#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/30/2223066.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2223066_Fobs loop_ _publ_author_name 'Jiang, Bin' 'Liu, Zhilu' _publ_section_title ; 2-Amino-9-[(1S,3R,4S)-4-hydroxy-3-hydroxymethyl-2-methylenecyclopentyl]-1,9-dihydro-6H-purin-6-one monohydrate ; _journal_coeditor_code HB5032 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2232 _journal_volume 65 _journal_year 2009 _space_group_IT_number 20 _symmetry_space_group_name_Hall 'C 2c 2' _symmetry_space_group_name_H-M 'C 2 2 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 6.9986 _cell_length_b 11.6229 _cell_length_c 33.9317 _exptl_crystal_F_000 1248.00 _reflns_d_resolution_high 0.8409 _[local]_cod_data_source_file hb5032Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' test in C222(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 358.39 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z+1/2' '-x, y, -z+1/2' 'x, -y, -z' 'x+1/2, y+1/2, z' '-x+1/2, -y+1/2, z+1/2' '-x+1/2, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 128440.54 100667.28 2924.77 o 4 0 0 2520.27 2068.71 38.55 o 6 0 0 244.64 241.39 15.29 o 1 1 0 1478.48 1530.22 28.08 o 3 1 0 5026.62 5530.67 60.80 o 5 1 0 104.95 112.01 9.93 o 7 1 0 21.67 28.43 7.36 o 0 2 0 728.41 594.51 19.93 o 2 2 0 318.86 350.30 9.04 o 4 2 0 2326.36 2493.16 34.48 o 6 2 0 126.90 145.83 11.22 o 8 2 0 1.47 -4.30 16.15 o 1 3 0 7263.20 7196.33 95.10 o 3 3 0 2712.48 2654.68 38.05 o 5 3 0 85.37 91.69 10.37 o 7 3 0 336.52 369.91 45.36 o 0 4 0 10865.02 11249.43 179.11 o 2 4 0 6540.98 6649.58 103.76 o 4 4 0 297.74 303.88 14.79 o 6 4 0 364.34 387.73 24.11 o 1 5 0 295.78 258.50 13.37 o 3 5 0 1233.34 1253.29 35.94 o 5 5 0 231.86 249.83 16.24 o 7 5 0 13.38 23.17 12.66 o 0 6 0 300.85 246.68 25.43 o 2 6 0 1456.85 1480.25 38.69 o 4 6 0 21.22 12.69 7.04 o 6 6 0 206.76 212.14 22.13 o 1 7 0 580.83 682.12 19.48 o 3 7 0 52.35 73.42 21.66 o 5 7 0 37.96 40.29 9.78 o 7 7 0 48.17 67.99 16.35 o 0 8 0 1032.98 1057.42 33.96 o 2 8 0 0.28 0.57 6.77 o 4 8 0 1688.78 1693.29 52.46 o 6 8 0 325.46 319.54 46.67 o 1 9 0 164.33 156.69 13.14 o 3 9 0 208.37 230.86 19.99 o 5 9 0 506.73 526.90 33.15 o 0 10 0 327.46 307.90 32.72 o 2 10 0 161.71 184.10 28.94 o 4 10 0 0.01 -4.20 9.29 o 1 11 0 341.06 369.51 33.87 o 3 11 0 26.72 0.42 10.09 o 5 11 0 75.74 51.06 15.66 o 0 12 0 258.62 253.78 34.50 o 2 12 0 0.01 5.93 8.49 o 4 12 0 8.66 -1.02 17.67 o 1 13 0 12.57 0.23 23.39 o 2 0 1 27548.27 27053.98 289.51 o 4 0 1 2584.43 2571.03 67.46 o 6 0 1 776.05 745.72 36.07 o 1 1 1 1836.78 1838.11 23.30 o 3 1 1 15510.52 16333.98 104.61 o 5 1 1 866.58 858.53 12.21 o 7 1 1 601.66 574.48 15.54 o 2 2 1 391.29 489.09 7.65 o 4 2 1 685.93 718.00 13.96 o 6 2 1 713.55 651.43 15.57 o 8 2 1 40.39 36.40 11.38 o 1 3 1 5945.89 6012.15 57.00 o 3 3 1 1879.36 1842.70 20.46 o 5 3 1 1007.76 1017.80 20.17 o 7 3 1 3.97 -2.23 6.04 o 0 4 1 260.80 295.27 10.08 o 2 4 1 168.15 188.93 7.85 o 4 4 1 640.33 673.85 15.26 o 6 4 1 372.07 405.08 15.96 o 1 5 1 1088.40 1100.28 16.09 o 3 5 1 1751.01 1759.92 23.00 o 5 5 1 1.99 4.24 4.77 o 7 5 1 73.70 91.56 12.20 o 0 6 1 6297.61 6487.79 80.84 o 2 6 1 2669.43 2826.14 33.08 o 4 6 1 588.86 592.91 15.89 o 6 6 1 391.42 360.73 19.42 o 1 7 1 816.74 803.79 15.18 o 3 7 1 114.22 110.16 8.73 o 5 7 1 28.65 35.73 