#------------------------------------------------------------------------------ #$Date: 2009-09-11 11:49:26 +0300 (Fri, 11 Sep 2009) $ #$Revision: 819 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2222831.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2222831_Fobs loop_ _publ_author_name 'La-o, Latipah' 'Pakawatchai, Chaveng' 'Saithong, Saowanit' 'Skelton, Brian W.' _publ_section_title ; Chlorido(1,3-dimethylthiourea-\kS)bis(triphenylphosphine-\kP)copper(I) acetonitrile hemisolvate ; _journal_coeditor_code PK2174 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m926 _journal_volume 65 _journal_year 2009 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 90.874 _cell_angle_gamma 90.000 _cell_length_a 13.7503 _cell_length_b 30.0495 _cell_length_c 18.4227 _exptl_crystal_F_000 3112.00 _reflns_d_resolution_high 0.8409 _[local]_cod_data_source_file pk2174Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' p032 in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 560.45 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 60726.20 68726.91 897.96 o 4 0 0 103496.26 112713.25 1473.46 o 6 0 0 2546.92 2188.19 175.44 o 8 0 0 5067.98 5562.60 127.88 o 10 0 0 732.14 816.80 64.72 o 12 0 0 14224.69 13344.07 523.31 o 14 0 0 1306.08 1389.01 168.21 o 16 0 0 1374.09 1193.84 170.93 o 1 1 0 1057.86 1306.93 22.66 o 2 1 0 10055.32 11932.41 124.80 o 3 1 0 119499.45 131670.52 1195.78 o 4 1 0 8840.18 8502.17 101.92 o 5 1 0 48968.67 53619.23 457.09 o 6 1 0 246.79 250.25 24.29 o 7 1 0 451.29 611.77 37.02 o 8 1 0 1697.68 1498.44 63.00 o 9 1 0 1698.27 1889.18 68.67 o 10 1 0 2400.82 2331.23 77.60 o 11 1 0 381.30 377.51 51.25 o 12 1 0 137.45 129.21 75.49 o 13 1 0 803.30 554.09 89.79 o 14 1 0 2588.64 2268.80 149.28 o 15 1 0 44.76 11.45 73.92 o 16 1 0 226.88 229.85 77.56 o 0 2 0 114.20 134.65 25.91 o 1 2 0 235.57 280.82 16.57 o 2 2 0 1923.69 1896.53 36.94 o 3 2 0 4512.43 4663.28 74.18 o 4 2 0 8365.54 8820.91 177.23 o 5 2 0 413.24 462.24 29.42 o 6 2 0 6928.48 6644.35 101.02 o 7 2 0 3.13 8.63 20.74 o 8 2 0 631.84 756.12 49.17 o 9 2 0 206.09 195.39 34.91 o 10 2 0 2950.70 2838.80 81.21 o 11 2 0 1012.60 942.69 56.45 o 12 2 0 2276.80 2570.43 143.13 o 13 2 0 88.62 -36.40 53.93 o 14 2 0 246.61 358.25 78.73 o 15 2 0 15.21 -15.54 60.71 o 16 2 0 1451.59 1445.90 135.42 o 1 3 0 10234.38 11673.95 122.84 o 2 3 0 9407.06 9673.72 110.47 o 3 3 0 13039.14 13368.76 151.56 o 4 3 0 803.03 796.63 47.11 o 5 3 0 58003.69 62597.83 568.81 o 6 3 0 4785.66 4653.99 81.53 o 7 3 0 1454.36 1448.62 54.87 o 8 3 0 10249.47 9347.86 171.69 o 9 3 0 2663.74 2668.60 84.45 o 10 3 0 5471.81 5074.97 116.14 