#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/32/2223228.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2223228_Fobs loop_ _publ_author_name 'Feng, Jian-Shen' 'Zou, Li-Ke' 'Xie, Bin' 'Wu, Yu' _publ_section_title ; (meso-5,5,7,12,12,14-Hexamethyl-1,4,8,11-tetraazacyclotetradecane)copper(II) bis(O,S-dibenzyl dithiophosphate) ; _journal_coeditor_code XU2568 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1022 _journal_volume 65 _journal_year 2009 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 99.782 _cell_angle_gamma 90.000 _cell_length_a 11.4757 _cell_length_b 17.5923 _cell_length_c 11.9448 _exptl_crystal_F_000 1022.00 _reflns_d_resolution_high 0.8240 _[local]_cod_data_source_file xu2568Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ZLK4 in p21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 215.09 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 46262.50 44965.91 223.79 o 2 0 0 7334.09 7516.46 33.14 o 3 0 0 9420.08 11074.02 51.61 o 4 0 0 4595.70 4610.01 40.40 o 5 0 0 2940.30 3077.64 39.80 o 6 0 0 2825.54 3031.21 39.63 o 7 0 0 649.39 791.14 23.79 o 8 0 0 206.59 198.59 16.75 o 9 0 0 23.15 0.01 22.51 o 10 0 0 169.57 169.67 18.05 o 11 0 0 38.47 42.60 17.33 o 12 0 0 3.87 0.02 25.09 o 13 0 0 37.78 62.07 28.07 o 1 1 0 27.03 0.00 6.68 o 2 1 0 0.09 0.00 9.07 o 3 1 0 91.14 100.86 6.99 o 4 1 0 493.74 489.84 13.51 o 5 1 0 1534.28 1652.83 26.67 o 6 1 0 3242.70 3351.18 41.39 o 7 1 0 5950.76 6417.37 64.48 o 8 1 0 2594.86 2770.16 45.35 o 9 1 0 78.45 73.31 15.85 o 10 1 0 176.21 146.81 19.60 o 11 1 0 17.64 47.03 14.33 o 12 1 0 55.98 86.93 14.90 o 13 1 0 57.36 50.02 19.87 o 0 2 0 4426.15 4793.16 15.22 o 1 2 0 14966.12 16205.64 182.92 o 2 2 0 61.88 64.45 6.62 o 3 2 0 6092.48 6272.10 40.40 o 4 2 0 5430.73 4945.37 40.22 o 5 2 0 2893.80 3196.93 39.11 o 6 2 0 723.85 724.54 21.72 o 7 2 0 2782.04 3130.50 46.20 o 8 2 0 1421.64 1558.25 37.10 o 9 2 0 13.53 27.99 19.67 o 10 2 0 19.24 0.01 26.23 o 11 2 0 368.37 329.17 24.03 o 12 2 0 80.39 92.41 17.52 o 13 2 0 102.58 139.31 20.65 o 1 3 0 4255.50 3766.34 27.74 o 2 3 0 4564.28 4933.23 33.63 o 3 3 0 25.06 53.07 7.35 o 4 3 0 737.77 952.02 19.45 o 5 3 0 2316.02 2756.51 35.34 o 6 3 0 3984.72 4519.16 50.10 o 7 3 0 1785.26 2030.99 36.99 o 8 3 0 300.30 308.87 18.16 o 9 3 0 85.60 99.47 18.16 o 10 3 0 1.68 0.01 23.74 o 11 3 0 16.54 37.14 25.81 o 12 3 0 8.26 5.87 27.96 o 13 3 0 0.03 9.75 28.03 o 0 4 0 16359.96 17086.06 57.88 o 1 4 0 5676.69 5716.65 22.54 o 2 4 0 3440.24 3304.70 30.54 o 3 4 0 8193.33 9039.86 54.82 o 4 4 0 7034.25 7854.38 59.12 o 5 4 0 20.50 0.00 16.37 o 6 4 0 601.27 595.73 19.87 o 7 4 0 1996.86 2260.02 40.58 o 8 4 0 429.26 423.93 22.65 o 9 4 0 1061.09 1309.84 39.18 o 10 4 0 269.34 278.50 21.20 o 11 4 0 737.52 690.87 33.87 o 12 4 0 653.31 605.20 32.83 o 13 4 0 410.99 529.71 30.80 o 1 5 0 325.78 296.31 10.93 o 2 5 0 87.03 65.31 9.77 o 3 5 0 805.22 953.68 20.11 o 4 5 0 11.12 11.54 16.15 o 5 5 0 9.63 12.73 14.93 o 6 5 0 271.95 224.89 14.99 o 7 5 0 165.37 167.26 14.13 o 8 5 0 2466.33 2462.37 47.21 o 9 5 0 967.81 890.59 31.39 o 10 5 0 15.19 47.78 14.62 o 11 5 0 26.37 0.01 28.38 o 12 5 0 118.88 131.04 20.38 o 13 5 0 53.67 110.48 18.92 o 0 6 0 5784.99 6242.44 30.90 o 1 