#------------------------------------------------------------------------------ #$Date: 2009-10-12 18:56:40 +0300 (Mon, 12 Oct 2009) $ #$Revision: 830 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2223200.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2223200_Fobs loop_ _publ_author_name 'Shang, Shao-Ming' 'Ren, Chun-Xia' 'Wang, Xin' 'Lu, Lu-De' 'Yang, Xu-Jie' _publ_section_title ; Bis[2,6-bis(4,5-dihydro-1H-imidazol-2-yl)pyridine]manganese(II) bis(perchlorate) acetonitrile solvate ; _journal_coeditor_code TK2501 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1023 _journal_page_last m1024 _journal_volume 65 _journal_year 2009 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 123.893 _cell_angle_gamma 90.000 _cell_length_a 20.5208 _cell_length_b 12.7323 _cell_length_c 14.6023 _exptl_crystal_F_000 1492.00 _reflns_d_resolution_high 0.8377 _[local]_cod_data_source_file tk2501Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 5 in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 518.12 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 7847.30 7176.03 121.17 o 4 0 0 5099.78 5738.57 132.72 o 6 0 0 41841.68 39625.07 417.30 o 8 0 0 2191.54 2414.88 206.27 o 10 0 0 11895.00 11932.47 223.25 o 12 0 0 12376.20 12735.58 254.06 o 14 0 0 161.24 47.93 91.11 o 16 0 0 19.64 -7.37 101.20 o 18 0 0 17.19 76.31 143.28 o 20 0 0 22.85 -4.88 271.10 o 1 1 0 24616.33 23055.09 177.71 o 3 1 0 37570.20 39568.37 266.72 o 5 1 0 7056.53 7592.62 92.23 o 7 1 0 107.47 84.08 30.45 o 9 1 0 11977.32 11572.81 150.06 o 11 1 0 2516.99 2560.69 121.69 o 13 1 0 688.30 677.75 72.41 o 15 1 0 428.03 460.71 79.00 o 17 1 0 0.74 -6.69 86.75 o 19 1 0 54.70 121.67 136.33 o 0 2 0 31907.60 34390.21 438.48 o 2 2 0 3091.88 3835.72 53.89 o 4 2 0 3.48 7.45 19.37 o 6 2 0 3430.23 3132.89 98.38 o 8 2 0 763.59 774.75 66.24 o 10 2 0 1917.65 2074.53 106.75 o 12 2 0 2261.85 2461.15 92.13 o 14 2 0 245.91 250.44 69.02 o 16 2 0 448.65 539.38 90.77 o 18 2 0 379.98 458.73 128.47 o 20 2 0 0.82 -7.13 147.75 o 1 3 0 17017.45 17653.19 219.37 o 3 3 0 6252.94 6416.36 108.01 o 5 3 0 735.50 875.84 41.47 o 7 3 0 1135.73 1176.51 61.62 o 9 3 0 2610.54 2493.41 103.09 o 11 3 0 546.80 503.35 59.92 o 13 3 0 3.41 13.46 63.12 o 15 3 0 999.99 1186.39 97.83 o 17 3 0 195.86 58.56 112.73 o 19 3 0 23.92 29.95 135.49 o 0 4 0 7627.21 8248.16 198.44 o 2 4 0 172.06 240.55 39.93 o 4 4 0 269.83 192.09 32.59 o 6 4 0 256.91 202.86 36.20 o 