#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/32/2223202.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2223202_Fobs loop_ _publ_author_name 'Iskenderov, Turganbay S.' 'Kalibabchuk, Valentina A.' 'Golenya, Irina A.' 'Dudarenko, Nikolay M.' 'Usenko, Natalia I.' _publ_section_title ; N-(2-Hydroxyethyl)-2-[2-(hydroxyimino)propanamido]ethanaminium 2-(hydroxyimino)propanoate ; _journal_coeditor_code TK2512 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2077 _journal_page_last o2078 _journal_volume 65 _journal_year 2009 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 96.990 _cell_angle_gamma 90.000 _cell_length_a 9.3550 _cell_length_b 6.9960 _cell_length_c 20.6060 _exptl_crystal_F_000 624.00 _reflns_d_resolution_high 0.7472 _[local]_cod_data_source_file tk2512Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' dnm5 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 174.10 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 3038.22 2771.77 43.95 o 3 0 0 8859.23 8392.36 120.91 o 4 0 0 10537.92 10409.79 354.65 o 5 0 0 859.30 837.37 49.61 o 6 0 0 419.03 402.78 24.54 o 7 0 0 5151.60 5100.06 74.43 o 8 0 0 720.36 686.68 35.22 o 9 0 0 33.30 21.92 32.45 o 10 0 0 68.24 48.90 45.95 o 11 0 0 31.83 43.56 40.80 o 1 1 0 29.52 28.51 3.79 o 2 1 0 924.24 868.66 11.40 o 3 1 0 1661.00 1636.67 32.73 o 4 1 0 142.81 127.73 7.64 o 5 1 0 8.99 25.06 8.95 o 6 1 0 7.08 15.30 9.25 o 7 1 0 21.49 37.63 18.01 o 8 1 0 1579.88 1561.19 44.84 o 9 1 0 458.58 451.67 22.74 o 10 1 0 115.02 116.94 35.11 o 11 1 0 231.60 234.98 35.19 o 12 1 0 109.86 104.75 43.88 o 0 2 0 5047.86 4910.39 239.90 o 1 2 0 1466.30 1429.98 35.85 o 2 2 0 4539.80 4147.09 34.93 o 3 2 0 80.29 78.85 9.72 o 4 2 0 1403.96 1538.22 17.83 o 5 2 0 124.77 122.77 12.59 o 6 2 0 195.36 182.53 13.95 o 7 2 0 338.58 320.73 18.52 o 8 2 0 131.66 115.85 22.00 o 9 2 0 903.44 976.27 35.12 o 10 2 0 5.71 9.60 27.13 o 11 2 0 50.97 51.36 32.85 o 1 3 0 311.45 326.41 8.38 o 2 3 0 88.37 81.84 6.53 o 3 3 0 399.07 442.40 15.46 o 4 3 0 539.12 581.60 14.45 o 5 3 0 202.27 183.35 14.37 o 6 3 0 188.13 190.07 16.79 o 7 3 0 252.36 258.86 17.65 o 8 3 0 17.85 18.93 18.01 o 9 3 0 50.12 91.54 27.23 o 10 3 0 37.98 26.99 22.93 o 11 3 0 84.22 77.38 28.27 o 0 4 0 780.79 754.61 29.88 o 1 4 0 334.93 296.66 10.13 o 2 4 0 7.66 26.55 10.86 o 3 4 0 2161.50 