#------------------------------------------------------------------------------ #$Date: 2009-09-11 11:49:26 +0300 (Fri, 11 Sep 2009) $ #$Revision: 819 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2222844.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2222844_Fobs loop_ _publ_author_name 'Miao, Jinling' 'Zhao, Zhitong' 'Chen, Hongwei' 'Wang, Daqi' 'Nie, Yong' _publ_section_title ; Bis{2-[(2-pyridyl)iminomethyl]phenolato}copper(II) ; _journal_coeditor_code PV2176 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m904 _journal_volume 65 _journal_year 2009 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 106.884 _cell_angle_beta 90.374 _cell_angle_gamma 90.289 _cell_length_a 3.8142 _cell_length_b 11.2170 _cell_length_c 11.9001 _exptl_crystal_F_000 235.00 _reflns_d_resolution_high 0.8403 _[local]_cod_data_source_file pv2176Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 090411b in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 111.61 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 2230.10 2504.01 40.46 o 2 0 0 215.56 213.46 6.49 o 3 0 0 413.51 401.09 8.19 o 4 0 0 31.32 28.40 4.22 o -4 1 0 53.32 49.84 4.77 o -3 1 0 103.27 115.70 5.74 o -2 1 0 845.19 892.75 17.84 o -1 1 0 121.26 116.56 3.65 o 0 1 0 1646.57 1628.88 15.56 o 1 1 0 915.29 969.13 12.42 o 2 1 0 461.84 462.85 11.98 o 3 1 0 236.36 229.45 5.86 o 4 1 0 0.12 -0.01 1.67 o -4 2 0 3.03 0.79 2.43 o -3 2 0 101.34 105.20 5.60 o -2 2 0 561.84 573.96 13.01 o -1 2 0 1725.01 1829.35 20.01 o 0 2 0 1341.32 1304.22 12.49 o 1 2 0 101.88 97.18 1.67 o 2 2 0 194.12 212.99 3.55 o 3 2 0 33.73 35.83 2.48 o 4 2 0 11.32 9.27 3.34 o -4 3 0 1.36 1.81 5.19 o -2 3 0 164.56 155.94 3.76 o -1 3 0 31.51 25.42 1.57 o 0 3 0 1293.85 1247.74 12.27 o 1 3 0 137.61 132.05 2.11 o 2 3 0 96.95 118.08 3.95 o 3 3 0 51.49 51.84 2.97 o 4 3 0 25.88 27.10 4.33 o -4 4 0 5.57 3.35 2.71 o -3 4 0 0.33 -1.41 1.13 o -2 4 0 443.91 405.41 13.99 o -1 4 0 774.91 807.46 15.84 o 0 4 0 312.23 289.99 3.86 o 1 4 0 1563.15 1649.93 16.35 o 2 4 0 654.96 724.20 11.54 o 3 4 0 56.03 54.45 3.09 o 4 4 0 9.74 8.32 3.31 o -4 5 0 5.66 7.07 2.64 o -3 5 0 204.53 185.50 7.12 o -2 5 0 664.49 648.18 15.05 o -1 5 0 326.49 325.85 8.54 o 0 5 0 1197.77 1216.11 13.79 o 1 5 0 1117.53 1195.28 18.79 o 2 5 0 235.21 250.35 5.84 o 3 5 0 69.21 