 5 4 4 228.74 217.94 2.55 o 6 4 4 25.81 26.67 1.11 o 7 4 4 30.40 29.80 1.43 o 8 4 4 2.00 0.35 1.26 o 0 5 4 765.94 788.50 11.63 o 1 5 4 304.99 302.37 2.86 o 2 5 4 499.56 520.02 4.84 o 3 5 4 181.11 175.65 1.74 o 4 5 4 28.40 24.40 0.68 o 5 5 4 35.84 30.58 1.12 o 6 5 4 12.00 9.25 0.97 o 7 5 4 25.80 23.72 1.51 o 8 5 4 1.57 -0.10 1.22 o 0 6 4 1526.84 1541.22 22.43 o 1 6 4 634.17 611.27 6.45 o 2 6 4 179.79 193.24 1.87 o 3 6 4 460.22 443.08 4.05 o 4 6 4 132.55 129.77 1.97 o 5 6 4 66.31 58.98 1.71 o 6 6 4 9.04 7.11 1.12 o 7 6 4 71.61 85.67 2.47 o 0 7 4 45.84 52.91 1.54 o 1 7 4 40.85 45.47 1.17 o 2 7 4 115.68 120.69 1.41 o 3 7 4 129.65 117.72 1.86 o 4 7 4 195.62 193.60 3.41 o 5 7 4 18.27 20.31 1.14 o 6 7 4 27.88 24.95 1.43 o 7 7 4 19.81 21.91 1.48 o 0 8 4 3.03 3.35 0.69 o 1 8 4 43.27 46.19 0.86 o 2 8 4 217.50 197.09 2.94 o 3 8 4 135.39 129.24 2.28 o 4 8 4 18.49 17.96 1.02 o 5 8 4 16.59 13.91 1.07 o 6 8 4 29.50 34.92 1.62 o 0 9 4 205.58 196.54 5.86 o 1 9 4 33.25 30.55 0.90 o 2 9 4 44.31 42.75 1.40 o 3 9 4 10.28 9.44 0.87 o 4 9 4 37.84 36.85 1.35 o 5 9 4 7.75 8.77 1.04 o 6 9 4 6.12 5.65 1.12 o 0 10 4 45.86 51.12 2.48 o 1 10 4 68.55 68.79 1.59 o 2 10 4 85.93 88.40 2.06 o 3 10 4 31.54 31.12 1.12 o 4 10 4 21.29 23.59 1.16 o 5 10 4 2.36 1.25 0.92 o 0 11 4 24.55 30.17 1.96 o 1 11 4 5.15 7.57 1.04 o 2 11 4 6.67 7.10 0.86 o 3 11 4 29.00 30.86 1.46 o 4 11 4 3.03 2.00 0.82 o 0 12 4 1.45 0.21 1.10 o 1 12 4 18.10 19.18 1.31 o 2 12 4 4.12 6.84 0.84 o 3 12 4 1.28 -0.33 0.87 o 1 0 5 30.35 33.54 0.68 o 2 0 5 958.76 1044.46 11.90 o 3 0 5 40.67 36.32 1.18 o 4 0 5 32.50 27.59 1.10 o 5 0 5 23.47 23.46 1.14 o 6 0 5 31.31 30.13 1.89 o 7 0 5 88.20 93.95 2.79 o 8 0 5 1.97 2.10 1.33 o 0 1 5 3021.04 2796.60 26.37 o 1 1 5 152.25 153.86 1.28 o 2 1 5 295.47 334.54 2.87 o 3 1 5 64.51 60.78 0.99 o 4 1 5 325.50 343.67 3.53 o 5 1 5 138.70 132.65 1.80 o 6 1 5 164.71 161.27 2.20 o 7 1 5 96.38 98.42 1.80 o 8 1 5 6.62 8.75 1.10 o 0 2 5 3099.13 3102.21 31.55 o 1 2 5 1364.50 1513.71 12.02 o 2 2 5 29.36 31.39 1.52 o 3 2 5 215.07 211.33 2.24 o 4 2 5 282.46 284.83 3.02 o 5 2 5 65.63 71.06 1.28 o 6 2 5 37.25 