8 4 0 67.96 61.17 39.96 o 10 4 0 38.40 41.86 50.85 o 12 4 0 1030.57 909.43 76.15 o 14 4 0 29.88 110.15 74.56 o 16 4 0 143.28 140.17 107.86 o 18 4 0 88.19 49.45 127.61 o 1 5 0 116.74 39.66 38.93 o 3 5 0 2799.84 2739.04 150.15 o 5 5 0 3834.06 4076.14 132.84 o 7 5 0 568.66 510.61 52.95 o 9 5 0 141.01 156.03 50.87 o 11 5 0 429.14 442.00 67.32 o 13 5 0 0.80 4.40 70.24 o 15 5 0 7.59 -14.34 90.25 o 17 5 0 21.56 6.99 112.29 o 19 5 0 5.09 12.26 141.02 o 0 6 0 801.62 734.73 94.47 o 2 6 0 3203.91 3281.18 112.46 o 4 6 0 1568.32 1525.27 78.60 o 6 6 0 1356.62 1402.81 108.68 o 8 6 0 838.27 804.06 66.28 o 10 6 0 32.19 26.54 58.80 o 12 6 0 1260.46 1192.21 78.37 o 14 6 0 878.07 878.82 98.25 o 16 6 0 1.46 -20.36 111.52 o 18 6 0 28.48 -27.45 137.61 o 1 7 0 6167.48 6733.08 196.39 o 3 7 0 2819.15 2968.27 119.07 o 5 7 0 1214.42 1035.71 92.54 o 7 7 0 25.08 6.82 60.41 o 9 7 0 62.27 50.68 61.34 o 11 7 0 4041.04 4154.67 191.68 o 13 7 0 875.26 962.69 97.98 o 15 7 0 2.98 -8.57 103.75 o 17 7 0 130.71 113.89 122.47 o 0 8 0 5194.46 5363.40 232.59 o 2 8 0 3180.06 3346.34 133.79 o 4 8 0 862.97 859.57 105.12 o 6 8 0 20.01 46.77 69.61 o 8 8 0 30.75 37.01 73.12 o 10 8 0 760.03 838.28 89.31 o 12 8 0 571.54 491.78 108.11 o 14 8 0 170.31 100.13 118.17 o 16 8 0 70.19 55.18 130.96 o 1 9 0 548.21 473.32 89.75 o 3 9 0 5.53 6.60 77.07 o 5 9 0 474.84 513.60 85.54 o 7 9 0 23.98 7.39 77.68 o 9 9 0 162.06 71.31 88.46 o 11 9 0 486.69 599.85 108.64 o 13 9 0 65.11 37.83 118.57 o 15 9 0 201.35 85.33 131.44 o 0 10 0 157.02 90.88 120.66 o 2 10 0 387.30 423.01 95.62 o 4 10 0 568.32 590.90 97.32 o 6 10 0 101.53 119.61 90.39 o 8 10 0 389.32 391.23 100.29 o 10 10 0 311.85 246.59 106.45 o 12 10 0 271.91 227.65 159.72 o 14 10 0 274.10 226.21 173.87 o 1 11 0 271.33 314.33 106.13 o 3 11 0 1.88 -7.43 103.92 o 5 11 0 105.51 197.97 98.44 o 7 11 0 59.30 16.10 99.03 o 9 11 0 142.44 188.48 112.71 o 11 11 0 171.69 63.64 157.79 o 13 11 0 97.60 80.53 176.55 o 0 12 0 455.62 640.77 174.31 o 2 12 0 49.62 63.85 119.35 o 4 12 0 7.84 -21.16 110.50 o 6 12 0 42.64 43.72 113.79 o 8 12 0 77.86 47.67 123.56 o 10 12 0 8.22 -21.17 175.64 o 12 12 0 16.55 42.13 173.30 o 1 13 0 10.07 -5.51 128.79 o 3 13 0 272.31 212.27 123.35 o 5 13 0 0.06 -10.24 130.08 o 7 13 0 12.04 2.13 130.14 o 9 13 0 46.53 15.67 177.33 o 0 14 0 1.59 35.17 192.80 o 2 14 0 39.84 9.03 151.88 o 4 14 0 12.88 -8.10 137.37 o 6 14 0 0.47 -17.41 146.88 o 1 15 0 7.29 -0.19 172.68 o 3 15 0 0.55 -16.60 145.53 o -21 1 1 26.95 66.60 150.07 o -19 1 1 0.18 10.32 97.99 o -17 1 1 176.13 117.18 86.69 o -15 1 1 0.79 -5.62 66.09 o -13 1 1 513.48 456.74 61.42 o -11 1 1 75.70 48.90 45.49 o -9 1 1 202.75 170.91 37.65 o -7 1 1 406.75 382.60 33.87 o -5 1 1 2070.50 2017.30 182.40 o -3 1 1 94.52 96.96 19.88 o -1 1 1 15271.29 15270.22 211.28 o 1 1 1 8807.67 8531.09 185.09 o 3 1 1 5429.63 5296.37 117.32 o 5 1 1 1130.42 1038.78 71.10 o 7 1 1 146.21 163.19 35.10 o 9 1 1 1359.21 1366.05 64.66 o 11 1 1 2370.90 2393.55 87.80 o 13 1 1 158.72 74.46 66.19 o 15 1 1 26.18 26.06 75.86 o 17 1 1 15.79 23.63 115.08 o 19 1 1 11.24 14.46 218.22 o -20 2 1 14.07 -11.19 139.75 o -18 2 1 90.75 131.68 95.10 o -16 2 1 60.02 56.64 78.36 o -14 2 1 321.47 244.76 69.71 o -12 2 1 1875.14 2386.82 90.21 o -10 2 1 3355.22 3357.33 111.85 o -8 2 1 53.56 76.03 34.48 o -6 2 1 5571.18 5455.05 117.24 o -4 2 1 78515.24 74138.98 604.56 o -2 2 1 252.57 260.63 25.42 o 0 2 1 11975.99 12103.29 132.16 o 2 2 1 22575.84 22508.26 212.21 o 4 2 1 436.87 462.68 24.45 o 6 2 1 4773.91 4423.68 55.51 o 8 2 1 2344.39 2543.88 77.00 o 10 2 1 930.04 1049.72 89.78 o 12 2 1 2050.49 2031.44 89.50 o 14 2 1 8.31 -8.53 70.00 o 16 2 1 6.84 8.95 104.90 o 18 2 1 18.38 8.34 130.38 o -19 3 1 147.10 101.87 129.27 o -17 3 1 1403.52 1453.29 111.08 o -15 3 1 1735.98 1998.26 116.61 o -13 3 1 950.74 990.74 98.94 o -11 3 1 678.86 596.35 61.79 o -9 3 1 4887.40 5241.90 124.28 o -7 3 1 1422.64 1558.93 138.99 o -5 3 1 22833.04 22091.62 471.41 o -3 3 1 52022.85 51125.89 780.04 o -1 3 1 2275.10 2250.54 64.24 o 1 3 1 23.94 6.95 18.72 o 3 3 1 14306.26 15050.51 146.66 o 5 3 1 4485.14 4248.55 115.78 o 7 3 1 801.71 836.63 50.65 o 9 3 1 998.87 993.91 61.11 o 11 3 1 27.31 78.53 56.85 o 13 3 1 9.21 6.71 65.98 o 15 3 1 93.45 85.43 95.56 o 17 3 1 133.05 101.27 110.17 o 19 3 1 21.75 21.37 221.75 o -20 4 1 36.17 -8.55 154.92 o -18 4 1 423.19 499.75 111.03 o -16 4 1 4531.46 4734.29 150.07 o -14 4 1 893.23 926.30 86.84 o -12 4 1 309.30 418.84 66.29 o -10 4 1 1917.86 1773.14 90.52 o -8 4 1 590.73 587.17 49.35 o -6 4 1 26800.38 25416.38 936.07 o -4 4 1 15552.63 15281.69 268.04 o -2 4 1 6177.08 6105.32 117.97 o 0 4 1 9699.66 9269.47 148.55 o 2 4 1 1819.71 1749.77 53.20 o 4 4 1 428.35 340.63 37.80 o 6 4 1 8911.82 9415.85 183.83 o 8 4 1 2830.37 2808.88 114.35 o 10 4 1 887.33 985.96 76.01 o 12 4 1 65.87 66.01 63.43 o 14 4 1 249.70 387.58 98.43 o 16 4 1 137.15 63.70 110.18 o 18 4 1 