2263.69 21.66 o 4 4 0 1695.92 1772.92 32.60 o 5 4 0 47.98 71.74 18.28 o 6 4 0 131.95 130.28 29.19 o 7 4 0 3.52 22.29 20.43 o 8 4 0 25.02 36.50 18.47 o 9 4 0 137.33 131.48 39.05 o 10 4 0 40.44 42.64 34.56 o 11 4 0 133.19 127.08 55.22 o 1 5 0 11.82 24.78 14.26 o 2 5 0 74.72 79.93 13.97 o 3 5 0 474.31 446.42 16.37 o 4 5 0 155.61 164.63 17.03 o 5 5 0 137.24 141.20 18.72 o 6 5 0 9.67 15.07 18.80 o 7 5 0 88.58 88.52 20.97 o 8 5 0 0.28 14.47 20.12 o 9 5 0 16.35 10.40 31.72 o 10 5 0 227.14 237.33 42.18 o 0 6 0 561.68 561.29 34.13 o 1 6 0 158.70 175.72 17.35 o 2 6 0 20.07 24.15 15.15 o 3 6 0 295.40 303.95 19.83 o 4 6 0 1.90 13.95 16.15 o 5 6 0 2.36 26.63 18.54 o 6 6 0 118.61 136.02 22.97 o 7 6 0 49.29 47.69 21.07 o 8 6 0 1.62 5.48 17.63 o 9 6 0 116.72 159.11 33.87 o 1 7 0 550.86 534.31 30.73 o 2 7 0 185.05 160.93 20.85 o 3 7 0 49.73 64.28 26.20 o 4 7 0 18.47 28.56 27.11 o 5 7 0 6.61 35.48 23.89 o 6 7 0 8.21 33.16 25.62 o 7 7 0 3.13 25.35 32.97 o 8 7 0 11.44 28.27 34.04 o 0 8 0 66.93 79.48 44.34 o 1 8 0 32.39 52.22 32.59 o 2 8 0 35.23 40.19 28.59 o 3 8 0 7.93 0.09 23.37 o 4 8 0 61.60 45.97 35.66 o 5 8 0 524.10 542.82 46.80 o 6 8 0 17.89 71.23 55.98 o -12 1 1 0.00 2.81 51.60 o -11 1 1 3.55 30.21 29.60 o -10 1 1 24.03 50.42 28.40 o -9 1 1 405.54 394.83 29.73 o -8 1 1 5.28 19.64 15.80 o -7 1 1 269.36 249.97 18.28 o -6 1 1 550.26 587.33 14.95 o -5 1 1 7.29 22.68 8.72 o -4 1 1 1152.00 1248.73 12.68 o -3 1 1 134.46 137.08 6.07 o -2 1 1 3952.61 3522.68 32.68 o -1 1 1 3.01 11.58 3.95 o 1 1 1 335.22 296.70 11.95 o 2 1 1 2.75 12.84 6.68 o 3 1 1 551.03 515.14 9.54 o 4 1 1 1068.74 1049.90 11.56 o 5 1 1 338.72 352.61 11.04 o 6 1 1 257.19 276.73 19.36 o 7 1 1 83.76 76.16 16.91 o 8 1 1 2.11 7.60 21.10 o 9 1 1 25.35 37.85 20.63 o 10 1 1 13.98 25.69 28.66 o 11 1 1 14.41 28.44 31.23 o -11 2 1 45.63 69.99 34.89 o -10 2 1 10.01 23.55 27.71 o -9 2 1 9.27 7.68 27.73 o -8 2 1 153.72 152.05 18.27 o -7 2 1 133.89 156.47 17.28 o -6 2 1 0.00 26.57 13.86 o -5 2 1 0.00 11.64 9.62 o -4 2 1 1289.67 1283.62 15.34 o -3 2 1 923.07 979.47 14.90 o -2 2 1 135.39 160.87 12.41 o -1 2 1 356.13 348.17 13.17 o 0 2 1 24856.29 22578.22 1004.46 o 2 2 1 211.45 183.57 8.71 o 3 2 1 5051.73 4900.21 61.91 o 4 2 1 4057.70 4086.68 59.06 o 5 2 1 635.42 687.09 14.89 o 6 2 1 123.12 133.99 17.27 o 7 2 1 1602.35 1682.76 26.19 o 