32.98 1.34 o 7 2 5 52.89 56.64 1.53 o 8 2 5 1.20 2.15 1.02 o 0 3 5 367.78 368.31 4.31 o 1 3 5 304.96 304.35 3.10 o 2 3 5 276.77 295.85 2.89 o 3 3 5 705.48 662.72 6.17 o 4 3 5 172.62 152.38 1.74 o 5 3 5 285.27 262.29 2.95 o 6 3 5 35.55 37.23 1.19 o 7 3 5 17.05 16.91 1.11 o 8 3 5 20.65 18.74 1.43 o 0 4 5 2231.09 2328.00 29.46 o 1 4 5 1764.17 1847.16 15.48 o 2 4 5 1434.45 1486.87 13.27 o 3 4 5 262.15 286.08 2.92 o 4 4 5 330.74 326.09 3.18 o 5 4 5 70.21 69.64 1.30 o 6 4 5 57.12 56.61 1.52 o 7 4 5 0.40 1.21 0.99 o 8 4 5 18.98 24.25 1.76 o 0 5 5 123.04 137.94 2.39 o 1 5 5 91.73 109.13 1.28 o 2 5 5 73.08 69.50 0.87 o 3 5 5 463.36 464.77 3.81 o 4 5 5 31.32 26.46 1.00 o 5 5 5 227.30 216.09 2.98 o 6 5 5 19.05 22.95 1.14 o 7 5 5 5.22 4.43 1.16 o 8 5 5 3.63 4.80 1.34 o 0 6 5 39.73 40.76 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6 85.73 78.83 1.37 o 3 8 6 12.82 14.82 0.90 o 4 8 6 55.18 48.65 1.48 o 5 8 6 40.05 36.85 1.51 o 6 8 6 11.62 8.50 1.16 o 0 9 6 0.02 1.16 1.14 o 1 9 6 16.85 19.64 0.97 o 2 9 6 95.59 89.70 1.83 o 3 9 6 89.84 80.30 1.77 o 4 9 6 32.73 34.78 1.62 o 5 9 6 4.84 4.30 0.98 o 6 9 6 5.11 2.51 1.08 o 0 10 6 26.70 24.54 2.03 o 1 10 6 4.72 3.51 0.81 o 2 10 6 1.07 2.35 0.77 o 3 10 6 37.49 44.04 1.89 o 4 10 6 2.44 1.33 0.88 o 5 10 6 4.70 5.56 1.17 o 0 11 6 2.38 4.01 1.39 o 1 11 6 58.81 61.10 4.41 o 2 11 6 29.81 28.71 1.50 o 3 11 6 13.22 13.44 1.20 o 4 11 6 0.06 0.47 0.80 o 0 12 6 28.75 31.89 2.41 o 1 12 6 51.05 56.76 2.13 o 2 12 6 13.33 14.42 1.07 o 3 12 6 6.07 11.39 1.46 o 1 0 7 1835.54 1952.61 21.91 o 2 0 7 184.48 235.92 3.42 o 3 0 7 23.96 25.10 1.20 o 4 0 7 193.38 173.20 4.25 o 5 0 7 416.84 418.91 6.14 o 6 0 7 283.02 291.47 4.79 o 7 0 7 36.62 35.23 1.71 o 8 0 7 18.34 18.74 1.83 o 0 1 7 3320.54 3397.22 37.82 o 1 1 7 113.47 121.63 1.22 o 2 1 7 111.98 115.48 1.86 o 3 1 7 391.49 421.06 4.40 o 4 1 7 190.43 209.13 2.75 o 5 1 7 26.10 31.30 1.01 o 6 1 7 83.91 83.85 1.56 o 7 1 7 80.76 78.49 1.73 o 8 1 7 12.10 18.29 1.27 o 0 2 7 397.51 366.92 4.92 o 1 2 7 1911.60 1991.78 16.66 o 2 2 7 833.92 875.06 7.98 o 3 2 7 181.25 190.64 2.25 o 4 2 7 542.05 505.49 5.73 o 5 