o 11 3 0 565.09 588.94 48.24 o 12 3 0 19.25 76.03 55.31 o 13 3 0 13.79 -72.55 48.37 o 14 3 0 53.03 21.96 59.72 o 15 3 0 196.57 267.31 75.99 o 16 3 0 20.53 86.27 74.49 o 0 4 0 143445.86 153225.38 6531.18 o 1 4 0 2763.53 2988.39 45.91 o 2 4 0 13910.81 14643.97 158.19 o 3 4 0 5884.31 6259.54 87.11 o 4 4 0 78.36 12.89 16.89 o 5 4 0 3563.97 3815.49 68.01 o 6 4 0 364.76 260.22 26.65 o 7 4 0 10505.83 10850.48 148.35 o 8 4 0 255.98 354.42 34.35 o 9 4 0 291.91 507.71 53.00 o 10 4 0 497.08 517.83 48.47 o 11 4 0 2417.48 2413.46 111.92 o 12 4 0 6111.75 5920.60 189.10 o 13 4 0 1282.19 1208.85 109.84 o 14 4 0 1187.20 1105.53 110.15 o 15 4 0 298.97 139.39 69.96 o 16 4 0 877.78 801.60 113.02 o 1 5 0 22817.36 24784.30 249.61 o 2 5 0 1793.94 2069.36 42.77 o 3 5 0 4900.48 5231.60 79.28 o 4 5 0 14302.01 15281.77 180.05 o 5 5 0 826.71 881.09 50.13 o 6 5 0 38.73 92.91 21.04 o 7 5 0 363.59 312.02 30.96 o 8 5 0 13093.37 13062.93 174.10 o 9 5 0 29.25 27.07 26.02 o 10 5 0 3700.27 3586.00 101.65 o 11 5 0 167.76 116.50 47.86 o 12 5 0 375.71 359.74 69.94 o 13 5 0 1397.97 1399.35 116.01 o 14 5 0 141.48 171.85 66.54 o 15 5 0 40.65 40.21 64.26 o 16 5 0 41.83 120.88 72.27 o 0 6 0 417.11 364.41 34.37 o 1 6 0 32973.89 35038.45 346.51 o 2 6 0 10082.13 10845.27 149.91 o 3 6 0 864.07 843.21 36.09 o 4 6 0 14896.61 15233.24 181.97 o 5 6 0 2234.11 2113.89 55.57 o 6 6 0 2133.86 1995.86 55.68 o 7 6 0 353.65 420.68 34.45 o 8 6 0 526.20 531.70 40.32 o 9 6 0 1054.67 1049.24 55.77 o 10 6 0 2346.72 2327.26 89.63 o 11 6 0 6365.85 6018.53 159.40 o 12 6 0 1665.87 1661.87 124.33 o 13 6 0 121.84 13.98 58.03 o 14 6 0 17.12 23.18 62.23 o 15 6 0 170.75 251.43 73.53 o 16 6 0 377.28 393.27 85.73 o 1 7 0 65480.88 71235.57 626.23 o 2 7 0 489.95 532.73 29.92 o 3 7 0 19047.43 19182.64 215.22 o 4 7 0 555.32 418.23 30.94 o 5 7 0 21744.49 22342.44 235.92 o 6 7 0 3356.86 3045.74 67.28 o 7 7 0 13090.57 12655.21 165.35 o 8 7 0 8437.01 8464.01 132.22 o 9 7 0 3254.72 3156.32 83.36 o 10 7 0 1286.23 1284.68 65.00 o 11 7 0 14821.01 13664.39 258.84 o 12 7 0 1781.83 1680.29 119.91 o 13 7 0 175.02 129.82 59.99 o 14 7 0 1022.78 1090.14 121.74 o 15 7 0 37.09 10.90 66.15 o 16 7 0 11.62 37.24 90.18 o 0 8 0 38626.21 41988.75 589.42 o 1 8 0 1549.06 1761.30 38.06 o 2 8 0 1189.71 1418.90 44.83 o 3 8 0 15191.71 16394.91 193.05 o 4 8 0 3552.53 3832.09 74.56 o 5 8 0 30527.52 30551.23 307.01 o 6 8 0 9709.81 9799.56 133.91 o 7 8 0 22451.38 22255.60 251.48 o 8 8 0 480.87 476.40 38.50 o 9 8 0 2983.03 2886.47 82.04 o 10 8 0 237.77 274.00 38.99 o 11 8 0 23.18 64.26 46.43 o 12 8 0 3765.77 3410.90 171.08 o 13 8 0 14.83 21.66 62.14 o 14 8 0 399.93 