#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/30/2223057.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2223057_Fobs loop_ _publ_author_name 'Gowda, B. Thimme' 'Foro, Sabine' 'Shakuntala, K.' 'Fuess, Hartmut' _publ_section_title ; o-Toluenesulfonamide: a redetermination ; _journal_coeditor_code FL2262 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2258 _journal_volume 65 _journal_year 2009 _space_group_IT_number 88 _symmetry_space_group_name_Hall '-I 4ad' _symmetry_space_group_name_H-M 'I 41/a :2' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 18.6700 _cell_length_b 18.6700 _cell_length_c 9.0570 _exptl_crystal_F_000 1440.00 _reflns_d_resolution_high 0.8389 _[local]_cod_data_source_file fl2262Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' SD2 I41/A' _shelx_refln_list_code 4 _shelx_f_calc_maximum 373.06 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-y+3/4, x+1/4, z+1/4' 'y+3/4, -x+3/4, z+3/4' 'x+1/2, y+1/2, z+1/2' '-x+1, -y+1/2, z+1' '-y+5/4, x+3/4, z+3/4' 'y+5/4, -x+5/4, z+5/4' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'y-3/4, -x-1/4, -z-1/4' '-y-3/4, x-3/4, -z-3/4' '-x+1/2, -y+1/2, -z+1/2' 'x, y+1/2, -z' 'y-1/4, -x+1/4, -z+1/4' '-y-1/4, x-1/4, -z-1/4' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 2 0 336.18 326.83 7.76 o 2 2 0 3736.78 3457.50 23.18 o -2 4 0 9111.47 9074.36 69.52 o 0 4 0 139176.20 142402.52 896.30 o 2 4 0 22141.35 22575.21 357.18 o 4 4 0 112.94 63.78 3.00 o -4 6 0 13197.61 14048.81 199.73 o -2 6 0 5495.65 5311.44 31.97 o 0 6 0 18050.05 18708.83 57.03 o 2 6 0 11331.28 11875.42 344.37 o 4 6 0 8154.35 8144.45 254.73 o 6 6 0 1729.96 2161.02 20.92 o -6 8 0 241.85 279.60 8.88 o -4 8 0 10290.50 10497.84 137.58 o -2 8 0 5062.82 5934.06 62.32 o 0 8 0 21660.24 21608.98 189.72 o 2 8 0 5944.09 6405.24 84.83 o 4 8 0 1473.87 1287.70 62.43 o 6 8 0 801.17 698.59 19.43 o 8 8 0 2458.93 2281.90 26.19 o -8 10 0 1573.45 1321.00 32.65 o -6 10 0 7928.77 6466.00 1462.43 o -4 10 0 118.77 70.58 3.48 o -2 10 0 299.36 404.74 6.11 o 0 10 0 2316.58 2344.74 48.35 o 2 10 0 11.25 9.14 3.96 o 4 10 0 115.31 97.56 7.99 o 6 10 0 1787.54 2256.84 140.65 o 8 10 0 489.14 425.47 13.72 o 10 10 0 6585.08 6580.61 120.78 o -10 12 0 1617.32 1684.86 47.54 o -8 12 0 1940.62 1731.41 61.26 o -6 12 0 123.34 66.20 