7.23 o 7 7 1 21.23 25.94 9.12 o 0 8 1 2987.82 2773.96 44.55 o 2 8 1 427.84 433.06 16.31 o 4 8 1 502.75 525.01 16.16 o 6 8 1 117.69 122.84 14.04 o 1 9 1 2281.76 2276.55 37.56 o 3 9 1 192.55 185.31 13.04 o 5 9 1 114.02 101.33 13.31 o 0 10 1 649.87 697.91 32.63 o 2 10 1 77.15 92.41 10.60 o 4 10 1 499.64 521.49 19.54 o 1 11 1 496.71 516.30 18.51 o 3 11 1 484.57 478.14 28.44 o 5 11 1 207.63 201.10 17.80 o 0 12 1 18.24 17.93 11.52 o 2 12 1 132.14 144.73 11.35 o 4 12 1 175.63 194.82 17.46 o 1 13 1 15.75 24.13 12.65 o 2 0 2 74366.28 68853.88 881.93 o 4 0 2 16369.21 16572.53 186.71 o 6 0 2 37.37 48.93 9.73 o 8 0 2 72.25 110.11 24.43 o 1 1 2 40025.72 38805.54 599.65 o 3 1 2 330.61 385.34 8.49 o 5 1 2 686.17 670.86 10.73 o 7 1 2 193.21 194.80 10.17 o 0 2 2 4589.07 4204.57 265.98 o 2 2 2 922.93 938.35 10.82 o 4 2 2 664.54 712.56 11.63 o 6 2 2 639.30 566.11 19.40 o 8 2 2 0.95 2.19 23.60 o 1 3 2 3240.48 3185.10 32.48 o 3 3 2 1236.65 1273.33 17.52 o 5 3 2 1154.24 1173.95 21.86 o 7 3 2 14.55 14.37 6.40 o 2 4 2 269.79 239.70 7.71 o 4 4 2 1262.59 1284.15 22.11 o 6 4 2 257.54 308.71 14.53 o 1 5 2 996.42 959.70 14.77 o 3 5 2 225.93 252.88 8.02 o 5 5 2 131.57 155.72 10.12 o 7 5 2 77.93 67.40 14.36 o 0 6 2 121.46 118.06 7.44 o 4 6 2 410.25 401.96 17.25 o 6 6 2 28.69 32.17 7.22 o 1 7 2 1578.75 1626.51 23.51 o 3 7 2 286.12 290.89 12.53 o 5 7 2 1163.12 1056.42 26.38 o 7 7 2 9.49 -2.55 7.11 o 0 8 2 157.85 178.73 10.34 o 2 8 2 250.56 264.18 13.31 o 4 8 2 366.56 367.16 13.99 o 6 8 2 55.33 52.82 11.75 o 1 9 2 165.69 152.10 10.09 o 3 9 2 256.90 262.86 13.48 o 5 9 2 74.02 82.83 10.24 o 0 10 2 633.51 673.00 32.06 o 2 10 2 266.22 291.38 15.79 o 4 10 2 636.77 620.37 31.60 o 1 11 2 147.91 136.86 11.46 o 3 11 2 431.48 403.70 17.58 o 5 11 2 5.88 0.96 11.61 o 0 12 2 17.26 17.50 11.38 o 2 12 2 88.68 84.29 10.22 o 4 12 2 207.00 219.47 26.93 o 1 13 2 151.06 152.01 15.32 o 2 0 3 15941.85 16287.61 158.31 o 4 0 3 16486.44 16483.47 166.05 o 6 0 3 3961.03 3605.67 50.25 o 8 0 3 65.54 35.24 17.62 o 3 1 3 1378.12 1516.83 15.60 o 5 1 3 401.50 439.61 9.60 o 7 1 3 123.63 130.03 9.68 o 0 2 3 30513.70 29233.11 362.30 o 2 2 3 643.33 652.70 9.09 o 4 2 3 357.46 367.21 8.38 o 6 2 3 8.87 18.52 5.02 o 8 2 3 24.17 31.21 13.58 o 1 3 3 25032.44 24818.18 204.17 o 3 3 3 7125.32 7331.95 62.49 o 5 3 3 216.80 260.65 11.10 o 7 3 3 11.42 11.33 6.12 o 0 4 3 10657.72 9686.21 581.48 o 2 4 3 681.71 686.56 14.07 o 4 4 3 679.46 715.52 14.16 o 6 4 3 3.15 10.16 5.93 o 1 5 3 1221.32 1236.85 17.50 o 3 5 3 311.36 331.21 9.71 o 5 5 3 1873.40 1805.71 33.74 o 7 5 3 144.66 146.99 14.49 o 0 6 3 2311.92 2612.49 55.03 o 2 6 3 4927.97 5079.59 59.85 o 4 6 3 1070.39 1073.59 21.74 o 6 6 3 138.37 138.73 11.42 o 1 7 3 3362.29 3478.77 37.95 o 3 7 3 1584.08 1640.96 29.78 o 5 7 3 58.91 61.13 11.23 o 7 7 3 0.48 10.06 8.06 o 0 8 3 0.01 6.99 4.45 o 2 8 3 2016.03 2072.27 38.49 o 4 8 3 186.98 192.26 15.63 o 6 8 3 39.25 37.96 9.40 o 1 9 3 262.69 287.24 12.98 o 3 9 3 304.63 311.56 23.01 o 5 9 3 660.96 684.14 22.73 o 0 10 3 3377.26 3335.81 64.53 o 2 10 3 1798.14 1711.25 33.77 o 4 10 3 1212.69 1180.19 29.80 o 1 11 3 58.08 45.46 9.65 o 3 11 3 157.26 153.13 14.03 o 5 11 3 17.09 11.24 8.73 o 0 12 3 228.81 230.68 29.57 o 2 12 3 37.10 34.56 8.02 o 4 12 3 28.47 13.31 8.02 o 1 13 3 211.73 214.65 17.36 o 2 0 4 22319.41 22538.55 