#------------------------------------------------------------------------------ #$Date: 2016-04-03 04:11:45 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181150 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/29/2222929.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2222929_Fobs loop_ _publ_author_name 'Asiri, Abdullah Mohamed' 'Khan, Salman A.' 'Ng, Seik Weng' _publ_section_title ; Pyridinium 5-[(1,3-diethyl-6-hydroxy-4-oxo-2-thioxo-1,2,3,4-tetrahydropyrimidin-5-yl)(2-methoxyphenyl)methyl]-1,3-diethyl-4,6-dioxo-2-thioxopyrimidin-5-ide ; _journal_coeditor_code XU2549 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1860 _journal_page_last o1861 _journal_volume 65 _journal_year 2009 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 90.316 _cell_angle_gamma 90.000 _cell_length_a 17.3713 _cell_length_b 19.8285 _cell_length_c 17.3969 _exptl_crystal_F_000 2528.00 _reflns_d_resolution_high 0.7696 _cod_data_source_file xu2549Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P21/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 415.94 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 108906.83 67098.48 6792.23 o 6 0 0 17596.69 17277.99 699.99 o 8 0 0 149.48 221.13 14.51 o 10 0 0 4458.58 4947.77 339.08 o 12 0 0 660.97 603.71 82.24 o 16 0 0 2164.13 2178.50 138.13 o 18 0 0 44.98 65.66 19.48 o 20 0 0 0.07 -19.39 18.36 o 22 0 0 9.13 -2.87 20.69 o 1 1 0 2642.98 1823.45 70.98 o 2 1 0 4162.77 3163.54 221.14 o 3 1 0 8.99 -2.08 1.62 o 4 1 0 114717.80 96349.20 4159.87 o 5 1 0 12093.93 10013.61 957.11 o 6 1 0 27076.61 26657.14 2020.65 o 7 1 0 1698.60 1315.99 171.59 o 8 1 0 5814.18 6289.37 727.28 o 9 1 0 67.61 70.60 5.36 o 10 1 0 317.10 307.39 19.44 o 11 1 0 205.17 253.85 12.74 o 12 1 0 389.71 367.31 20.32 o 13 1 0 2.19 -8.20 5.47 o 14 1 0 79.66 83.60 8.89 o 15 1 0 990.69 966.95 47.00 o 16 1 0 608.04 629.75 34.39 o 17 1 0 203.24 180.17 17.79 o 18 1 0 13.80 -13.50 12.41 o 19 1 0 42.36 43.64 14.39 o 20 1 0 16.00 3.03 13.70 o 21 1 0 11.52 10.10 14.66 o 22 1 0 1.24 2.30 14.33 o 0 2 0 40482.07 36219.73 1452.71 o 1 2 0 8534.68 8893.57 268.21 o 2 2 0 3041.21 3730.01 120.68 o 3 2 0 49.73 26.70 2.90 o 4 2 0 169270.95 126601.05 4481.64 o 5 2 0 6074.41 5139.17 330.19 o 6 2 0 6723.79 4881.62 188.40 o 7 2 0 893.86 933.90 127.13 o 8 2 0 10546.51 9773.05 728.35 o 9 2 0 129.85 