563.94 93.13 o 15 8 0 72.20 222.94 114.23 o 1 9 0 13532.43 14063.48 152.05 o 2 9 0 1918.94 1661.23 51.49 o 3 9 0 7.63 12.07 18.45 o 4 9 0 219.37 205.23 21.45 o 5 9 0 23.21 31.69 17.98 o 6 9 0 14.55 -14.77 19.57 o 7 9 0 4670.41 4323.11 102.03 o 8 9 0 4726.43 4717.25 95.01 o 9 9 0 1222.84 1244.96 72.35 o 10 9 0 2465.44 2443.49 84.23 o 11 9 0 248.80 333.03 58.33 o 12 9 0 1044.48 931.37 95.43 o 13 9 0 1420.17 1557.85 120.76 o 14 9 0 6.15 48.52 66.45 o 15 9 0 298.54 426.95 94.40 o 0 10 0 110.15 144.12 30.03 o 1 10 0 1279.61 1538.12 39.85 o 2 10 0 10874.79 11564.59 151.88 o 3 10 0 20.72 20.27 20.50 o 4 10 0 3096.37 3405.88 63.51 o 5 10 0 3841.17 3793.92 71.90 o 6 10 0 11823.26 11867.74 202.63 o 7 10 0 669.92 723.08 42.35 o 8 10 0 4125.96 4159.81 93.10 o 9 10 0 110.82 161.32 32.33 o 10 10 0 13763.97 12780.57 200.30 o 11 10 0 4896.81 4694.66 178.00 o 12 10 0 242.58 197.75 52.92 o 13 10 0 23.53 37.46 70.24 o 14 10 0 802.94 685.51 112.31 o 15 10 0 447.13 631.62 190.26 o 1 11 0 27157.16 28893.75 285.02 o 2 11 0 7553.05 7997.72 121.03 o 3 11 0 25038.99 27144.16 303.82 o 4 11 0 2353.25 2631.05 56.62 o 5 11 0 8094.36 8130.09 120.19 o 6 11 0 6354.54 6327.48 147.15 o 7 11 0 2744.19 2714.45 71.34 o 8 11 0 195.32 225.45 42.48 o 9 11 0 735.87 729.28 49.72 o 10 11 0 31.30 20.38 36.01 o 11 11 0 5.93 38.02 41.74 o 12 11 0 1721.48 2191.26 168.82 o 13 11 0 1208.70 1245.23 177.73 o 14 11 0 52.78 81.71 77.62 o 15 11 0 195.68 335.92 96.09 o 0 12 0 14919.92 16705.79 245.52 o 1 12 0 30970.33 32000.15 314.87 o 2 12 0 662.75 783.27 42.88 o 3 12 0 2400.69 2524.99 70.28 o 4 12 0 11.02 0.76 22.36 o 5 12 0 148.64 302.40 28.75 o 6 12 0 27.92 -4.64 20.28 o 7 12 0 13241.96 13152.56 214.94 o 8 12 0 2129.62 2085.47 69.62 o 9 12 0 3102.99 3031.48 97.47 o 10 12 0 786.98 778.60 60.65 o 11 12 0 12.98 13.99 71.71 o 12 12 0 1445.23 1403.93 113.03 o 13 12 0 3491.12 3578.75 271.91 o 14 12 0 76.09 81.28 70.64 o 15 12 0 66.23 149.35 113.51 o 1 13 0 13474.23 13312.47 158.00 o 2 13 0 548.05 534.78 39.35 o 3 13 0 1032.32 1103.70 52.89 o 4 13 0 2212.83 2213.34 74.86 o 5 13 0 2357.14 2356.24 59.34 o 6 13 0 1315.01 1383.08 51.32 o 7 13 0 181.40 279.33 44.64 o 8 13 0 274.93 276.84 34.73 o 9 13 0 2506.76 2389.56 90.76 o 10 13 0 257.92 305.69 52.52 o 11 13 0 264.33 361.52 87.83 o 12 13 0 509.95 369.96 73.94 o 13 13 0 2107.55 2225.66 174.41 o 14 13 0 23.53 79.14 81.40 o 15 13 0 1150.16 1396.09 158.05 o 0 14 0 1940.01 1668.00 67.58 o 1 14 0 10043.28 9932.22 130.32 o 2 14 0 18199.55 19685.85 243.78 o 3 14 0 9808.77 9756.86 160.25 o 4 14 0 1191.66 1348.26 75.94 o 5 14 0 6867.31 6142.11 117.76 o 6 14 0 3606.77 