#------------------------------------------------------------------------------ #$Date: 2009-09-11 11:49:26 +0300 (Fri, 11 Sep 2009) $ #$Revision: 819 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2222833.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2222833_Fobs loop_ _publ_author_name 'Mahmoodi, Niusha' 'Ne\H,3H)-dione ; _journal_coeditor_code PK2176 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1866 _journal_volume 65 _journal_year 2009 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 113.111 _cell_angle_gamma 90.000 _cell_length_a 9.9714 _cell_length_b 24.1041 _cell_length_c 9.3805 _exptl_crystal_F_000 856.00 _reflns_d_resolution_high 0.8409 _[local]_cod_data_source_file pk2176Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' v in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 259.45 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 67316.09 64854.15 461.45 o 3 0 0 9356.75 9203.02 87.20 o 4 0 0 3571.20 3653.84 41.58 o 5 0 0 823.60 721.70 10.82 o 6 0 0 708.17 697.40 42.02 o 7 0 0 385.74 376.55 22.18 o 8 0 0 479.15 454.39 32.07 o 9 0 0 25.98 47.09 25.42 o 10 0 0 5.10 0.00 45.47 o 2 1 0 16637.59 16584.14 57.19 o 3 1 0 5551.57 5698.87 28.31 o 4 1 0 6032.44 6083.52 40.22 o 5 1 0 841.25 892.07 15.89 o 6 1 0 1257.55 1257.11 31.65 o 7 1 0 65.53 56.96 13.30 o 8 1 0 74.11 68.80 15.12 o 9 1 0 93.85 88.34 22.60 o 10 1 0 3.85 0.00 26.43 o 1 2 0 2603.00 1292.53 16.24 o 2 2 0 2537.86 2393.94 34.94 o 3 2 0 70.32 61.74 4.51 o 4 2 0 10746.52 11071.31 64.01 o 5 2 0 969.14 1025.90 16.50 o 6 2 0 2303.44 2400.55 34.40 o 7 2 0 3.40 0.00 11.26 o 8 2 0 118.66 59.57 18.48 o 9 2 0 86.23 61.90 21.15 o 10 2 0 4.06 0.00 25.77 o 1 3 0 1878.42 1892.23 19.17 o 2 3 0 965.61 918.90 8.84 o 3 3 0 13872.80 14013.70 121.07 o 4 3 0 5132.57 5234.94 42.81 o 5 3 0 2598.02 2502.39 33.75 o 6 3 0 4575.38 4560.44 74.49 o 7 3 0 251.82 248.83 17.26 o 8 3 0 536.93 439.45 20.64 o 9 3 0 0.45 0.00 21.14 o 10 3 0 11.72 14.42 26.48 o 0 4 0 21703.86 20626.94 43.68 o 1 4 0 1118.30 870.01 6.63 o 2 4 0 6580.70 7000.57 48.35 o 3 4 0 285.64 307.85 5.23 o 4 4 0 110.89 114.37 5.18 o 5 4 0 178.15 173.15 7.14 o 6 4 0 489.79 492.03 11.94 o 7 4 0 1214.93 1178.28 25.23 o 8 4 0 880.18 810.61 28.65 o 9 4 0 196.62 183.40 25.82 o 10 4 0 255.53 239.34 41.05 o 1 5 0 1194.47 1149.64 9.23 o 2 5 0 245.85 267.55 5.16 o 3 5 0 1350.44 