10.02 o -4 12 0 14107.40 7896.33 3715.89 o -2 12 0 2252.68 2787.91 68.34 o 0 12 0 18808.04 19395.96 476.39 o 2 12 0 393.56 513.81 17.46 o 4 12 0 10896.86 10846.51 702.70 o 6 12 0 1123.86 855.21 95.18 o 8 12 0 14581.80 14575.43 1171.36 o 10 12 0 4464.26 4561.12 148.63 o 12 12 0 8097.01 8460.32 277.24 o -12 14 0 3414.90 3500.44 47.93 o -10 14 0 53.39 66.59 8.04 o -8 14 0 4056.39 4157.73 176.40 o -6 14 0 692.48 731.76 47.67 o -4 14 0 3525.75 3199.41 391.93 o -2 14 0 136.55 132.74 27.39 o 0 14 0 2050.36 2222.91 90.34 o 2 14 0 788.95 670.25 26.25 o 4 14 0 689.68 667.33 45.74 o 6 14 0 454.71 365.01 40.84 o 8 14 0 4966.63 4904.74 539.67 o 10 14 0 111.79 121.41 9.56 o 12 14 0 12.16 48.15 21.90 o 14 14 0 34.48 47.21 7.93 o -14 16 0 60.68 73.36 6.99 o -12 16 0 1758.17 1860.20 64.53 o -10 16 0 3.02 16.02 9.97 o -8 16 0 1035.28 1046.47 27.51 o -6 16 0 2480.54 2233.61 108.64 o -4 16 0 1660.07 1692.71 61.31 o -2 16 0 1033.33 852.67 91.94 o 0 16 0 57.32 96.62 18.86 o 2 16 0 2628.10 2484.49 104.65 o 4 16 0 66.48 78.39 10.39 o 6 16 0 2998.22 2449.80 350.90 o 8 16 0 2607.46 2812.45 168.06 o 10 16 0 1464.59 1588.41 94.31 o 12 16 0 2083.30 2182.30 69.47 o 14 16 0 1181.08 1245.46 41.08 o -12 18 0 1229.13 1263.96 20.91 o -10 18 0 190.53 211.34 6.94 o -8 18 0 2509.34 2809.49 86.51 o -6 18 0 6.04 10.96 6.73 o -4 18 0 2241.69 2212.37 167.93 o -2 18 0 4.79 6.81 4.73 o 0 18 0 327.27 309.45 17.95 o 2 18 0 506.79 373.07 51.52 o 4 18 0 59.69 64.90 5.24 o 6 18 0 1270.60 1191.76 53.55 o 8 18 0 706.96 705.81 42.44 o 10 18 0 388.88 355.79 8.71 o 12 18 0 69.56 73.87 5.65 o -8 20 0 247.33 267.37 7.06 o -6 20 0 1386.57 1238.84 32.01 o -4 20 0 170.68 201.82 10.38 o -2 20 0 937.33 833.72 75.73 o 0 20 0 39.17 58.81 7.73 o 2 20 0 595.12 507.67 26.58 o 4 20 0 926.68 909.14 58.77 o 6 20 0 391.92 355.59 26.16 o 8 20 0 1960.61 2117.16 105.86 o -2 22 0 72.42 73.01 4.20 o 0 22 0 18.61 20.04 3.57 o 2 22 0 166.12 141.65 15.47 o 0 1 1 848.79 842.14 19.45 o -1 2 1 30472.05 29459.86 578.95 o 1 2 1 8308.20 8182.10 80.81 o -2 3 1 28966.38 28868.77 502.63 o 0 3 1 14223.18 13641.70 314.10 o 2 3 1 56318.02 53925.48 1668.07 o -3 4 1 5125.22 4627.38 52.19 o -1 4 1 27458.42 27383.99 210.00 o 1 4 1 3181.78 3316.88 103.27 o 3 4 1 27017.95 26492.92 410.64 o -4 5 1 1584.45 1486.74 15.83 o -2 5 1 9168.28 