348.16 o 4 0 4 6484.67 6715.94 74.52 o 6 0 4 3847.10 3702.79 51.29 o 8 0 4 478.08 492.76 44.83 o 1 1 4 2445.97 2606.63 24.72 o 3 1 4 5261.14 5669.16 46.39 o 5 1 4 649.70 653.48 11.67 o 7 1 4 147.25 163.10 10.64 o 0 2 4 1.16 -2.63 2.63 o 2 2 4 66.67 68.07 3.63 o 4 2 4 1684.09 1669.97 19.57 o 6 2 4 777.50 757.29 18.71 o 8 2 4 9.72 15.02 9.13 o 1 3 4 4058.99 3923.59 36.51 o 3 3 4 1177.22 1233.39 14.79 o 5 3 4 508.71 516.48 12.19 o 7 3 4 39.93 42.20 8.20 o 0 4 4 9074.97 8805.55 159.69 o 2 4 4 179.29 155.00 6.28 o 4 4 4 967.31 979.52 16.91 o 6 4 4 224.69 228.80 13.97 o 1 5 4 887.69 928.10 16.16 o 3 5 4 1405.43 1483.19 22.59 o 5 5 4 1697.44 1720.66 32.92 o 7 5 4 8.67 11.53 7.54 o 0 6 4 4086.59 3919.79 75.22 o 2 6 4 150.69 147.56 7.14 o 4 6 4 1348.41 1394.19 25.11 o 6 6 4 1222.06 1129.23 28.11 o 1 7 4 1433.00 1380.54 19.93 o 3 7 4 117.84 116.18 9.08 o 5 7 4 526.79 535.38 18.82 o 7 7 4 71.78 68.89 11.83 o 0 8 4 1789.32 1868.89 34.21 o 2 8 4 613.18 603.40 19.23 o 4 8 4 2.56 2.50 4.91 o 6 8 4 107.02 100.47 13.07 o 1 9 4 503.75 508.28 16.28 o 3 9 4 100.29 125.11 10.30 o 5 9 4 577.76 598.44 21.35 o 0 10 4 4324.27 4071.82 74.25 o 2 10 4 2119.33 2058.64 37.73 o 4 10 4 418.08 434.02 20.37 o 1 11 4 1678.96 1691.13 34.68 o 3 11 4 8.57 10.49 6.61 o 0 12 4 44.02 55.94 14.70 o 2 12 4 138.24 161.48 15.14 o 4 12 4 5.59 20.84 7.66 o 1 13 4 54.05 82.48 13.78 o 2 0 5 8934.83 9487.96 158.32 o 4 0 5 5712.52 5676.14 64.67 o 6 0 5 1087.94 1033.53 27.52 o 8 0 5 929.83 923.21 40.60 o 1 1 5 9083.81 8749.21 74.23 o 3 1 5 4412.63 4540.76 34.76 o 5 1 5 2205.64 2085.69 21.97 o 7 1 5 98.71 100.39 9.07 o 0 2 5 407.18 295.80 9.30 o 2 2 5 6329.21 5952.45 54.04 o 4 2 5 2527.53 2629.99 26.97 o 6 2 5 410.43 375.82 15.38 o 8 2 5 7.71 9.47 6.95 o 1 3 5 2084.83 1953.53 22.17 o 3 3 5 47.92 45.07 3.30 o 5 3 5 1579.38 1619.45 22.82 o 7 3 5 16.43 12.47 6.44 o 2 4 5 5511.91 5580.22 57.19 o 4 4 5 126.77 129.97 7.06 o 6 4 5 676.56 704.02 20.71 o 1 5 5 225.85 242.66 14.96 o 3 5 5 631.73 656.51 14.05 o 5 5 5 106.75 106.03 9.63 o 7 5 5 13.12 14.15 6.88 o 0 6 5 1786.90 1753.67 34.26 o 2 6 5 203.47 202.88 8.27 o 4 6 5 1087.92 1075.18 24.74 o 6 6 5 78.30 83.53 9.47 o 1 7 5 1137.55 1201.17 19.00 o 3 7 5 167.37 160.98 9.95 o 5 7 5 232.06 241.14 13.88 o 7 7 5 23.33 21.37 8.68 o 0 8 5 1251.80 1364.51 27.99 o 2 8 5 360.47 342.58 14.68 o 4 8 5 229.21 236.57 13.67 o 6 8 5 161.60 138.91 12.55 o 1 9 5 763.53 743.33 19.84 o 3 9 5 1330.46 1349.72 28.82 o 5 9 5 176.63 184.40 13.81 o 0 10 5 46.40 56.73 10.42 o 2 10 5 269.97 287.40 14.52 o 4 10 5 699.43 711.61 26.24 o 1 11 5 95.37 102.49 10.47 o 3 11 5 418.19 363.25 21.66 o 0 12 5 738.70 755.67 37.47 o 2 12 5 55.05 89.20 12.14 o 4 12 5 287.10 290.09 24.35 o 1 13 5 54.40 76.00 11.92 o 0 0 6 6678.11 6162.56 142.62 o 2 0 6 19284.79 18018.81 198.29 o 4 0 6 2383.12 2494.97 34.02 o 6 0 6 24.88 41.00 9.53 o 8 0 6 531.24 495.80 30.14 o 1 1 6 4428.21 4282.22 38.97 o 3 1 6 139.08 157.92 4.45 o 5 1 6 2124.28 2137.99 22.36 o 7 1 6 546.23 550.17 18.80 o 4 2 6 1856.95 1863.34 22.49 o 6 2 6 127.88 125.54 12.89 o 8 2 6 105.71 96.25 12.19 o 1 3 6 4663.65 4645.80 51.04 o 3 3 6 375.75 328.67 7.78 o 5 3 6 542.74 536.24 13.76 o 7 3 6 65.88 71.58 9.39 o 0 4 6 14348.02 13885.44 180.13 o 2 4 6 650.13 602.66 11.98 o 4 4 6 1389.18 1410.13 21.13 o 6 4 6 111.26 118.96 10.41 