1371.74 15.44 o 4 5 0 2849.98 3083.54 32.19 o 5 5 0 972.87 986.09 10.62 o 6 5 0 241.25 256.96 11.03 o 7 5 0 2425.18 2445.15 72.77 o 8 5 0 388.87 398.69 20.91 o 9 5 0 633.26 583.24 33.71 o 10 5 0 364.59 408.65 38.93 o 0 6 0 86.32 95.35 7.14 o 1 6 0 196.17 214.57 4.94 o 2 6 0 3927.90 4145.24 31.92 o 3 6 0 452.37 456.90 5.29 o 4 6 0 3470.31 3501.58 38.98 o 5 6 0 325.07 314.14 9.60 o 6 6 0 219.70 227.48 9.45 o 7 6 0 96.96 84.41 16.57 o 8 6 0 174.07 145.66 27.78 o 9 6 0 1247.84 1189.98 75.31 o 10 6 0 3.53 1.70 30.84 o 1 7 0 3608.18 3469.59 24.52 o 2 7 0 2.42 11.57 3.95 o 3 7 0 499.33 501.94 5.65 o 4 7 0 1471.43 1508.05 11.21 o 5 7 0 55.82 42.44 7.46 o 6 7 0 229.26 198.98 9.90 o 7 7 0 384.81 387.12 15.04 o 8 7 0 40.98 22.33 19.81 o 9 7 0 11.33 6.97 25.26 o 10 7 0 98.58 114.33 36.36 o 0 8 0 3176.02 3001.00 25.84 o 1 8 0 117.09 147.09 4.91 o 2 8 0 123.37 150.90 4.49 o 3 8 0 41.70 51.61 4.59 o 4 8 0 380.14 352.94 5.60 o 5 8 0 758.73 753.66 11.55 o 6 8 0 165.12 134.35 11.38 o 7 8 0 1085.47 1066.22 19.85 o 8 8 0 15.96 17.69 20.38 o 9 8 0 53.48 49.59 27.25 o 10 8 0 234.52 194.83 41.71 o 1 9 0 1741.16 1641.44 14.53 o 2 9 0 1762.95 1589.94 13.67 o 3 9 0 163.63 141.29 5.13 o 4 9 0 0.12 0.55 4.70 o 5 9 0 94.90 100.13 10.91 o 6 9 0 2.14 1.14 9.90 o 7 9 0 80.43 71.85 14.17 o 8 9 0 39.58 54.67 23.54 o 9 9 0 33.35 5.93 27.68 o 10 9 0 252.94 296.54 42.13 o 0 10 0 338.07 350.44 7.07 o 1 10 0 1544.32 1526.23 12.82 o 2 10 0 0.03 4.09 4.64 o 3 10 0 2609.60 2914.96 32.17 o 4 10 0 12.03 5.93 5.46 o 5 10 0 51.34 63.22 10.50 o 6 10 0 14.13 11.41 11.61 o 7 10 0 69.40 83.76 14.82 o 8 10 0 4.02 0.00 24.53 o 9 10 0 9.65 7.26 28.60 o 10 10 0 30.54 12.91 35.31 o 1 11 0 6611.53 7133.04 48.07 o 2 11 0 372.85 421.10 6.62 o 3 11 0 959.80 1007.45 12.53 o 4 11 0 400.75 445.80 7.54 o 5 11 0 28.70 30.23 9.14 o 6 11 0 240.57 233.96 13.82 o 7 11 0 2.31 0.00 15.52 o 8 11 0 4.54 0.00 24.73 o 9 11 0 0.43 2.24 30.04 o 10 11 0 8.08 8.22 36.72 o 0 12 0 6237.61 7006.56 79.51 o 1 12 0 97.22 154.78 9.00 o 2 12 0 449.61 481.93 7.12 o 3 12 0 669.54 660.29 8.83 o 4 12 0 34.17 35.21 6.71 o 5 12 0 813.29 830.84 16.61 o 6 12 0 33.61 28.84 14.05 o 7 12 0 512.05 511.77 17.78 o 8 12 0 139.43 139.43 24.97 o 9 12 0 0.30 0.00 32.02 o 1 13 0 0.31 5.58 5.55 o 2 13 0 87.59 64.55 6.78 o 3 13 0 22.32 5.12 6.09 o 4 13 0 0.26 2.18 8.41 o 5 13 0 24.29 24.87 10.58 o 6 13 