126.82 7.50 o 10 2 0 1111.61 796.66 44.26 o 11 2 0 1368.01 1367.01 113.03 o 12 2 0 1311.77 1059.00 43.87 o 13 2 0 3549.11 3650.83 198.20 o 14 2 0 39.40 51.49 7.20 o 15 2 0 11.27 -12.18 9.92 o 16 2 0 145.82 119.89 32.35 o 17 2 0 32.67 43.00 13.91 o 18 2 0 157.99 149.34 17.50 o 19 2 0 321.94 379.59 26.40 o 20 2 0 0.20 17.02 13.34 o 21 2 0 290.55 304.71 24.96 o 22 2 0 7.78 -3.90 14.31 o 1 3 0 500.30 497.80 16.51 o 2 3 0 173005.06 150828.94 5099.32 o 3 3 0 342.86 393.86 17.87 o 4 3 0 68066.23 52015.75 1822.60 o 5 3 0 6777.18 6523.73 239.86 o 6 3 0 78.66 114.94 6.53 o 7 3 0 2226.63 1376.69 86.27 o 8 3 0 9519.52 10134.57 631.94 o 9 3 0 691.84 674.48 41.88 o 10 3 0 3520.35 3605.73 243.44 o 11 3 0 446.71 390.20 20.86 o 12 3 0 992.47 751.98 31.84 o 13 3 0 743.92 726.97 42.80 o 14 3 0 415.72 405.77 27.08 o 15 3 0 238.56 234.43 26.86 o 16 3 0 15.12 -9.68 11.12 o 17 3 0 1235.68 1311.31 61.95 o 18 3 0 262.05 228.83 20.49 o 19 3 0 65.17 64.12 14.99 o 20 3 0 0.52 19.78 15.04 o 21 3 0 26.17 53.40 15.88 o 22 3 0 133.05 222.35 21.35 o 0 4 0 22049.07 20897.88 821.09 o 1 4 0 2622.75 2994.91 89.77 o 2 4 0 49261.94 49061.73 1728.68 o 3 4 0 2112.62 2107.16 71.80 o 4 4 0 118.87 95.09 6.06 o 5 4 0 11551.46 8161.50 329.39 o 6 4 0 3587.08 3820.75 283.87 o 7 4 0 7684.81 7155.58 451.17 o 8 4 0 3818.73 3300.88 117.39 o 9 4 0 6922.65 6447.03 523.35 o 10 4 0 6744.56 7225.70 476.05 o 11 4 0 409.09 341.48 23.80 o 12 4 0 8463.96 8306.02 906.40 o 13 4 0 1.72 -9.61 6.41 o 14 4 0 14.03 0.59 7.47 o 15 4 0 47.25 53.12 8.84 o 16 4 0 552.02 618.36 33.80 o 17 4 0 67.54 93.06 14.69 o 18 4 0 3.75 -16.19 10.79 o 19 4 0 33.20 51.49 13.84 o 20 4 0 59.67 13.57 14.35 o 21 4 0 24.88 29.18 14.80 o 22 4 0 36.13 37.19 16.25 o 1 5 0 318.86 271.87 9.67 o 2 5 0 12551.33 12983.98 386.49 o 3 5 0 5537.50 6117.30 181.82 o 4 5 0 27201.93 27021.04 1718.03 o 5 5 0 3622.92 2363.45 143.63 o 6 5 0 55448.25 58073.98 2216.87 o 7 5 0 11.70 45.69 4.77 o 8 5 0 19421.50 17520.13 724.14 o 9 5 0 5171.75 4896.26 295.10 o 10 5 0 9.07 14.91 5.79 o 11 5 0 1650.95 1844.10 145.59 o 12 5 0 138.69 127.24 8.51 o 13 5 0 1140.71 1107.24 78.73 o 14 5 0 731.63 751.02 40.92 o 15 5 0 268.18 217.87 13.49 o 16 5 0 42.97 48.83 12.63 o 17 5 0 7.66 -14.05 11.91 o 18 5 0 88.50 63.28 13.63 o 19 5 0 3.29 -10.97 12.43 o 20 5 0 39.22 12.00 14.33 o 21 5 0 354.34 516.68 33.25 o 