2 7 26.58 28.92 0.95 o 6 2 7 243.16 252.34 3.04 o 7 2 7 5.48 8.03 1.04 o 8 2 7 48.77 58.35 2.30 o 0 3 7 5.61 7.97 0.72 o 1 3 7 1164.85 1201.43 10.78 o 2 3 7 54.52 55.61 0.81 o 3 3 7 898.94 874.98 8.06 o 4 3 7 111.66 102.22 1.57 o 5 3 7 92.39 83.76 1.44 o 6 3 7 18.77 18.69 0.94 o 7 3 7 6.27 4.15 1.09 o 8 3 7 9.73 10.64 1.27 o 0 4 7 666.68 731.94 31.51 o 1 4 7 555.91 565.53 5.00 o 2 4 7 18.81 22.22 0.58 o 3 4 7 48.94 54.78 1.21 o 4 4 7 196.69 196.59 3.15 o 5 4 7 141.50 143.41 2.12 o 6 4 7 84.15 82.33 1.80 o 7 4 7 34.85 39.02 2.02 o 8 4 7 45.74 57.87 2.29 o 0 5 7 1111.37 1070.53 15.84 o 1 5 7 151.40 166.44 1.89 o 2 5 7 250.55 257.01 2.61 o 3 5 7 20.13 15.62 0.58 o 4 5 7 8.36 8.58 0.63 o 5 5 7 6.94 6.86 1.13 o 6 5 7 36.85 32.04 1.50 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8 47.11 43.25 1.36 o 4 8 8 90.52 85.78 2.01 o 5 8 8 26.78 27.19 1.41 o 6 8 8 35.36 38.46 1.72 o 0 9 8 90.30 116.99 4.32 o 1 9 8 147.76 147.12 3.67 o 2 9 8 44.25 44.07 1.22 o 3 9 8 24.51 26.47 1.17 o 4 9 8 1.90 1.27 0.82 o 5 9 8 17.54 16.63 1.30 o 0 10 8 84.15 85.48 3.80 o 1 10 8 27.59 24.24 1.16 o 2 10 8 36.71 40.57 1.54 o 3 10 8 45.29 47.44 1.45 o 4 10 8 26.34 25.29 1.30 o 5 10 8 1.43 1.54 0.98 o 0 11 8 0.14 -0.57 1.44 o 1 11 8 22.99 24.42 1.85 o 2 11 8 5.34 7.70 1.26 o 3 11 8 16.31 18.61 1.33 o 4 11 8 24.08 24.84 1.30 o 0 12 8 7.08 7.47 1.73 o 1 12 8 6.52 7.75 1.29 o 2 12 8 27.08 32.92 1.69 o 1 0 9 0.16 1.53 0.61 o 2 0 9 83.36 78.49 1.81 o 3 0 9 1672.45 1751.11 25.74 o 4 0 9 6.42 3.28 0.83 o 5 0 9 86.49 88.79 2.46 o 6 0 9 0.57 -0.89 0.89 o 7 0 9 18.03 16.33 1.35 o 8 0 9 1.16 -2.08 2.33 o 0 1 9 67.66 85.48 2.18 o 1 1 9 170.79 155.48 1.73 o 2 1 9 129.44 139.10 1.75 o 3 1 9 12.75 11.17 0.63 o 4 1 9 152.03 133.02 2.04 o 5 1 9 157.28 152.45 2.37 o 6 1 9 49.55 41.64 1.23 o 7 1 9 36.38 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283.25 283.95 4.32 o 4 6 9 26.54 25.27 1.25 o 5 6 9 10.88 11.25 1.06 o 6 6 9 48.53 47.80 2.69 o 7 6 9 4.23 0.97 1.41 o 0 7 9 12.81 11.08 0.91 o 1 7 9 152.87 153.98 2.52 o 2 7 9 27.85 27.61 1.59 o 3 7 9 97.65 96.26 2.34 o 4 7 9 23.80 22.11 1.18 o 5 7 9 