8441.32 126.07 o 0 5 1 39323.21 39108.58 625.35 o 2 5 1 32452.89 32165.64 639.90 o 4 5 1 10979.23 10407.87 149.48 o -5 6 1 5441.16 6190.29 89.26 o -3 6 1 5788.25 5444.27 106.57 o -1 6 1 2095.30 2199.57 39.53 o 1 6 1 174.48 76.50 4.42 o 3 6 1 5806.95 6215.01 124.86 o 5 6 1 1327.48 1004.82 13.99 o -6 7 1 3297.99 2988.36 67.53 o -4 7 1 1182.10 1222.75 15.27 o -2 7 1 5.30 45.76 15.59 o 0 7 1 3319.78 3016.67 58.10 o 2 7 1 1287.75 1340.92 41.36 o 4 7 1 1508.46 1504.96 64.11 o 6 7 1 17.41 46.58 12.56 o -7 8 1 43.15 60.39 14.61 o -5 8 1 55.71 66.91 3.36 o -3 8 1 48.98 65.78 3.97 o -1 8 1 46.66 83.44 3.93 o 1 8 1 15415.53 16351.05 547.71 o 3 8 1 666.38 466.32 37.33 o 5 8 1 7815.98 7450.79 1003.39 o 7 8 1 1026.29 1039.47 21.75 o -8 9 1 107.39 77.25 4.33 o -6 9 1 2732.02 2901.73 81.79 o -4 9 1 5280.28 6155.09 117.92 o -2 9 1 12011.66 12574.91 269.02 o 0 9 1 1506.33 2432.97 344.04 o 2 9 1 14061.40 14819.20 539.08 o 4 9 1 271.33 260.78 29.66 o 6 9 1 1357.91 901.59 379.12 o 8 9 1 2077.60 2129.63 50.88 o -9 10 1 475.53 552.21 10.43 o -7 10 1 1295.27 1308.66 47.08 o -5 10 1 131.33 97.77 7.97 o -3 10 1 3556.16 3357.05 73.57 o -1 10 1 2363.09 2624.01 48.60 o 1 10 1 855.45 611.52 27.63 o 3 10 1 3692.89 4085.50 239.49 o 5 10 1 2972.67 1816.96 615.35 o 7 10 1 76.60 70.53 15.60 o 9 10 1 2432.58 2600.20 81.35 o -10 11 1 155.33 182.84 7.44 o -8 11 1 6566.39 6868.85 292.00 o -6 11 1 1463.08 1221.92 140.50 o -4 11 1 5007.74 5484.66 204.96 o -2 11 1 120.12 96.70 4.59 o 0 11 1 1575.66 1435.15 33.54 o 2 11 1 58.25 71.61 8.60 o 4 11 1 7.26 17.19 8.14 o 6 11 1 5147.31 2746.21 1350.56 o 8 11 1 429.85 440.78 66.54 o 10 11 1 741.69 756.27 28.45 o -11 12 1 345.19 377.96 10.53 o -9 12 1 1479.54 1366.84 70.38 o -7 12 1 245.09 248.11 19.05 o -5 12 1 1336.84 843.18 202.24 o -3 12 1 902.21 914.49 29.19 o -1 12 1 2576.89 2371.87 83.79 o 1 12 1 1272.38 1427.65 64.37 o 3 12 1 2892.44 2571.74 228.45 o 5 12 1 837.04 779.50 223.93 o 7 12 1 3159.85 2150.00 905.88 o 9 12 1 8.86 34.93 7.70 o 11 12 1 1934.44 2054.90 63.59 o -12 13 1 931.77 998.50 17.36 o -10 13 1 2326.62 2453.60 54.28 o -8 13 1 1004.78 949.82 49.12 o -6 13 1 1069.27 1034.43 69.26 o -4 13 1 177.25 169.39 32.22 o -2 13 1 1205.58 1341.35 38.37 o 0 13 1 626.53 469.77 23.63 o 2 13 1 1958.04 1863.93 115.63 o 4 13 1 2144.52 