0 170.46 172.21 15.39 o 7 13 0 200.90 203.27 19.85 o 8 13 0 36.50 49.15 27.59 o 9 13 0 31.58 20.27 34.16 o 0 14 0 549.24 658.16 13.10 o 1 14 0 78.75 68.33 6.71 o 2 14 0 960.74 989.75 10.18 o 3 14 0 794.32 815.94 10.32 o 4 14 0 794.64 816.22 15.23 o 5 14 0 751.50 762.67 15.75 o 6 14 0 71.02 49.01 15.97 o 7 14 0 35.31 10.83 18.77 o 8 14 0 0.00 5.86 21.89 o 9 14 0 48.31 47.23 34.88 o 1 15 0 7.73 8.24 6.15 o 2 15 0 29.30 33.44 6.68 o 3 15 0 528.65 550.05 9.39 o 4 15 0 93.45 82.58 12.65 o 5 15 0 458.90 417.54 14.22 o 6 15 0 40.75 27.08 15.06 o 7 15 0 245.04 239.90 22.03 o 8 15 0 92.52 91.88 24.53 o 9 15 0 4.57 0.00 37.16 o 0 16 0 4.16 0.00 10.09 o 1 16 0 202.83 217.23 9.24 o 2 16 0 73.83 70.25 7.87 o 3 16 0 215.14 216.74 10.06 o 4 16 0 270.45 283.33 13.31 o 5 16 0 53.11 45.96 12.93 o 6 16 0 1226.72 1260.68 22.40 o 7 16 0 30.17 26.43 19.57 o 8 16 0 178.19 126.59 27.67 o 9 16 0 0.35 0.00 38.42 o 1 17 0 695.09 670.46 10.50 o 2 17 0 7.08 9.81 8.19 o 3 17 0 637.49 684.93 11.80 o 4 17 0 381.18 349.97 14.28 o 5 17 0 0.38 0.00 13.67 o 6 17 0 21.82 29.02 17.04 o 7 17 0 39.28 40.06 19.70 o 8 17 0 225.24 262.22 28.02 o 0 18 0 214.58 238.46 13.44 o 1 18 0 0.40 12.20 7.71 o 2 18 0 2.82 1.47 8.90 o 3 18 0 119.53 119.85 12.44 o 4 18 0 3.98 0.00 13.57 o 5 18 0 315.16 313.34 17.39 o 6 18 0 111.39 95.88 18.64 o 7 18 0 38.31 8.97 23.69 o 8 18 0 12.02 0.00 25.64 o 1 19 0 102.41 130.83 9.75 o 2 19 0 15.76 6.79 9.80 o 3 19 0 213.13 185.93 12.44 o 4 19 0 23.86 18.82 15.46 o 5 19 0 16.74 5.89 17.12 o 6 19 0 2.42 0.00 17.49 o 7 19 0 1.03 0.00 22.49 o 8 19 0 3.88 0.00 28.02 o 0 20 0 721.62 733.82 18.78 o 1 20 0 484.17 490.66 10.96 o 2 20 0 0.22 0.00 10.96 o 3 20 0 458.76 444.29 15.90 o 4 20 0 126.63 112.42 17.26 o 5 20 0 19.94 20.85 19.38 o 6 20 0 0.28 0.00 18.65 o 7 20 0 3.17 0.00 23.58 o 1 21 0 17.89 25.73 10.24 o 2 21 0 112.10 86.63 13.52 o 3 21 0 294.26 280.58 19.04 o 4 21 0 8.57 13.59 17.12 o 5 21 0 5.05 6.72 19.41 o 6 21 0 0.09 0.00 23.06 o 7 21 0 0.52 0.00 26.25 o 0 22 0 81.74 97.65 14.89 o 1 22 0 45.18 40.25 12.19 o 2 22 0 14.98 14.23 13.63 o 3 22 0 6.68 0.00 16.59 o 4 22 0 74.18 69.50 18.57 o 5 22 0 19.28 9.00 21.04 o 6 22 0 80.09 89.70 26.05 o 1 23 0 135.23 92.93 14.31 o 2 23 0 191.66 170.62 15.31 o 3 23 0 5.12 0.00 18.55 o 4 23 0 67.55 75.65 21.86 o 5 23 0 0.04 0.00 22.87 o 6 23 0 90.05 69.51 26.55 o 0 24 0 100.79 77.46 