8 2 1 0.06 25.40 17.30 o 9 2 1 21.33 29.59 19.73 o 10 2 1 50.56 56.78 28.59 o 11 2 1 71.13 54.22 29.27 o -11 3 1 198.47 235.76 31.09 o -10 3 1 36.14 37.16 25.85 o -9 3 1 18.09 24.53 24.27 o -8 3 1 215.07 202.16 23.05 o -7 3 1 222.43 197.71 18.98 o -6 3 1 160.99 167.90 16.91 o -5 3 1 447.32 442.89 14.13 o -4 3 1 314.01 313.83 16.86 o -3 3 1 119.80 109.54 10.43 o -2 3 1 171.84 192.20 8.54 o -1 3 1 179.32 164.33 9.00 o 0 3 1 170.74 158.31 8.77 o 1 3 1 5.22 16.01 6.46 o 2 3 1 1369.56 1487.21 21.11 o 3 3 1 71.10 82.76 12.44 o 4 3 1 353.06 381.83 14.24 o 5 3 1 31.26 61.15 14.11 o 6 3 1 6.08 22.04 13.24 o 7 3 1 31.48 43.57 20.49 o 8 3 1 229.77 207.42 25.88 o 9 3 1 87.32 141.16 33.95 o 10 3 1 31.48 48.18 21.83 o 11 3 1 30.46 35.04 34.68 o -11 4 1 51.74 31.50 51.82 o -10 4 1 37.95 43.47 36.82 o -9 4 1 4.31 16.94 23.94 o -8 4 1 3.66 28.51 20.33 o -7 4 1 175.62 175.16 20.47 o -6 4 1 127.63 100.35 23.20 o -5 4 1 16.09 26.81 15.01 o -4 4 1 9.41 22.71 12.96 o -3 4 1 240.45 267.98 14.99 o -2 4 1 4.04 18.85 13.38 o -1 4 1 201.43 189.71 9.08 o 0 4 1 4.47 22.43 9.21 o 1 4 1 1417.20 1454.93 20.47 o 2 4 1 186.18 170.72 15.14 o 3 4 1 30.01 37.72 15.44 o 4 4 1 73.88 55.36 14.34 o 5 4 1 166.34 162.91 17.96 o 6 4 1 402.95 414.82 18.73 o 7 4 1 9.91 6.11 22.32 o 8 4 1 172.04 207.56 36.03 o 9 4 1 121.73 126.42 34.99 o 10 4 1 16.14 33.49 37.01 o -10 5 1 27.85 54.12 35.61 o -9 5 1 5.10 23.27 24.11 o -8 5 1 0.35 16.31 21.23 o -7 5 1 6.07 19.47 17.18 o -6 5 1 108.77 105.12 21.21 o -5 5 1 49.99 31.60 17.96 o -4 5 1 21.55 40.35 19.30 o -3 5 1 72.83 59.29 15.36 o -2 5 1 13.91 26.57 15.74 o -1 5 1 152.60 144.58 12.86 o 0 5 1 0.00 17.64 10.91 o 1 5 1 5.70 19.34 12.94 o 2 5 1 38.60 47.93 13.92 o 3 5 1 121.77 157.37 16.99 o 4 5 1 278.07 312.00 17.15 o 5 5 1 299.35 312.06 20.80 o 6 5 1 0.43 14.44 18.31 o 7 5 1 14.58 18.61 20.75 o 8 5 1 143.76 144.19 20.16 o 9 5 1 195.00 190.72 30.21 o -9 6 1 56.28 50.15 38.17 o -8 6 1 40.99 72.28 25.77 o -7 6 1 50.03 61.28 21.56 o -6 6 1 9.99 20.21 19.24 o -5 6 1 176.94 135.68 22.22 o -4 6 1 121.81 144.37 16.17 o -3 6 1 0.28 15.83 14.30 o -2 6 1 414.49 394.53 18.43 o -1 6 1 28.06 31.35 20.91 o 0 6 1 199.42 201.14 24.41 o 1 6 1 116.72 118.73 18.39 o 2 6 1 93.17 121.63 17.52 o 3 6 1 541.64 534.86 20.71 o 4 6 1 52.11 60.95 18.80 o 5 6 1 23.81 18.10 20.00 o 6 6 1 31.92 44.39 