70.12 69.68 1.95 o 6 7 9 22.08 24.89 1.48 o 1 8 9 18.90 14.23 1.21 o 2 8 9 43.86 40.06 1.42 o 3 8 9 27.33 27.77 1.38 o 4 8 9 66.66 57.77 1.68 o 5 8 9 5.36 6.10 0.99 o 6 8 9 0.97 1.79 1.05 o 0 9 9 48.64 45.51 2.79 o 1 9 9 19.71 20.24 1.49 o 2 9 9 34.81 33.54 1.32 o 3 9 9 104.92 99.21 2.09 o 4 9 9 21.02 23.58 1.23 o 5 9 9 15.02 15.69 1.23 o 0 10 9 24.30 34.29 2.63 o 1 10 9 22.91 20.65 1.14 o 2 10 9 13.28 10.84 1.27 o 3 10 9 19.87 19.33 1.08 o 4 10 9 56.16 52.43 1.71 o 0 11 9 0.38 -0.18 1.53 o 1 11 9 11.69 11.76 1.08 o 2 11 9 43.04 49.75 1.80 o 3 11 9 40.40 41.11 1.82 o 0 12 9 26.04 26.22 2.68 o 1 12 9 5.95 7.79 1.31 o 2 12 9 0.74 3.49 1.47 o 0 0 10 158.44 192.60 5.87 o 1 0 10 487.62 454.95 7.15 o 2 0 10 856.81 1012.64 15.18 o 3 0 10 9.02 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6 6 12 43.04 50.96 1.96 o 0 7 12 106.89 131.50 3.54 o 1 7 12 108.10 101.87 3.06 o 2 7 12 179.01 177.94 3.56 o 3 7 12 60.33 54.52 1.88 o 4 7 12 85.37 81.99 2.41 o 5 7 12 2.02 0.20 1.23 o 6 7 12 6.90 6.03 1.18 o 0 8 12 135.23 145.25 5.59 o 1 8 12 144.63 144.10 3.95 o 2 8 12 40.33 36.06 1.56 o 3 8 12 38.96 36.99 1.66 o 4 8 12 0.52 0.57 1.09 o 5 8 12 12.06 14.74 1.23 o 0 9 12 10.36 7.33 1.82 o 1 9 12 9.68 11.85 2.53 o 2 9 12 39.72 40.89 2.15 o 3 9 12 19.03 18.88 1.32 o 4 9 12 2.38 3.26 0.93 o 5 9 12 2.36 0.15 0.93 o 0 10 12 9.58 10.08 2.10 o 1 10 12 9.95 11.53 2.13 o 2 10 12 5.99 7.46 1.47 o 3 10 12 69.55 73.42 1.93 o 4 10 12 6.11 5.67 1.01 o 0 11 12 11.96 13.87 2.28 o 1 11 12 20.81 21.68 1.72 o 2 11 12 9.91 11.57 1.33 o 1 0 13 141.30 151.65 3.03 o 2 0 13 463.30 478.89 7.77 o 3 0 13 77.56 68.13 2.00 o 4 0 13 40.90 32.96 3.01 o 5 0 13 13.58 11.90 1.37 o 6 0 13 1.06 0.37 1.29 o 7 0 13 0.00 -1.16 1.16 o 0 1 13 777.33 781.02 27.96 o 1 1 13 125.49 118.94 1.82 o 2 1 13 49.65 54.35 1.22 o 3 1 13 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60.11 4.20 o 0 0 18 2181.39 2087.29 53.68 o 1 0 18 54.98 52.55 2.56 o 2 0 18 85.31 86.69 2.52 o 3 0 18 34.03 29.79 1.74 o 4 0 18 267.10 255.29 5.22 o 5 0 18 2.65 4.62 1.64 o 6 0 18 3.94 0.96 1.80 o 0 1 18 203.49 208.47 5.21 o 1 1 18 170.82 170.01 