#------------------------------------------------------------------------------ #$Date: 2016-04-03 04:13:44 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181152 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/31/2223141.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2223141_Fobs loop_ _publ_author_name 'Li, Zhi-Feng' 'Wang, Chun-Xiang' 'Wang, Ping' _publ_section_title ; Poly[diaqua-\m~2~-oxalato-di-\m~4~-succinato-diyttrium(III)] ; _journal_coeditor_code JJ2005 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1095 _journal_volume 65 _journal_year 2009 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 101.589 _cell_angle_beta 101.843 _cell_angle_gamma 101.492 _cell_length_a 6.6099 _cell_length_b 7.6892 _cell_length_c 8.0181 _exptl_crystal_F_000 262.00 _reflns_d_resolution_high 0.8038 _cod_data_source_file jj2005Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' tref in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 106.11 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 5450.27 5699.44 297.80 o 2 0 0 363.68 330.96 8.44 o 3 0 0 897.13 822.22 19.58 o 4 0 0 310.17 272.37 8.72 o 5 0 0 220.53 236.26 9.27 o 6 0 0 218.50 221.59 10.20 o 7 0 0 67.47 58.50 7.53 o -7 1 0 134.82 150.49 9.38 o -6 1 0 1505.56 1565.34 38.06 o -5 1 0 587.01 626.37 17.07 o -4 1 0 1255.47 1298.02 30.23 o -3 1 0 2819.65 2871.50 62.63 o -2 1 0 165.53 148.45 4.36 o -1 1 0 2010.17 2043.50 32.47 o 0 1 0 3234.05 3400.29 140.65 o 1 1 0 1537.86 1571.30 20.92 o 2 1 0 3165.31 3155.31 50.35 o 3 1 0 937.24 938.81 22.38 o 4 1 0 258.49 256.20 8.68 o 5 1 0 17.49 21.90 4.22 o 6 1 0 299.20 330.84 12.81 o 7 1 0 244.20 241.04 12.03 o -8 2 0 278.07 314.26 15.33 o -7 2 0 1175.21 1250.36 32.34 o -6 2 0 691.17 739.92 20.41 o -5 2 0 520.70 538.70 14.86 o -4 2 0 1877.96 1856.02 41.67 o -3 2 0 505.85 491.98 12.05 o -2 2 0 546.53 598.66 10.27 o -1 2 0 2455.70 2484.93 58.66 o 0 2 0 731.25 743.13 11.16 o 1 2 0 1605.29 1635.63 26.67 o 2 2 0 46.10 41.98 2.21 o 3 2 0 381.74 367.12 8.00 o 4 2 0 689.52 688.04 18.39 o 5 2 0 454.71 442.45 14.13 o 6 2 0 780.35 775.16 22.66 o 7 2 0 626.52 637.66 21.42 o -6 3 0 666.76 670.84 18.31 o -5 3 0 408.69 383.11 8.78 o -4 3 0 323.89 317.17 7.08 o -3 3 0 447.66 452.67 8.54 o -2 3 0 48.30 52.96 2.01 o -1 3 0 63.54 56.93 4.33 o 0 3 0 3298.27 3288.12 78.54 o 1 3 0 6995.39 6936.10 105.71 o 2 3 0 2838.39 2873.06 35.25 o 3 3 0 1161.71 1151.80 20.54 o 4 3 0 147.13 147.91 5.76 o 5 3 0 808.51 794.12 22.31 o 6 3 0 