#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/32/2223259.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2223259_Fobs loop_ _publ_author_name 'Zhan, Cai-Hong' 'Chen, Ling-Xian' 'Feng, Yun-Long' _publ_section_title ; 2-[(2-Carboxyphenyl)sulfanyl]acetic acid ; _journal_coeditor_code AT2858 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2315 _journal_volume 65 _journal_year 2009 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 69.980 _cell_angle_beta 81.959 _cell_angle_gamma 79.732 _cell_length_a 5.1786 _cell_length_b 9.2973 _cell_length_c 10.4776 _exptl_crystal_F_000 220.00 _reflns_d_resolution_high 0.7642 _[local]_cod_data_source_file at2858Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' z in P1 P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 99.42 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 0.65 -0.12 0.12 o 2 0 0 1410.59 1283.54 18.21 o 3 0 0 115.41 107.58 1.89 o 4 0 0 38.66 31.83 0.80 o 5 0 0 58.93 52.66 1.24 o 6 0 0 50.87 49.09 1.55 o -6 1 0 8.78 8.77 0.95 o -5 1 0 0.16 4.24 0.59 o -4 1 0 27.80 21.94 0.59 o -3 1 0 89.93 86.94 1.74 o -2 1 0 216.18 248.31 4.25 o -1 1 0 233.70 222.73 5.16 o 0 1 0 42.93 28.45 0.69 o 1 1 0 1605.02 1476.95 45.69 o 2 1 0 8.52 11.67 0.25 o 3 1 0 0.30 1.62 0.14 o 4 1 0 48.18 44.34 1.05 o 5 1 0 0.79 2.05 0.31 o 6 1 0 53.41 50.20 1.28 o -6 2 0 12.14 13.62 0.82 o -5 2 0 1.60 1.59 0.34 o -4 2 0 146.82 155.30 4.46 o -3 2 0 343.88 348.66 7.60 o -2 2 0 813.58 910.11 17.31 o -1 2 0 2.16 4.91 0.46 o 0 2 0 2891.44 2616.75 74.60 o 1 2 0 418.29 433.33 7.53 o 2 2 0 147.23 145.96 2.13 o 3 2 0 463.10 487.53 7.31 o 4 2 0 1.00 0.19 0.16 o 5 2 0 14.32 15.44 0.57 o 6 2 0 2.71 3.66 0.46 o -6 3 0 6.68 8.31 0.76 o -5 3 0 21.61 27.29 0.92 o -4 3 0 4.27 4.91 0.55 o -3 3 0 2.11 4.27 0.30 o -2 3 0 103.65 98.94 2.01 o -1 3 0 6.11 7.27 0.36 o 0 3 0 417.94 445.47 6.88 o 1 3 0 72.54 82.89 1.26 o 2 3 0 98.65 91.82 1.40 o 3 3 0 210.24 202.97 2.77 o 4 3 0 244.80 206.52 3.66 o 5 3 0 43.29 52.04 1.25 o 6 3 0 0.25 0.17 0.38 o -5 4 0 0.01 0.86 0.52 o -4 4 0 41.96 35.87 1.48 o -3 4 0 27.39 30.27 0.89 o -2 4 0 26.35 11.75 0.33 o -1 4 0 1.87 1.98 0.15 o 0 4 