18.77 o 1 24 0 21.78 22.77 12.92 o 2 24 0 8.96 6.83 15.17 o 3 24 0 0.06 3.63 20.50 o 4 24 0 11.11 17.33 22.66 o 5 24 0 4.64 1.31 25.07 o 1 25 0 5.77 0.19 14.15 o 2 25 0 1.68 5.50 15.67 o 3 25 0 106.13 95.99 24.91 o 4 25 0 41.78 49.72 24.23 o 5 25 0 51.93 49.09 27.60 o 0 26 0 10.61 1.14 21.15 o 1 26 0 29.76 23.37 16.87 o 2 26 0 2.61 15.98 18.25 o 3 26 0 138.43 163.85 26.90 o 4 26 0 0.58 0.00 26.65 o 1 27 0 37.48 27.18 18.57 o 2 27 0 30.79 65.44 22.53 o 3 27 0 3.50 36.76 24.45 o 0 28 0 2.60 11.22 29.77 o 1 28 0 23.22 25.22 24.19 o 2 28 0 4.16 9.87 31.53 o -11 1 1 13.65 24.31 38.32 o -10 1 1 63.51 31.98 30.39 o -9 1 1 46.80 42.73 19.78 o -8 1 1 668.56 653.11 21.24 o -7 1 1 28.53 31.86 11.33 o -6 1 1 18.27 27.60 7.29 o -5 1 1 136.81 139.03 4.19 o -4 1 1 901.33 990.27 8.84 o -3 1 1 102.94 128.21 3.90 o -2 1 1 1870.15 2039.25 21.15 o 1 1 1 1698.12 1954.66 12.48 o 2 1 1 3667.37 3788.92 28.05 o 3 1 1 125.27 110.98 5.07 o 4 1 1 3640.40 3860.92 29.58 o 5 1 1 354.68 351.51 7.65 o 6 1 1 182.23 165.11 10.71 o 7 1 1 11.05 11.94 11.99 o 8 1 1 34.77 38.23 15.67 o 9 1 1 7.16 0.00 19.25 o 10 1 1 40.68 34.92 29.70 o -11 2 1 19.50 9.23 39.04 o -10 2 1 1.94 14.12 23.86 o -9 2 1 1.79 2.35 18.77 o -8 2 1 97.11 91.51 16.47 o -7 2 1 168.89 146.63 15.92 o -6 2 1 5.74 5.27 6.11 o -5 2 1 822.11 913.85 8.47 o -4 2 1 417.56 403.27 6.01 o -3 2 1 1675.14 1642.51 13.67 o -2 2 1 6414.82 6537.71 34.85 o -1 2 1 1196.16 1168.36 12.56 o 0 2 1 17014.43 16742.66 45.07 o 1 2 1 1731.25 1812.50 14.80 o 2 2 1 607.26 605.88 9.18 o 3 2 1 132.73 133.19 5.24 o 4 2 1 4305.12 4334.76 30.51 o 5 2 1 206.36 217.09 7.78 o 6 2 1 5.48 5.34 8.36 o 7 2 1 193.28 201.92 15.07 o 8 2 1 85.58 106.05 18.17 o 9 2 1 22.37 37.54 23.39 o 10 2 1 37.71 31.87 31.30 o -11 3 1 48.95 43.52 31.29 o -10 3 1 25.13 0.00 24.43 o -9 3 1 51.80 58.58 19.08 o -8 3 1 272.80 246.21 19.59 o -7 3 1 317.66 306.11 16.92 o -6 3 1 881.46 912.20 10.13 o -5 3 1 866.66 895.51 11.47 o -4 3 1 3.17 1.75 4.35 o -3 3 1 2959.01 2910.00 26.82 o -2 3 1 5.75 1.07 3.54 o -1 3 1 10977.70 10452.78 76.00 o 0 3 1 1111.36 1428.05 11.65 o 1 3 1 4299.52 4624.47 42.06 o 2 3 1 416.39 367.76 6.53 o 3 3 1 63.82 67.91 5.28 o 4 3 1 348.49 325.39 6.93 o 5 3 1 246.00 213.49 7.74 o 6 3 1 23.74 15.03 8.66 o 7 3 1 69.94 79.94 13.95 o 8 3 1 78.47 70.89 21.62 o 9 3 1 14.16 22.86 22.69 o 10 3 1 26.47 41.60 36.03 o -11 4 