20.51 o 7 6 1 48.23 48.69 21.28 o 8 6 1 445.53 460.50 29.38 o 9 6 1 1.24 42.10 28.93 o -8 7 1 90.28 110.74 53.94 o -7 7 1 80.42 70.73 27.53 o -6 7 1 101.30 92.84 24.93 o -5 7 1 48.47 35.60 29.01 o -4 7 1 108.38 132.29 26.79 o -3 7 1 339.53 316.60 27.40 o -2 7 1 111.63 91.61 27.23 o -1 7 1 85.88 87.96 28.65 o 0 7 1 216.81 203.97 30.24 o 1 7 1 162.98 153.44 29.30 o 2 7 1 22.10 14.21 25.71 o 3 7 1 38.58 67.69 27.93 o 4 7 1 166.68 164.21 27.73 o 5 7 1 33.68 34.69 20.38 o 6 7 1 3.89 14.09 21.19 o 7 7 1 0.48 20.58 25.34 o 8 7 1 4.47 10.18 34.78 o -6 8 1 14.04 50.25 50.70 o -5 8 1 11.69 -3.91 34.29 o -4 8 1 53.62 71.17 32.20 o -3 8 1 114.40 99.54 43.58 o -2 8 1 263.12 262.45 51.46 o -1 8 1 25.15 14.58 42.51 o 0 8 1 98.13 69.60 35.88 o 1 8 1 27.03 58.76 43.92 o 2 8 1 21.64 36.10 39.04 o 3 8 1 0.10 60.11 47.31 o 4 8 1 3.17 8.37 34.80 o 5 8 1 437.21 411.57 42.06 o 6 8 1 3.12 12.91 46.68 o -11 0 2 1045.55 1140.32 69.42 o -10 0 2 282.99 368.36 55.44 o -9 0 2 1047.70 1007.78 47.80 o -8 0 2 1479.86 1450.15 46.12 o -7 0 2 490.44 499.45 33.29 o -6 0 2 268.73 281.83 18.12 o -5 0 2 2527.65 2638.30 27.85 o -4 0 2 5030.12 5103.42 105.07 o -3 0 2 631.44 565.17 44.21 o -2 0 2 808.28 810.38 18.78 o 1 0 2 923.60 860.75 13.49 o 2 0 2 9011.64 8073.95 302.79 o 3 0 2 501.38 533.31 30.50 o 4 0 2 723.87 696.64 27.01 o 5 0 2 1460.78 1510.34 25.15 o 6 0 2 938.77 969.40 30.97 o 7 0 2 39.77 71.76 22.71 o 8 0 2 1707.46 1758.34 48.62 o 9 0 2 133.17 88.16 39.65 o 10 0 2 63.34 114.91 35.53 o 11 0 2 77.60 95.67 41.29 o -11 1 2 4.74 23.34 29.38 o -10 1 2 4.72 21.51 29.99 o -9 1 2 147.51 141.45 18.75 o -8 1 2 147.12 148.84 20.65 o -7 1 2 219.71 205.27 18.71 o -6 1 2 0.34 18.69 10.00 o -5 1 2 1070.79 1155.50 12.66 o -4 1 2 213.10 199.79 7.80 o -3 1 2 27.96 35.69 5.75 o -2 1 2 6657.75 6246.70 71.88 o -1 1 2 1003.83 1097.73 10.16 o 0 1 2 376.43 348.37 8.40 o 1 1 2 126.82 130.21 6.22 o 2 1 2 2967.61 2879.76 26.65 o 3 1 2 4660.51 4600.98 95.13 o 4 1 2 294.39 322.90 11.75 o 5 1 2 88.71 73.62 10.41 o 6 1 2 1.41 9.67 9.76 o 7 1 2 49.50 51.12 17.01 o 8 1 2 41.29 44.66 18.11 o 9 1 2 357.03 337.94 34.25 o 10 1 2 11.46 27.48 28.87 o 11 1 2 17.07 6.02 30.98 o -11 2 2 65.92 83.35 29.93 o -10 2 2 20.34 41.30 31.56 o -9 2 2 984.53 1042.16 26.66 o -8 2 2 37.05 46.93 18.85 o -7 2 2 1209.39 1205.53 39.89 o -6 2 2 852.53 858.43 