0 213.09 226.99 3.56 o 1 4 0 817.14 863.77 11.62 o 2 4 0 280.32 275.06 3.75 o 3 4 0 85.14 88.64 1.50 o 4 4 0 4.41 3.82 0.38 o 5 4 0 37.43 36.24 1.17 o 6 4 0 3.33 4.64 0.68 o -5 5 0 19.62 17.77 1.30 o -4 5 0 1.38 0.87 0.38 o -3 5 0 0.00 0.19 0.20 o -2 5 0 70.68 58.01 1.29 o -1 5 0 188.33 169.84 2.75 o 0 5 0 53.87 40.10 0.74 o 1 5 0 59.89 80.02 1.34 o 2 5 0 334.20 360.15 5.57 o 3 5 0 21.86 17.94 0.46 o 4 5 0 0.92 4.59 0.56 o 5 5 0 30.79 28.06 1.01 o 6 5 0 2.55 3.12 0.64 o -5 6 0 3.86 2.30 0.77 o -4 6 0 51.81 52.91 1.87 o -3 6 0 117.47 113.62 2.76 o -2 6 0 0.11 0.42 0.24 o -1 6 0 847.64 849.68 12.83 o 0 6 0 0.58 0.47 0.14 o 1 6 0 305.02 301.36 4.68 o 2 6 0 1.71 23.86 1.19 o 3 6 0 52.53 44.22 0.96 o 4 6 0 31.92 30.60 1.04 o 5 6 0 27.25 27.51 1.04 o 6 6 0 1.33 1.20 0.55 o -4 7 0 0.32 0.42 0.54 o -3 7 0 10.05 11.65 0.56 o -2 7 0 7.88 9.24 0.49 o -1 7 0 51.90 57.03 1.33 o 0 7 0 330.58 275.40 4.74 o 1 7 0 24.50 20.45 0.55 o 2 7 0 153.13 142.18 3.22 o 3 7 0 33.71 45.78 2.60 o 4 7 0 0.09 0.00 0.34 o 5 7 0 66.20 63.45 2.19 o -4 8 0 5.43 7.27 1.10 o -3 8 0 30.04 33.81 1.38 o -2 8 0 28.98 25.48 0.86 o -1 8 0 167.95 143.64 2.97 o 0 8 0 48.66 38.93 0.92 o 1 8 0 5.88 6.42 0.35 o 2 8 0 75.88 69.72 1.29 o 3 8 0 17.21 20.59 1.11 o 4 8 0 0.09 0.45 0.40 o 5 8 0 3.07 3.21 0.64 o -3 9 0 1.40 2.56 0.54 o -2 9 0 33.88 37.16 1.55 o -1 9 0 23.01 22.06 0.74 o 0 9 0 18.31 13.43 0.55 o 1 9 0 53.65 52.78 1.34 o 2 9 0 14.86 15.22 0.49 o 3 9 0 42.62 40.63 1.22 o 4 9 0 4.12 27.89 2.63 o -2 10 0 0.14 0.26 0.40 o -1 10 0 14.03 15.16 0.75 o 0 10 0 3.55 4.03 0.51 o 1 10 0 2.89 4.45 0.51 o 2 10 0 0.65 12.01 0.78 o 3 10 0 0.51 0.47 0.28 o 4 10 0 19.56 13.15 1.19 o 0 11 0 0.63 3.03 0.73 o 1 11 0 3.61 3.76 0.52 o 2 11 0 16.57 13.98 0.75 o -1 -11 1 0.17 -0.29 0.46 o 0 -11 1 4.36 5.94 1.02 o -3 -10 1 2.51 3.14 0.52 o -2 -10 1 9.98 18.93 0.82 o -1 -10 1 1.29 1.79 0.41 o 0 -10 1 4.93 6.09 0.59 o 1 -10 1 19.35 23.34 0.97 o -4 -9 1 14.56 27.93 2.69 o -3 -9 1 0.62 2.13 0.40 o -2 -9 1 39.36 38.56 1.02 o -1 -9 1 25.84 36.62 0.94 o 0 -9 1 1.31 2.43 0.37 o 1 -9 1 49.37 39.95 1.12 o 2 -9 1 6.04 7.59 1.07 o 3 -9 1 1.64 1.44 0.66 o -5 -8 1 0.39 1.03 