1741.54 287.88 o 6 13 1 89.04 75.07 13.61 o 8 13 1 949.45 863.42 182.24 o 10 13 1 1194.92 1349.15 38.23 o 12 13 1 489.76 517.68 19.84 o -13 14 1 110.66 101.84 6.39 o -11 14 1 239.26 278.39 17.51 o -9 14 1 69.56 63.48 6.53 o -7 14 1 1878.73 1873.89 103.39 o -5 14 1 125.93 145.24 17.85 o -3 14 1 4026.67 2504.63 826.02 o -1 14 1 260.61 311.69 16.74 o 1 14 1 1400.84 1353.20 67.10 o 3 14 1 681.87 694.29 63.46 o 5 14 1 1805.59 1265.53 375.65 o 7 14 1 258.58 257.83 52.92 o 9 14 1 1597.45 1764.17 85.85 o 11 14 1 11.89 1.55 10.50 o 13 14 1 316.42 337.85 14.93 o -14 15 1 18.02 29.23 9.59 o -12 15 1 817.59 842.89 17.89 o -10 15 1 8.41 7.73 6.76 o -8 15 1 1458.60 1569.23 26.64 o -6 15 1 480.46 430.65 25.13 o -4 15 1 394.10 390.04 46.77 o -2 15 1 1169.96 900.90 223.89 o 0 15 1 524.32 527.31 28.89 o 2 15 1 1912.39 1864.78 106.45 o 4 15 1 1982.97 1738.03 222.35 o 6 15 1 6131.70 4249.58 1323.40 o 8 15 1 414.83 431.15 14.03 o 10 15 1 2254.68 2354.54 176.94 o 12 15 1 37.11 44.48 5.91 o 14 15 1 1185.59 1333.98 50.63 o -15 16 1 89.50 77.82 4.81 o -13 16 1 1917.76 2049.17 31.74 o -11 16 1 14.70 25.03 7.09 o -9 16 1 2226.99 2404.58 38.92 o -7 16 1 4.66 18.47 7.28 o -5 16 1 2067.32 2002.69 121.97 o -3 16 1 1372.39 1139.02 99.21 o -1 16 1 1925.48 1269.95 383.58 o 1 16 1 134.27 118.62 17.26 o 3 16 1 62.13 70.72 6.20 o 5 16 1 3.69 5.52 9.31 o 7 16 1 49.58 73.99 6.18 o 9 16 1 105.64 84.90 6.43 o 11 16 1 131.28 164.59 10.39 o 13 16 1 136.84 162.26 8.78 o 15 16 1 26.08 46.85 4.14 o -14 17 1 498.47 492.93 8.61 o -12 17 1 59.77 61.98 5.20 o -10 17 1 874.93 861.37 15.43 o -8 17 1 5.33 2.54 8.51 o -6 17 1 57.57 60.90 12.52 o -4 17 1 762.74 687.26 45.76 o -2 17 1 86.83 93.86 5.55 o 0 17 1 1080.74 805.16 183.93 o 2 17 1 53.56 61.72 7.35 o 4 17 1 2243.21 2008.96 196.39 o 6 17 1 6.47 13.61 10.77 o 8 17 1 1704.09 1753.89 94.30 o 10 17 1 20.68 29.71 7.15 o 12 17 1 1280.96 1444.06 77.42 o 14 17 1 10.37 5.79 5.71 o -11 18 1 717.84 745.98 13.80 o -9 18 1 348.93 335.48 8.66 o -7 18 1 1057.13 1044.71 20.54 o -5 18 1 524.47 514.29 10.83 o -3 18 1 1024.38 938.27 78.25 o -1 18 1 930.71 817.15 59.33 o 1 18 1 73.39 61.70 13.04 o 3 18 1 221.29 177.81 18.52 o 5 18 1 159.02 163.17 13.77 o 7 18 1 6.24 5.34 6.86 o 9 18 1 652.86 698.06 26.50 o 11 18 1 111.66 138.99 7.07 o -10 19 1 128.53 152.33 