6 0 5734.87 5856.42 47.84 o 2 6 0 7402.07 6609.65 50.97 o 3 6 0 3878.15 4412.74 43.49 o 4 6 0 5256.46 6176.57 58.03 o 5 6 0 2.93 11.39 14.37 o 6 6 0 8.00 0.01 17.78 o 7 6 0 267.86 305.43 18.61 o 8 6 0 1428.06 1507.02 36.95 o 9 6 0 747.40 705.22 31.73 o 10 6 0 974.00 968.82 35.60 o 11 6 0 282.54 267.61 22.88 o 12 6 0 293.03 250.41 24.47 o 13 6 0 55.31 38.62 33.58 o 1 7 0 717.49 695.92 19.15 o 2 7 0 55.02 35.06 15.18 o 3 7 0 0.50 11.87 15.91 o 4 7 0 268.90 329.43 16.16 o 5 7 0 172.04 232.63 14.96 o 6 7 0 207.89 232.28 16.74 o 7 7 0 137.03 126.76 15.25 o 8 7 0 48.39 68.38 15.12 o 9 7 0 37.98 58.03 23.62 o 10 7 0 0.69 0.87 26.74 o 11 7 0 0.04 3.86 23.70 o 12 7 0 48.45 22.22 33.14 o 0 8 0 4165.96 4077.19 29.59 o 1 8 0 2194.01 2025.80 33.14 o 2 8 0 3884.53 4070.95 46.05 o 3 8 0 2290.52 2384.12 36.52 o 4 8 0 1780.30 1861.00 34.66 o 5 8 0 2394.41 2701.65 45.76 o 6 8 0 1224.30 1358.84 32.75 o 7 8 0 1287.75 1442.22 36.77 o 8 8 0 546.34 620.64 27.49 o 9 8 0 573.23 459.03 25.60 o 10 8 0 41.85 21.75 25.21 o 11 8 0 31.35 7.94 27.33 o 12 8 0 118.79 131.19 23.03 o 1 9 0 471.10 453.93 17.36 o 2 9 0 632.98 716.90 22.62 o 3 9 0 1010.86 1192.87 27.69 o 4 9 0 128.60 160.68 13.95 o 5 9 0 82.17 37.53 23.70 o 6 9 0 11.82 30.75 11.90 o 7 9 0 14.07 0.01 24.54 o 8 9 0 48.94 69.80 17.74 o 9 9 0 163.05 211.24 21.46 o 10 9 0 0.12 4.68 25.21 o 11 9 0 48.26 45.02 27.72 o 12 9 0 153.78 161.82 21.44 o 0 10 0 345.15 342.65 11.00 o 1 10 0 502.20 399.79 17.79 o 2 10 0 61.87 109.37 11.86 o 3 10 0 971.84 929.86 26.62 o 4 10 0 2257.78 2214.07 44.62 o 5 10 0 1505.03 1674.71 37.34 o 6 10 0 1680.34 1811.73 40.97 o 7 10 0 150.68 143.50 17.84 o 8 10 0 305.35 322.64 23.63 o 9 10 0 363.77 348.58 24.56 o 10 10 0 45.82 40.86 27.89 o 11 10 0 65.03 72.84 19.59 o 12 10 0 25.08 0.02 35.17 o 1 11 0 228.24 260.41 17.26 o 2 11 0 606.19 543.72 21.79 o 3 11 0 91.42 80.65 14.30 o 4 11 0 100.25 135.71 15.03 o 5 11 0 31.54 70.17 13.28 o 6 11 0 166.40 203.30 18.47 o 7 11 0 20.97 0.01 25.66 o 8 11 0 68.37 0.01 31.13 o 9 11 0 7.49 0.01 29.12 o 10 11 0 10.47 8.09 27.29 o 11 11 0 183.62 186.75 26.44 o 0 12 0 542.16 571.81 24.36 o 1 12 0 451.96 386.15 20.18 o 2 12 0 965.08 810.64 27.71 o 3 12 0 604.85 603.42 25.41 o 4 12 0 10.20 15.26 21.98 o 5 12 0 37.91 62.51 14.55 o 6 12 0 2.00 0.01 24.84 o 7 12 0 103.00 152.14 20.15 o 8 12 0 290.22 295.94 23.77 o 9 12 0 253.95 259.65 26.99 o 10 12 0 143.17 122.66 21.09 o 11 12 0 204.34 182.33 28.39 o 1 13 0 0.97 0.01 21.69 o 2 13 0 186.27 216.01 19.43 o 3 13 0 52.74 30.97 24.36 o 4 13 0 92.14 84.85 14.62 o 5 13 0 141.06 111.95 18.02 o 6 13 0 80.45 105.81 17.46 o 7 13 0 447.89 573.11 30.77 o 8 13 0 209.34 160.26 21.94 o 9 13 0 19.07 2.05 33.69 o 10 13 0 165.68 187.43 24.80 o 0 14 0 29.80 0.01 27.79 o 1 14 0 1.73 9.88 23.02 o 2 14 0 32.30 12.15 27.55 o 3 14 0 12.73 0.01 25.25 o 4 14 0 48.98 86.18 18.36 o 5 14 0 274.59 334.31 23.24 o 6 14 0 227.61 263.28 23.84 o 7 14 0 316.56 303.95 28.14 o 8 14 0 196.19 220.80 22.54 o 9 14 0 8.41 12.91 30.29 o 10 14 0 229.49 164.32 26.99 o 1 15 0 0.02 0.01 33.31 o 2 15 0 2.50 6.23 31.72 o 3 15 0 129.23 106.32 18.76 o 4 15 0 67.47 54.12 32.58 o 5 15 0 4.36 0.01 29.59 o 6 15 0 8.10 0.01 31.59 o 7 15 0 25.73 0.01 33.68 o 8 15 