18.59 o -5 2 2 217.74 188.99 13.10 o -4 2 2 39.62 53.49 7.65 o -3 2 2 1.91 14.24 7.53 o -2 2 2 5886.85 5714.38 80.96 o -1 2 2 4994.81 4809.31 89.37 o 0 2 2 11015.70 11371.71 82.23 o 1 2 2 53.71 51.87 5.25 o 2 2 2 12.63 21.42 5.52 o 3 2 2 812.95 835.46 11.72 o 4 2 2 71.07 61.95 12.31 o 5 2 2 10.24 16.11 10.94 o 6 2 2 4003.59 4186.04 42.94 o 7 2 2 9.92 20.21 14.45 o 8 2 2 101.06 103.64 18.97 o 9 2 2 73.36 117.86 31.92 o 10 2 2 20.54 52.14 28.23 o 11 2 2 8.49 27.14 36.23 o -11 3 2 56.49 86.15 27.40 o -10 3 2 82.74 103.52 38.74 o -9 3 2 26.07 57.95 23.91 o -8 3 2 82.47 81.00 18.37 o -7 3 2 100.65 99.71 15.19 o -6 3 2 3.50 26.84 17.05 o -5 3 2 20.66 51.00 15.94 o -4 3 2 94.32 99.38 16.17 o -3 3 2 20.71 25.57 9.06 o -2 3 2 336.01 379.48 13.90 o -1 3 2 1763.66 1724.04 31.28 o 0 3 2 752.32 792.85 31.41 o 1 3 2 1471.90 1381.23 27.86 o 2 3 2 331.65 315.47 12.32 o 3 3 2 787.06 763.06 15.17 o 4 3 2 181.62 188.10 12.94 o 5 3 2 31.26 35.25 14.16 o 6 3 2 118.96 133.90 17.83 o 7 3 2 87.63 80.39 23.70 o 8 3 2 565.53 591.33 26.04 o 9 3 2 51.81 60.76 21.37 o 10 3 2 32.62 48.02 28.64 o 11 3 2 31.50 68.87 33.87 o -11 4 2 193.30 226.58 59.55 o -10 4 2 6.24 19.54 28.07 o -9 4 2 245.38 210.08 23.89 o -8 4 2 530.01 531.81 24.38 o -7 4 2 174.53 143.92 22.66 o -6 4 2 146.37 133.10 17.62 o -5 4 2 649.89 694.20 23.95 o -4 4 2 483.44 476.85 15.54 o -3 4 2 223.37 196.56 13.28 o -2 4 2 268.50 268.75 10.32 o -1 4 2 1033.89 993.64 30.71 o 0 4 2 1809.08 1777.90 19.35 o 1 4 2 485.09 512.65 14.02 o 2 4 2 1019.97 960.85 18.79 o 3 4 2 148.16 144.38 13.57 o 4 4 2 42.76 46.03 19.09 o 5 4 2 0.18 19.36 16.24 o 6 4 2 156.62 157.46 18.21 o 7 4 2 48.21 48.83 22.81 o 8 4 2 13.40 13.61 26.83 o 9 4 2 38.37 45.92 31.08 o 10 4 2 25.49 61.41 37.43 o -10 5 2 128.84 174.21 41.91 o -9 5 2 17.96 51.04 35.46 o -8 5 2 110.87 137.94 36.62 o -7 5 2 28.21 34.53 17.83 o -6 5 2 81.91 52.25 21.61 o -5 5 2 81.66 75.51 18.99 o -4 5 2 41.06 56.96 15.53 o -3 5 2 52.29 63.69 16.21 o -2 5 2 809.97 772.34 28.04 o -1 5 2 119.36 111.22 11.45 o 0 5 2 6.44 12.86 9.07 o 1 5 2 105.24 102.62 13.25 o 2 5 2 238.47 246.98 16.39 o 3 5 2 88.90 79.35 13.18 o 4 5 2 31.24 50.61 16.45 o 5 5 2 0.09 13.61 15.15 o 6 5 2 369.56 364.01 23.82 o 7 5 2 18.98 38.87 19.58 o 8 5 2 0.03 29.42 23.01 o 9 5 2 10.44 25.57 28.26 o -9 6 2 2.82 30.73 27.17 o -8 6 2 