0.50 o -4 -8 1 0.07 0.46 0.41 o -3 -8 1 33.11 35.57 1.92 o -2 -8 1 8.10 6.34 0.36 o -1 -8 1 107.28 98.56 1.94 o 0 -8 1 64.24 62.00 1.32 o 1 -8 1 4.40 3.62 0.38 o 2 -8 1 61.63 59.84 3.68 o 3 -8 1 1.61 3.93 0.60 o -5 -7 1 5.00 6.28 0.95 o -4 -7 1 1.38 2.17 0.81 o -3 -7 1 27.33 17.09 0.55 o -2 -7 1 44.68 35.37 1.07 o -1 -7 1 34.86 30.68 0.72 o 0 -7 1 18.17 16.44 0.50 o 1 -7 1 18.53 15.05 0.54 o 2 -7 1 49.61 44.44 1.63 o 3 -7 1 3.77 4.27 0.48 o 4 -7 1 10.44 9.44 0.75 o -5 -6 1 29.80 33.49 1.17 o -4 -6 1 46.64 49.06 1.80 o -3 -6 1 0.64 1.19 0.24 o -2 -6 1 70.20 82.68 1.61 o -1 -6 1 20.04 21.66 0.55 o 0 -6 1 442.82 418.00 7.09 o 1 -6 1 3.34 23.18 0.87 o 2 -6 1 69.26 59.04 1.97 o 3 -6 1 61.13 56.13 1.56 o 4 -6 1 3.22 4.22 0.59 o 5 -6 1 11.37 10.38 1.11 o -6 -5 1 1.22 2.24 0.57 o -5 -5 1 6.91 9.52 0.88 o -4 -5 1 60.42 55.28 1.51 o -3 -5 1 0.39 0.13 0.17 o -2 -5 1 152.62 135.83 2.46 o -1 -5 1 21.23 24.72 0.58 o 0 -5 1 19.98 20.35 0.51 o 1 -5 1 76.61 69.75 1.34 o 2 -5 1 7.07 9.20 0.43 o 3 -5 1 0.34 0.13 0.22 o 4 -5 1 2.05 4.18 0.44 o 5 -5 1 0.34 0.44 0.53 o -6 -4 1 5.18 8.46 0.84 o -5 -4 1 5.96 5.48 0.52 o -4 -4 1 67.77 60.92 1.43 o -3 -4 1 92.81 77.97 1.48 o -2 -4 1 70.85 74.57 1.29 o -1 -4 1 92.55 92.41 1.55 o 0 -4 1 578.93 687.97 9.79 o 1 -4 1 10.57 12.74 0.32 o 2 -4 1 17.35 18.62 0.62 o 3 -4 1 0.07 0.14 0.18 o 4 -4 1 7.38 8.84 0.48 o 5 -4 1 1.76 2.26 0.66 o -6 -3 1 9.89 9.57 0.70 o -5 -3 1 18.80 19.50 0.65 o -4 -3 1 0.04 1.33 0.22 o -3 -3 1 43.90 34.23 0.71 o -2 -3 1 194.83 242.40 11.83 o -1 -3 1 7.06 6.99 0.21 o 0 -3 1 0.83 -0.09 0.09 o 1 -3 1 587.86 615.41 9.52 o 2 -3 1 34.68 44.36 1.00 o 3 -3 1 56.32 54.13 1.40 o 4 -3 1 15.39 16.85 0.64 o 5 -3 1 21.51 17.71 1.39 o 6 -3 1 1.64 2.49 0.52 o -6 -2 1 0.44 0.40 0.32 o -5 -2 1 0.51 1.17 0.27 o -4 -2 1 93.47 100.18 2.36 o -3 -2 1 119.52 129.56 1.94 o -2 -2 1 29.43 30.66 0.58 o -1 -2 1 204.45 179.59 3.50 o 0 -2 1 443.34 424.49 6.22 o 1 -2 1 1968.57 1848.81 31.61 o 2 -2 1 80.17 97.92 1.99 o 3 -2 1 429.46 421.08 9.16 o 4 -2 1 9.84 19.10 0.92 o 5 -2 1 0.01 0.20 0.26 o 6 -2 1 10.07 9.42 0.69 o -6 -1 1 12.62 14.06 0.75 o -5 -1 1 1.26 1.08 0.28 o -4 -1 1 5.32 