0 37.46 0.01 34.07 o 9 15 0 10.20 0.01 40.38 o 0 16 0 607.35 632.66 36.66 o 1 16 0 105.81 113.05 18.84 o 2 16 0 9.63 0.01 32.33 o 3 16 0 73.10 57.30 17.70 o 4 16 0 312.22 314.69 25.57 o 5 16 0 426.46 510.69 30.71 o 6 16 0 522.31 513.21 31.79 o 7 16 0 174.62 204.19 22.68 o 8 16 0 18.44 65.01 28.75 o 9 16 0 71.56 75.34 20.82 o 1 17 0 95.51 95.99 20.77 o 2 17 0 2.27 0.01 34.02 o 3 17 0 0.43 0.01 30.83 o 5 17 0 352.92 365.11 28.77 o 6 17 0 362.13 434.48 31.80 o 7 17 0 109.57 200.66 23.75 o 8 17 0 128.28 152.77 24.93 o 0 18 0 352.07 503.11 32.20 o 1 18 0 1379.61 1549.16 49.35 o 2 18 0 582.68 761.63 38.48 o 3 18 0 117.65 129.14 21.58 o 5 18 0 22.47 38.53 33.86 o 6 18 0 0.94 0.01 38.57 o 7 18 0 10.90 52.09 32.72 o 1 19 0 24.33 56.25 37.76 o 2 19 0 0.30 20.13 33.15 o 3 19 0 6.60 0.02 31.96 o 4 19 0 0.71 17.63 33.88 o 5 19 0 43.36 18.52 23.92 o 6 19 0 64.90 46.95 39.28 o 0 20 0 100.76 53.04 44.72 o 1 20 0 2.20 0.01 38.79 o 2 20 0 39.00 68.16 37.33 o 3 20 0 95.09 141.17 23.20 o 4 20 0 13.39 73.18 36.03 o 1 21 0 6.87 50.35 36.20 o 2 21 0 10.60 57.45 21.00 o -13 1 1 192.65 190.52 21.99 o -12 1 1 336.74 349.17 28.37 o -11 1 1 1.88 0.02 22.61 o -10 1 1 617.53 676.16 27.02 o -9 1 1 63.50 40.63 24.03 o -8 1 1 305.36 283.95 18.26 o -7 1 1 192.77 260.25 16.59 o -6 1 1 293.82 304.37 24.03 o -5 1 1 568.33 709.84 18.47 o -4 1 1 406.10 488.48 19.09 o -3 1 1 243.49 225.03 9.07 o -2 1 1 544.92 556.09 13.61 o -1 1 1 1959.67 2021.76 14.76 o 0 1 1 4965.30 5148.69 14.80 o 1 1 1 8021.84 8996.36 32.44 o 2 1 1 35.97 13.36 9.77 o 3 1 1 24003.87 25997.04 317.66 o 4 1 1 5130.41 4916.21 41.45 o 5 1 1 5307.77 5775.44 50.31 o 6 1 1 6403.40 6805.64 60.20 o 7 1 1 6466.11 7159.97 70.76 o 8 1 1 4668.22 5217.46 65.09 o 9 1 1 646.83 658.34 27.02 o 10 1 1 162.15 154.74 18.89 o 11 1 1 547.65 528.00 28.22 o 12 1 1 44.37 16.81 30.44 o 13 1 1 85.11 84.35 19.33 o -13 2 1 40.06 39.79 30.76 o -12 2 1 11.76 0.01 30.60 o -11 2 1 11.93 0.01 24.27 o -10 2 1 816.21 925.23 32.75 o -9 2 1 1646.64 1443.58 37.26 o -8 2 1 1127.08 915.93 28.55 o -7 2 1 460.99 343.21 24.26 o -6 2 1 57.66 64.60 11.36 o -5 2 1 794.05 967.33 21.91 o -4 2 1 1891.19 1952.22 30.63 o -3 2 1 4955.86 4966.52 36.64 o -2 2 1 21840.37 21509.83 261.33 o -1 2 1 4111.96 4803.39 25.14 o 1 2 1 7835.16 8682.94 37.67 o 2 2 1 3132.86 3038.36 25.49 o 4 2 1 2175.64 1898.21 26.54 o 5 2 1 8054.25 9388.39 64.09 o 6 2 1 22.67 7.56 15.70 o 7 2 1 204.86 238.37 15.02 o 8 2 1 1031.18 1246.06 35.02 o 9 2 1 74.18 35.32 26.37 o 10 2 1 118.92 133.34 19.31 o 11 2 1 531.78 519.49 28.69 o 12 2 1 235.37 247.18 24.69 o 13 2 1 221.51 256.09 24.87 o -13 3 1 87.01 5.16 34.94 o -12 3 1 156.60 151.69 19.94 o -11 3 1 234.65 263.92 22.31 o -10 3 1 2465.09 2258.01 49.04 o -9 3 1 2305.59 2173.26 46.30 o -8 3 1 4548.59 4228.44 58.51 o -7 3 1 2843.65 2572.90 47.63 o -6 3 1 4575.78 4385.88 54.59 o -5 3 1 581.54 525.10 16.29 o -4 3 1 973.81 979.30 22.68 o -3 3 1 86.47 125.04 8.12 o -2 3 1 46.42 20.47 10.66 o -1 3 1 15936.05 14964.09 202.53 o 0 3 1 43111.00 42766.01 234.40 o 1 3 1 5559.49 5769.88 35.32 o 2 3 1 12.54 33.58 11.11 o 3 3 1 460.71 425.59 13.24 o 4 3 1 478.17 574.39 15.82 o 5 3 1 2949.95 3365.44 39.85 o 6 3 1 881.33 1107.35 25.32 o 7 3 1 116.29 