22 5 0 10.84 57.27 17.64 o 0 6 0 8307.75 9306.41 364.65 o 1 6 0 8811.45 10354.16 286.28 o 2 6 0 22984.63 24201.84 722.52 o 3 6 0 7863.95 9034.48 269.48 o 4 6 0 688.47 615.68 23.05 o 5 6 0 16138.28 18092.91 610.38 o 6 6 0 2984.65 2737.87 93.97 o 7 6 0 3959.10 4452.29 151.10 o 8 6 0 5015.66 3307.76 117.72 o 9 6 0 228.75 171.71 10.83 o 10 6 0 1250.45 1167.04 44.04 o 11 6 0 163.20 223.89 20.73 o 12 6 0 53.63 46.46 7.50 o 13 6 0 835.95 991.57 49.44 o 14 6 0 50.91 45.24 8.09 o 15 6 0 2.45 -7.46 7.50 o 16 6 0 0.72 -16.36 11.31 o 17 6 0 113.87 109.90 15.93 o 18 6 0 73.66 71.79 14.05 o 19 6 0 35.83 34.91 13.92 o 20 6 0 37.21 91.48 28.50 o 21 6 0 46.06 23.95 14.89 o 1 7 0 562.01 351.22 11.53 o 2 7 0 4039.81 4139.91 124.10 o 3 7 0 2441.03 2336.83 70.99 o 4 7 0 14232.09 13990.03 371.15 o 5 7 0 20124.19 20894.94 705.41 o 6 7 0 408.98 389.61 17.22 o 7 7 0 75.56 92.24 8.36 o 8 7 0 600.60 654.48 42.44 o 9 7 0 810.68 752.11 29.07 o 10 7 0 3061.84 2658.69 143.21 o 11 7 0 80.93 97.60 12.26 o 12 7 0 492.62 319.90 14.30 o 13 7 0 1020.36 1072.40 62.25 o 14 7 0 17.99 21.88 8.17 o 15 7 0 0.19 0.28 8.31 o 16 7 0 4.57 -6.26 11.54 o 17 7 0 150.90 142.34 20.00 o 18 7 0 0.14 -15.62 11.87 o 19 7 0 18.70 13.94 12.32 o 20 7 0 0.14 2.62 14.20 o 21 7 0 1.98 -7.46 14.67 o 0 8 0 492.77 688.83 29.20 o 1 8 0 2166.48 2466.43 69.24 o 2 8 0 1187.48 1048.06 36.49 o 3 8 0 674.43 732.53 21.05 o 4 8 0 5678.57 6357.32 169.99 o 5 8 0 859.07 741.13 21.55 o 6 8 0 403.16 490.50 17.30 o 7 8 0 0.58 17.85 11.20 o 8 8 0 6003.10 6937.44 281.44 o 9 8 0 216.48 251.65 23.85 o 10 8 0 1029.67 993.20 63.51 o 11 8 0 778.87 588.09 22.48 o 12 8 0 12.51 31.90 7.55 o 13 8 0 395.09 331.57 16.27 o 14 8 0 608.89 592.52 23.29 o 15 8 0 54.69 84.68 9.74 o 16 8 0 344.77 373.57 24.50 o 17 8 0 8.81 2.57 11.43 o 18 8 0 24.69 34.33 13.32 o 19 8 0 18.40 40.01 14.51 o 20 8 0 164.79 216.08 28.85 o 1 9 0 16631.19 17948.90 495.03 o 2 9 0 84.76 131.81 6.95 o 3 9 0 11887.78 12962.81 386.61 o 4 9 0 4996.22 5560.59 149.13 o 5 9 0 144.45 271.98 10.10 o 6 9 0 116.47 176.51 8.25 o 7 9 0 275.44 298.09 12.93 o 8 9 0 48.10 36.86 6.36 o 9 9 0 2374.89 1868.73 123.11 o 10 9 0 236.32 210.36 15.01 o 11 9 0 188.03 162.57 12.65 o 12 9 0 52.09 32.50 8.65 o 13 9 0 6.74 -15.26 13.96 o 14 9 0 116.52 101.87 11.29 o 15 9 0 1792.77 2116.20 151.46 o 16 9 0 613.70 528.88 41.99 o 17 9 0 