685.06 662.00 20.62 o -7 4 0 4.72 4.90 7.84 o -6 4 0 190.10 186.18 11.50 o -5 4 0 125.45 127.15 8.34 o -4 4 0 123.95 128.35 7.93 o -3 4 0 789.46 765.99 21.55 o -2 4 0 87.52 83.92 5.61 o -1 4 0 1744.58 1693.55 43.45 o 0 4 0 2932.20 3014.52 36.91 o 1 4 0 1052.40 1009.46 13.39 o 2 4 0 1548.67 1558.77 26.80 o 3 4 0 1614.85 1617.27 28.27 o 4 4 0 821.24 808.59 16.48 o 5 4 0 64.28 60.00 7.20 o 6 4 0 3.62 5.17 6.89 o -7 5 0 193.31 197.15 14.02 o -6 5 0 711.34 727.71 24.50 o -5 5 0 524.11 527.25 18.66 o -4 5 0 1558.19 1513.45 40.02 o -3 5 0 1283.60 1238.48 33.58 o -2 5 0 931.96 878.95 25.70 o -1 5 0 649.16 642.18 20.72 o 0 5 0 1161.90 1260.27 20.63 o 1 5 0 618.58 639.46 9.52 o 2 5 0 48.31 49.18 3.58 o 3 5 0 88.93 84.71 4.82 o 4 5 0 10.55 6.65 5.76 o 5 5 0 1.61 2.32 4.71 o -7 6 0 477.25 497.86 22.47 o -6 6 0 645.71 606.64 22.75 o -5 6 0 1298.28 1137.05 33.34 o -4 6 0 1531.44 1465.35 40.57 o -3 6 0 238.35 217.11 12.06 o -2 6 0 82.02 79.90 8.57 o -1 6 0 162.23 162.02 10.99 o 0 6 0 34.96 34.03 4.13 o 1 6 0 0.70 5.23 6.13 o 2 6 0 238.78 221.14 12.87 o 3 6 0 222.36 227.96 13.67 o 4 6 0 298.68 320.35 16.69 o -6 7 0 169.35 207.51 14.68 o -5 7 0 98.85 85.69 9.71 o -4 7 0 6.23 6.51 6.65 o -3 7 0 67.45 70.94 9.48 o -2 7 0 4.14 11.05 7.87 o -1 7 0 58.98 72.77 5.00 o 0 7 0 299.10 299.95 16.33 o 1 7 0 631.55 660.14 24.24 o 2 7 0 731.33 755.02 26.63 o 3 7 0 228.23 257.79 16.29 o -5 8 0 6.57 5.17 9.83 o -4 8 0 189.85 179.33 14.17 o -3 8 0 465.74 449.27 21.22 o -2 8 0 482.03 478.74 22.00 o -1 8 0 629.07 664.22 26.29 o 0 8 0 277.64 330.45 18.72 o 1 8 0 548.62 593.00 24.66 o 2 8 0 435.32 480.61 22.57 o -4 9 0 405.35 354.38 21.60 o -3 9 0 387.07 344.94 20.04 o -2 9 0 342.20 345.97 21.21 o -1 9 0 219.22 219.43 17.37 o 0 9 0 345.00 376.92 21.85 o 0 -9 1 11.13 9.96 9.99 o 1 -9 1 5.85 5.53 11.24 o 2 -9 1 45.67 60.33 12.67 o 3 -9 1 47.55 39.28 11.16 o 4 -9 1 134.54 128.66 13.84 o -2 -8 1 78.26 67.52 11.68 o -1 -8 1 24.16 28.05 10.33 o 0 -8 1 35.53 35.33 9.17 o 1 -8 1 187.15 197.33 14.80 o 2 -8 1 1012.10 972.49 33.09 o 3 -8 1 877.88 778.43 28.34 o 4 -8 1 419.57 412.89 19.88 o 5 -8 1 209.03 213.81 14.96 o -4 -7 1 36.24 43.44 10.68 o -3 -7 1 144.16 139.47 12.61 o -2 -7 1 404.59 438.00 19.51 o -1 -7 1 938.60 947.45 30.91 o 0 -7 1 1508.44 1585.21 45.21 o 1 -7 1 613.01 629.38 23.64 o 2 -7 1 729.12 672.48 24.40 o 3 -7 1 816.24 730.52 25.19 o 4 -7 1 885.15 801.83 26.90 o 5 -7 1 368.02 339.49 17.18 o 6 -7 1 79.49 88.73 10.50 o -4 -6 1 241.77 241.07 13.96 o -3 -6 1 494.90 467.20 18.49 o -2 -6 1 585.87 608.05 21.74 o -1 -6 1 577.02 621.78 21.91 o 0 -6 1 499.84 514.58 19.60 o 1 -6 1 1878.19 1886.21 50.77 o 2 -6 1 799.81 797.14 25.46 o 3 -6 1 448.75 448.25 17.13 o 4 -6 1 60.19 45.22 7.11 o 5 -6 1 14.40 20.49 6.95 o 6 -6 1 98.66 96.36 9.53 o 7 -6 1 6.66 13.84 9.72 o -5 -5 1 631.59 608.95 14.78 o -4 -5 1 1126.32 1068.47 31.98 o -3 -5 1 1422.67 1343.10 24.54 o -2 -5 1 442.30 427.25 9.65 o -1 -5 1 25.86 31.49 4.12 o 0 -5 1 67.84 90.21 7.71 o 1 -5 1 67.67 63.17 6.94 o 2 -5 1 0.83 2.20 3.88 o 3 -5 1 164.21 156.71 8.98 o 4 -5 1 475.42 493.56 16.71 o 5 -5 1 607.39 619.49 20.86 o 6 -5 1 145.82 176.01 11.60 o 7 -5 1 338.32 347.02 17.12 o -6 -4 1 441.64 438.62 16.81 o -5 -4 1 261.26 256.29 8.65 o -4 -4 1 245.55 234.16 7.37 o -3 -4 1 308.47 304.53 7.16 o -2 -4 1 122.37 134.39 4.34 o -1 -4 1 336.81 332.82 5.31 o 0 -4 1 78.51 76.61 2.98 o 1 -4 1 3343.87 3296.11 52.95 o 2 -4 1 2487.85 2455.79 39.92 o 3 -4 1 496.99 487.94 15.42 o 4 -4 1 1168.47 1128.32 19.93 o 5 -4 1 2217.90 2111.67 53.74 o 6 -4 1 847.11 814.30 25.57 o 7 -4 1 461.96 477.09 19.75 o -6 -3 1 7.64 9.43 5.85 o -5 -3 1 30.78 40.98 5.49 o -4 -3 1 6.56 31.86 18.63 o -3 -3 1 27.11 30.56 2.60 o -2 -3 1 739.86 727.38 11.36 o -1 -3 1 1622.36 1616.95 25.08 o 0 -3 1 571.94 560.08 10.27 o 1 -3 1 2041.02 1843.41 30.07 o 2 -3 1 4246.47 4340.81 68.80 o 3 -3 1 3484.32 3549.70 56.79 o 4 -3 1 2310.38 2282.48 37.64 o 5 -3 1 81.58 85.25 4.08 o 6 -3 1 50.82 57.22 5.64 o 7 -3 1 110.62 105.78 7.81 o -7 -2 1 68.82 67.28 8.32 o -6 -2 1 458.18 441.44 15.31 o -5 -2 1 749.69 747.70 20.62 o -4 -2 1 1013.58 1019.22 16.77 o -3 -2 1 2609.04 2492.52 41.43 o -2 -2 1 8847.86 8741.96 137.41 o -1 -2 1 116.47 101.93 2.23 o 0 -2 1 116.61 102.14 5.85 o 1 -2 1 640.99 624.67 10.77 o 2 -2 1 394.65 355.29 6.77 o 3 -2 1 1025.92 1007.11 23.30 o 4 -2 1 854.28 829.46 20.27 o 5 -2 1 3.87 4.59 3.11 o 6 -2 1 201.05 196.62 9.14 o 7 -2 1 81.73 82.78 7.56 o -7 -1 1 157.83 163.16 10.09 o -6 -1 1 524.40 554.80 17.25 o -5 -1 1 1978.04 1975.97 46.06 o -4 -1 1 1403.00 1421.93 28.00 o -3 -1 1 3643.81 3693.38 67.05 o -2 -1 1 4144.17 4020.31 63.69 o -1 -1 1 2513.75 2410.83 38.41 o 0 -1 1 829.98 878.00 21.29 o 1 -1 1 595.32 677.38 28.59 o 2 -1 1 846.41 986.97 22.48 o 3 -1 1 396.47 439.18 11.53 o 4 -1 1 517.93 576.79 15.26 o 5 -1 1 281.15 281.96 10.03 o 6 -1 1 755.99 791.09 21.92 o 7 -1 1 536.70 536.86 17.74 o -7 0 1 611.13 638.42 20.11 o -6 0 1 441.17 436.22 14.40 o -5 0 1 82.67 81.61 