13.62 0.76 o -3 -1 1 134.46 124.62 1.86 o -2 -1 1 0.12 0.49 0.08 o -1 -1 1 1826.11 1820.53 50.06 o 0 -1 1 2008.38 1849.88 40.80 o 1 -1 1 2520.52 2307.72 40.91 o 2 -1 1 362.51 366.95 5.71 o 3 -1 1 31.79 33.94 0.78 o 4 -1 1 145.93 130.87 2.32 o 5 -1 1 14.29 12.20 0.59 o 6 -1 1 2.57 2.93 0.54 o -6 0 1 1.80 3.82 0.58 o -5 0 1 13.05 11.53 0.46 o -4 0 1 18.32 22.84 0.63 o -3 0 1 463.73 439.32 7.28 o -2 0 1 11.72 9.71 0.23 o -1 0 1 2052.87 1826.89 42.06 o 0 0 1 512.99 575.84 13.97 o 1 0 1 978.50 849.66 15.28 o 2 0 1 351.19 313.09 4.59 o 3 0 1 4.88 27.19 0.59 o 4 0 1 58.22 55.98 1.11 o 5 0 1 26.02 29.09 0.82 o 6 0 1 9.00 8.90 0.90 o -6 1 1 9.64 9.54 0.78 o -5 1 1 54.93 57.67 1.59 o -4 1 1 0.70 1.19 0.19 o -3 1 1 434.31 423.58 6.40 o -2 1 1 98.07 167.98 2.82 o -1 1 1 69.84 79.57 1.58 o 0 1 1 123.51 109.76 4.86 o 1 1 1 772.79 719.22 14.21 o 2 1 1 14.13 11.50 0.25 o 3 1 1 43.10 56.96 0.87 o 4 1 1 1.52 2.30 0.19 o 5 1 1 97.66 92.87 2.01 o 6 1 1 3.41 4.63 0.46 o -6 2 1 0.09 0.06 0.35 o -5 2 1 3.29 5.55 0.49 o -4 2 1 65.91 63.84 1.62 o -3 2 1 4.59 4.27 0.29 o -2 2 1 147.04 157.83 6.20 o -1 2 1 24.85 25.48 0.78 o 0 2 1 40.29 49.60 2.01 o 1 2 1 7.71 7.60 0.24 o 2 2 1 1.50 7.43 0.19 o 3 2 1 313.79 311.45 4.46 o 4 2 1 1.98 2.11 0.19 o 5 2 1 31.52 30.93 0.88 o 6 2 1 14.07 16.24 0.71 o -6 3 1 8.30 8.95 1.53 o -5 3 1 7.43 6.88 0.76 o -4 3 1 14.04 12.66 0.66 o -3 3 1 17.61 14.41 0.50 o -2 3 1 15.88 16.22 0.38 o -1 3 1 26.07 36.47 1.56 o 0 3 1 527.36 540.07 11.58 o 1 3 1 685.50 667.84 8.99 o 2 3 1 716.76 656.86 9.20 o 3 3 1 6.42 6.78 0.22 o 4 3 1 35.07 32.08 0.64 o 5 3 1 3.19 9.60 0.68 o 6 3 1 29.22 27.62 1.21 o -5 4 1 1.87 1.11 0.33 o -4 4 1 1.36 0.30 0.30 o -3 4 1 36.70 37.21 1.02 o -2 4 1 89.90 86.45 1.99 o -1 4 1 561.59 531.21 13.31 o 0 4 1 703.40 871.78 24.58 o 1 4 1 47.56 57.79 0.92 o 2 4 1 740.16 698.85 9.81 o 3 4 1 119.67 142.19 2.28 o 4 4 1 2.38 3.60 0.29 o 5 4 1 0.19 0.44 0.27 o 6 4 1 0.02 0.28 0.42 o -5 5 1 5.67 6.79 0.95 o -4 5 1 1.61 2.12 0.43 o -3 5 1 44.93 42.65 1.17 o -2 5 1 280.74 295.91 6.29 o -1 5 1 0.01 0.42 0.18 o 0 5 1 182.73 164.35 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0.70 o -1 9 1 