68.26 3.53 o 4 5 0 8.78 7.88 3.16 o -4 6 0 139.53 157.83 9.24 o -3 6 0 122.38 108.45 6.17 o -2 6 0 30.88 33.51 3.83 o -1 6 0 439.95 461.56 11.21 o 0 6 0 806.67 807.24 9.33 o 1 6 0 141.69 118.06 2.53 o 2 6 0 19.34 22.46 2.16 o 3 6 0 87.40 90.34 6.23 o -3 7 0 40.97 46.86 5.02 o -2 7 0 157.74 171.71 7.27 o -1 7 0 96.50 89.11 4.53 o 0 7 0 17.12 12.45 1.47 o 1 7 0 170.28 158.00 4.31 o 2 7 0 100.44 96.00 3.80 o 3 7 0 72.85 78.13 6.01 o -3 8 0 18.56 15.57 3.92 o -2 8 0 16.18 14.52 3.08 o -1 8 0 32.70 34.26 3.29 o 0 8 0 341.96 340.75 6.84 o 1 8 0 174.31 172.61 6.00 o 2 8 0 45.23 43.21 2.84 o 3 8 0 5.34 4.10 2.73 o -3 9 0 0.34 -1.32 2.49 o -2 9 0 0.40 -1.81 1.86 o -1 9 0 14.80 14.04 2.91 o 0 9 0 442.99 473.96 12.26 o 1 9 0 128.46 131.13 4.39 o 2 9 0 1.11 -0.61 1.44 o 3 9 0 0.93 -1.80 2.65 o -2 10 0 227.44 236.67 9.81 o -1 10 0 0.94 -2.05 1.66 o 0 10 0 23.11 23.00 3.34 o 1 10 0 99.76 100.46 4.11 o 2 10 0 20.41 28.73 3.09 o -2 11 0 220.42 230.11 10.08 o -1 11 0 67.74 64.59 4.84 o 0 11 0 32.26 32.57 4.00 o 1 11 0 199.74 193.24 6.05 o 2 11 0 40.11 43.41 5.58 o -1 12 0 93.49 80.56 5.80 o 0 12 0 107.57 113.15 6.50 o 1 12 0 203.61 205.41 15.91 o -1 -12 1 84.07 87.39 5.40 o 0 -12 1 175.97 178.70 7.96 o 1 -12 1 55.74 63.78 5.11 o -2 -11 1 80.75 79.04 6.24 o -1 -11 1 224.08 222.80 6.38 o 0 -11 1 173.31 168.15 7.20 o 1 -11 1 0.46 0.91 1.90 o 2 -11 1 30.48 48.72 5.62 o -2 -10 1 57.94 60.94 5.54 o -1 -10 1 73.94 76.82 3.48 o 0 -10 1 154.24 151.76 6.45 o 1 -10 1 16.28 14.74 3.03 o 2 -10 1 3.15 3.31 2.70 o -3 -9 1 12.84 19.09 4.34 o -2 -9 1 1.38 1.42 2.26 o -1 -9 1 38.89 46.76 2.66 o 0 -9 1 182.68 183.40 4.00 o 1 -9 1 279.77 291.57 9.44 o 2 -9 1 46.60 44.85 4.35 o 3 -9 1 3.90 6.52 3.16 o -3 -8 1 22.44 28.62 4.68 o -2 -8 1 12.22 12.83 4.31 o -1 -8 1 236.36 245.55 5.79 o 0 -8 1 371.59 380.55 5.85 o 1 -8 1 87.63 88.59 4.74 o 2 -8 1 24.65 25.29 3.70 o 3 -8 1 47.71 49.43 4.73 o -3 -7 1 96.08 104.88 7.12 o -2 -7 1 104.07 110.05 3.95 o -1 -7 1 174.89 164.39 4.57 o 0 -7 1 170.91 143.43 3.14 o 1 -7 1 24.65 19.88 2.66 o 2 -7 1 66.58 67.99 4.53 o 3 -7 1 5.32 5.73 2.65 o -4 -6 1 21.30 18.61 4.34 o -3 -6 1 121.62 117.90 7.20 o -2 -6 1 146.61 146.18 6.59 o -1 -6 1 58.56 50.36 1.65 o 0 -6 1 122.78 102.34 2.33 o 1 -6 1 303.97 310.00 8.64 o 2 -6 1 82.39 75.97 4.53 o 3 -6 1 1.79 3.33 1.66 