1 73.25 119.99 40.69 o -10 4 1 30.45 22.07 24.58 o -9 4 1 10.93 5.45 18.75 o -8 4 1 1007.27 1028.53 29.34 o -7 4 1 10.06 8.10 12.92 o -6 4 1 230.50 240.92 9.50 o -5 4 1 200.20 211.10 6.31 o -4 4 1 250.55 274.80 5.52 o -3 4 1 188.02 173.86 5.02 o -2 4 1 3758.10 3683.01 28.14 o -1 4 1 1810.67 1761.58 13.46 o 0 4 1 20308.86 20316.30 78.86 o 1 4 1 40.82 39.13 4.65 o 2 4 1 8190.52 8247.92 62.54 o 3 4 1 340.36 377.40 7.07 o 4 4 1 7869.51 8320.35 59.48 o 5 4 1 931.28 892.25 11.54 o 6 4 1 5.31 11.18 9.74 o 7 4 1 534.90 508.88 26.08 o 8 4 1 20.79 16.59 19.02 o 9 4 1 346.56 314.12 36.45 o 10 4 1 156.12 136.33 42.38 o -11 5 1 14.26 6.09 37.03 o -10 5 1 14.78 0.00 29.00 o -9 5 1 22.37 19.09 18.88 o -8 5 1 48.03 22.12 15.36 o -7 5 1 6.94 7.06 12.57 o -6 5 1 10.58 8.62 8.09 o -5 5 1 354.11 400.50 8.00 o -4 5 1 66.13 57.52 5.80 o -3 5 1 120.41 133.93 3.83 o -2 5 1 6.94 2.30 3.59 o -1 5 1 232.25 208.47 4.37 o 0 5 1 11.85 8.75 4.07 o 1 5 1 130.50 163.16 5.62 o 2 5 1 77.65 87.56 4.83 o 3 5 1 1574.51 1685.19 23.65 o 4 5 1 1420.61 1467.16 18.27 o 5 5 1 117.47 95.80 8.53 o 6 5 1 1768.00 1824.76 48.21 o 7 5 1 139.49 154.05 19.38 o 8 5 1 220.39 154.16 26.10 o 9 5 1 120.02 106.67 31.87 o 10 5 1 0.01 14.08 38.02 o -11 6 1 4.55 0.00 40.00 o -10 6 1 0.76 0.00 30.57 o -9 6 1 255.00 254.15 30.29 o -8 6 1 117.83 110.43 18.33 o -7 6 1 88.59 75.20 16.29 o -6 6 1 608.54 618.07 18.04 o -5 6 1 253.70 274.66 7.03 o -4 6 1 10.31 12.30 3.95 o -3 6 1 89.15 87.23 3.77 o -2 6 1 918.86 953.90 12.73 o -1 6 1 57.26 68.49 4.15 o 0 6 1 612.61 723.00 7.43 o 1 6 1 46.24 26.53 4.73 o 2 6 1 0.43 0.00 4.92 o 3 6 1 1.75 5.26 4.81 o 4 6 1 60.04 61.63 7.35 o 5 6 1 721.76 672.61 10.49 o 6 6 1 97.85 93.66 12.26 o 7 6 1 1152.78 1171.71 31.23 o 8 6 1 43.95 61.90 24.38 o 9 6 1 23.95 18.47 29.69 o 10 6 1 0.79 0.00 36.27 o -10 7 1 5.45 4.22 32.49 o -9 7 1 24.65 12.99 23.97 o -8 7 1 8.35 1.04 17.94 o -7 7 1 367.26 334.32 17.44 o -6 7 1 116.28 106.68 10.11 o -5 7 1 425.20 404.15 7.84 o -4 7 1 482.82 417.35 5.24 o -3 7 1 40.25 55.07 3.79 o -2 7 1 2120.26 2286.07 24.78 o -1 7 1 629.97 682.95 6.33 o 0 7 1 219.05 213.16 4.79 o 1 7 1 416.56 387.12 6.55 o 2 7 1 3368.05 3235.70 43.46 o 3 7 1 367.55 386.84 6.77 o 4 7 1 45.16 35.28 7.37 o 5 7 1 249.26 253.90 9.46 o 6 7 1 4.91 10.03 11.48 o 7 7 1 1.57 1.45 14.18 o 8 7 1 813.54 796.18 71.46 o 9 7 1 100.45 106.15 33.17 o 