o 1 5 6 6651.74 7134.98 65.20 o 3 5 6 1334.57 1315.13 21.13 o 5 5 6 320.16 325.87 14.69 o 7 5 6 35.86 38.01 8.18 o 0 6 6 323.29 389.93 18.95 o 2 6 6 5548.89 5537.22 59.78 o 4 6 6 884.21 906.43 22.72 o 6 6 6 398.25 420.21 17.90 o 1 7 6 889.88 880.67 15.34 o 3 7 6 310.47 327.29 13.28 o 5 7 6 77.59 67.18 8.72 o 7 7 6 42.31 41.25 10.32 o 0 8 6 2446.93 2466.09 47.49 o 2 8 6 464.98 465.12 16.50 o 4 8 6 462.83 455.02 23.13 o 6 8 6 108.88 122.06 12.73 o 1 9 6 3096.26 2894.18 44.39 o 3 9 6 1325.17 1341.69 33.40 o 5 9 6 284.68 288.92 16.41 o 0 10 6 5380.06 5499.33 93.33 o 2 10 6 1987.78 1912.10 33.17 o 4 10 6 156.74 167.42 15.13 o 1 11 6 590.21 594.64 19.88 o 3 11 6 133.22 137.08 12.40 o 0 12 6 114.64 126.30 19.43 o 2 12 6 176.95 164.61 15.00 o 1 13 6 376.44 435.38 33.48 o 4 0 7 61.74 66.82 5.27 o 6 0 7 40.76 30.07 7.59 o 8 0 7 22.15 16.08 10.78 o 1 1 7 9403.10 9338.54 79.73 o 3 1 7 129.26 119.43 4.00 o 5 1 7 376.66 395.86 9.42 o 7 1 7 52.01 50.91 10.64 o 0 2 7 7928.64 7537.47 100.01 o 2 2 7 3025.59 2973.97 30.64 o 4 2 7 224.69 231.20 7.29 o 6 2 7 559.11 537.40 14.66 o 8 2 7 77.24 94.42 13.26 o 1 3 7 16319.65 16664.86 139.45 o 3 3 7 6208.38 6203.33 54.46 o 5 3 7 213.08 198.93 9.22 o 7 3 7 253.25 242.73 14.67 o 0 4 7 5175.93 5550.40 79.13 o 2 4 7 4587.67 4562.59 48.58 o 4 4 7 826.41 891.81 18.29 o 6 4 7 691.78 670.97 20.36 o 1 5 7 8070.19 8733.22 78.19 o 3 5 7 292.20 324.97 13.07 o 5 5 7 798.02 793.75 34.94 o 7 5 7 70.30 61.67 10.28 o 0 6 7 466.73 440.07 27.35 o 2 6 7 109.21 127.69 7.10 o 4 6 7 509.26 537.22 17.48 o 6 6 7 6.58 12.79 6.34 o 1 7 7 424.03 455.24 12.46 o 3 7 7 2078.67 1999.32 36.65 o 5 7 7 454.74 485.11 18.05 o 7 7 7 50.70 44.16 10.44 o 0 8 7 984.80 926.56 25.98 o 2 8 7 559.50 551.50 15.32 o 4 8 7 285.46 328.77 23.33 o 6 8 7 165.57 176.64 20.04 o 1 9 7 256.30 271.02 11.61 o 3 9 7 290.66 288.47 16.55 o 5 9 7 36.36 25.52 7.66 o 0 10 7 258.79 281.22 18.06 o 2 10 7 269.76 311.56 13.63 o 4 10 7 900.74 940.15 30.19 o 1 11 7 57.93 69.64 8.97 o 3 11 7 94.24 89.29 10.43 o 0 12 7 181.77 189.39 22.12 o 2 12 7 65.99 70.31 11.00 o 1 13 7 166.31 161.39 15.73 o 0 0 8 18026.92 17260.06 381.73 o 4 0 8 3223.10 3251.27 45.42 o 6 0 8 496.74 480.15 18.38 o 8 0 8 67.76 69.93 15.29 o 1 1 8 6627.05 6623.52 58.56 o 3 1 8 1556.76 1681.04 17.41 o 5 1 8 12.59 13.37 3.80 o 7 1 8 115.23 124.42 10.87 o 0 2 8 22873.54 21293.64 231.07 o 2 2 8 2271.04 2183.46 24.46 o 4 2 8 567.46 529.70 10.02 o 6 2 8 596.53 552.11 19.08 o 8 2 8 29.73 26.61 11.72 o 1 3 8 24.61 26.04 3.02 o 3 3 8 176.35 199.91 7.32 o 5 3 8 257.91 232.07 13.08 o 7 3 8 44.21 42.02 8.20 o 0 4 8 2614.57 2864.06 39.72 o 2 4 8 2032.99 2215.30 27.84 o 4 4 8 445.23 465.61 12.23 o 6 4 8 354.04 386.22 16.37 o 1 5 8 2609.18 2542.23 28.38 o 3 5 8 764.82 818.10 16.24 o 5 5 8 597.16 632.23 19.45 o 7 5 8 210.00 212.98 16.60 o 0 6 8 7249.37 7591.05 108.74 o 2 6 8 2092.10 2172.41 29.79 o 4 6 8 867.70 867.43 25.16 o 6 6 8 21.02 36.67 7.67 o 1 7 8 0.62 1.58 3.10 o 3 7 8 153.42 149.14 11.82 o 5 7 8 589.54 590.82 19.98 o 0 8 8 167.05 148.17 11.78 o 2 8 8 2001.14 1938.41 30.73 o 4 8 8 199.86 187.78 14.22 o 6 8 8 9.43 10.80 7.05 o 1 9 8 2298.57 2251.92 40.26 o 3 9 8 1557.92 1513.29 35.90 o 5 9 8 117.00 120.45 11.79 o 0 10 8 709.39 692.31 26.02 o 2 10 8 1124.17 1096.14 26.93 o 4 10 8 641.71 608.52 24.15 o 1 