3704.15 105.45 o 7 14 0 1037.22 1170.65 51.87 o 8 14 0 1546.55 1537.65 73.86 o 9 14 0 3819.27 3701.64 128.87 o 10 14 0 956.04 1040.91 98.89 o 11 14 0 2684.92 2378.96 142.52 o 12 14 0 179.24 118.49 64.74 o 13 14 0 544.50 661.67 138.96 o 14 14 0 314.63 526.33 220.74 o 15 14 0 1242.95 1632.33 168.96 o 1 15 0 8650.55 8254.97 134.75 o 2 15 0 2691.35 2145.98 70.83 o 3 15 0 125.40 80.63 28.68 o 4 15 0 2912.10 2388.55 78.45 o 5 15 0 2355.84 2722.96 84.00 o 6 15 0 8692.09 8596.28 128.70 o 7 15 0 7138.82 6722.23 133.14 o 8 15 0 17.37 25.38 36.67 o 9 15 0 2270.92 2563.42 115.93 o 10 15 0 948.92 967.31 80.42 o 11 15 0 399.62 436.61 78.78 o 12 15 0 317.46 414.23 83.63 o 13 15 0 31.31 80.99 82.56 o 14 15 0 1250.46 1417.85 156.13 o 0 16 0 41558.94 41511.56 542.99 o 1 16 0 9318.36 9201.64 130.47 o 2 16 0 8448.34 7860.50 135.19 o 3 16 0 8553.40 9415.84 154.08 o 4 16 0 2315.43 2305.63 79.45 o 5 16 0 1236.36 1304.69 65.62 o 6 16 0 1193.31 1249.72 69.04 o 7 16 0 5879.00 5544.52 124.55 o 8 16 0 786.89 883.90 73.09 o 9 16 0 682.21 659.63 68.10 o 10 16 0 2.00 25.30 44.28 o 11 16 0 20.39 69.87 58.53 o 12 16 0 2704.30 2897.65 179.01 o 13 16 0 878.99 873.30 129.99 o 14 16 0 215.11 257.89 102.43 o 1 17 0 1668.50 1634.47 55.83 o 2 17 0 401.01 460.08 42.85 o 3 17 0 6313.32 6063.61 121.84 o 4 17 0 363.67 378.04 43.81 o 5 17 0 3507.98 3438.59 98.13 o 6 17 0 4188.70 3929.43 105.24 o 7 17 0 275.70 317.16 82.99 o 8 17 0 2603.82 2587.82 117.85 o 9 17 0 287.37 381.59 123.65 o 10 17 0 69.21 138.28 49.15 o 11 17 0 103.83 230.33 66.34 o 12 17 0 107.41 202.50 67.43 o 13 17 0 199.73 229.21 86.04 o 14 17 0 113.39 356.18 132.97 o 0 18 0 3035.47 3107.94 150.11 o 1 18 0 7792.68 7916.45 120.02 o 2 18 0 15525.55 15151.64 216.43 o 3 18 0 10006.21 9610.20 162.52 o 4 18 0 11354.24 11156.96 181.76 o 5 18 0 9574.39 9126.11 163.73 o 6 18 0 7603.47 7143.77 144.58 o 7 18 0 588.79 723.01 69.92 o 8 18 0 1.55 18.96 49.39 o 9 18 0 388.67 485.08 64.70 o 10 18 0 8.10 -40.76 43.28 o 11 18 0 666.93 739.86 90.66 o 12 18 0 272.10 287.53 78.25 o 13 18 0 1112.31 1134.58 137.64 o 14 18 0 240.89 342.87 105.92 o 1 19 0 22.18 65.25 23.52 o 2 19 0 2908.40 2907.53 90.73 o 3 19 0 2390.70 2304.21 87.65 o 4 19 0 5980.90 5736.28 150.71 o 5 19 0 1736.91 1752.01 82.06 o 6 19 0 4414.87 3817.94 110.78 o 7 19 0 5894.18 5402.20 150.09 o 8 19 0 134.03 172.43 50.61 o 9 19 0 721.59 623.45 74.82 o 10 19 0 2051.31 1904.95 116.46 o 11 19 0 80.10 168.65 74.78 o 12 19 0 1442.00 1507.30 131.97 o 13 19 0 8.16 228.60 90.56 o 0 20 0 8106.06 7291.82 163.98 o 1 20 0 2207.95 2255.14 65.45 o 2 20 0 514.87 651.85 75.45 o 3 20 0 8.48 -44.57 29.71 o 4 20 0 