77.39 12.98 o 8 3 1 9.62 11.50 19.97 o 9 3 1 78.50 33.64 27.90 o 10 3 1 686.42 736.82 30.11 o 11 3 1 647.97 640.58 30.95 o 12 3 1 575.10 584.21 33.19 o 13 3 1 143.33 165.20 23.39 o -13 4 1 18.15 7.34 28.27 o -12 4 1 3.46 30.49 25.06 o -11 4 1 4.84 0.01 27.91 o -10 4 1 228.86 173.12 20.25 o -9 4 1 249.88 215.26 18.30 o -8 4 1 398.04 353.05 20.19 o -7 4 1 466.70 448.75 19.08 o -6 4 1 214.98 181.11 19.53 o -5 4 1 15.24 12.11 16.57 o -4 4 1 423.20 445.91 18.63 o -3 4 1 476.94 528.97 13.79 o -2 4 1 4221.56 4536.10 35.18 o -1 4 1 2477.82 2205.81 22.45 o 0 4 1 6067.20 6743.72 26.92 o 1 4 1 523.31 570.96 13.32 o 2 4 1 3463.62 3607.94 32.62 o 3 4 1 4967.29 4921.22 41.19 o 4 4 1 391.51 395.85 14.43 o 5 4 1 424.65 437.08 16.18 o 6 4 1 24.75 30.19 16.58 o 7 4 1 1.08 0.01 21.90 o 8 4 1 159.27 153.78 16.18 o 9 4 1 1103.03 1134.88 35.22 o 10 4 1 86.55 45.89 31.94 o 11 4 1 0.04 7.39 25.93 o 12 4 1 82.90 77.38 16.39 o 13 4 1 28.50 0.02 34.22 o -13 5 1 76.94 69.41 23.72 o -12 5 1 104.09 73.77 31.69 o -11 5 1 169.18 180.10 18.78 o -10 5 1 298.87 274.82 21.47 o -9 5 1 708.27 596.63 25.17 o -8 5 1 1817.10 1662.06 37.77 o -7 5 1 422.89 433.82 19.67 o -6 5 1 8.98 0.01 16.34 o -5 5 1 3986.26 4576.57 56.91 o -4 5 1 6794.85 6293.80 58.26 o -3 5 1 11690.34 13259.07 70.19 o -2 5 1 3580.58 3057.46 30.68 o -1 5 1 1737.01 1354.86 19.85 o 0 5 1 412.57 449.80 8.74 o 1 5 1 5380.10 5084.53 40.34 o 2 5 1 147.06 104.44 8.34 o 3 5 1 764.79 816.02 18.41 o 4 5 1 2561.67 2695.17 36.58 o 5 5 1 378.14 338.36 14.98 o 6 5 1 406.31 334.90 17.16 o 7 5 1 1764.88 1914.22 38.56 o 8 5 1 25.61 47.79 12.69 o 9 5 1 28.36 28.28 25.20 o 10 5 1 166.63 118.94 32.46 o 11 5 1 107.28 130.51 17.84 o 12 5 1 34.66 30.06 28.37 o 13 5 1 2.80 43.33 25.18 o -13 6 1 16.13 28.37 32.11 o -12 6 1 0.16 0.02 30.59 o -11 6 1 156.74 216.67 20.16 o -10 6 1 350.73 315.81 22.31 o -9 6 1 928.50 861.07 29.55 o -8 6 1 270.07 313.23 20.26 o -7 6 1 453.03 436.19 20.12 o -6 6 1 24.34 19.09 19.63 o -5 6 1 177.76 194.41 13.62 o -4 6 1 506.54 523.00 18.13 o -3 6 1 9.98 5.29 15.04 o -2 6 1 2145.73 2020.14 27.70 o -1 6 1 14.51 25.63 6.53 o 0 6 1 1125.07 1104.97 13.59 o 1 6 1 106.26 82.87 8.37 o 2 6 1 15.16 0.00 13.00 o 3 6 1 1239.78 1296.08 25.12 o 4 6 1 306.33 298.22 15.13 o 5 6 1 344.87 334.69 16.39 o 6 6 1 38.01 30.52 20.62 o 7 6 1 1.93 20.78 12.73 o 8 6 1 52.24 54.53 13.85 o 9 6 1 100.30 99.76 17.72 o 10 6 1 362.73 356.03 25.69 o 11 6 1 101.45 69.15 35.44 o 12 6 1 117.51 138.98 20.08 o -13 7 1 217.61 197.43 24.40 o -12 7 1 104.63 74.50 32.32 o -11 7 1 173.12 196.81 20.31 o -10 7 1 140.99 60.31 30.28 o -9 7 1 148.68 89.66 26.73 o -8 7 1 207.95 198.71 31.01 o -7 7 1 13.01 14.09 17.79 o -6 7 1 4.34 36.32 9.24 o -5 7 1 320.58 222.23 14.77 o -4 7 1 6995.18 7090.20 68.69 o -3 7 1 1401.58 1295.95 24.93 o -2 7 1 25.07 48.95 7.19 o -1 7 1 941.54 781.01 18.01 o 0 7 1 582.02 645.40 12.14 o 1 7 1 42.16 50.08 7.49 o 2 7 1 2872.43 3181.14 37.49 o 3 7 1 16208.82 17426.98 98.43 o 4 7 1 4880.44 5084.84 56.82 o 5 7 1 2623.68 2789.23 42.59 o 6 7 1 3737.80 4305.66 56.79 o 7 7 1 3094.35 3386.07 54.50 o 8 7 1 931.09 1069.29 34.14 o 9 7 1 528.25 533.41 27.31 o 10 7 1 242.61 195.49 22.03 o 11 7 1 55.29 45.24 30.73 o 12 7 1 40.35 