5.42 o -4 0 1 119.03 110.37 7.69 o -3 0 1 3837.04 4070.81 224.39 o -2 0 1 859.96 923.72 21.12 o -1 0 1 152.75 163.52 4.56 o 0 0 1 703.68 796.46 17.82 o 1 0 1 1572.01 1591.10 34.89 o 2 0 1 505.43 436.00 10.95 o 3 0 1 689.88 638.16 15.93 o 4 0 1 1608.14 1598.94 37.17 o 5 0 1 2113.40 2185.27 50.62 o 6 0 1 365.41 387.21 13.82 o 7 0 1 110.10 115.46 9.18 o -8 1 1 215.59 231.21 13.28 o -7 1 1 80.75 86.11 7.74 o -6 1 1 83.37 87.96 5.95 o -5 1 1 385.64 405.19 12.27 o -4 1 1 505.05 555.89 42.11 o -3 1 1 587.75 618.42 26.18 o -2 1 1 1426.16 1435.22 31.60 o -1 1 1 5056.52 5011.87 79.56 o 0 1 1 388.13 399.95 5.29 o 1 1 1 809.93 797.82 10.27 o 2 1 1 2669.79 2462.64 39.68 o 3 1 1 3143.45 3170.83 69.87 o 4 1 1 928.38 887.49 22.51 o 5 1 1 945.59 944.26 24.79 o 6 1 1 175.86 176.91 9.88 o 7 1 1 4.17 4.43 6.58 o -8 2 1 27.59 19.77 7.13 o -7 2 1 100.21 106.38 7.82 o -6 2 1 74.61 77.28 6.04 o -5 2 1 260.24 290.82 9.54 o -4 2 1 955.42 978.49 23.06 o -3 2 1 4075.15 3958.26 154.23 o -2 2 1 7615.63 7500.60 117.87 o -1 2 1 4869.73 4862.65 104.73 o 0 2 1 3566.51 3448.07 57.68 o 1 2 1 1607.92 1596.60 19.87 o 2 2 1 1658.06 1677.59 21.16 o 3 2 1 92.00 83.44 3.71 o 4 2 1 339.92 353.96 11.67 o 5 2 1 35.36 33.06 5.32 o 6 2 1 32.91 45.29 6.69 o -6 3 1 1407.92 1525.85 36.25 o -5 3 1 1534.17 1573.22 27.10 o -4 3 1 536.01 514.09 9.98 o -3 3 1 205.85 190.51 4.41 o -2 3 1 4210.83 4469.50 70.57 o -1 3 1 3917.21 3957.63 93.70 o 0 3 1 51.40 49.50 1.78 o 1 3 1 3.53 3.77 1.19 o 2 3 1 18.09 21.53 2.26 o 3 3 1 24.61 26.90 5.30 o 4 3 1 14.39 14.14 3.03 o 5 3 1 143.84 155.01 9.32 o 6 3 1 806.63 817.59 24.55 o -7 4 1 524.04 589.60 22.86 o -6 4 1 221.41 235.35 12.80 o -5 4 1 341.91 352.87 13.99 o -4 4 1 319.71 329.62 12.35 o -3 4 1 336.09 350.34 12.23 o -2 4 1 115.01 112.01 7.39 o -1 4 1 75.09 70.86 6.13 o 0 4 1 602.57 615.79 9.40 o 1 4 1 28.20 30.11 1.98 o 2 4 1 888.65 886.18 12.58 o 3 4 1 911.76 912.70 17.54 o 4 4 1 856.75 838.08 17.10 o 5 4 1 743.73 710.61 21.54 o -7 5 1 149.95 178.77 12.92 o -6 5 1 79.72 90.73 9.53 o -5 5 1 28.66 31.28 6.52 o -4 5 1 146.89 144.28 9.14 o -3 5 1 44.93 40.89 5.41 o -2 5 1 218.84 227.52 11.38 o -1 5 1 2251.63 2306.77 63.13 o 0 5 1 1319.09 1396.51 22.79 o 1 5 1 716.76 794.51 14.36 o 2 5 1 1233.61 1223.11 39.74 o 3 5 1 567.92 569.18 12.82 o 4 5 1 280.17 271.73 9.36 o 5 5 1 750.89 784.86 23.99 o -7 6 1 11.38 10.10 9.93 o -6 6 1 34.06 40.49 8.11 o -5 6 1 599.83 617.03 22.03 o -4 6 1 1069.07 957.72 29.22 o -3 6 1 472.37 411.27 16.63 o -2 