1.60 3.16 0.36 o 0 9 1 14.07 14.24 0.43 o 1 9 1 39.66 32.93 0.82 o 2 9 1 0.51 0.10 0.19 o 3 9 1 34.92 30.73 0.86 o 4 9 1 1.63 10.52 1.07 o 5 9 1 11.54 10.41 1.32 o -2 10 1 10.28 11.27 0.83 o -1 10 1 4.86 6.14 0.59 o 0 10 1 6.19 7.69 0.80 o 1 10 1 8.60 7.71 0.41 o 2 10 1 0.02 6.88 0.50 o 3 10 1 5.47 6.02 0.45 o 4 10 1 3.07 3.58 0.56 o -1 11 1 6.89 7.67 1.13 o 0 11 1 1.40 4.87 0.97 o 1 11 1 0.48 -0.02 0.31 o 2 11 1 24.37 17.89 1.30 o 3 11 1 0.07 1.56 0.92 o -3 -10 2 1.98 0.81 0.62 o -2 -10 2 0.65 0.27 0.32 o -1 -10 2 8.33 9.64 0.70 o 0 -10 2 19.43 18.65 0.85 o 1 -10 2 0.03 4.94 0.99 o -4 -9 2 7.37 10.26 0.90 o -3 -9 2 8.70 8.19 0.65 o -2 -9 2 27.45 21.43 0.65 o -1 -9 2 5.34 33.64 1.70 o 0 -9 2 47.49 41.37 1.17 o 1 -9 2 37.26 36.28 1.23 o 2 -9 2 9.53 13.24 1.22 o -4 -8 2 1.54 1.67 0.53 o -3 -8 2 17.17 25.45 1.10 o -2 -8 2 11.34 7.96 0.37 o -1 -8 2 10.82 8.91 0.34 o 0 -8 2 50.69 44.91 1.18 o 1 -8 2 42.58 39.31 1.09 o 2 -8 2 12.38 13.74 1.16 o 3 -8 2 23.16 23.25 1.68 o -5 -7 2 1.07 1.72 0.55 o -4 -7 2 3.49 5.25 0.67 o -3 -7 2 50.36 49.88 1.45 o -2 -7 2 0.71 1.78 0.27 o -1 -7 2 199.01 175.68 2.87 o 0 -7 2 122.61 121.55 2.28 o 1 -7 2 29.59 27.80 0.82 o 2 -7 2 1.60 1.44 0.44 o 3 -7 2 12.51 13.47 0.79 o 4 -7 2 10.27 12.13 1.11 o -5 -6 2 33.00 31.46 1.38 o -4 -6 2 14.29 12.56 0.76 o -3 -6 2 2.63 4.27 0.42 o -2 -6 2 67.78 199.97 8.02 o -1 -6 2 0.39 0.42 0.16 o 0 -6 2 379.71 354.92 5.73 o 1 -6 2 4.77 13.68 0.69 o 2 -6 2 89.91 84.72 2.73 o 3 -6 2 54.54 49.42 1.44 o 4 -6 2 11.98 11.45 0.74 o -5 -5 2 16.19 14.11 0.85 o -4 -5 2 23.26 34.37 0.97 o -3 -5 2 79.19 78.20 1.73 o -2 -5 2 1.45 0.15 0.15 o -1 -5 2 0.37 8.90 0.49 o 0 -5 2 21.25 19.64 0.45 o 1 -5 2 70.97 67.06 1.31 o 2 -5 2 12.76 32.51 1.55 o 3 -5 2 11.51 6.56 0.43 o 4 -5 2 28.07 21.53 0.83 o 5 -5 2 0.35 0.41 0.54 o -6 -4 2 2.68 6.06 1.07 o -5 -4 2 10.67 8.15 0.64 o -4 -4 2 48.14 38.43 1.18 o -3 -4 2 138.47 135.93 2.75 o -2 -4 2 125.65 113.55 1.89 o -1 -4 2 316.70 264.31 4.11 o 0 -4 2 124.88 210.60 4.39 o 1 -4 2 64.00 56.07 1.10 o 2 -4 2 137.34 142.25 3.30 o 3 -4 2 76.03 63.49 1.66 o 4 -4 2 0.41 0.28 0.25 o 5 -4 2 0.60 0.99 0.55 o -6 -3 2 1.20 2.29 0.74 