637.88 741.44 54.37 o 18 9 0 391.24 466.63 41.33 o 19 9 0 117.19 105.22 21.72 o 0 10 0 13799.36 15686.97 612.49 o 1 10 0 802.89 748.04 22.83 o 2 10 0 290.18 367.84 13.13 o 3 10 0 4390.86 4573.23 127.88 o 4 10 0 2166.66 2470.56 67.42 o 5 10 0 2905.53 3040.31 82.71 o 6 10 0 1049.69 1140.23 32.47 o 7 10 0 4.51 -3.16 4.35 o 8 10 0 229.84 259.41 10.94 o 9 10 0 4020.37 3981.77 143.52 o 10 10 0 241.09 224.19 18.34 o 11 10 0 218.24 149.33 16.16 o 12 10 0 7232.55 8142.59 281.14 o 13 10 0 102.02 161.93 20.89 o 14 10 0 221.06 174.43 43.35 o 15 10 0 6.36 15.56 9.48 o 16 10 0 0.11 20.78 17.12 o 17 10 0 325.73 319.56 33.45 o 1 11 0 381.14 508.56 16.93 o 2 11 0 10211.38 10886.58 301.49 o 3 11 0 108.74 88.29 7.13 o 4 11 0 5.90 -6.47 4.32 o 5 11 0 5087.04 5009.70 134.89 o 6 11 0 974.07 972.18 28.29 o 7 11 0 730.95 650.33 20.27 o 8 11 0 1233.85 1211.72 34.82 o 9 11 0 171.20 148.01 8.69 o 10 11 0 590.12 645.85 23.55 o 11 11 0 211.62 173.12 15.13 o 12 11 0 117.35 157.49 19.70 o 13 11 0 224.65 215.43 24.01 o 14 11 0 49.86 113.30 14.43 o 15 11 0 235.67 193.34 42.77 o 0 12 0 78.97 38.48 7.96 o 1 12 0 1207.49 1227.93 36.20 o 2 12 0 4398.62 4463.17 124.79 o 3 12 0 0.29 15.98 5.06 o 4 12 0 50.87 51.56 5.11 o 5 12 0 3978.33 3725.93 109.93 o 6 12 0 912.27 796.99 23.98 o 7 12 0 1910.88 2248.58 62.21 o 8 12 0 228.77 247.04 12.04 o 9 12 0 4110.21 4201.05 126.40 o 10 12 0 591.42 578.98 19.61 o 11 12 0 252.81 280.14 15.25 o 12 12 0 666.06 735.93 38.14 o 13 12 0 837.56 968.35 85.66 o 14 12 0 617.55 649.08 39.28 o 15 12 0 8.55 9.34 8.65 o 1 13 0 9.60 49.37 6.02 o 2 13 0 1718.60 1999.86 57.32 o 3 13 0 6.15 -0.95 5.29 o 4 13 0 1139.94 1067.33 29.00 o 5 13 0 7376.11 7256.19 183.44 o 6 13 0 4153.25 4590.24 116.69 o 7 13 0 1838.36 1819.73 55.58 o 8 13 0 493.37 460.57 16.46 o 9 13 0 0.84 -7.93 8.76 o 10 13 0 28.58 20.85 14.79 o 11 13 0 72.19 108.46 10.80 o 12 13 0 3.20 -3.38 8.93 o 13 13 0 1220.34 1330.14 49.00 o 14 13 0 188.76 286.58 22.21 o 15 13 0 0.75 2.22 13.56 o 0 14 0 104.47 161.59 21.82 o 1 14 0 3106.79 3010.18 85.14 o 2 14 0 129.49 135.96 8.91 o 3 14 0 212.78 184.68 10.09 o 4 14 0 1.84 -7.85 5.23 o 5 14 0 2673.00 2746.55 70.86 o 6 14 0 3043.28 3242.33 83.50 o 7 14 0 2685.63 2791.09 79.18 o 8 14 0 6.07 -13.66 9.11 o 9 14 0 3008.29 3473.24 117.31 o 10 14 0 74.11 108.52 10.77 o 11 14 0 1114.58 1495.68 54.41 o 12 