10 7 1 332.06 346.76 45.64 o -10 8 1 130.02 101.07 33.29 o -9 8 1 52.10 62.97 25.66 o -8 8 1 364.86 330.85 24.82 o -7 8 1 408.48 397.14 16.58 o -6 8 1 121.12 119.24 10.41 o -5 8 1 140.02 153.38 7.60 o -4 8 1 1026.30 1020.61 8.47 o -3 8 1 1232.31 1229.06 14.24 o -2 8 1 36.63 43.38 4.52 o -1 8 1 667.34 683.91 6.64 o 0 8 1 915.91 979.33 8.37 o 1 8 1 1646.90 1575.53 17.11 o 2 8 1 504.61 515.36 8.64 o 3 8 1 73.50 65.39 5.77 o 4 8 1 0.69 5.39 5.95 o 5 8 1 609.57 581.28 15.85 o 6 8 1 80.53 73.09 14.06 o 7 8 1 151.64 171.39 18.73 o 8 8 1 0.37 0.00 24.25 o 9 8 1 134.59 141.09 36.85 o 10 8 1 4.83 4.29 39.38 o -10 9 1 25.28 31.89 33.15 o -9 9 1 27.31 28.33 26.94 o -8 9 1 5.14 6.08 20.78 o -7 9 1 71.94 55.47 13.79 o -6 9 1 35.70 31.38 10.05 o -5 9 1 146.75 131.95 8.23 o -4 9 1 15.01 5.34 4.70 o -3 9 1 56.76 57.99 4.76 o -2 9 1 20.77 16.10 4.52 o -1 9 1 107.13 93.61 4.40 o 0 9 1 1082.15 910.64 8.07 o 1 9 1 1035.75 853.06 7.79 o 2 9 1 56.32 61.98 5.81 o 3 9 1 4.74 1.09 5.15 o 4 9 1 681.98 722.91 9.95 o 5 9 1 1018.94 1002.46 19.74 o 6 9 1 31.95 33.70 13.23 o 7 9 1 602.39 586.78 16.94 o 8 9 1 87.02 48.89 27.46 o 9 9 1 27.01 25.64 35.15 o -10 10 1 14.25 0.00 33.94 o -9 10 1 69.65 39.38 27.04 o -8 10 1 464.08 446.10 29.09 o -7 10 1 395.90 389.30 15.30 o -6 10 1 14.63 17.15 9.62 o -5 10 1 36.40 39.95 8.53 o -4 10 1 111.82 101.76 6.07 o -3 10 1 248.42 268.90 5.57 o -2 10 1 81.98 83.91 5.36 o -1 10 1 740.70 799.79 7.59 o 0 10 1 170.76 184.44 5.17 o 1 10 1 75.38 90.27 5.08 o 2 10 1 196.95 182.03 5.83 o 3 10 1 290.85 324.80 6.64 o 4 10 1 33.41 32.67 7.56 o 5 10 1 666.79 638.51 16.85 o 6 10 1 474.12 503.29 18.01 o 7 10 1 684.04 676.17 16.45 o 8 10 1 6.35 0.00 29.88 o 9 10 1 2.92 0.00 35.64 o -10 11 1 55.09 55.67 35.14 o -9 11 1 275.69 273.08 36.12 o -8 11 1 103.38 80.01 28.26 o -7 11 1 346.05 374.29 15.97 o -6 11 1 99.02 100.33 12.01 o -5 11 1 18.53 15.99 8.26 o -4 11 1 7.79 7.83 6.19 o -3 11 1 123.38 160.95 6.00 o -2 11 1 494.76 397.99 6.55 o -1 11 1 2074.73 2084.96 17.48 o 0 11 1 1462.40 1491.62 12.16 o 1 11 1 7572.66 8012.75 54.62 o 2 11 1 54.61 48.65 5.83 o 3 11 1 1000.37 1067.56 11.49 o 4 11 1 219.01 210.75 7.98 o 5 11 1 76.78 63.44 10.44 o 6 11 1 0.42 0.00 11.97 o 7 11 1 131.73 130.13 17.21 o 8 11 1 2.09 0.00 27.69 o 9 11 1 63.82 75.88 35.20 o -10 12 1 1.52 2.53 38.71 o -9 12 1 9.30 5.99 29.59 o -8 12 1 19.90 8.62 24.03 