0.14 22.76 23.80 o -7 6 2 31.45 45.63 21.59 o -6 6 2 1081.86 1099.91 33.14 o -5 6 2 12.95 28.79 16.70 o -4 6 2 5.09 11.69 17.51 o -3 6 2 259.12 284.79 21.56 o -2 6 2 607.57 591.79 22.38 o -1 6 2 23.22 33.22 20.97 o 0 6 2 27.05 54.06 22.30 o 1 6 2 775.30 760.00 37.75 o 2 6 2 455.52 475.94 24.71 o 3 6 2 7.09 20.34 14.08 o 4 6 2 259.53 264.41 20.53 o 5 6 2 9.88 30.92 17.38 o 6 6 2 9.10 4.63 29.27 o 7 6 2 21.39 16.65 21.73 o 8 6 2 0.02 11.24 24.28 o -7 7 2 106.79 138.64 38.68 o -6 7 2 19.33 35.96 26.80 o -5 7 2 4.12 21.40 23.30 o -4 7 2 45.73 47.65 21.12 o -3 7 2 0.40 15.43 25.64 o -2 7 2 53.62 76.61 28.64 o -1 7 2 21.08 32.03 23.58 o 0 7 2 0.16 10.09 23.59 o 1 7 2 188.74 208.93 38.51 o 2 7 2 26.58 23.78 26.30 o 3 7 2 304.41 273.94 22.60 o 4 7 2 136.14 113.52 24.99 o 5 7 2 10.06 35.33 22.50 o 6 7 2 0.64 33.80 29.44 o 7 7 2 2.61 27.68 37.64 o -6 8 2 1.21 11.84 44.37 o -5 8 2 27.81 41.32 35.86 o -4 8 2 178.32 187.27 31.77 o -3 8 2 12.58 52.44 37.07 o -2 8 2 0.02 11.90 45.87 o -1 8 2 1.04 21.24 43.78 o 0 8 2 26.21 52.80 34.96 o 1 8 2 114.58 170.15 50.38 o 2 8 2 85.20 108.69 49.62 o 3 8 2 615.84 700.17 55.03 o 4 8 2 33.99 57.88 32.05 o 5 8 2 10.84 42.83 40.99 o -2 9 2 23.57 22.74 53.45 o -1 9 2 114.02 121.92 58.50 o 0 9 2 10.48 28.95 42.41 o 1 9 2 2.72 14.26 51.61 o 2 9 2 35.98 51.62 47.73 o 3 9 2 1.15 25.95 45.42 o -11 1 3 9.00 7.00 30.23 o -10 1 3 2.23 21.51 26.90 o -9 1 3 778.35 765.97 24.82 o -8 1 3 0.18 12.38 17.36 o -7 1 3 74.62 74.68 19.89 o -6 1 3 49.16 67.51 11.86 o -5 1 3 90.70 95.73 9.31 o -4 1 3 68.41 53.95 7.18 o -3 1 3 3428.56 3199.86 23.48 o -2 1 3 374.32 364.88 6.13 o -1 1 3 3307.32 3187.12 66.90 o 0 1 3 2533.15 2313.36 41.44 o 1 1 3 1079.88 972.37 25.25 o 2 1 3 33.86 35.46 7.04 o 3 1 3 3751.15 3668.48 91.53 o 4 1 3 21.54 20.34 6.34 o 5 1 3 7.28 11.34 9.22 o 6 1 3 1103.53 1071.01 35.33 o 7 1 3 712.47 631.36 25.37 o 8 1 3 62.95 32.01 18.33 o 9 1 3 445.62 480.40 32.73 o 10 1 3 233.25 270.34 40.27 o 11 1 3 91.29 134.60 33.27 o -11 2 3 0.00 43.82 34.73 o -10 2 3 9.85 20.39 27.41 o -9 2 3 78.12 78.65 23.16 o -8 2 3 1135.96 1135.93 27.20 o -7 2 3 96.44 68.59 16.71 o -6 2 3 590.52 565.15 16.03 o -5 2 3 5619.67 5779.14 41.52 o -4 2 3 3236.38 3281.47 52.11 o -3 2 3 23.86 31.01 6.66 o -2 2 3 620.75 592.78 20.78 o -1 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