o -5 -3 2 22.01 19.28 0.93 o -4 -3 2 81.90 75.44 1.65 o -3 -3 2 175.81 165.70 2.69 o -2 -3 2 164.40 220.55 8.22 o -1 -3 2 52.68 30.03 0.51 o 0 -3 2 250.32 230.46 3.18 o 1 -3 2 441.92 472.81 6.78 o 2 -3 2 18.56 11.42 0.45 o 3 -3 2 0.60 0.76 0.23 o 4 -3 2 60.90 52.56 1.46 o 5 -3 2 19.84 15.56 0.89 o 6 -3 2 1.51 1.50 0.48 o -6 -2 2 0.27 0.15 0.37 o -5 -2 2 6.65 6.55 0.62 o -4 -2 2 64.19 64.40 1.93 o -3 -2 2 40.00 41.30 0.80 o -2 -2 2 368.44 341.44 4.60 o -1 -2 2 16.57 20.56 0.47 o 0 -2 2 746.27 720.59 11.23 o 1 -2 2 501.07 602.60 13.00 o 2 -2 2 1196.26 1209.36 20.42 o 3 -2 2 274.86 264.50 6.67 o 4 -2 2 8.10 19.50 1.80 o 5 -2 2 48.05 44.47 1.68 o 6 -2 2 2.44 4.69 0.88 o -6 -1 2 0.51 1.20 0.45 o -5 -1 2 5.53 6.02 0.41 o -4 -1 2 0.17 84.85 7.17 o -3 -1 2 191.64 180.86 3.50 o -2 -1 2 914.67 874.69 13.16 o -1 -1 2 2215.87 2143.74 32.74 o 0 -1 2 284.26 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1.20 1.71 0.55 o 0 4 12 23.48 29.73 0.99 o 1 4 12 74.00 67.09 2.19 o 2 4 12 3.43 5.65 0.69 o 3 4 12 12.68 12.52 0.93 o -2 5 12 11.64 13.04 1.02 o -1 5 12 34.36 32.42 1.76 o 0 5 12 8.61 11.68 0.94 o 1 5 12 21.82 23.75 1.22 o 2 5 12 38.13 33.46 1.12 o 3 5 12 0.26 0.54 0.41 o -1 6 12 23.32 20.12 1.28 o 0 6 12 0.28 -0.16 0.35 o 1 6 12 7.00 7.76 0.91 o 2 6 12 14.88 14.58 0.65 o 3 6 12 2.52 2.69 0.59 o -1 7 12 18.64 17.26 1.15 o 0 7 12 12.81 8.26 0.78 o 1 7 12 1.62 1.89 0.57 o 2 7 12 19.27 23.98 0.84 o 3 7 12 35.12 32.96 1.14 o 0 8 12 0.11 0.58 0.42 o 1 8 12 26.89 26.63 1.57 o 2 8 12 4.64 6.37 0.72 o 3 8 12 48.64 52.31 2.69 o 1 9 12 21.16 27.68 1.62 o 2 9 12 26.43 29.08 1.32 o 0 1 13 0.95 1.09 0.79 o 1 1 13 9.54 12.75 1.33 o 0 2 13 0.16 0.42 0.67 o 1 2 13 24.97 27.40 1.85 o 2 2 13 5.15 6.68 1.26 o -1 3 13 8.56 11.21 0.68 o 0 3 13 19.91 17.68 1.32 o 1 3 13 35.85 39.96 2.27 o 2 3 13 18.56 19.72 1.59 o -1 4 13 3.28 6.85 0.94 o 0 4 13 7.40 6.78 1.03 o 1 4 13 6.78 5.79 1.03 o 2 4 13 23.99 24.20 2.03 o -1 5 13 5.48 8.05 0.99 o 0 5 13 0.01 0.02 0.41 o 1 5 13 0.05 0.53 0.63 o 2 5 13 1.54 0.56 0.43 o 0 6 13 0.13 1.29 0.53 o 1 6 13 2.02 2.69 0.68 o 2 6 13 9.05 8.79 0.55 o 1 7 13 1.68 1.76 0.62 o 2 7 13 11.19 9.72 0.75 o