51.91 28.16 o -12 8 1 1.62 28.37 27.54 o -11 8 1 57.25 59.03 17.48 o -10 8 1 165.99 126.98 20.28 o -9 8 1 0.00 16.09 24.39 o -8 8 1 6.46 0.01 26.47 o -7 8 1 75.09 64.77 12.58 o -6 8 1 88.85 88.62 22.56 o -5 8 1 187.25 215.93 16.07 o -4 8 1 723.51 750.23 22.46 o -3 8 1 786.87 826.58 21.93 o -2 8 1 1065.99 1024.25 22.47 o -1 8 1 3769.27 3587.37 40.95 o 0 8 1 2671.79 3457.96 27.64 o 1 8 1 16.62 0.39 15.49 o 2 8 1 673.74 592.19 20.44 o 3 8 1 1615.25 1635.04 31.45 o 4 8 1 1060.85 1042.75 25.55 o 5 8 1 28.07 14.69 9.85 o 6 8 1 14.24 10.45 21.71 o 7 8 1 128.72 100.89 16.89 o 8 8 1 193.68 180.96 19.23 o 9 8 1 14.79 10.94 25.01 o 10 8 1 3.79 0.01 29.17 o 11 8 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o -2 16 3 6.54 0.91 27.28 o -1 16 3 1.91 0.01 28.70 o 0 16 3 195.20 233.78 23.54 o 1 16 3 0.29 0.01 29.31 o 2 16 3 129.08 150.75 19.67 o 3 16 3 12.74 0.01 29.04 o 4 16 3 7.77 0.01 34.33 o 5 16 3 58.63 15.90 34.23 o 6 16 3 168.37 160.84 25.61 o 7 16 3 50.50 23.89 35.63 o 8 16 3 7.89 1.21 35.17 o -8 17 3 88.12 28.92 37.21 o -7 17 3 257.16 254.22 26.30 o -6 17 3 338.69 349.76 27.98 o -5 17 3 229.15 229.29 24.75 o -4 17 3 129.95 60.36 35.99 o -3 17 3 169.54 177.14 21.87 o -2 17 3 202.86 199.09 23.15 o -1 17 3 121.16 121.80 18.32 o 0 17 3 52.34 95.58 21.91 o 1 17 3 352.97 411.89 28.32 o 2 17 3 99.70 88.10 33.26 o 3 17 3 3.03 0.01 32.75 o 5 17 3 34.81 10.61 32.51 o 6 17 3 90.55 65.25 37.95 o 7 17 3 14.52 0.02 32.83 o -7 18 3 1.49 22.18 30.63 o -6 18 3 1.14 0.02 30.82 o -5 18 3 18.96 34.43 18.43 o -4 18 3 23.66 0.01 36.13 o -3 18 3 0.12 12.35 30.97 o -2 18 3 2.30 21.08 27.48 o -1 18 3 53.34 7.15 36.37 o 0 18 3 83.64 57.33 34.80 o 1 18 3 46.54 28.20 33.53 o 2 18 3 0.74 0.01 33.88 o 3 18 3 36.60 36.97 29.03 o 5 18 3 4.47 0.02 35.37 o 6 18 3 43.85 3.59 37.16 o -6 19 3 156.49 149.62 30.11 o -5 19 3 133.75 122.11 26.03 o -4 19 3 202.83 294.85 29.93 o -2 19 3 343.93 368.79 29.40 o -1 19 3 139.53 133.42 26.25 o 0 19 3 52.03 55.03 36.28 o 1 19 3 50.20 0.01 37.73 o 2 19 3 70.53 59.92 36.22 o 3 19 3 4.10 4.52 29.78 o 5 19 3 120.17 66.21 44.64 o -4 20 3 14.38 0.02 37.10 o -2 20 3 2.97 0.02 32.42 o -1 20 3 3.62 0.02 37.32 o 0 20 3 4.31 0.02 34.82 o 1 20 3 44.41 0.02 37.64 o 2 20 3 27.89 37.29 31.96 o 3 20 3 0.04 0.02 30.69 o -13 0 4 63.24 51.40 32.31 o -12 0 4 168.80 241.81 23.36 o -11 0 4 29.06 6.91 27.29 o -10 0 4 26.11 4.69 24.65 o -9 0 4 321.09 266.98 17.79 o -8 0 4 166.64 186.74 15.54 o -7 0 4 1194.32 1278.84 31.15 o -6 0 4 767.05 749.97 21.96 o -5 0 4 12.74 39.39 9.39 o -4 0 4 1503.87 1721.85 27.82 o -3 0 4 708.05 609.20 15.94 o -2 0 4 52.93 69.24 8.55 o -1 0 4 11610.72 11815.60 59.88 o 0 0 4 1643.02 1848.14 17.03 o 1 0 4 263.15 294.55 11.25 o 2 0 4 6495.86 6321.46 48.47 o 3 0 4 7400.11 7502.84 56.63 o 4 0 4 469.66 347.15 20.43 o 5 0 4 2925.85 3002.92 41.83 o 6 0 4 1954.42 1994.83 37.43 o 7 0 4 1259.80 1148.31 32.72 o 8 0 4 860.38 775.59 28.81 o 9 0 4 746.76 734.81 33.20 o 10 0 4 203.65 236.74 24.80 o 11 0 4 207.17 208.02 24.98 o 12 0 4 314.02 327.73 30.08 o -13 1 4 5.55 0.02 28.10 o -12 1 4 157.70 184.05 22.42 o -11 1 4 48.77 17.30 27.48 o -10 1 4 50.80 69.83 14.85 o -9 1 4 269.19 215.33 17.78 o -8 1 4 887.70 868.07 27.11 o -7 1 4 66.06 58.07 