11 8 125.58 99.73 12.55 o 3 11 8 307.54 312.11 16.86 o 0 12 8 0.89 1.80 12.64 o 2 12 8 75.04 73.75 10.92 o 1 13 8 26.20 34.09 9.11 o 2 0 9 44.48 43.06 4.94 o 4 0 9 1334.33 1363.49 26.20 o 6 0 9 62.97 57.15 13.50 o 8 0 9 2.45 4.66 9.96 o 1 1 9 2852.81 2810.59 26.20 o 3 1 9 190.04 231.11 6.46 o 5 1 9 21.99 17.72 4.14 o 7 1 9 255.28 263.44 13.15 o 0 2 9 3836.76 3889.92 42.66 o 2 2 9 5677.37 5559.12 52.41 o 4 2 9 2267.84 2199.50 26.17 o 6 2 9 3.67 6.81 4.84 o 8 2 9 41.16 46.86 9.04 o 1 3 9 10949.38 11357.59 91.37 o 3 3 9 583.54 607.57 12.62 o 5 3 9 106.40 105.67 8.46 o 7 3 9 13.29 10.14 6.01 o 0 4 9 37.49 65.62 5.49 o 2 4 9 269.27 297.30 7.15 o 4 4 9 375.60 351.07 13.48 o 6 4 9 49.15 59.48 7.68 o 1 5 9 4858.15 4552.77 42.21 o 3 5 9 875.35 843.61 19.30 o 5 5 9 788.69 737.03 21.00 o 7 5 9 93.34 71.03 11.22 o 0 6 9 6441.97 6346.14 93.79 o 2 6 9 2477.92 2570.17 29.59 o 4 6 9 734.43 765.49 23.84 o 6 6 9 41.84 52.48 8.29 o 1 7 9 424.60 427.36 16.24 o 3 7 9 121.01 128.23 11.21 o 5 7 9 187.00 204.62 13.29 o 0 8 9 3017.19 2863.65 53.65 o 2 8 9 412.10 490.72 14.57 o 4 8 9 89.15 76.78 10.51 o 6 8 9 4.50 5.14 6.79 o 1 9 9 239.06 250.68 10.56 o 3 9 9 904.86 902.78 24.40 o 5 9 9 78.07 110.27 12.89 o 0 10 9 721.20 731.16 32.25 o 2 10 9 442.11 444.69 23.53 o 4 10 9 808.99 777.78 27.37 o 1 11 9 1317.73 1347.47 30.69 o 3 11 9 270.03 272.04 16.13 o 0 12 9 25.21 61.66 17.83 o 2 12 9 55.17 43.14 9.75 o 1 13 9 2.57 4.20 7.14 o 0 0 10 15807.11 14768.58 295.05 o 2 0 10 1.79 3.48 4.25 o 4 0 10 1795.23 1694.42 33.88 o 6 0 10 204.62 172.97 14.79 o 8 0 10 9.97 13.92 10.85 o 1 1 10 276.83 285.13 6.28 o 3 1 10 421.93 423.61 8.55 o 5 1 10 796.53 793.07 15.67 o 7 1 10 209.36 190.77 11.77 o 2 2 10 1553.61 1673.62 20.82 o 4 2 10 7.78 10.97 3.39 o 6 2 10 593.49 575.56 21.97 o 1 3 10 282.72 249.43 6.37 o 3 3 10 732.22 725.91 12.50 o 5 3 10 750.45 730.36 16.47 o 7 3 10 65.07 72.29 9.58 o 0 4 10 170.12 149.82 7.51 o 2 4 10 1275.68 1241.45 16.44 o 4 4 10 106.19 115.77 7.29 o 6 4 10 402.09 424.22 24.25 o 1 5 10 2675.45 2946.04 32.66 o 3 5 10 1312.99 1325.39 25.34 o 5 5 10 477.72 493.59 17.31 o 7 5 10 38.29 33.18 13.06 o 0 6 10 466.23 466.70 14.39 o 2 6 10 1109.29 1093.31 18.16 o 4 6 10 1789.27 1757.91 37.81 o 6 6 10 206.78 198.54 13.70 o 1 7 10 707.31 688.52 15.79 o 3 7 10 197.72 208.53 13.51 o 5 7 10 157.27 184.49 12.98 o 0 8 10 2570.95 2541.03 49.82 o 2 8 10 1619.25 1599.56 27.80 o 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12.99 o 5 3 22 171.87 186.50 13.10 o 0 4 22 38.24 40.58 6.79 o 2 4 22 299.39 293.14 10.71 o 4 4 22 766.47 743.50 25.40 o 6 4 22 378.02 351.58 16.38 o 1 5 22 1327.50 1289.92 21.93 o 3 5 22 1647.91 1626.38 27.11 o 5 5 22 319.02 330.28 15.31 o 0 6 22 602.33 620.92 23.96 o 2 6 22 547.24 557.39 16.64 o 4 6 22 348.81 368.42 17.24 o 1 7 22 1442.17 1416.40 27.10 o 3 7 22 505.08 484.00 16.52 o 5 7 22 307.17 285.92 20.56 o 0 8 22 4.51 7.26 9.73 o 2 8 22 9.10 7.44 6.53 o 4 8 22 26.20 25.04 12.14 o 1 9 22 463.29 475.88 21.30 o 3 9 22 91.85 100.49 11.22 o 0 10 22 10.46 13.04 11.48 o 2 10 22 43.53 56.98 12.29 o 1 11 22 73.34 69.55 13.79 o 2 0 23 9.90 10.07 7.12 o 4 0 23 161.74 180.37 22.79 o 6 0 23 262.00 294.03 26.30 o 1 1 23 440.10 454.46 12.69 o 3 1 23 520.80 525.22 14.16 o 5 1 23 269.18 260.05 13.26 o 0 2 23 1708.33 1651.76 35.86 o 2 2 23 817.63 