125.51 213.89 138.82 o -19 5 1 139.50 196.16 149.02 o -17 5 1 278.17 261.53 97.54 o -15 5 1 1270.60 1262.48 101.12 o -13 5 1 585.14 701.25 79.44 o -11 5 1 303.50 306.39 60.05 o -9 5 1 2206.46 2203.95 79.81 o -7 5 1 10412.40 10690.86 225.03 o -5 5 1 3632.74 3480.12 95.64 o -3 5 1 1295.31 1364.01 72.25 o -1 5 1 8304.15 7590.78 148.64 o 1 5 1 126.73 129.13 44.69 o 3 5 1 9355.46 9584.56 225.22 o 5 5 1 7501.19 7373.62 127.44 o 7 5 1 397.91 373.23 59.55 o 9 5 1 684.09 705.97 84.56 o 11 5 1 731.50 816.86 77.73 o 13 5 1 1113.77 1050.73 110.04 o 15 5 1 210.02 311.30 107.32 o 17 5 1 86.07 40.95 123.84 o -18 6 1 33.58 -14.05 128.40 o -16 6 1 111.45 124.89 94.86 o -14 6 1 41.40 10.25 73.17 o -12 6 1 3.17 8.89 64.23 o -10 6 1 508.54 601.37 67.13 o -8 6 1 450.71 535.38 60.43 o -6 6 1 1499.78 1591.32 175.88 o -4 6 1 723.07 730.70 74.00 o -2 6 1 347.22 366.36 57.42 o 0 6 1 4527.35 3976.91 269.81 o 2 6 1 3098.95 3011.05 95.72 o 4 6 1 291.85 325.20 48.28 o 6 6 1 3200.79 3236.57 136.84 o 8 6 1 260.50 246.71 59.76 o 10 6 1 597.43 549.92 74.96 o 12 6 1 6375.90 6788.65 194.86 o 14 6 1 167.80 148.67 107.01 o 16 6 1 6.07 44.84 124.00 o -17 7 1 5.68 -5.00 103.16 o -15 7 1 17.21 0.88 71.38 o -13 7 1 1.01 8.05 75.90 o -11 7 1 530.19 516.81 74.49 o -9 7 1 621.21 612.09 104.76 o -7 7 1 1824.18 1700.94 91.96 o -5 7 1 133.02 66.54 58.14 o -3 7 1 14.38 25.26 61.36 o -1 7 1 1567.91 1525.28 96.84 o 1 7 1 231.14 368.90 72.14 o 3 7 1 5634.36 5815.75 145.64 o 5 7 1 752.02 671.20 73.91 o 7 7 1 249.06 260.85 61.74 o 9 7 1 3279.17 3611.08 120.14 o 11 7 1 2205.42 2161.10 169.12 o 13 7 1 101.24 59.44 100.53 o 15 7 1 287.88 249.90 119.39 o 17 7 1 50.42 4.87 142.05 o -18 8 1 7.83 -24.24 137.44 o -16 8 1 71.37 78.20 127.36 o -14 8 1 0.65 11.13 84.42 o -12 8 1 20.22 -2.01 74.32 o -10 8 1 87.41 71.45 76.37 o -8 8 1 52.99 91.18 75.77 o -6 8 1 453.38 445.08 76.93 o -4 8 1 408.15 409.56 82.09 o -2 8 1 5084.37 5128.81 164.53 o 0 8 1 1466.98 1300.26 164.81 o 2 8 1 1868.33 1637.42 105.66 o 4 8 1 170.29 102.91 66.49 o 6 8 1 283.04 449.01 79.71 o 8 8 1 101.00 33.12 68.15 o 10 8 1 3.97 0.00 94.00 o 12 8 1 109.20 85.56 107.73 o 14 8 1 30.67 6.99 123.21 o 16 8 1 8.80 17.87 134.34 o -17 9 1 0.52 -12.25 151.41 o -15 9 1 5.14 -8.57 127.61 o -13 9 1 304.91 228.79 105.94 o -11 9 1 310.14 249.62 95.92 o -9 9 1 158.09 63.79 81.98 o -7 9 1 322.88 316.32 83.08 o -5 9 1 721.65 844.55 97.61 o -3 9 1 260.62 124.35 78.33 o -1 9 1 570.27 484.46 