5.67 o -8 19 1 18.91 20.94 6.81 o -6 19 1 0.96 -3.26 11.28 o -4 19 1 7.37 24.37 6.23 o -2 19 1 9.92 13.79 5.93 o 0 19 1 3.11 2.42 4.85 o 2 19 1 208.25 180.78 13.95 o 4 19 1 1.85 5.01 6.58 o 6 19 1 1007.66 1021.83 76.70 o 8 19 1 216.20 203.57 15.72 o 10 19 1 593.38 620.93 10.65 o -9 20 1 384.20 374.88 11.97 o -7 20 1 23.52 18.00 4.31 o -5 20 1 425.45 424.42 9.27 o -3 20 1 165.50 153.47 6.44 o -1 20 1 812.74 775.65 63.00 o 1 20 1 8.58 8.63 5.48 o 3 20 1 76.48 99.55 12.98 o 5 20 1 1.12 -7.14 7.65 o 7 20 1 5.30 20.24 7.40 o 9 20 1 19.12 1.19 6.61 o -6 21 1 217.12 261.59 6.58 o -4 21 1 166.56 149.23 5.81 o -2 21 1 112.02 139.64 6.06 o 0 21 1 11.02 14.13 4.85 o 2 21 1 10.51 7.25 5.46 o 4 21 1 50.84 38.75 6.83 o 6 21 1 41.37 51.82 7.20 o -1 22 1 4.78 -2.64 6.04 o 1 22 1 136.79 144.12 7.66 o 1 1 2 703.84 663.21 15.21 o 0 2 2 7733.08 8404.85 172.80 o 2 2 2 56553.64 53639.35 1152.86 o -1 3 2 1273.82 1365.14 26.29 o 1 3 2 28718.63 27660.52 852.95 o 3 3 2 1371.83 1467.84 16.52 o -2 4 2 19781.36 20740.96 156.16 o 0 4 2 3465.65 3446.37 53.26 o 2 4 2 22209.65 23208.77 343.02 o 4 4 2 295.12 289.33 5.26 o -3 5 2 4409.47 4395.68 80.80 o -1 5 2 8495.56 8536.00 181.62 o 1 5 2 5193.53 5344.84 51.10 o 3 5 2 198.80 171.21 3.94 o 5 5 2 61.93 84.92 5.18 o -4 6 2 2781.63 2528.85 39.27 o -2 6 2 2369.54 1647.41 30.40 o 0 6 2 448.15 533.68 10.20 o 2 6 2 22979.20 21752.07 307.02 o 4 6 2 9588.27 9906.80 123.35 o 6 6 2 8542.81 8762.89 140.91 o -5 7 2 1605.50 1754.42 26.15 o -3 7 2 2910.58 2858.10 82.30 o -1 7 2 743.75 669.28 19.18 o 1 7 2 1322.25 1286.51 32.59 o 3 7 2 24.34 22.02 4.85 o 5 7 2 2745.43 3102.23 56.92 o 7 7 2 478.74 429.21 7.01 o -6 8 2 7899.46 8038.37 173.54 o -4 8 2 230.48 200.32 6.89 o -2 8 2 4580.60 4988.71 109.48 o 0 8 2 173.90 185.37 6.22 o 2 8 2 8681.33 9742.53 275.47 o 4 8 2 4064.83 3709.05 102.65 o 6 8 2 1205.42 1498.72 35.38 o 8 8 2 1399.10 1428.01 33.99 o -7 9 2 31.67 32.42 3.99 o -5 9 2 59.76 56.00 4.24 o -3 9 2 921.14 884.56 24.42 o -1 9 2 68.14 71.51 7.30 o 1 9 2 2533.80 2748.30 98.13 o 3 9 2 2199.45 2106.50 64.25 o 5 9 2 1017.12 1098.53 53.23 o 7 9 2 4.34 86.26 33.79 o 9 9 2 89.18 105.47 5.26 o -8 10 2 17.31 33.55 7.48 o -6 10 2 2969.08 2902.13 132.52 o -4 10 2 2.81 9.56 4.39 o -2 10 2 7511.38 6916.81 214.23 o 0 10 2 894.00 968.65 38.15 o 2 