870.93 17.48 o 4 2 23 308.72 267.84 12.70 o 6 2 23 469.03 524.07 20.79 o 1 3 23 8.88 9.82 3.89 o 3 3 23 350.95 333.58 13.17 o 5 3 23 54.52 72.52 7.87 o 0 4 23 2542.54 2581.65 52.03 o 2 4 23 158.92 175.42 9.30 o 4 4 23 778.04 782.21 20.82 o 6 4 23 212.11 233.74 14.08 o 1 5 23 479.62 442.84 14.11 o 3 5 23 67.31 83.23 8.39 o 5 5 23 18.34 15.25 6.01 o 0 6 23 47.50 41.69 9.91 o 2 6 23 2281.51 2139.76 35.02 o 4 6 23 429.31 466.56 18.93 o 1 7 23 1107.06 1075.48 26.24 o 3 7 23 703.72 759.42 20.79 o 5 7 23 303.46 283.30 19.51 o 0 8 23 1044.26 978.85 41.34 o 2 8 23 421.56 404.48 15.91 o 4 8 23 544.29 534.92 24.51 o 1 9 23 268.55 273.46 17.60 o 3 9 23 320.55 274.16 16.38 o 0 10 23 203.75 254.37 25.77 o 2 10 23 228.24 238.32 21.23 o 1 11 23 0.04 1.61 7.77 o 0 0 24 252.77 288.57 22.49 o 2 0 24 2.44 1.34 5.66 o 4 0 24 0.62 -1.74 12.45 o 6 0 24 89.09 75.52 15.70 o 1 1 24 329.69 317.72 15.68 o 3 1 24 34.78 27.62 5.54 o 5 1 24 139.95 152.17 11.12 o 0 2 24 165.74 154.52 17.41 o 2 2 24 1201.90 1134.72 20.68 o 4 2 24 542.20 524.89 16.68 o 6 2 24 152.80 163.66 13.59 o 1 3 24 376.04 393.20 10.80 o 3 3 24 1192.82 1208.87 35.63 o 5 3 24 229.46 218.79 11.94 o 0 4 24 37.30 44.57 10.88 o 2 4 24 3438.29 3247.50 40.74 o 4 4 24 1752.58 1746.69 32.62 o 6 4 24 115.70 117.96 11.19 o 1 5 24 720.92 733.01 18.23 o 3 5 24 269.90 235.17 12.29 o 5 5 24 76.38 67.35 10.70 o 0 6 24 0.01 0.81 6.44 o 2 6 24 341.54 323.05 13.71 o 4 6 24 519.52 511.81 19.72 o 1 7 24 685.80 586.04 19.53 o 3 7 24 405.77 366.30 20.06 o 5 7 24 166.09 179.86 16.78 o 0 8 24 458.63 538.62 31.16 o 2 8 24 822.30 801.38 24.77 o 4 8 24 73.93 82.41 11.14 o 1 9 24 509.67 464.58 26.34 o 3 9 24 507.15 469.84 20.28 o 0 10 24 67.17 77.15 16.38 o 2 10 24 169.26 197.61 19.47 o 2 0 25 126.37 127.65 12.40 o 4 0 25 22.34 23.14 7.76 o 6 0 25 617.48 566.30 40.32 o 1 1 25 3031.83 2966.28 40.16 o 3 1 25 124.58 112.70 8.07 o 5 1 25 102.58 108.81 9.92 o 0 2 25 0.71 13.39 5.81 o 2 2 25 702.78 696.69 16.28 o 4 2 25 259.03 245.88 12.75 o 6 2 25 27.55 48.51 9.05 o 1 3 25 1469.37 1408.53 21.35 o 3 3 25 712.90 661.76 18.25 o 5 3 25 745.61 727.12 21.12 o 0 4 25 5596.08 5339.47 89.48 o 2 4 25 1198.40 1163.88 25.70 o 4 4 25 123.37 123.02 10.22 o 6 4 25 64.79 54.07 8.87 o 1 5 25 700.50 711.73 18.27 o 3 5 25 247.87 284.66 14.60 o 5 5 25 52.64 67.77 8.97 o 0 6 25 268.86 282.56 18.01 o 2 6 25 20.33 21.43 6.12 o 4 6 25 23.51 22.30 7.50 o 1 7 25 1058.29 1030.88 26.11 o 3 7 25 811.22 732.01 23.14 o 0 8 25 107.89 116.61 17.99 o 2 8 25 344.59 309.63 16.77 o 4 8 25 51.46 59.07 10.40 o 1 9 25 290.10 293.53 18.72 o 3 9 25 149.64 166.61 13.88 o 0 10 25 5.52 7.69 21.34 o 2 10 25 75.23 129.50 18.76 o 0 0 26 599.79 598.24 36.55 o 2 0 26 17.74 12.65 6.53 o 6 0 26 3.96 1.30 11.43 o 1 1 26 956.92 1051.71 21.30 o 3 1 26 130.52 140.19 9.34 o 5 1 26 18.26 32.65 7.26 o 0 2 26 2001.47 1965.74 43.65 o 2 2 26 1033.96 1046.14 20.40 o 4 2 26 560.49 581.38 18.13 o 6 2 26 206.07 241.26 16.16 o 1 3 26 1006.99 971.15 17.56 o 3 3 26 555.16 571.19 17.20 o 5 3 26 212.79 197.66 16.46 o 0 4 26 895.41 826.62 27.67 o 2 4 26 197.33 185.63 10.80 o 4 4 26 144.82 137.25 10.81 o 1 5 26 476.46 457.68 16.75 o 3 5 26 925.33 893.63 22.32 o 5 5 26 315.74 329.63 15.03 o 0 6 26 1358.29 1305.98 46.78 o 2 6 26 149.20 124.79 10.87 o 4 6 26 159.35 168.35 13.65 o 1 7 26 