3.24 o 2 1 18 110.73 110.59 2.04 o 3 1 18 179.08 169.53 2.80 o 4 1 18 58.76 62.65 1.82 o 5 1 18 1.35 1.40 0.94 o 6 1 18 2.43 2.11 1.59 o 0 2 18 197.69 186.17 4.78 o 1 2 18 35.82 36.17 2.05 o 2 2 18 104.81 108.47 2.05 o 3 2 18 145.59 145.43 2.74 o 4 2 18 10.21 12.65 1.08 o 5 2 18 27.69 30.10 1.67 o 6 2 18 5.40 6.36 1.33 o 0 3 18 344.71 369.97 18.21 o 1 3 18 8.71 8.05 1.17 o 2 3 18 14.11 13.65 1.13 o 3 3 18 2.73 1.99 0.89 o 4 3 18 76.72 70.55 2.14 o 5 3 18 7.43 6.06 1.24 o 6 3 18 3.77 2.32 1.20 o 0 4 18 0.07 -0.09 1.57 o 1 4 18 87.47 78.44 4.21 o 2 4 18 76.57 78.62 2.44 o 3 4 18 30.61 31.06 1.51 o 4 4 18 1.88 2.45 1.01 o 5 4 18 8.25 10.66 1.81 o 0 5 18 18.90 19.36 2.66 o 1 5 18 63.62 66.75 3.95 o 2 5 18 21.36 24.51 1.53 o 3 5 18 3.38 1.80 1.08 o 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4.73 1.34 o 1 1 20 71.68 67.31 2.04 o 2 1 20 27.77 27.78 1.81 o 3 1 20 18.14 14.65 1.13 o 4 1 20 11.87 11.15 1.14 o 5 1 20 14.93 16.33 1.65 o 0 2 20 176.40 171.52 4.73 o 1 2 20 96.57 99.55 3.14 o 2 2 20 21.54 22.03 1.57 o 3 2 20 21.91 25.41 1.52 o 4 2 20 23.05 22.16 1.89 o 5 2 20 43.47 46.06 2.05 o 0 3 20 79.11 75.53 4.57 o 1 3 20 22.16 21.42 3.75 o 2 3 20 16.06 16.32 1.93 o 3 3 20 24.29 28.04 1.56 o 4 3 20 4.86 4.26 1.17 o 5 3 20 2.56 0.98 1.18 o 0 4 20 2.31 3.37 1.97 o 1 4 20 56.78 68.55 4.37 o 2 4 20 0.44 -1.27 1.27 o 3 4 20 87.06 90.29 2.54 o 4 4 20 0.39 0.80 1.23 o 5 4 20 18.05 19.23 1.79 o 0 5 20 117.56 120.50 5.80 o 1 5 20 53.61 53.85 2.78 o 2 5 20 27.43 31.68 2.35 o 3 5 20 21.81 20.88 1.71 o 4 5 20 19.56 23.22 1.80 o 0 6 20 124.83 124.47 5.85 o 1 6 20 7.82 7.45 1.67 o 2 6 20 16.29 16.55 2.06 o 3 6 20 16.65 18.01 1.67 o 4 6 20 24.73 26.18 1.91 o 0 7 20 5.70 3.83 2.37 o 1 7 20 42.42 41.34 2.59 o 2 7 20 11.70 6.25 2.56 o 3 7 20 22.68 28.10 2.38 o 0 8 20 10.62 11.37 2.69 o 1 8 20 43.98 47.98 2.89 o 2 8 20 5.04 4.16 1.76 o 1 0 21 3.32 1.47 1.38 o 2 0 21 3.22 1.93 1.41 o 3 0 21 3.79 1.97 1.19 o 4 0 21 4.60 4.44 1.86 o 5 0 21 4.59 9.37 2.89 o 0 1 21 150.35 166.40 4.74 o 1 1 21 129.56 132.89 2.96 o 2 1 21 73.68 74.19 2.57 o 3 1 21 5.13 3.95 1.22 o 4 1 21 25.06 