o -7 12 1 315.64 321.16 16.74 o -6 12 1 552.96 555.36 13.92 o -5 12 1 16.77 13.77 8.32 o -4 12 1 485.94 464.47 8.98 o -3 12 1 271.85 217.14 6.54 o -2 12 1 399.58 381.61 6.92 o -1 12 1 368.57 430.85 7.15 o 0 12 1 62.92 55.07 5.75 o 1 12 1 2743.71 2828.11 23.90 o 2 12 1 142.99 154.09 6.57 o 3 12 1 53.04 59.54 6.65 o 4 12 1 54.65 62.62 7.95 o 5 12 1 29.72 19.02 10.04 o 6 12 1 84.02 68.58 14.50 o 7 12 1 144.10 157.85 18.26 o 8 12 1 2.47 0.00 29.26 o 9 12 1 13.06 31.49 35.14 o 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197.21 13.29 o 5 15 2 131.03 121.59 15.02 o 6 15 2 1.30 0.00 16.44 o 7 15 2 0.21 0.00 20.02 o 8 15 2 0.88 0.00 24.28 o -9 16 2 38.54 37.47 37.65 o -8 16 2 58.96 63.28 19.10 o -7 16 2 363.30 348.32 18.12 o -6 16 2 1053.39 1116.68 16.68 o -5 16 2 384.12 367.35 12.22 o -4 16 2 186.37 155.95 10.70 o -3 16 2 327.90 304.88 10.12 o -2 16 2 105.48 85.52 8.75 o -1 16 2 58.35 60.39 8.54 o 0 16 2 0.85 0.00 6.94 o 1 16 2 94.31 87.35 8.78 o 2 16 2 0.07 0.00 8.09 o 3 16 2 166.52 171.71 10.99 o 4 16 2 31.84 22.37 11.25 o 5 16 2 56.53 40.65 15.10 o 6 16 2 70.64 53.52 17.59 o 7 16 2 194.16 198.75 24.93 o 8 16 2 90.28 102.42 28.83 o -9 17 2 0.60 0.00 32.56 o -8 17 2 21.09 17.71 18.44 o -7 17 2 0.79 0.00 15.77 o -6 17 2 295.63 300.02 15.41 o -5 17 2 761.39 756.91 14.07 o -4 17 2 167.59 147.18 12.73 o -3 17 2 1219.54 1188.53 14.41 o -2 17 2 517.76 539.81 10.59 o -1 17 2 28.79 36.05 8.35 o 0 17 2 8.41 0.00 7.24 o 1 17 2 0.73 2.78 8.20 o 2 17 2 1.25 0.00 9.03 o 3 17 2 79.66 100.16 11.29 o 4 17 2 182.34 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31.67 o -8 20 2 0.03 0.00 25.46 o -7 20 2 34.26 49.02 23.19 o -6 20 2 34.67 33.70 19.53 o -5 20 2 54.84 39.94 15.54 o -4 20 2 1.98 0.00 14.51 o -3 20 2 547.45 523.54 18.63 o -2 20 2 82.99 102.28 12.28 o -1 20 2 494.22 490.84 12.62 o 0 20 2 11.94 0.00 10.91 o 1 20 2 191.57 211.53 12.76 o 2 20 2 103.29 106.79 13.89 o 3 20 2 535.83 579.20 17.88 o 4 20 2 26.71 25.46 18.09 o 5 20 2 1.31 0.00 20.96 o 6 20 2 4.22 0.00 23.90 o -7 21 2 20.70 11.31 25.07 o -6 21 2 184.49 191.98 24.33 o -5 21 2 22.47 8.13 16.81 o -4 21 2 6.60 8.29 15.64 o -3 21 2 174.02 174.32 19.28 o -2 21 2 458.93 479.52 14.13 o -1 21 2 36.30 41.19 11.60 o 0 21 2 3.87 0.00 11.88 o 1 21 2 732.44 736.24 15.47 o 2 21 2 90.84 75.36 13.35 o 3 21 2 1026.76 1149.38 20.10 o 4 21 2 56.54 60.49 22.47 