#------------------------------------------------------------------------------ #$Date: 2016-04-03 04:14:40 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181153 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/32/2223280.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2223280_Fobs loop_ _publ_author_name 'Fan, Ping' 'Wang, Lei' 'Zhang, Huidong' _publ_section_title ; Pyridine-4-carboximidamidate chloride ; _journal_coeditor_code BH2242 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2408 _journal_volume 65 _journal_year 2009 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 7.3928 _cell_length_b 10.4467 _cell_length_c 18.9252 _exptl_crystal_F_000 656.00 _reflns_d_resolution_high 0.8107 _cod_data_source_file bh2242Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 1 in Pbca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 173.50 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 3625.04 3495.46 59.48 o 4 0 0 8932.72 9499.11 142.15 o 6 0 0 282.29 270.21 12.83 o 8 0 0 4.51 4.57 3.68 o 2 1 0 14233.58 14070.97 86.20 o 4 1 0 2332.40 2221.41 48.42 o 6 1 0 238.25 240.68 7.01 o 8 1 0 80.17 86.24 4.83 o 0 2 0 4124.46 4408.21 54.86 o 2 2 0 949.75 903.31 33.95 o 4 2 0 2372.45 2463.01 75.12 o 6 2 0 32.19 31.69 4.10 o 8 2 0 6.56 3.50 3.68 o 2 3 0 4582.02 4732.00 83.98 o 4 3 0 5933.90 5704.81 119.04 o 6 3 0 1230.87 1216.80 40.22 o 8 3 0 142.17 152.22 8.28 o 0 4 0 10658.75 11020.24 123.71 o 2 4 0 102.73 89.33 3.55 o 4 4 0 1058.90 1141.26 37.06 o 6 4 0 22.20 18.21 3.74 o 8 4 0 14.94 13.90 5.59 o 2 5 0 582.03 575.67 22.19 o 4 5 0 3.67 -2.61 2.61 o 6 5 0 21.50 18.42 4.65 o 8 5 0 11.08 22.34 5.98 o 0 6 0 1735.81 1722.66 60.67 o 2 6 0 199.21 163.00 6.17 o 4 6 0 622.02 683.06 28.22 o 6 6 0 180.42 177.73 8.15 o 8 6 0 2.58 -0.42 7.79 o 2 7 0 39.81 33.86 4.94 o 4 7 0 245.77 224.73 11.66 o 6 7 0 28.24 24.90 4.78 o 0 8 0 704.20 633.28 27.00 o 2 8 0 12.07 7.63 3.16 o 4 8 0 20.40 10.63 4.21 o 6 8 0 23.72 22.99 4.83 o 2 9 0 3851.95 3906.85 124.26 o 4 9 0 25.56 28.69 5.64 o 6 9 0 6.21 2.27 5.36 o 0 10 0 997.68 1043.25 42.60 o 2 10 0 19.96 26.81 4.99 o 4 10 0 413.64 414.61 18.22 o 2 11 0 247.53 237.96 9.54 o 4 11 0 68.12 69.69 6.95 o 0 12 0 385.17 387.68 17.54 o 2 12 0 570.70 571.11 22.85 o 1 1 1 314.26 262.23 3.13 o 2 1 1 30102.97 29587.27 92.01 o 3 1 1 1905.04 1845.18 27.29 o 4 1 1 251.15 291.75 5.26 o 5 1 1 327.69 362.59 6.99 o 