10 2 26323.94 26163.08 917.08 o 4 10 2 796.82 1069.03 34.76 o 6 10 2 12389.55 12519.34 402.24 o 8 10 2 640.51 581.90 17.56 o 10 10 2 4135.45 4185.13 203.26 o -9 11 2 593.66 670.53 48.67 o -7 11 2 71.74 92.91 4.91 o -5 11 2 46.75 44.90 4.52 o -3 11 2 78.83 85.54 6.42 o -1 11 2 502.03 456.29 21.84 o 1 11 2 99.96 109.55 6.29 o 3 11 2 165.85 153.02 12.34 o 5 11 2 3.79 50.91 20.03 o 7 11 2 1820.04 1724.18 86.51 o 9 11 2 27.06 25.92 7.90 o 11 11 2 51.97 60.00 5.25 o -10 12 2 479.54 514.75 41.73 o -8 12 2 313.53 285.93 17.18 o -6 12 2 1511.09 1429.74 89.99 o -4 12 2 366.34 301.71 47.96 o -2 12 2 1521.16 1628.85 61.55 o 0 12 2 2.44 2.56 4.95 o 2 12 2 3972.12 3773.22 181.31 o 4 12 2 3745.04 3604.09 165.59 o 6 12 2 2786.89 2733.90 226.15 o 8 12 2 493.73 444.82 20.62 o 10 12 2 238.65 253.02 12.21 o 12 12 2 976.51 1020.03 33.71 o -11 13 2 37.73 48.04 5.97 o -9 13 2 140.52 161.68 11.89 o -7 13 2 61.08 48.58 7.15 o -5 13 2 683.97 634.78 47.82 o -3 13 2 4.08 6.02 5.00 o -1 13 2 1037.87 1017.43 45.13 o 1 13 2 442.85 410.63 12.53 o 3 13 2 1276.37 1266.02 51.45 o 5 13 2 192.33 180.39 21.19 o 7 13 2 680.68 584.20 68.46 o 9 13 2 35.86 50.33 4.78 o 11 13 2 62.94 65.88 7.82 o 13 13 2 0.13 -1.51 9.71 o -12 14 2 4.21 19.51 7.37 o -10 14 2 5636.18 5998.34 155.41 o -8 14 2 1328.87 1145.50 115.12 o -6 14 2 6590.34 6110.36 498.53 o -4 14 2 2384.59 2066.24 170.37 o -2 14 2 9687.97 7278.97 1812.64 o 0 14 2 2196.19 2044.22 121.35 o 2 14 2 11318.52 11480.46 530.76 o 4 14 2 3082.68 2750.19 199.16 o 6 14 2 2733.62 2452.55 378.48 o 8 14 2 3251.25 2560.64 531.18 o 10 14 2 1441.84 1594.25 98.65 o 12 14 2 567.05 599.67 27.72 o 14 14 2 1658.00 1751.19 28.70 o -13 15 2 526.97 525.00 12.16 o -11 15 2 25.68 28.45 5.38 o -9 15 2 57.53 80.57 6.52 o -7 15 2 46.29 49.04 9.53 o -5 15 2 20.06 23.79 4.59 o -3 15 2 7.84 -0.72 6.78 o -1 15 2 0.58 9.71 13.43 o 1 15 2 70.12 100.10 5.64 o 3 15 2 30.91 30.94 5.32 o 5 15 2 128.35 153.08 17.43 o 7 15 2 575.08 518.69 86.03 o 9 15 2 1.80 2.35 7.62 o 11 15 2 0.51 -9.75 9.75 o 13 15 2 423.86 438.02 22.44 o 15 15 2 153.05 194.18 9.22 o -14 16 2 46.08 57.48 4.79 o -12 16 2 441.35 456.65 26.90 o -10 16 2 158.11 193.38 9.18 o -8 16 2 116.09 132.60 7.05 o -6 16 2 1039.12 977.76 106.13 o -4 16 2 0.35 -0.31 6.51 o -2 16 2 50.70 60.59 5.40 o 0 16 2 67.16 