o 5 21 2 0.03 0.00 22.68 o 6 21 2 20.88 20.84 26.91 o -7 22 2 0.06 6.60 27.47 o -6 22 2 128.37 162.45 25.48 o -5 22 2 1.21 0.00 18.63 o -4 22 2 134.12 119.34 17.81 o -3 22 2 62.68 74.88 17.85 o -2 22 2 38.03 43.82 13.57 o -1 22 2 150.26 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5488.60 5996.35 51.01 o 0 3 3 419.29 512.63 6.77 o 1 3 3 846.66 777.24 10.60 o 2 3 3 26.39 29.73 4.73 o 3 3 3 26.53 15.28 6.30 o 4 3 3 3.37 0.00 7.01 o 5 3 3 183.09 197.64 9.77 o 6 3 3 9.27 7.12 10.37 o 7 3 3 60.73 49.87 17.85 o 8 3 3 36.74 14.78 23.99 o 9 3 3 4.18 0.00 37.87 o -11 4 3 77.85 67.22 34.44 o -10 4 3 403.29 463.31 33.87 o -9 4 3 805.39 871.51 25.30 o -8 4 3 222.30 219.18 16.46 o -7 4 3 92.20 113.49 11.31 o -6 4 3 122.04 121.96 8.12 o -5 4 3 5776.89 6162.54 49.29 o -4 4 3 316.06 293.60 4.80 o -3 4 3 1979.84 1928.63 15.73 o -2 4 3 72.20 55.98 5.30 o -1 4 3 299.33 356.26 6.37 o 0 4 3 343.87 311.61 5.93 o 1 4 3 2.29 0.73 4.46 o 2 4 3 11.57 8.46 5.05 o 3 4 3 582.30 596.16 9.63 o 4 4 3 32.46 28.67 7.52 o 5 4 3 0.09 4.74 8.82 o 6 4 3 9.33 0.00 11.96 o 7 4 3 15.25 8.82 15.31 o 8 4 3 8.79 17.66 28.67 o 9 4 3 3.14 0.00 38.61 o -11 5 3 2.11 0.00 39.20 o -10 5 3 48.46 57.59 25.70 o -9 5 3 45.35 51.60 21.42 o -8 5 3 237.14 243.03 16.21 o -7 5 3 760.92 718.14 13.42 o -6 5 3 2574.81 2693.41 23.09 o -5 5 3 235.98 261.70 6.57 o -4 5 3 782.92 778.84 7.52 o -3 5 3 4366.71 4157.78 34.46 o -2 5 3 916.36 762.39 8.73 o -1 5 3 2.77 0.00 4.59 o 0 5 3 112.51 101.42 5.41 o 1 5 3 10.82 2.06 5.01 o 2 5 3 283.27 300.73 6.52 o 3 5 3 211.19 203.62 7.57 o 4 5 3 318.28 310.52 8.96 o 5 5 3 71.45 70.75 10.30 o 6 5 3 138.08 140.36 16.16 o 7 5 3 128.42 118.56 22.02 o 8 5 3 42.39 32.53 31.83 o 9 5 3 15.39 0.00 39.54 o -11 6 3 1.37 0.00 33.01 o -10 6 3 0.82 0.00 23.70 o -9 6 3 118.95 127.55 21.68 o -8 6 3 232.61 242.39 16.22 o -7 6 3 103.84 103.24 10.60 o -6 6 3 926.89 971.47 10.55 o -5 6 3 78.00 91.18 7.44 o -4 6 3 4158.63 4683.81 36.08 o -3 6 3 593.75 490.44 6.31 o -2 6 3 1926.62 2077.81 21.12 o -1 6 3 6.32 6.54 4.87 o 0 6 3 481.00 432.29 7.23 o 1 6 3 12.89 22.56 5.69 o 2 6 3 0.81 3.46 5.26 o 3 6 3 5.30 3.69 6.67 o 4 6 3 68.88 55.49 9.84 o 5 6 3 146.80 141.62 12.00 o 6 6 3 93.95 85.46 17.34 o 7 6 3 44.76 22.00 19.41 o 8 6 3 2.59 0.00 30.71 o 9 6 3 32.86 42.52 39.85 o -11 7 3 64.06 67.08 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