2112.84 2120.13 90.11 o 5 20 0 1222.78 1105.76 70.10 o 6 20 0 6984.87 6412.00 224.61 o 7 20 0 2667.59 2554.51 121.72 o 8 20 0 1075.04 1190.89 89.53 o 9 20 0 78.63 148.33 54.69 o 10 20 0 812.67 846.74 86.88 o 11 20 0 1555.86 1459.15 125.83 o 12 20 0 347.88 561.76 109.57 o 13 20 0 241.92 504.35 104.83 o 1 21 0 3888.11 3788.13 98.03 o 2 21 0 95.62 74.32 33.24 o 3 21 0 2112.86 2086.43 94.98 o 4 21 0 9.33 -1.29 33.76 o 5 21 0 2121.49 2333.30 96.41 o 6 21 0 219.40 309.99 58.23 o 7 21 0 1041.80 1185.11 88.87 o 8 21 0 146.22 155.42 52.89 o 9 21 0 125.66 145.00 54.07 o 10 21 0 78.32 222.97 60.11 o 11 21 0 92.67 71.26 65.50 o 12 21 0 466.23 600.05 132.55 o 13 21 0 11.75 14.26 78.69 o 0 22 0 439.26 491.12 55.94 o 1 22 0 732.85 811.88 55.47 o 2 22 0 1706.11 1739.98 93.30 o 3 22 0 225.37 242.29 44.92 o 4 22 0 49.10 29.47 37.43 o 5 22 0 354.29 411.50 60.03 o 6 22 0 504.78 596.16 71.27 o 7 22 0 1047.07 1070.21 88.26 o 8 22 0 946.87 864.27 85.22 o 9 22 0 74.56 125.31 54.19 o 10 22 0 202.26 299.68 65.95 o 11 22 0 0.35 47.14 68.32 o 12 22 0 461.41 738.37 106.10 o 1 23 0 2720.94 2504.44 88.83 o 2 23 0 2810.65 2637.21 110.80 o 3 23 0 170.64 181.47 43.56 o 4 23 0 1437.83 1296.42 77.49 o 5 23 0 3905.26 3530.59 138.41 o 6 23 0 522.73 543.43 68.94 o 7 23 0 715.96 560.01 71.81 o 8 23 0 714.09 667.62 77.60 o 9 23 0 816.83 1015.10 128.40 o 10 23 0 10.93 89.43 58.66 o 11 23 0 3163.46 3251.80 186.32 o 12 23 0 2.76 -105.83 70.55 o 0 24 0 7492.38 6910.03 216.34 o 1 24 0 8.13 10.29 37.95 o 2 24 0 418.58 453.77 50.33 o 3 24 0 1.56 -38.88 35.06 o 4 24 0 2096.51 1977.66 132.66 o 5 24 0 507.00 344.22 73.07 o 6 24 0 4257.44 4035.31 154.12 o 7 24 0 311.53 393.23 66.28 o 8 24 0 439.08 427.49 70.50 o 9 24 0 87.42 63.76 58.32 o 10 24 0 594.65 716.25 89.56 o 11 24 0 266.27 323.55 86.71 o 12 24 0 271.41 304.92 88.08 o 1 25 0 55.67 38.94 40.35 o 2 25 0 13.37 29.73 41.62 o 3 25 0 959.91 918.01 65.82 o 4 25 0 1301.71 1283.65 93.84 o 5 25 0 43.26 82.20 51.87 o 6 25 0 54.98 157.24 55.50 o 7 25 0 834.10 812.43 85.38 o 8 25 0 358.88 398.97 72.77 o 9 25 0 137.58 246.55 70.48 o 10 25 0 286.30 397.15 90.47 o 11 25 0 3.49 67.11 72.66 o 0 26 0 960.77 861.41 102.92 o 1 26 0 1461.89 1523.23 89.48 o 2 26 0 417.42 424.66 58.19 o 3 26 0 4.71 67.63 49.87 o 4 26 0 123.30 160.95 53.25 o 5 26 0 246.57 178.52 57.43 o 6 26 0 1473.83 1457.34 104.69 o 7 26 0 276.63 283.80 69.93 o 8 26 0 1087.54 989.19 95.75 o 9 26 0 399.23 503.81 78.36 o 10 26 0 874.92 900.41 109.73 o 11 26 0 8.56 38.40 81.34 o 1 27 0 2370.52 2322.72 136.43 o 2 27 0 332.76 380.71 58.31 o 3 27 0 758.37 788.63 72.07 o 4 27 0 13.98 -33.55 44.85 o 5 27 0 