10.37 o -6 1 4 80.51 128.12 12.34 o -4 1 4 124.38 120.32 10.09 o -3 1 4 142.76 189.07 10.09 o -2 1 4 1195.71 1211.65 20.45 o -1 1 4 189.38 198.72 10.21 o 0 1 4 63.71 64.73 5.26 o 1 1 4 2.91 6.36 11.60 o 2 1 4 45.49 4.37 14.03 o 3 1 4 1159.64 1341.18 23.91 o 4 1 4 22.24 25.98 7.76 o 5 1 4 1108.06 1028.90 25.95 o 6 1 4 464.99 429.54 19.39 o 7 1 4 788.21 762.63 27.37 o 8 1 4 220.48 245.14 19.64 o 9 1 4 4.76 0.01 26.19 o 10 1 4 265.48 248.66 20.95 o 11 1 4 8.66 0.02 31.16 o 12 1 4 149.38 130.40 22.88 o -13 2 4 139.06 149.29 19.49 o -12 2 4 141.87 152.68 21.77 o -11 2 4 87.93 96.48 20.09 o -10 2 4 455.82 448.12 23.85 o -9 2 4 249.78 262.50 20.09 o -8 2 4 3.66 0.01 21.11 o -7 2 4 6.37 0.01 19.75 o -6 2 4 23.95 44.68 9.90 o -5 2 4 783.02 944.50 23.52 o -4 2 4 165.90 194.71 11.72 o -3 2 4 391.79 419.48 14.34 o -2 2 4 2655.93 2788.51 31.23 o -1 2 4 8281.64 7833.65 50.09 o 0 2 4 3392.25 3288.47 22.83 o 1 2 4 9640.69 10592.30 60.72 o 2 2 4 1306.40 1343.04 22.48 o 3 2 4 1216.48 1162.71 23.99 o 4 2 4 3276.10 3201.69 40.93 o 5 2 4 1857.11 1954.30 41.05 o 6 2 4 2035.25 2046.76 38.23 o 7 2 4 2620.31 2624.59 48.16 o 8 2 4 1637.53 1477.41 39.44 o 9 2 4 456.98 413.20 23.73 o 10 2 4 590.52 529.67 29.85 o 11 2 4 145.14 69.03 35.72 o 12 2 4 3.16 51.35 26.32 o -13 3 4 48.62 42.77 29.48 o -12 3 4 16.25 0.01 32.34 o -11 3 4 161.67 243.48 21.15 o -10 3 4 106.25 47.08 26.57 o -9 3 4 96.02 35.29 27.79 o -8 3 4 139.42 129.86 13.65 o -7 3 4 89.78 109.59 14.10 o -6 3 4 436.08 444.03 19.72 o -5 3 4 162.99 213.93 13.17 o -4 3 4 1149.41 1354.02 25.95 o -3 3 4 0.58 0.00 15.57 o -2 3 4 2.92 0.00 13.27 o -1 3 4 6176.05 5637.52 43.49 o 0 3 4 5730.94 5921.58 31.68 o 1 3 4 4428.30 4495.76 29.58 o 2 3 4 897.42 893.15 19.80 o 3 3 4 4935.09 5449.35 50.26 o 4 3 4 6.40 0.01 16.40 o 5 3 4 2.48 22.97 15.60 o 6 3 4 117.54 84.91 13.75 o 7 3 4 66.03 81.46 14.50 o 8 3 4 3.63 0.01 25.73 o 9 3 4 101.48 75.44 16.05 o 10 3 4 176.03 189.36 22.13 o 11 3 4 169.61 154.44 20.63 o 12 3 4 54.20 50.69 31.76 o -13 4 4 201.24 244.28 26.18 o -12 4 4 177.07 205.31 21.34 o -11 4 4 261.45 313.41 24.24 o -10 4 4 578.46 571.96 26.65 o -9 4 4 1271.84 1229.89 36.29 o -8 4 4 1706.64 1558.38 37.66 o -7 4 4 1137.24 1076.39 28.87 o -6 4 4 1853.10 1792.81 35.25 o -5 4 4 37.06 55.42 9.10 o -4 4 4 1232.05 1070.54 24.62 o -3 4 4 3033.77 2853.92 35.43 o -2 4 4 4467.93 4338.28 28.62 o -1 4 4 2354.97 2068.29 28.32 o 0 4 4 21155.46 21454.01 64.33 o 1 4 4 4048.79 3849.59 39.31 o 2 4 4 266.36 266.65 12.18 o 3 4 4 577.13 640.64 18.46 o 4 4 4 168.64 163.85 12.54 o 5 4 4 1035.98 1062.81 29.01 o 6 4 4 2638.59 2750.98 45.86 o 7 4 4 362.80 442.71 23.50 o 8 4 4 62.48 0.01 28.41 o 9 4 4 198.03 244.27 20.69 o 10 4 4 177.19 189.25 21.42 o 11 4 4 16.63 0.02 28.83 o 12 4 4 62.90 67.19 31.16 o -13 5 4 64.79 93.31 19.29 o -12 5 4 39.34 31.02 31.97 o -11 5 4 8.50 26.42 24.93 o -10 5 4 0.01 44.83 19.19 o -9 5 4 0.30 12.06 21.67 o -8 5 4 461.29 371.52 20.64 o -7 5 4 165.54 155.92 15.20 o -6 5 4 45.60 33.05 20.45 o -5 5 4 50.40 67.05 17.64 o -4 5 4 532.70 436.03 18.07 o -3 5 4 102.08 90.72 10.04 o -2 5 4 2243.60 2529.80 33.38 o -1 5 4 3113.86 2671.35 33.06 o 0 5 4 5786.64 6153.37 34.98 o 1 5 4 761.39 774.87 19.43 o 2 5 4 5542.63 