6 1 251.20 248.80 13.56 o -1 6 1 1292.21 1350.28 27.18 o 0 6 1 950.50 996.08 17.88 o 1 6 1 991.77 1019.69 30.64 o 2 6 1 318.06 318.47 15.06 o 3 6 1 137.58 125.28 10.70 o 4 6 1 187.15 193.80 13.52 o -6 7 1 266.27 299.14 18.28 o -5 7 1 448.45 451.99 20.14 o -4 7 1 434.56 404.08 18.31 o -3 7 1 680.31 647.19 23.87 o -2 7 1 1928.10 1970.20 32.41 o -1 7 1 504.40 535.13 12.31 o 0 7 1 7.92 6.64 7.90 o 1 7 1 3.34 5.97 8.03 o 2 7 1 7.79 8.79 8.08 o 3 7 1 19.64 16.30 9.24 o -5 8 1 295.09 258.24 17.72 o -4 8 1 107.09 93.55 12.50 o -3 8 1 15.98 15.56 10.11 o -2 8 1 89.63 87.32 6.18 o -1 8 1 37.74 34.66 10.53 o 0 8 1 1.83 11.71 9.41 o 1 8 1 138.99 142.57 13.78 o -3 9 1 26.25 26.02 6.25 o -2 9 1 114.04 132.61 15.61 o -1 9 1 121.55 145.47 15.34 o -1 -9 2 224.36 247.38 16.95 o 0 -9 2 238.93 248.76 17.94 o 1 -9 2 576.58 598.30 26.42 o 2 -9 2 536.77 539.81 25.13 o 3 -9 2 201.50 204.11 16.77 o 4 -9 2 119.77 127.95 14.60 o -2 -8 2 548.65 546.13 23.92 o -1 -8 2 750.15 750.94 28.14 o 0 -8 2 287.64 303.79 17.83 o 1 -8 2 375.51 330.95 18.32 o 2 -8 2 15.85 16.32 9.53 o 3 -8 2 94.10 92.69 11.60 o 4 -8 2 2.33 -1.77 8.66 o 5 -8 2 3.97 2.04 9.49 o -4 -7 2 152.32 143.44 12.66 o -3 -7 2 82.52 102.67 10.55 o -2 -7 2 164.84 157.47 11.82 o -1 -7 2 30.92 37.05 8.72 o 0 -7 2 26.92 33.51 8.49 o 1 -7 2 2.51 3.49 7.51 o 2 -7 2 174.92 183.96 12.42 o 3 -7 2 398.46 377.95 17.05 o 4 -7 2 343.52 342.36 16.44 o 5 -7 2 808.08 720.69 25.19 o 6 -7 2 253.39 246.36 15.93 o -5 -6 2 8.25 3.61 5.62 o -4 -6 2 29.03 21.42 4.66 o -3 -6 2 27.87 32.11 9.70 o -2 -6 2 41.97 42.75 7.86 o -1 -6 2 893.40 905.54 28.41 o 0 -6 2 242.74 283.33 14.40 o 1 -6 2 544.08 520.88 19.24 o 2 -6 2 2025.78 1907.10 50.63 o 3 -6 2 1168.66 1044.83 30.54 o 4 -6 2 670.95 616.86 20.83 o 5 -6 2 553.66 559.76 20.27 o 6 -6 2 260.06 253.32 14.07 o -5 -5 2 4.52 4.81 4.72 o -4 -5 2 1024.83 955.50 17.25 o -3 -5 2 1323.94 1319.86 21.68 o -2 -5 2 1495.31 1491.66 26.47 o -1 -5 2 1061.77 1052.21 23.69 o 0 -5 2 1414.48 1411.53 24.61 o 1 -5 2 2424.74 2410.65 61.12 o 2 -5 2 1881.50 1733.09 45.04 o 3 -5 2 206.15 190.54 9.50 o 4 -5 2 466.60 456.06 16.34 o 5 -5 2 210.05 220.76 12.23 o 6 -5 2 281.79 305.96 15.31 o 7 -5 2 19.57 17.61 7.98 o -6 -4 2 295.48 284.30 13.39 o -5 -4 2 535.64 487.55 12.03 o -4 -4 2 385.14 389.35 9.02 o -3 -4 2 194.29 194.66 6.88 o -2 -4 2 2389.96 2367.26 39.53 o -1 -4 2 2220.79 2226.08 37.01 o 0 -4 2 1190.08 1180.20 20.60 o 1 -4 2 1634.88 1601.04 38.61 o 2 -4 2 126.87 122.71 4.39 o 3 -4 2 