o 4 -6 1 18.13 20.74 3.68 o -4 -5 1 41.15 43.81 5.67 o -3 -5 1 69.70 65.15 5.20 o -2 -5 1 70.63 63.79 2.77 o -1 -5 1 1408.81 1558.31 16.22 o 0 -5 1 1768.11 1828.95 18.11 o 1 -5 1 117.93 120.79 3.38 o 2 -5 1 201.38 185.88 4.55 o 3 -5 1 252.80 258.63 13.93 o 4 -5 1 21.84 29.00 4.44 o -4 -4 1 4.13 2.17 2.86 o -3 -4 1 103.89 101.21 4.00 o -2 -4 1 93.59 88.15 2.22 o -1 -4 1 1433.58 1472.19 14.74 o 0 -4 1 2499.11 2511.97 34.79 o 1 -4 1 940.52 970.06 10.09 o 2 -4 1 1159.83 1098.09 14.37 o 4 -4 1 2.95 6.38 5.03 o -4 -3 1 2.22 5.99 3.05 o -3 -3 1 254.71 252.90 6.36 o -2 -3 1 83.10 75.79 2.03 o -1 -3 1 203.20 246.41 3.33 o 0 -3 1 1131.78 1153.90 11.38 o 1 -3 1 212.09 205.24 4.06 o 2 -3 1 135.76 125.87 5.34 o 3 -3 1 28.84 32.51 4.17 o 4 -3 1 4.23 2.91 2.59 o -4 -2 1 14.69 21.58 4.06 o -3 -2 1 66.32 60.56 2.99 o -2 -2 1 39.58 32.22 1.40 o -1 -2 1 1.97 1.45 0.40 o 0 -2 1 1746.97 1770.58 17.17 o 1 -2 1 4867.42 5005.53 55.59 o 2 -2 1 300.20 335.98 9.27 o 3 -2 1 159.77 168.87 7.33 o 4 -2 1 0.22 -2.56 2.01 o -4 -1 1 4.46 2.42 2.67 o -3 -1 1 19.85 16.36 5.67 o -2 -1 1 560.19 571.58 8.46 o -1 -1 1 1.59 2.11 0.50 o 0 -1 1 1838.61 1798.05 20.60 o 1 -1 1 2400.14 2557.43 41.71 o 2 -1 1 4.93 6.21 1.75 o 3 -1 1 71.55 66.74 6.91 o 4 -1 1 6.38 11.89 3.72 o -4 0 1 19.86 20.68 4.26 o -3 0 1 236.62 228.44 7.87 o -2 0 1 463.70 460.87 10.49 o -1 0 1 137.23 147.08 3.76 o 0 0 1 3850.62 3483.07 54.96 o 1 0 1 12456.09 11587.08 134.64 o 2 0 1 274.23 292.88 5.79 o 3 0 1 365.88 368.51 7.74 o 4 0 1 62.32 56.89 4.97 o -4 1 1 41.23 49.29 5.26 o -3 1 1 180.00 183.21 7.14 o -2 1 1 409.17 418.16 9.98 o -1 1 1 4764.00 4944.59 61.17 o 0 1 1 703.91 733.22 12.30 o 1 1 1 390.35 414.43 6.24 o 2 1 1 184.92 194.64 4.58 o 3 1 1 189.95 190.22 5.36 o 4 1 1 49.91 48.46 4.75 o -4 2 1 0.46 -3.22 2.46 o -2 2 1 1096.73 1068.07 30.81 o -1 2 1 345.75 325.56 7.30 o 0 2 1 16.45 17.59 1.20 o 1 2 1 941.10 961.02 12.67 o 2 2 1 1.81 0.32 0.99 o 3 2 1 28.55 32.63 7.89 o 4 2 1 20.25 24.38 7.17 o -4 3 1 0.59 1.29 2.31 o -3 3 1 93.03 88.10 3.35 o -2 3 1 28.30 25.26 1.66 o -1 3 1 131.85 171.97 5.16 o 0 3 1 426.37 410.96 10.15 o 1 3 1 452.46 437.43 6.98 o 2 3 1 55.13 57.18 2.73 o 3 3 1 11.62 9.57 4.06 o 4 3 1 5.21 7.29 3.15 o -4 4 1 3.50 2.27 2.15 o -3 4 1 59.53 45.87 2.50 o -2 4 1 4.29 1.20 1.52 o -1 4 1 715.48 724.30 