5996.06 52.16 o 3 5 4 19.30 56.56 8.69 o 4 5 4 109.94 128.06 11.80 o 5 5 4 597.72 574.69 21.82 o 6 5 4 100.47 88.84 13.72 o 7 5 4 413.82 439.07 23.30 o 8 5 4 252.82 256.79 20.16 o 9 5 4 0.14 0.01 23.40 o 10 5 4 0.61 0.02 27.23 o 11 5 4 100.45 89.12 18.82 o 12 5 4 31.28 24.28 32.11 o -13 6 4 90.52 56.17 36.75 o -12 6 4 68.27 28.60 30.61 o -11 6 4 334.27 311.75 25.65 o -10 6 4 321.89 269.96 22.44 o -9 6 4 328.74 253.61 20.74 o -8 6 4 3154.38 2748.46 51.08 o -7 6 4 4253.52 4042.27 57.71 o -6 6 4 4482.79 4310.42 56.27 o -5 6 4 3611.28 3672.19 49.67 o -4 6 4 2517.61 2247.33 38.47 o -3 6 4 2464.19 3011.95 39.51 o -2 6 4 4.98 0.00 14.59 o -1 6 4 492.56 475.64 16.42 o 0 6 4 387.51 426.07 10.91 o 1 6 4 187.03 187.53 12.37 o 2 6 4 345.78 309.24 14.25 o 3 6 4 125.88 99.40 10.50 o 4 6 4 1759.45 1811.51 34.28 o 5 6 4 204.22 240.31 16.18 o 6 6 4 69.77 53.29 22.73 o 7 6 4 37.34 38.58 27.05 o 8 6 4 232.57 242.91 20.94 o 9 6 4 29.30 0.01 29.59 o 10 6 4 76.25 71.14 17.55 o 11 6 4 178.55 186.61 22.79 o -13 7 4 111.60 131.43 25.16 o -12 7 4 102.33 112.23 20.53 o -11 7 4 23.60 0.01 31.91 o -10 7 4 43.31 0.01 28.63 o -9 7 4 301.04 256.46 18.82 o -8 7 4 2.19 0.01 26.56 o -7 7 4 495.72 479.81 23.23 o -6 7 4 674.91 702.30 25.77 o -5 7 4 94.58 86.73 12.69 o -4 7 4 18.51 0.01 18.00 o -3 7 4 641.71 678.46 20.86 o -2 7 4 653.48 631.81 19.93 o -1 7 4 1910.96 2047.95 32.78 o 0 7 4 1962.43 2064.93 22.84 o 1 7 4 97.32 52.51 10.98 o 2 7 4 2460.16 2083.34 34.87 o 3 7 4 10.44 14.25 16.81 o 4 7 4 223.77 237.51 16.00 o 5 7 4 346.49 332.58 19.54 o 6 7 4 1211.86 1294.07 37.09 o 7 7 4 1816.39 1678.75 43.53 o 8 7 4 279.87 303.58 22.94 o 9 7 4 191.23 186.11 21.50 o 10 7 4 200.30 208.07 22.89 o 11 7 4 19.96 0.02 32.19 o -12 8 4 69.32 116.76 17.73 o -11 8 4 184.88 213.41 22.78 o -10 8 4 21.45 37.21 24.54 o -9 8 4 12.41 10.02 23.51 o -8 8 4 1392.66 1526.97 41.17 o -7 8 4 13.38 0.01 26.25 o -6 8 4 33.83 29.77 11.79 o -5 8 4 61.80 37.46 23.06 o -4 8 4 865.18 815.18 25.54 o -3 8 4 3490.71 3523.42 48.62 o -2 8 4 1154.16 1212.86 27.73 o -1 8 4 1739.25 1406.59 29.63 o 0 8 4 1368.45 1536.11 20.92 o 1 8 4 1440.42 1400.88 29.89 o 2 8 4 997.20 925.49 25.25 o 3 8 4 4658.61 4911.90 58.86 o 4 8 4 2280.88 2242.32 42.65 o 5 8 4 364.34 350.79 20.62 o 6 8 4 3.24 0.01 25.57 o 7 8 4 595.05 572.92 28.90 o 8 8 4 322.93 324.35 26.51 o 9 8 4 1121.16 1054.20 39.94 o 10 8 4 525.52 485.73 31.09 o 11 8 4 51.34 84.48 29.26 o -12 9 4 28.37 0.02 38.74 o -11 9 4 73.19 95.25 21.16 o -10 9 4 55.71 54.58 27.24 o -9 9 4 0.45 0.01 26.26 o -8 9 4 40.69 9.67 30.05 o -7 9 4 1009.45 982.34 32.94 o -6 9 4 149.28 143.51 18.01 o -5 9 4 3.57 32.46 12.92 o -4 9 4 895.19 1134.19 32.43 o -3 9 4 238.99 249.84 17.01 o -2 9 4 17.41 3.22 19.13 o -1 9 4 653.17 745.04 24.19 o 0 9 4 777.42 914.27 17.89 o 1 9 4 325.74 331.49 18.38 o 2 9 4 16.95 11.92 20.07 o 3 9 4 781.61 832.32 26.71 o 4 9 4 104.98 109.29 15.74 o 5 9 4 272.58 285.30 20.13 o 6 9 4 5.65 0.01 23.75 o 7 9 4 4.42 20.34 25.92 o 8 9 4 155.63 131.02 21.38 o 9 9 4 36.24 22.71 32.34 o 10 9 4 8.79 19.23 27.82 o 11 9 4 45.79 6.96 30.58 o -12 10 4 54.58 64.04 36.45 o -11 10 4 166.21 162.95 21.59 o -10 10 4 107.17 84.59 18.48 o -9 10 4 208.24 203.07 22.07 o -8 10 4 17.72 