98.37 95.18 10.31 o 3 7 26 402.94 434.27 19.15 o 0 8 26 141.41 131.64 18.95 o 2 8 26 86.30 68.39 17.55 o 4 8 26 512.07 501.33 25.00 o 1 9 26 111.11 105.30 13.02 o 3 9 26 53.98 69.28 10.35 o 0 10 26 40.93 45.77 14.94 o 2 10 26 26.55 40.54 10.63 o 2 0 27 658.07 611.96 27.32 o 4 0 27 2826.64 2595.74 58.15 o 6 0 27 32.66 48.98 14.52 o 1 1 27 202.76 199.27 10.31 o 3 1 27 193.53 201.87 12.43 o 5 1 27 143.23 131.99 12.44 o 0 2 27 2210.34 2300.73 48.90 o 2 2 27 494.67 467.36 13.74 o 4 2 27 122.01 139.12 10.73 o 6 2 27 69.82 95.30 11.46 o 1 3 27 2511.46 2528.99 37.71 o 3 3 27 2334.47 2213.22 36.81 o 5 3 27 85.54 95.51 9.93 o 0 4 27 3302.09 3133.86 62.28 o 2 4 27 1831.87 1724.83 30.90 o 4 4 27 98.67 107.97 9.94 o 1 5 27 841.75 813.49 22.49 o 3 5 27 152.20 152.15 10.99 o 5 5 27 56.98 60.38 8.09 o 0 6 27 421.58 385.59 26.37 o 2 6 27 865.57 816.78 23.59 o 4 6 27 100.74 107.08 11.42 o 1 7 27 36.83 40.88 8.05 o 3 7 27 65.41 81.12 10.19 o 0 8 27 16.15 29.81 27.32 o 2 8 27 69.66 75.14 10.36 o 1 9 27 9.38 -3.53 7.21 o 0 10 27 277.36 335.42 32.19 o 0 0 28 502.04 459.54 36.60 o 2 0 28 1830.46 1757.19 43.15 o 4 0 28 1545.12 1468.79 41.69 o 1 1 28 66.79 73.81 7.39 o 3 1 28 317.04 320.79 13.44 o 5 1 28 282.16 274.31 19.34 o 0 2 28 1403.41 1337.44 35.47 o 2 2 28 1246.80 1178.52 24.36 o 4 2 28 587.60 579.83 18.56 o 1 3 28 249.47 251.22 11.77 o 3 3 28 511.90 519.70 16.90 o 5 3 28 2.54 12.16 5.69 o 0 4 28 11.48 13.19 10.36 o 2 4 28 410.02 411.34 14.93 o 4 4 28 511.25 510.23 17.99 o 1 5 28 258.13 248.17 15.31 o 3 5 28 46.67 55.06 7.79 o 5 5 28 119.81 104.85 10.97 o 0 6 28 128.00 127.99 18.25 o 2 6 28 33.61 41.76 9.50 o 4 6 28 22.85 26.85 9.71 o 1 7 28 131.63 111.54 12.73 o 3 7 28 33.14 16.46 8.84 o 0 8 28 359.40 335.85 27.97 o 2 8 28 468.81 429.43 19.56 o 1 9 28 151.92 137.30 15.37 o 2 0 29 372.15 384.38 27.32 o 4 0 29 30.81 20.03 10.31 o 1 1 29 53.98 63.55 8.09 o 3 1 29 312.57 298.06 13.36 o 5 1 29 321.92 331.52 20.72 o 0 2 29 153.17 180.75 19.24 o 2 2 29 1173.33 1221.44 25.24 o 4 2 29 150.87 188.99 12.22 o 1 3 29 3155.68 2946.16 47.72 o 3 3 29 464.74 447.81 16.26 o 5 3 29 295.48 283.16 15.25 o 0 4 29 147.55 147.52 14.34 o 2 4 29 698.10 730.60 24.25 o 4 4 29 494.86 481.69 17.95 o 1 5 29 423.86 409.76 16.98 o 3 5 29 71.89 77.80 8.62 o 0 6 29 539.40 497.80 29.76 o 2 6 29 12.81 11.06 7.11 o 4 6 29 81.27 77.99 10.76 o 1 7 29 178.00 205.06 15.68 o 3 7 29 183.97 189.13 14.34 o 0 8 29 612.06 645.05 35.66 o 2 8 29 156.93 162.24 18.30 o 1 9 29 256.94 268.94 23.01 o 0 0 30 4615.41 4308.46 141.05 o 2 0 30 2300.35 2251.49 51.57 o 4 0 30 11.12 11.45 12.85 o 1 1 30 119.61 118.39 11.03 o 3 1 30 1152.33 1113.48 24.95 o 5 1 30 171.19 186.95 15.90 o 0 2 30 66.94 66.92 13.38 o 2 2 30 568.12 555.84 16.80 o 4 2 30 907.92 895.07 23.67 o 1 3 30 1501.32 1342.42 29.83 o 3 3 30 277.07 308.59 14.36 o 5 3 30 189.09 204.14 13.82 o 0 4 30 97.80 91.55 12.52 o 2 4 30 105.84 92.30 10.36 o 4 4 30 156.32 175.17 12.41 o 1 5 30 574.52 580.25 22.58 o 3 5 30 427.67 442.63 16.86 o 0 6 30 296.08 323.26 26.10 o 2 6 30 9.61 9.76 6.86 o 4 6 30 139.44 152.99 14.33 o 1 7 30 57.18 55.93 10.37 o 3 7 30 47.79 35.78 10.33 o 0 8 30 3.51 11.36 12.34 o 2 8 30 37.05 34.24 11.15 o 1 9 30 22.78 27.59 9.66 o 2 0 31 460.83 394.41 20.74 o 4 0 31 542.29 553.73 32.22 o 1 1 31 173.47 150.91 13.20 o 3 1 31 