3088.84 3066.07 143.55 o 6 27 0 154.30 183.80 71.56 o 7 27 0 7.23 100.11 68.69 o 8 27 0 62.24 117.39 64.75 o 9 27 0 26.46 105.34 64.05 o 10 27 0 31.35 67.91 72.23 o 0 28 0 2852.06 2638.17 165.87 o 1 28 0 2675.65 2513.76 115.82 o 2 28 0 14.46 -33.79 50.91 o 3 28 0 201.29 317.42 78.09 o 4 28 0 160.33 246.32 61.31 o 5 28 0 262.19 301.08 64.25 o 6 28 0 141.15 185.96 66.67 o 7 28 0 894.00 875.02 109.63 o 8 28 0 131.68 215.36 70.06 o 9 28 0 159.52 425.83 80.50 o 10 28 0 196.63 337.65 86.80 o 1 29 0 339.85 258.00 54.14 o 2 29 0 151.84 119.26 49.73 o 3 29 0 2.05 15.58 52.24 o 4 29 0 3.63 47.83 56.56 o 5 29 0 422.46 439.03 76.56 o 6 29 0 15.42 102.28 60.75 o 7 29 0 368.70 362.01 90.88 o 8 29 0 32.74 193.78 73.43 o 9 29 0 18.77 116.59 71.66 o 0 30 0 892.32 995.15 116.42 o 1 30 0 237.66 295.99 58.81 o 2 30 0 350.79 490.37 75.19 o 3 30 0 39.66 -32.91 52.62 o 4 30 0 347.80 252.34 68.09 o 5 30 0 68.50 74.63 58.82 o 6 30 0 726.43 611.60 83.72 o 7 30 0 378.12 371.08 77.17 o 8 30 0 445.38 450.18 98.53 o 1 31 0 790.80 815.68 77.51 o 2 31 0 365.40 359.43 71.71 o 3 31 0 82.02 140.02 64.36 o 4 31 0 1590.74 1478.42 115.61 o 5 31 0 1430.19 1348.41 109.06 o 6 31 0 303.08 458.80 82.50 o 7 31 0 466.90 517.19 84.26 o 8 31 0 11.15 167.51 74.37 o 0 32 0 615.36 603.03 103.48 o 1 32 0 2226.81 1991.57 127.68 o 2 32 0 4.77 92.99 65.24 o 3 32 0 970.29 1138.93 104.83 o 4 32 0 1.83 113.58 64.37 o 5 32 0 23.28 127.50 69.69 o 6 32 0 40.05 151.14 68.69 o 7 32 0 18.34 137.59 70.24 o 1 33 0 140.39 157.82 63.11 o 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236.27 109.75 o -6 3 20 133.67 47.86 81.81 o -5 3 20 115.94 101.41 66.29 o -4 3 20 8.42 106.18 69.63 o -3 3 20 113.68 436.53 95.66 o -2 3 20 22.96 155.54 64.62 o -1 3 20 22.77 140.97 55.52 o 0 3 20 26.86 148.39 53.48 o 1 3 20 3.65 109.05 52.70 o 2 3 20 14.63 105.15 52.80 o 3 3 20 83.28 113.74 58.49 o 4 3 20 170.63 226.06 69.17 o 5 3 20 351.23 321.16 84.78 o 6 3 20 99.43 172.31 93.16 o -6 4 20 164.79 234.43 76.01 o -5 4 20 241.20 564.10 88.66 o -4 4 20 1195.01 1344.40 144.88 o -3 4 20 70.99 172.88 66.93 o -2 4 20 794.43 1052.35 143.56 o -1 4 20 41.24 105.19 51.39 o 0 4 20 425.42 539.56 69.76 o 1 4 20 78.67 103.29 54.41 o 2 4 20 3.94 53.80 57.38 o 3 4 20 329.10 384.70 101.11 o 4 4 20 74.79 58.77 68.12 o 5 4 20 152.97 257.21 85.84 o 6 4 20 94.92 73.77 91.83 o -6 5 20 96.89 204.18 76.48 o -5 5 20 261.17 252.42 83.40 o -4 5 20 28.83 187.11 71.94 o -3 5 20 466.43 624.70 91.52 o -2 5 20 5.46 77.88 103.21 o -1 5 20 1.56 64.51 52.55 o 0 5 20 741.93 817.95 76.96 o 1 5 20 46.56 20.82 53.08 o 2 5 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