85.41 o 1 9 1 1152.25 1149.64 146.59 o 3 9 1 2578.48 2569.37 118.95 o 5 9 1 74.29 34.53 75.87 o 7 9 1 1384.48 1346.12 235.23 o 9 9 1 7.93 1.02 90.88 o 11 9 1 13.21 11.13 106.69 o 13 9 1 107.94 56.92 125.84 o 15 9 1 21.96 47.42 142.25 o -16 10 1 0.26 23.62 203.32 o -14 10 1 30.57 70.60 188.43 o -12 10 1 21.55 -15.70 101.04 o -10 10 1 40.56 20.13 97.16 o -8 10 1 101.89 120.20 88.45 o -6 10 1 54.11 -2.05 82.90 o -4 10 1 81.87 62.70 96.14 o -2 10 1 2295.03 2212.03 140.20 o 0 10 1 38.49 40.82 88.77 o 2 10 1 24.58 21.51 88.10 o 4 10 1 157.36 175.59 90.20 o 6 10 1 65.31 41.49 88.91 o 8 10 1 563.89 506.18 104.79 o 10 10 1 252.18 230.97 157.56 o 12 10 1 19.54 0.70 155.30 o 14 10 1 24.28 3.18 142.97 o -13 11 1 1.30 42.87 201.01 o -11 11 1 187.91 117.83 118.03 o -9 11 1 43.01 7.13 104.34 o -7 11 1 250.60 230.10 97.03 o -5 11 1 380.32 334.77 103.08 o -3 11 1 94.74 -2.62 106.86 o -1 11 1 60.45 36.38 103.38 o 1 11 1 917.48 1144.32 126.88 o 3 11 1 117.95 4.93 92.23 o 5 11 1 1.88 -7.34 100.71 o 7 11 1 660.47 747.37 119.03 o 9 11 1 2.82 8.99 157.94 o 11 11 1 123.77 171.92 179.61 o 13 11 1 77.42 14.95 179.93 o -12 12 1 19.95 26.19 212.56 o -10 12 1 47.89 32.20 123.92 o -8 12 1 240.90 285.69 125.93 o -6 12 1 3.43 -8.96 109.19 o -4 12 1 38.61 2.43 118.81 o -2 12 1 510.90 637.33 133.76 o 0 12 1 112.50 104.95 118.43 o 2 12 1 35.43 0.46 104.39 o 4 12 1 315.48 360.42 120.44 o 6 12 1 133.20 126.45 117.98 o 8 12 1 12.79 22.14 162.86 o 10 12 1 224.27 242.43 183.55 o -11 13 1 61.55 150.95 233.62 o -9 13 1 40.02 58.62 132.77 o -7 13 1 38.49 75.26 125.55 o -5 13 1 395.34 584.72 144.61 o -3 13 1 30.95 37.49 130.28 o -1 13 1 29.27 -10.67 131.21 o 1 13 1 305.37 353.97 130.45 o 3 13 1 10.96 22.56 119.74 o 5 13 1 217.92 96.34 129.83 o 7 13 1 230.93 156.57 183.81 o 9 13 1 28.01 -22.47 190.67 o -8 14 1 122.36 141.26 154.91 o -6 14 1 91.38 17.66 151.09 o -4 14 1 222.38 124.18 135.01 o -2 14 1 274.78 179.34 148.89 o 0 14 1 0.56 65.30 151.74 o 2 14 1 47.17 54.97 140.69 o 4 14 1 300.77 278.98 145.54 o 6 14 1 142.02 94.40 208.64 o -3 15 1 152.15 163.75 180.35 o -1 15 1 57.27 51.31 173.53 o 1 15 1 34.01 43.38 160.53 o -20 0 2 398.56 418.52 162.84 o -18 0 2 1.73 -31.97 112.23 o -14 0 2 1686.90 2259.37 131.48 o -12 0 2 1505.01 1628.29 103.47 o -10 0 2 6443.75 5497.51 572.10 o -6 0 2 2684.86 3067.37 72.59 o -4 0 2 41377.07 42251.01 620.71 o 2 0 2 52821.82 51653.13 475.84 o 4 0 2 1427.34 950.85 128.87 o 6 0 2 457.61 