0.01 29.42 o -7 10 4 54.37 85.13 18.16 o -6 10 4 107.38 46.56 30.80 o -5 10 4 273.46 210.20 19.38 o -4 10 4 394.06 510.38 25.16 o -3 10 4 1962.05 1732.85 39.39 o -2 10 4 2998.44 2962.34 47.52 o -1 10 4 2193.34 1915.49 38.20 o 0 10 4 2574.98 2379.56 29.21 o 1 10 4 2822.59 2586.22 45.00 o 2 10 4 4322.78 3653.67 52.89 o 3 10 4 862.26 861.31 29.04 o 4 10 4 1312.26 1419.25 36.38 o 5 10 4 794.22 847.16 31.88 o 6 10 4 485.39 533.87 28.45 o 7 10 4 242.57 302.72 24.28 o 8 10 4 1108.90 1064.60 40.87 o 9 10 4 408.74 376.90 28.59 o 10 10 4 220.55 236.61 23.47 o -11 11 4 2.76 0.02 32.16 o -10 11 4 5.29 0.02 29.40 o -9 11 4 133.07 70.43 33.97 o -8 11 4 847.12 779.79 35.17 o -7 11 4 102.21 62.63 17.42 o -6 11 4 633.18 601.35 28.49 o -5 11 4 201.64 217.49 19.32 o -4 11 4 500.46 573.12 27.81 o -3 11 4 2070.83 2311.82 45.23 o -2 11 4 2281.41 2311.72 45.09 o -1 11 4 1591.08 1438.86 35.45 o 0 11 4 2341.53 1974.09 41.52 o 1 11 4 2077.09 1912.37 40.79 o 2 11 4 858.27 725.24 27.06 o 3 11 4 640.55 585.10 26.33 o 4 11 4 108.57 91.65 16.03 o 5 11 4 371.40 422.12 24.62 o 6 11 4 863.18 938.84 35.24 o 7 11 4 241.21 248.99 22.91 o 8 11 4 182.86 174.96 23.07 o 9 11 4 155.97 166.20 21.33 o 10 11 4 17.13 26.33 29.26 o -11 12 4 76.54 44.43 34.91 o -10 12 4 377.44 336.86 27.14 o -9 12 4 725.70 585.63 31.98 o -8 12 4 699.26 673.16 31.52 o -7 12 4 1886.76 1737.33 47.09 o -6 12 4 2648.75 2690.25 57.46 o -5 12 4 1208.90 1103.69 38.36 o -4 12 4 572.52 646.31 30.30 o -3 12 4 365.15 435.56 24.27 o -2 12 4 83.98 55.39 14.99 o -1 12 4 11.46 0.01 25.03 o 0 12 4 283.84 253.47 21.16 o 1 12 4 330.23 294.74 20.12 o 2 12 4 10.50 21.81 23.92 o 3 12 4 35.45 0.01 27.23 o 4 12 4 131.62 168.15 19.06 o 5 12 4 775.33 750.32 35.01 o 6 12 4 94.45 125.81 19.67 o 7 12 4 1.42 0.01 32.71 o 8 12 4 0.82 0.01 34.39 o 9 12 4 1.07 0.02 35.36 o 10 12 4 2.49 0.02 31.36 o -10 13 4 6.36 0.02 31.18 o -9 13 4 51.34 26.19 33.37 o -8 13 4 0.04 0.98 30.57 o -7 13 4 4.54 5.65 29.71 o -6 13 4 23.92 0.01 31.99 o -5 13 4 26.74 28.34 26.15 o -4 13 4 227.42 251.04 23.46 o -3 13 4 1155.93 1316.40 40.87 o -2 13 4 139.20 115.02 18.65 o -1 13 4 140.42 162.87 15.94 o 0 13 4 1.36 41.30 22.39 o 1 13 4 833.56 778.58 30.84 o 2 13 4 0.74 0.01 28.31 o 3 13 4 7.55 0.01 24.57 o 4 13 4 39.28 31.81 28.71 o 5 13 4 183.66 158.20 22.39 o 6 13 4 197.82 217.27 21.61 o 7 13 4 36.45 0.01 35.50 o 8 13 4 43.33 44.43 31.61 o 9 13 4 6.68 1.17 34.31 o -10 14 4 228.61 184.68 25.69 o -9 14 4 378.74 299.28 30.11 o -8 14 4 637.09 648.72 35.23 o -7 14 4 739.27 709.06 33.90 o -6 14 4 455.08 467.51 28.21 o -5 14 4 627.75 543.41 31.72 o -4 14 4 348.53 421.79 26.29 o -3 14 4 746.17 933.82 35.24 o -2 14 4 458.40 509.02 26.25 o -1 14 4 117.40 145.79 16.55 o 0 14 4 13.10 0.01 28.43 o 1 14 4 591.70 509.75 26.40 o 2 14 4 1.55 0.01 28.89 o 3 14 4 182.67 187.26 20.19 o 4 14 4 17.02 0.01 30.04 o 5 14 4 28.19 1.83 31.31 o 6 14 4 69.79 101.78 22.06 o 7 14 4 17.58 30.81 32.38 o 8 14 4 49.27 49.06 34.48 o -9 15 4 8.27 0.02 30.84 o -8 15 4 5.06 16.17 14.10 o -7 15 4 1.05 0.02 26.44 o -6 15 4 65.51 57.09 18.67 o -5 15 4 19.19 8.08 32.36 o -4 15 4 0.09 14.79 26.18 o -3 15 4 36.29 44.79 27.81 o -2 15 4 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