14.55 o 0 4 1 179.71 171.34 4.87 o 1 4 1 175.16 170.69 5.33 o 2 4 1 303.22 335.28 6.93 o 3 4 1 124.12 130.53 4.73 o 4 4 1 9.41 10.62 3.65 o -4 5 1 0.16 -0.22 2.71 o -3 5 1 69.66 66.97 4.80 o -2 5 1 256.96 262.21 8.45 o -1 5 1 89.01 83.03 3.91 o 0 5 1 482.39 501.71 7.87 o 1 5 1 1098.03 1148.82 16.56 o 2 5 1 118.41 124.62 4.07 o 3 5 1 33.61 35.37 3.12 o 4 5 1 17.48 16.99 4.22 o -3 6 1 417.06 411.15 12.64 o -2 6 1 301.99 290.94 9.41 o -1 6 1 227.77 227.68 7.16 o 0 6 1 692.78 686.37 14.31 o 1 6 1 264.20 265.48 5.72 o 2 6 1 74.80 74.55 3.29 o 3 6 1 30.30 24.82 8.30 o -3 7 1 14.65 11.65 3.27 o -2 7 1 345.97 362.39 11.11 o -1 7 1 355.23 342.05 9.72 o 0 7 1 356.49 339.31 9.14 o 1 7 1 117.75 108.62 4.97 o 2 7 1 45.32 46.28 2.80 o 3 7 1 42.47 41.43 4.82 o -3 8 1 1.45 -1.98 2.05 o -2 8 1 40.33 42.70 4.12 o -1 8 1 26.68 23.07 3.06 o 0 8 1 196.12 195.20 6.88 o 1 8 1 551.03 530.47 13.87 o 2 8 1 24.72 28.06 2.76 o 3 8 1 17.24 20.49 4.20 o -3 9 1 2.26 -0.13 2.85 o -2 9 1 31.03 33.91 4.46 o -1 9 1 0.77 -0.04 1.58 o 0 9 1 1.90 1.33 1.61 o 1 9 1 270.57 277.63 6.86 o 2 9 1 23.67 19.20 2.56 o 3 9 1 4.84 9.23 3.64 o -2 10 1 224.29 227.52 9.71 o -1 10 1 316.59 323.07 10.81 o 0 10 1 1.01 1.52 1.76 o 1 10 1 62.65 61.88 3.39 o 2 10 1 14.74 15.66 2.62 o -2 11 1 57.20 56.28 5.40 o -1 11 1 191.47 172.69 8.11 o 0 11 1 81.01 84.24 5.46 o 1 11 1 142.40 151.53 5.51 o 2 11 1 73.80 72.91 4.91 o -1 12 1 21.88 24.20 4.40 o 0 12 1 20.15 16.71 3.61 o 0 -13 2 19.60 23.49 4.07 o -1 -12 2 45.87 44.95 4.64 o 0 -12 2 143.60 144.66 7.04 o 1 -12 2 36.26 31.74 4.24 o -2 -11 2 31.07 45.29 5.83 o -1 -11 2 228.03 225.25 6.33 o 0 -11 2 205.23 210.66 4.82 o 1 -11 2 77.17 77.04 5.16 o 2 -11 2 0.44 4.14 2.81 o -2 -10 2 39.85 42.10 5.19 o -1 -10 2 79.72 82.56 7.18 o 0 -10 2 116.07 121.73 4.19 o 1 -10 2 83.52 86.84 5.26 o 2 -10 2 14.81 13.40 3.27 o 3 -10 2 4.50 1.10 2.80 o -3 -9 2 132.33 133.25 8.46 o -2 -9 2 15.90 17.29 3.70 o -1 -9 2 34.91 45.04 3.60 o 0 -9 2 186.04 195.82 4.08 o 1 -9 2 77.46 85.39 3.62 o 2 -9 2 93.92 92.44 5.75 o 3 -9 2 21.86 22.66 4.39 o -3 -8 2 15.88 19.23 4.21 o -2 -8 2 46.34 48.35 4.54 o -1 -8 2 72.72 80.74 2.44 o 0 -8 2 306.73 306.63 5.04 o 1 -8 2 229.63 230.32 11.48 o 2 -8 2 58.17 55.20 4.28 o 3 -8 2 11.69 16.66 3.89 o -3 -7 2 14.89 14.89 3.80 o -2 -7 2 115.37 109.07 3.85 o -1 -7 2 195.53 207.14 3.78 o 0 -7 2 192.18 163.30 3.23 o 1 -7 2 38.91 32.61 2.46 o 2 -7 2 71.03 68.78 4.54 o 3 -7 2 28.08 31.41 3.08 o -4 -6 2 31.85 29.49 5.44 o -3 -6 2 142.90 142.61 7.90 o -2 -6 2 145.74 139.99 6.27 o -1 -6 2 433.60 440.53 6.11 o 0 -6 2 589.71 603.59 7.31 o 1 -6 2 24.70 19.94 1.80 o 2 -6 2 60.28 57.75 2.68 o 3 -6 2 8.60 11.84 3.62 o 4 -6 2 1.64 -2.05 3.08 o -4 -5 2 48.03 41.06 5.62 o -3 -5 2 167.99 166.75 8.40 o -2 -5 2 126.95 106.69 4.48 o -1 -5 2 83.53 70.26 1.77 o 0 -5 2 2757.00 2829.98 27.02 o 1 -5 2 627.46 636.41 9.04 o 2 -5 2 90.85 91.55 3.15 o 3 -5 2 70.61 81.03 3.86 o 4 -5 2 2.70 10.19 4.75 o -4 -4 2 11.05 14.42 3.91 o -3 -4 2 63.60 59.13 5.06 o -2 -4 2 273.77 276.03 4.35 o -1 -4 2 19.46 11.14 1.18 o 0 -4 2 1331.77 1291.66 19.64 o 1 -4 2 348.89 328.58 4.52 o 2 -4 2 450.00 477.49 12.37 o 3 -4 2 361.64 379.61 12.21 o 4 -4 2 1.90 -0.21 2.60 o -4 -3 2 2.06 0.34 2.46 o -3 -3 2 58.48 53.36 4.80 o -2 -3 2 494.00 492.85 6.44 o -1 -3 2 19.32 17.94 0.82 o 0 -3 2 276.61 267.50 3.35 o 1 -3 2 495.72 486.86 10.93 o 2 -3 2 183.17 187.78 6.87 o 3 -3 2 148.79 145.28 7.02 o 4 -3 2 30.50 21.05 4.34 o -4 -2 2 7.40 7.48 3.28 o -3 -2 2 117.99 122.08 3.70 o -2 -2 2 200.59 184.46 3.83 o -1 -2 2 95.58 92.93 3.03 o 0 -2 2 1813.67 1800.70 25.54 o 1 -2 2 2639.99 2709.88 31.13 o 2 -2 2 319.57 327.13 9.28 o 3 -2 2 1.95 1.97 1.93 o 4 -2 2 10.54 8.15 3.38 o -4 -1 2 17.91 13.09 3.55 o -3 -1 2 105.16 108.29 3.66 o -2 -1 2 271.92 274.42 5.03 o -1 -1 2 818.56 822.11 10.10 o 0 -1 2 128.52 141.77 2.28 o 1 -1 2 3008.26 3266.85 30.62 o 2 -1 2 900.29 923.48 13.10 o 3 -1 2 17.92 16.54 1.98 o 4 -1 2 33.56 24.79 4.26 o -3 0 2 216.25 223.53 5.53 o -2 0 2 532.89 528.03 11.21 o -1 0 2 20.42 14.03 0.66 o 0 0 2 63.47 66.77 1.40 o 1 0 2 716.43 725.66 7.66 o 2 0 2 267.32 293.28 5.78 o 3 0 2 80.56 78.77 3.33 o 4 0 2 95.51 100.50 6.59 o -4 1 2 0.15 -0.54 3.15 o -3 1 2 81.34 78.12 2.93 o -2 1 2 315.87 311.10 5.20 o -1 1 2 283.78 300.36 6.50 o 0 1 2 1800.85 1771.23 20.13 o 1 1 2 199.48 189.19 2.59 o 2 1 2 79.00 73.78 2.74 o 3 1 2 0.85 -0.62 1.04 o 4 1 2 3.16 2.14 2.51 o -3 2 2 4.32 4.84 1.84 o -2 2 2 1091.71 1124.34 13.91 o -1 2 2 1106.47 1125.40 19.72 o 0 2 2 33.99 28.62 1.62 o 1 2 2 804.98 834.54 11.46 o 2 2 2 253.72 268.93 5.78 o 3 2 2 1.77 2.03 1.36 o 4 2 2 0.31 -0.37 2.54 