522.76 110.13 o 8 0 2 7766.55 6681.69 156.66 o 10 0 2 142.84 89.50 72.98 o 12 0 2 1357.18 1162.30 113.65 o 14 0 2 498.72 613.96 118.24 o 16 0 2 16.47 -2.82 259.54 o 18 0 2 122.60 35.68 310.63 o -21 1 2 197.99 153.58 132.35 o -19 1 2 455.70 577.71 105.04 o -17 1 2 121.82 80.05 78.79 o -15 1 2 411.85 224.82 65.97 o -13 1 2 5507.72 5523.67 121.54 o -11 1 2 338.06 244.63 61.18 o -9 1 2 730.86 729.64 83.41 o -7 1 2 5495.09 5420.87 101.85 o -5 1 2 3406.45 2896.08 38.65 o -1 1 2 22864.79 25565.57 153.29 o 1 1 2 40130.71 41058.52 640.52 o 3 1 2 11.21 13.03 15.37 o 5 1 2 8714.57 8421.07 113.31 o 7 1 2 1164.61 1406.67 55.80 o 9 1 2 6.52 5.28 42.51 o 11 1 2 2179.67 2367.40 95.97 o 13 1 2 11.32 7.23 63.65 o 15 1 2 13.36 20.67 100.60 o 17 1 2 126.54 121.71 195.58 o -20 2 2 143.08 108.71 121.03 o -18 2 2 288.63 168.30 89.47 o -16 2 2 2205.26 2647.22 114.72 o -14 2 2 1013.54 1150.45 82.38 o -12 2 2 32.52 7.46 46.91 o -10 2 2 5840.75 4753.47 546.69 o -8 2 2 1849.34 1768.05 40.18 o -6 2 2 11960.57 11391.69 131.39 o -4 2 2 268451.47 250069.86 2054.11 o 0 2 2 2980.36 3984.87 54.42 o 2 2 2 38257.17 39985.57 242.27 o 4 2 2 1733.65 1401.77 37.76 o 6 2 2 6938.20 7279.51 83.38 o 8 2 2 10324.23 9567.78 136.22 o 10 2 2 570.50 507.54 58.89 o 12 2 2 459.93 454.69 102.07 o 14 2 2 479.96 640.01 106.14 o 16 2 2 4.98 -3.27 181.48 o 18 2 2 184.59 74.87 214.76 o -21 3 2 5.49 -26.83 153.66 o -19 3 2 80.31 59.36 109.27 o -17 3 2 24.54 24.88 84.01 o -15 3 2 95.42 8.47 64.64 o -13 3 2 1622.12 1639.39 310.89 o -11 3 2 95.36 78.03 47.22 o -9 3 2 1685.59 1731.80 103.17 o -7 3 2 7207.32 7413.50 106.19 o -5 3 2 42014.03 41365.96 341.08 o -3 3 2 297.70 236.37 31.91 o -1 3 2 27098.48 28855.36 382.84 o 1 3 2 3487.42 3919.37 103.30 o 3 3 2 74.90 56.64 21.87 o 5 3 2 8061.89 7468.29 84.51 o 7 3 2 532.64 708.32 54.79 o 9 3 2 1094.97 1162.98 68.40 o 11 3 2 26.42 48.40 59.67 o 13 3 2 188.37 135.03 91.39 o 15 3 2 516.26 490.19 116.77 o 17 3 2 38.76 14.15 205.48 o -20 4 2 18.67 -15.61 119.01 o -18 4 2 469.65 297.30 109.75 o -16 4 2 163.52 65.30 79.87 o -14 4 2 79.54 11.23 65.99 o -12 4 2 28.77 18.51 51.59 o -10 4 2 43.11 37.60 43.51 o -8 4 2 1679.93 1788.06 64.88 o -6 4 2 851.71 798.95 49.36 o -4 4 2 486.52 533.70 38.04 o -2 4 2 4839.25 4950.70 108.59 o 0 4 2 697.28 610.67 57.68 o 2 4 2 26.01 15.24 28.59 o 4 4 2 0.33 9.75 33.40 o 6 4 2 460.91 585.34 51.63 o 8 4 2 1178.41 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