14 0 24.12 33.71 9.88 o 13 14 0 2.20 -4.54 12.04 o 14 14 0 76.34 112.47 17.06 o 15 14 0 473.86 511.83 47.18 o 1 15 0 2325.39 2297.34 65.94 o 2 15 0 3002.36 3235.89 91.76 o 3 15 0 2181.47 2379.87 68.41 o 4 15 0 55.13 62.99 6.79 o 5 15 0 6.68 6.44 6.15 o 6 15 0 82.47 62.42 8.78 o 7 15 0 61.49 70.23 8.79 o 8 15 0 79.53 84.10 9.36 o 9 15 0 798.90 652.69 22.61 o 10 15 0 474.58 464.38 22.59 o 11 15 0 207.61 194.12 40.19 o 12 15 0 1428.09 1497.42 161.03 o 13 15 0 13.89 4.47 14.57 o 14 15 0 813.45 922.18 55.71 o 15 15 0 352.45 402.60 33.56 o 0 16 0 4.02 10.04 10.07 o 1 16 0 1031.32 1097.86 33.96 o 2 16 0 176.44 215.26 12.01 o 3 16 0 2.11 -6.92 7.08 o 4 16 0 1544.77 1572.47 46.52 o 5 16 0 225.42 204.62 12.20 o 6 16 0 1441.23 1480.46 44.09 o 7 16 0 4422.74 4636.09 129.80 o 8 16 0 216.45 252.67 13.56 o 9 16 0 378.76 372.64 16.22 o 10 16 0 682.17 726.62 28.43 o 11 16 0 0.16 -9.14 10.72 o 12 16 0 436.10 529.53 23.60 o 13 16 0 1461.98 1503.92 111.00 o 14 16 0 0.17 7.81 18.92 o 15 16 0 109.88 149.30 23.26 o 1 17 0 1949.97 1928.73 56.58 o 2 17 0 728.04 691.63 23.86 o 3 17 0 0.00 2.91 14.22 o 4 17 0 223.67 279.78 15.88 o 5 17 0 31.63 58.06 11.95 o 6 17 0 151.12 123.26 10.53 o 7 17 0 21.32 -0.80 8.32 o 8 17 0 89.71 134.94 12.64 o 9 17 0 1538.26 1525.07 51.56 o 10 17 0 149.33 167.09 13.77 o 11 17 0 0.00 -16.06 10.71 o 12 17 0 13.86 15.89 11.36 o 13 17 0 901.97 981.39 59.03 o 14 17 0 17.52 8.17 19.58 o 15 17 0 3.95 7.15 19.74 o 0 18 0 3463.49 3704.53 149.64 o 1 18 0 522.84 553.74 23.71 o 2 18 0 1411.70 1276.16 44.18 o 3 18 0 400.97 375.51 27.20 o 4 18 0 229.76 178.46 16.50 o 5 18 0 1444.43 1447.03 43.58 o 6 18 0 140.21 127.19 10.59 o 7 18 0 27.01 24.13 10.80 o 8 18 0 765.30 679.28 27.44 o 9 18 0 65.18 46.22 11.85 o 10 18 0 278.60 254.92 17.30 o 11 18 0 0.93 -8.96 14.92 o 12 18 0 59.63 40.66 12.68 o 13 18 0 253.42 208.80 26.10 o 14 18 0 453.98 444.34 37.49 o 15 18 0 24.63 66.50 22.48 o 1 19 0 4638.16 4450.79 141.35 o 2 19 0 133.99 114.84 12.29 o 3 19 0 7.89 -15.04 10.03 o 4 19 0 11.71 7.63 8.96 o 5 19 0 369.18 393.53 20.14 o 6 19 0 261.80 211.30 15.10 o 7 19 0 50.29 47.47 12.19 o 8 19 0 18.31 20.96 12.28 o 9 19 0 384.60 411.61 21.08 o 10 19 0 35.61 27.26 12.28 o 11 19 0 562.51 601.72 26.53 o 12 19 0 144.83 145.05 14.84 o 13 19 0 486.43 540.05 40.80 o 14 19 0 223.03 240.45 29.07 o 15 19 0 164.98 235.81 