76.77 14.38 o 2 16 2 582.36 521.61 34.80 o 4 16 2 495.95 402.39 29.97 o 6 16 2 247.90 214.24 31.94 o 8 16 2 404.43 401.48 10.79 o 10 16 2 66.55 76.64 8.52 o 12 16 2 94.39 82.28 9.59 o 14 16 2 23.84 24.43 5.07 o -13 17 2 82.58 88.24 6.78 o -11 17 2 1.94 -5.39 5.53 o -9 17 2 240.24 257.27 8.51 o -7 17 2 42.79 50.78 11.03 o -5 17 2 8.07 11.03 8.01 o -3 17 2 96.23 110.53 8.62 o -1 17 2 393.26 369.90 16.08 o 1 17 2 88.71 94.50 11.21 o 3 17 2 0.18 -6.06 9.51 o 5 17 2 3.43 8.75 9.06 o 7 17 2 75.19 76.90 6.06 o 9 17 2 153.20 156.19 7.39 o 11 17 2 45.93 61.86 5.19 o 13 17 2 39.70 47.70 5.87 o -12 18 2 113.28 118.17 4.96 o -10 18 2 1429.03 1411.57 22.30 o -8 18 2 492.17 444.61 17.24 o -6 18 2 1162.84 1208.15 36.83 o -4 18 2 691.73 618.38 49.38 o -2 18 2 1280.22 1253.72 79.99 o 0 18 2 954.65 825.29 56.97 o 2 18 2 2544.42 2052.56 206.43 o 4 18 2 1368.66 1178.12 95.34 o 6 18 2 714.00 751.15 43.68 o 8 18 2 1263.89 1235.58 51.18 o 10 18 2 373.23 426.97 25.89 o 12 18 2 434.42 488.84 15.35 o -9 19 2 18.83 12.60 8.01 o -7 19 2 8.37 11.29 6.30 o -5 19 2 203.99 201.92 7.49 o -3 19 2 46.14 42.42 4.67 o -1 19 2 71.80 51.38 4.92 o 1 19 2 3.64 8.50 4.84 o 3 19 2 0.38 -4.84 8.15 o 5 19 2 51.45 64.34 7.38 o 7 19 2 0.18 0.83 4.68 o 9 19 2 10.37 4.60 5.97 o -8 20 2 592.37 589.91 12.92 o -6 20 2 948.66 1086.12 35.92 o -4 20 2 282.20 302.09 8.00 o -2 20 2 5.94 17.34 4.56 o 0 20 2 202.62 181.48 12.54 o 2 20 2 112.81 107.06 5.02 o 4 20 2 264.57 224.27 8.91 o 6 20 2 43.93 42.25 4.74 o 8 20 2 53.00 43.23 7.67 o -5 21 2 76.49 67.00 6.32 o -3 21 2 42.29 41.50 4.78 o -1 21 2 0.25 0.85 4.86 o 1 21 2 16.95 11.04 3.53 o 3 21 2 166.03 172.57 16.71 o 5 21 2 9.81 8.47 4.87 o 0 1 3 9572.81 9392.25 155.90 o -1 2 3 7.35 58.22 25.52 o 1 2 3 14927.40 15098.19 227.13 o -2 3 3 6109.33 6211.80 201.33 o 0 3 3 169.03 153.66 6.62 o 2 3 3 30411.59 31247.97 377.96 o -3 4 3 781.22 1013.43 19.91 o -1 4 3 23656.44 23480.02 487.25 o 1 4 3 3791.28 4033.78 93.60 o 3 4 3 111.17 79.93 4.19 o -4 5 3 1335.48 1559.15 18.82 o -2 5 3 159.26 249.85 12.03 o 0 5 3 945.14 1015.19 44.56 o 2 5 3 3291.21 3746.63 88.30 o 4 5 3 17755.36 17864.88 69.40 o -5 6 3 607.44 806.91 42.96 o -3 6 3 13769.31 14068.23 164.02 o -1 6 3 1206.63 1057.57 15.12 o 1 6 3 134.76 111.04 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