252.63 248.20 14.27 o 5 1 31 8.66 15.03 7.74 o 0 2 31 2520.61 2488.77 70.21 o 2 2 31 30.18 58.12 11.12 o 4 2 31 204.88 217.11 19.19 o 1 3 31 153.90 176.20 14.45 o 3 3 31 233.42 243.04 14.43 o 5 3 31 264.54 251.62 15.31 o 0 4 31 255.00 255.94 18.05 o 2 4 31 41.88 46.48 9.74 o 4 4 31 16.47 15.33 6.51 o 1 5 31 180.14 213.79 15.91 o 3 5 31 81.08 89.82 12.87 o 0 6 31 0.24 11.52 10.30 o 2 6 31 70.47 57.41 10.39 o 1 7 31 90.10 110.16 13.18 o 3 7 31 20.08 29.30 9.38 o 0 8 31 0.24 2.92 11.08 o 2 8 31 171.16 181.99 20.38 o 0 0 32 1938.30 1681.69 79.18 o 2 0 32 588.50 592.43 25.15 o 4 0 32 574.55 640.78 35.68 o 1 1 32 856.40 829.70 26.86 o 3 1 32 217.16 242.36 14.82 o 5 1 32 67.36 75.65 11.01 o 0 2 32 336.24 429.19 28.04 o 2 2 32 310.57 295.50 15.32 o 4 2 32 161.96 196.10 14.24 o 1 3 32 267.44 261.38 14.56 o 3 3 32 694.83 659.81 19.82 o 0 4 32 678.04 665.01 34.33 o 2 4 32 105.85 98.79 12.19 o 4 4 32 152.19 136.24 11.96 o 1 5 32 70.14 60.90 12.12 o 3 5 32 212.75 208.99 15.01 o 0 6 32 15.50 18.18 11.33 o 2 6 32 371.94 434.83 22.36 o 1 7 32 107.49 131.22 16.69 o 0 8 32 134.88 187.37 24.08 o 2 0 33 0.75 12.58 7.54 o 4 0 33 45.78 59.97 20.87 o 1 1 33 425.05 425.97 23.05 o 3 1 33 7.19 13.92 6.28 o 0 2 33 1498.08 1353.69 87.46 o 2 2 33 497.56 515.95 22.76 o 4 2 33 132.42 137.93 16.00 o 1 3 33 34.89 31.92 7.50 o 3 3 33 245.05 216.86 14.44 o 0 4 33 9.97 17.85 10.01 o 2 4 33 45.35 46.31 9.96 o 4 4 33 1.76 3.61 5.71 o 1 5 33 25.70 33.06 9.61 o 3 5 33 0.33 11.53 7.84 o 0 6 33 142.26 208.78 23.61 o 2 6 33 60.97 48.35 10.20 o 0 0 34 14.22 19.09 14.47 o 2 0 34 93.27 98.11 17.21 o 4 0 34 304.67 302.26 26.99 o 1 1 34 274.78 259.98 17.24 o 3 1 34 470.73 505.45 19.37 o 0 2 34 58.57 51.68 13.13 o 2 2 34 7.29 15.43 6.96 o 4 2 34 25.28 20.13 8.58 o 1 3 34 154.53 183.56 15.28 o 3 3 34 240.06 242.68 17.66 o 0 4 34 111.03 114.37 20.61 o 2 4 34 68.85 66.38 11.32 o 1 5 34 328.93 376.06 20.92 o 3 5 34 210.19 238.18 18.38 o 0 6 34 271.01 225.26 37.23 o 2 6 34 264.53 369.77 21.73 o 1 7 34 409.98 432.97 27.57 o 2 0 35 70.13 92.03 16.87 o 4 0 35 371.81 369.35 46.93 o 1 1 35 113.04 106.06 12.36 o 3 1 35 84.96 80.45 9.96 o 0 2 35 703.17 600.29 33.80 o 2 2 35 85.53 81.69 12.40 o 1 3 35 82.22 96.30 12.30 o 3 3 35 684.50 706.55 27.24 o 0 4 35 409.99 425.68 31.19 o 2 4 35 49.25 41.67 9.83 o 1 5 35 75.57 94.68 14.36 o 0 6 35 70.36 85.05 26.85 o 2 6 35 64.36 88.00 13.30 o 0 0 36 216.77 236.38 34.61 o 2 0 36 36.70 64.72 15.62 o 1 1 36 46.01 68.24 12.71 o 3 1 36 79.39 105.13 23.93 o 0 2 36 74.29 73.78 15.94 o 2 2 36 166.03 202.73 20.52 o 1 3 36 68.56 65.96 12.99 o 3 3 36 30.80 24.74 10.82 o 0 4 36 12.63 11.79 10.73 o 2 4 36 103.53 118.07 14.57 o 1 5 36 29.63 30.63 10.29 o 0 6 36 834.22 893.91 65.75 o 2 0 37 329.49 348.06 29.09 o 1 1 37 124.40 131.19 16.45 o 3 1 37 296.69 282.98 19.47 o 0 2 37 145.36 202.93 23.79 o 2 2 37 371.84 405.50 26.26 o 1 3 37 217.73 284.45 22.37 o 0 4 37 156.31 138.87 21.32 o 2 4 37 0.51 6.75 7.63 o 1 5 37 5.80 16.01 9.27 o 0 0 38 523.43 580.87 50.23 o 2 0 38 94.01 125.93 19.89 o 1 1 38 149.24 171.16 16.20 o 0 2 38 162.75 203.59 39.06 o 2 2 38 380.40 468.64 28.61 o 1 3 38 379.71 361.62 25.44 o 0 4 38 0.01 18.88 17.72 o 2 0 39 534.18 537.00 35.65 o 1 1 39 37.60 41.58 10.12 o 0 2 39 8.58 -9.58 14.37 o 1 3 39 60.08 76.46 14.38 o 0 0 40 43.56 35.34 18.14 o