28.84 o 0 20 0 241.69 259.46 26.88 o 1 20 0 164.19 212.62 17.52 o 2 20 0 440.92 356.95 26.37 o 3 20 0 152.65 175.31 14.19 o 4 20 0 51.92 63.89 11.83 o 5 20 0 3.40 2.16 10.91 o 6 20 0 605.43 554.42 24.84 o 7 20 0 467.75 401.67 21.55 o 8 20 0 77.07 97.61 13.82 o 9 20 0 142.07 138.35 27.88 o 10 20 0 53.32 39.41 13.06 o 11 20 0 3.98 -11.17 15.06 o 12 20 0 10.05 -0.12 13.82 o 13 20 0 9.66 15.45 21.38 o 14 20 0 63.33 53.08 23.47 o 1 21 0 0.39 -15.81 12.20 o 2 21 0 71.36 94.46 20.94 o 3 21 0 926.38 753.55 39.60 o 4 21 0 114.66 102.53 15.60 o 5 21 0 2.53 -16.46 10.97 o 6 21 0 17.05 -6.58 11.91 o 7 21 0 58.67 34.61 12.73 o 8 21 0 113.58 91.59 14.08 o 9 21 0 195.39 224.47 17.15 o 10 21 0 640.00 758.30 31.65 o 11 21 0 43.00 37.23 14.16 o 12 21 0 10.96 9.04 27.01 o 13 21 0 191.33 192.80 28.01 o 0 22 0 502.51 468.39 38.05 o 1 22 0 10.14 26.37 13.99 o 2 22 0 671.53 653.97 38.50 o 3 22 0 52.78 37.41 14.18 o 4 22 0 114.40 70.70 15.19 o 5 22 0 0.15 -18.84 13.71 o 6 22 0 667.18 752.76 36.07 o 7 22 0 731.16 747.71 31.33 o 8 22 0 108.76 131.16 15.55 o 9 22 0 3.85 20.21 13.97 o 10 22 0 1329.83 1478.10 52.65 o 11 22 0 95.85 160.63 17.00 o 1 23 0 158.45 201.42 18.89 o 2 23 0 9.66 7.97 13.99 o 3 23 0 846.34 805.67 37.76 o 4 23 0 7.12 -8.74 14.17 o 5 23 0 139.21 128.78 17.56 o 6 23 0 225.88 234.64 20.75 o 7 23 0 101.27 71.97 16.92 o 8 23 0 100.95 45.32 16.80 o 9 23 0 229.45 312.40 20.67 o 10 23 0 0.02 -17.78 14.21 o 0 24 0 0.01 -4.05 20.26 o 1 24 0 338.14 404.13 26.83 o 2 24 0 6.85 29.67 15.23 o 3 24 0 1074.00 1031.62 45.97 o 4 24 0 28.96 14.85 15.62 o 5 24 0 155.69 156.48 18.99 o 6 24 0 978.08 1131.70 49.39 o 7 24 0 68.87 40.48 16.67 o 8 24 0 52.60 82.18 17.87 o 1 25 0 968.57 1027.51 46.43 o 2 25 0 15.59 4.10 20.99 o 3 25 0 240.09 254.00 26.73 o 4 25 0 4.77 -14.48 15.41 o 5 25 0 320.65 324.15 24.44 o -21 0 1 18.35 11.82 20.62 o -19 0 1 92.97 1.37 19.11 o -17 0 1 625.82 288.66 32.10 o -15 0 1 700.57 595.71 45.70 o -13 0 1 1278.69 1453.43 68.96 o -11 0 1 1530.00 1567.95 110.62 o -9 0 1 4675.54 4675.78 158.11 o -7 0 1 904.01 1144.16 39.47 o -5 0 1 1537.85 1754.96 59.45 o -3 0 1 26666.63 26193.46 1019.34 o -1 0 1 2531.17 3407.97 207.67 o 3 0 1 40607.80 33400.18 1097.90 o 5 0 1 870.01 197.81 15.25 o 9 0 1 3487.75 3766.27 155.13 o 11 0 1 1817.00 1653.05 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