13.69 17.62 2.47 o 4 -4 2 30.32 32.05 3.16 o 5 -4 2 103.66 108.08 6.70 o 6 -4 2 205.19 183.95 11.74 o 7 -4 2 133.74 133.76 11.31 o -7 -3 2 404.29 377.97 16.08 o -6 -3 2 445.37 434.38 15.68 o -5 -3 2 1486.91 1373.37 22.86 o -4 -3 2 589.76 578.02 11.14 o -3 -3 2 293.78 276.59 7.02 o -2 -3 2 10.90 12.48 2.01 o -1 -3 2 8.64 13.12 1.77 o 0 -3 2 17.22 16.44 1.92 o 1 -3 2 2.16 4.80 1.56 o 2 -3 2 735.23 771.40 13.89 o 3 -3 2 1005.35 1027.81 18.10 o 4 -3 2 2113.16 2090.20 83.23 o 5 -3 2 536.86 543.11 11.66 o 6 -3 2 232.88 219.75 7.52 o 7 -3 2 744.34 714.11 17.05 o -7 -2 2 109.84 112.89 9.25 o -6 -2 2 420.47 392.66 14.19 o -5 -2 2 713.22 721.41 18.64 o -4 -2 2 229.89 230.15 6.06 o -3 -2 2 55.53 54.85 3.08 o -2 -2 2 2312.27 2253.74 36.86 o -1 -2 2 2290.51 2253.05 55.85 o 0 -2 2 34.92 50.12 4.94 o 1 -2 2 1314.96 1404.05 64.69 o 2 -2 2 2090.16 2275.10 98.52 o 3 -2 2 4077.40 4636.97 100.71 o 4 -2 2 1895.31 2073.69 47.07 o 5 -2 2 967.51 1020.14 25.70 o 6 -2 2 916.45 956.42 25.47 o 7 -2 2 627.46 624.09 19.96 o -7 -1 2 7.33 4.90 5.88 o -6 -1 2 11.19 3.29 4.47 o -5 -1 2 188.07 169.75 10.90 o -4 -1 2 210.85 194.05 7.64 o -3 -1 2 532.94 510.16 9.95 o -2 -1 2 377.27 329.78 4.70 o -1 -1 2 2673.49 2691.10 52.03 o 0 -1 2 11258.90 10770.55 302.87 o 1 -1 2 5856.94 5989.03 98.16 o 2 -1 2 193.36 185.70 6.26 o 3 -1 2 1203.38 1282.37 29.81 o 4 -1 2 332.29 349.97 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2 8 532.09 524.00 16.02 o -3 2 8 67.91 81.22 7.16 o -2 2 8 422.90 413.30 10.97 o -1 2 8 92.49 91.15 6.14 o 0 2 8 6.87 8.98 5.02 o 1 2 8 65.36 57.65 6.22 o -5 3 8 157.98 147.34 9.61 o -4 3 8 9.52 22.98 6.61 o -3 3 8 63.57 78.84 8.30 o -2 3 8 118.68 98.86 8.99 o -1 3 8 30.34 34.82 7.66 o 0 3 8 233.50 208.22 12.00 o -3 4 8 43.92 48.29 8.33 o -2 4 8 197.58 184.29 11.67 o -2 -5 9 133.76 148.51 11.81 o -1 -5 9 147.38 146.98 11.42 o 0 -5 9 389.38 360.39 17.07 o 1 -5 9 187.10 178.01 12.82 o -3 -4 9 286.57 272.31 14.52 o -2 -4 9 2.89 -1.10 7.46 o -1 -4 9 1.47 2.54 7.03 o 0 -4 9 80.19 79.89 9.72 o 1 -4 9 111.78 107.99 11.07 o -4 -3 9 26.01 28.27 8.73 o -3 -3 9 5.28 7.38 6.70 o -2 -3 9 109.96 120.94 10.40 o -1 -3 9 95.04 100.56 9.22 o 0 -3 9 268.06 256.73 14.29 o 1 -3 9 412.87 402.18 18.16 o -4 -2 9 128.18 123.96 11.41 o -3 -2 9 865.42 847.23 26.66 o -2 -2 9 331.97 337.07 15.62 o -1 -2 9 317.15 295.44 14.12 o 0 -2 9 629.33 587.69 21.37 o 1 -2 9 551.36 595.16 21.73 o -4 -1 9 598.87 642.76 22.87 o 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