o -3 3 2 92.03 86.08 3.19 o -2 3 2 292.33 274.95 7.89 o -1 3 2 296.10 267.23 6.77 o 0 3 2 1131.41 1154.47 20.16 o 1 3 2 554.35 545.54 8.43 o 2 3 2 87.09 82.84 3.13 o 3 3 2 129.31 138.26 4.78 o 4 3 2 26.25 23.88 2.94 o -4 4 2 17.92 20.33 4.04 o -3 4 2 15.42 14.36 2.82 o -2 4 2 1.10 -0.02 1.31 o -1 4 2 72.61 56.64 3.01 o 0 4 2 515.40 492.45 10.43 o 1 4 2 440.97 426.55 8.74 o 2 4 2 251.81 247.06 5.86 o 3 4 2 53.59 52.02 3.13 o 4 4 2 15.52 19.15 2.95 o -4 5 2 0.26 -1.87 2.64 o -3 5 2 14.98 20.55 3.51 o -2 5 2 529.99 537.36 13.33 o -1 5 2 22.22 15.64 2.26 o 0 5 2 53.68 44.03 2.71 o 1 5 2 396.88 412.40 8.89 o 2 5 2 89.98 84.75 3.47 o 3 5 2 16.70 15.27 3.20 o 4 5 2 8.50 6.84 3.05 o -3 6 2 79.67 79.77 5.34 o -2 6 2 460.83 477.33 12.82 o -1 6 2 353.15 360.03 9.69 o 0 6 2 541.20 526.40 12.07 o 1 6 2 277.09 275.95 6.05 o 2 6 2 1.19 -0.70 1.05 o 3 6 2 27.63 25.51 5.34 o -3 7 2 2.65 0.06 2.08 o -2 7 2 98.10 102.74 5.81 o -1 7 2 241.96 229.15 7.67 o 0 7 2 94.24 86.98 4.43 o 1 7 2 793.32 793.69 14.38 o 2 7 2 82.76 84.77 3.76 o 3 7 2 2.98 0.02 1.67 o -3 8 2 4.34 -0.16 2.36 o -2 8 2 57.86 61.49 4.76 o -1 8 2 25.30 32.24 3.56 o 0 8 2 51.10 42.35 3.38 o 1 8 2 334.85 334.56 11.66 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79.92 6.27 o -1 -9 11 45.16 38.18 4.53 o 0 -9 11 48.12 49.61 4.63 o 1 -9 11 13.82 15.93 3.56 o -2 -8 11 100.39 129.73 7.13 o -1 -8 11 15.34 13.00 3.12 o 0 -8 11 12.65 18.72 3.43 o 1 -8 11 21.26 25.31 4.04 o 2 -8 11 8.04 4.86 2.19 o -2 -7 11 59.24 64.74 5.16 o -1 -7 11 3.75 5.85 2.45 o 0 -7 11 43.43 42.39 4.01 o 1 -7 11 20.54 24.84 3.96 o 2 -7 11 0.14 -0.16 1.60 o -2 -6 11 58.75 46.29 4.49 o -1 -6 11 169.81 150.84 7.19 o 0 -6 11 90.31 97.26 5.68 o 1 -6 11 12.70 8.66 2.70 o 2 -6 11 47.13 45.40 7.29 o -2 -5 11 122.86 134.24 7.16 o -1 -5 11 72.90 74.91 5.12 o 0 -5 11 205.85 190.05 7.69 o 1 -5 11 240.13 239.77 8.97 o 2 -5 11 68.32 62.72 3.68 o -2 -4 11 55.90 53.00 4.76 o -1 -4 11 1.22 2.73 2.22 o 0 -4 11 187.94 182.89 7.47 o 1 -4 11 40.63 41.73 2.70 o 2 -4 11 4.07 7.01 2.94 o -2 -3 11 114.02 102.95 6.42 o -1 -3 11 20.96 27.62 3.70 o 0 -3 11 1.42 0.43 1.69 o 1 -3 11 18.38 17.77 2.24 o 2 -3 11 21.67 22.65 4.14 o -2 -2 11 130.27 123.54 7.19 o -1 -2 11 1.63 -2.04 1.77 o 0 -2 11 22.92 24.54 3.43 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