25.63 1.82 o 5 1 21 12.45 12.76 1.69 o 0 2 21 72.83 79.03 4.72 o 1 2 21 23.50 27.96 2.81 o 2 2 21 0.91 0.01 1.39 o 3 2 21 18.75 20.91 1.48 o 4 2 21 12.01 8.73 1.31 o 5 2 21 1.89 2.64 1.28 o 0 3 21 0.08 0.09 1.92 o 1 3 21 28.55 25.48 3.48 o 2 3 21 6.35 5.49 1.62 o 3 3 21 31.40 33.26 1.73 o 4 3 21 12.89 13.06 1.39 o 5 3 21 3.46 0.76 1.27 o 0 4 21 1.92 -0.71 1.97 o 1 4 21 62.80 69.37 3.23 o 2 4 21 18.59 13.27 6.09 o 3 4 21 26.27 28.07 1.87 o 4 4 21 6.52 5.14 1.41 o 0 5 21 90.69 107.85 5.70 o 1 5 21 3.70 4.04 1.64 o 2 5 21 54.01 57.40 4.39 o 3 5 21 4.07 4.88 1.36 o 4 5 21 17.67 21.01 1.81 o 0 6 21 1.46 5.09 2.56 o 1 6 21 21.56 22.50 2.17 o 2 6 21 38.26 37.59 3.78 o 3 6 21 10.06 13.94 3.37 o 0 7 21 0.01 -1.99 1.99 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1.17 2.63 2.50 o 0 1 23 0.27 3.08 2.30 o 1 1 23 0.06 0.88 1.79 o 2 1 23 23.85 24.23 2.16 o 3 1 23 17.22 20.05 2.16 o 4 1 23 0.25 0.46 1.41 o 0 2 23 28.76 26.91 3.38 o 1 2 23 53.97 57.20 2.95 o 2 2 23 4.86 3.23 1.66 o 3 2 23 19.95 20.56 2.60 o 4 2 23 2.91 0.71 1.45 o 0 3 23 3.63 1.73 2.42 o 1 3 23 23.05 26.46 2.32 o 2 3 23 14.13 13.50 2.13 o 3 3 23 1.38 1.87 1.37 o 0 4 23 69.33 74.05 4.81 o 1 4 23 48.56 44.76 2.84 o 2 4 23 24.56 24.17 2.42 o 3 4 23 3.59 1.64 1.71 o 0 5 23 8.57 7.14 2.86 o 1 5 23 8.39 11.85 2.10 o 2 5 23 0.74 3.73 1.78 o 0 6 23 3.96 6.09 2.75 o 1 6 23 7.76 7.97 2.01 o 0 1 24 47.05 41.00 3.74 o 1 1 24 7.88 6.19 3.09 o 2 1 24 32.60 35.28 3.41 o 3 1 24 5.74 6.22 2.72 o 0 2 24 9.67 10.01 2.57 o 1 2 24 11.34 14.01 1.99 o 2 2 24 12.04 15.32 2.53 o 3 2 24 13.68 12.48 4.87 o 0 3 24 19.57 20.78 3.10 o 1 3 24 13.15 16.23 2.12 o 2 3 24 10.77 12.05 2.03 o 3 3 24 10.15 14.95 3.99 o 0 4 24 1.28 0.08 2.41 o 1 4 24 22.64 26.55 2.43 o 2 4 24 105.05 107.68 4.35 o 0 5 24 1.12 4.01 2.42 o 1 5 24 5.70 9.31 2.11 o 0 1 25 33.18 30.68 3.67 o 1 1 25 11.09 12.23 2.78 o 2 1 25 5.46 6.85 2.71 o 0 2 25 19.09 21.13 3.32 o 1 2 25 2.32 3.30 1.73 o 2 2 25 20.21 24.30 2.53 o 0 3 25 0.59 3.81 2.71 o 1 3 25 7.75 7.25 3.15 o 2 3 25 12.62 13.95 3.51 o 0 4 25 0.30 -2.22 2.44 o 1 4 25 29.16 39.12 4.03 o 0 2 26 30.58 38.20 3.88 o