6 1 1 240.34 246.53 4.99 o 7 1 1 371.82 368.77 8.34 o 8 1 1 3.05 4.98 2.40 o 9 1 1 44.66 42.82 3.29 o 0 2 1 37.27 48.37 3.87 o 1 2 1 401.85 486.77 7.42 o 2 2 1 6385.60 6351.78 95.52 o 3 2 1 302.11 266.95 7.53 o 4 2 1 1896.72 1997.08 51.31 o 5 2 1 32.60 27.74 2.75 o 6 2 1 396.51 380.21 9.41 o 7 2 1 438.79 466.03 14.30 o 8 2 1 168.60 142.38 10.17 o 9 2 1 55.22 49.93 4.71 o 1 3 1 106.54 109.29 2.43 o 2 3 1 189.89 196.47 4.98 o 3 3 1 2191.17 2229.51 46.83 o 4 3 1 41.99 51.34 7.20 o 5 3 1 7.80 11.66 2.11 o 6 3 1 1.37 2.16 2.14 o 7 3 1 3.19 -0.85 2.75 o 8 3 1 19.66 21.01 5.66 o 0 4 1 2225.09 2430.68 40.80 o 1 4 1 6731.94 6761.38 92.66 o 2 4 1 17.20 21.93 1.72 o 3 4 1 67.84 69.82 3.67 o 4 4 1 71.14 81.50 3.13 o 5 4 1 1340.88 1334.25 49.24 o 6 4 1 145.99 146.51 5.02 o 7 4 1 82.48 86.30 11.00 o 8 4 1 16.52 12.34 3.13 o 1 5 1 166.24 144.26 2.75 o 2 5 1 1670.39 1689.40 98.67 o 3 5 1 3604.99 3596.44 79.19 o 4 5 1 129.00 138.70 4.16 o 5 5 1 13.93 14.24 2.80 o 6 5 1 3.80 10.73 3.02 o 7 5 1 97.54 99.24 5.06 o 8 5 1 15.74 9.96 3.71 o 0 6 1 32.52 37.22 4.44 o 1 6 1 9.63 6.75 1.16 o 2 6 1 0.06 -0.59 1.76 o 3 6 1 19.86 17.85 2.19 o 4 6 1 86.23 88.12 3.93 o 5 6 1 46.10 48.07 3.38 o 6 6 1 132.83 130.55 4.99 o 7 6 1 65.81 64.10 6.28 o 8 6 1 3.67 -2.03 3.24 o 1 7 1 891.57 879.65 16.39 o 2 7 1 0.05 1.44 3.67 o 3 7 1 756.53 724.72 35.95 o 4 7 1 182.17 174.20 5.24 o 5 7 1 279.90 293.55 10.57 o 6 7 1 73.11 75.16 4.81 o 7 7 1 107.33 120.11 9.26 o 0 8 1 532.90 508.66 14.64 o 1 8 1 1172.20 1143.60 20.86 o 2 8 1 14.68 13.80 2.36 o 3 8 1 2.08 1.30 2.27 o 4 8 1 192.92 192.53 5.76 o 5 8 1 487.84 509.04 15.06 o 6 8 1 9.13 7.58 4.70 o 7 8 1 124.99 127.16 5.89 o 1 9 1 374.24 360.18 8.20 o 2 9 1 168.38 176.87 5.64 o 3 9 1 9.80 11.88 2.99 o 4 9 1 19.69 16.45 2.92 o 5 9 1 0.00 3.04 3.06 o 6 9 1 103.07 103.93 5.43 o 0 10 1 1197.70 1192.54 31.83 o 1 10 1 49.30 52.98 3.25 o 2 10 1 75.62 75.69 4.19 o 3 10 1 68.86 68.69 4.64 o 4 10 1 99.34 101.42 5.28 o 5 10 1 208.33 208.63 7.05 o 1 11 1 122.24 124.92 3.76 o 2 11 1 252.35 264.89 8.20 o 3 11 1 90.07 80.31 10.62 o 4 11 1 155.11 159.27 6.43 o 0 12 1 112.80 124.65 6.00 o 1 12 1 5.01 7.54 3.02 o 2 12 1 2.13 2.15 6.01 o 3 12 1 21.27 27.29 5.37 o 0 0 2 51.01 35.43 1.54 o 1 0 2 2124.15 1915.78 24.72 o 2 0 2 5634.37 5554.08 76.40 o 3 0 2 8604.30 8771.57 116.02 o 4 0 2 44.45 52.36 3.32 o 5 0 2 2909.74 2783.34 89.67 o 6 0 2 1099.15 1082.09 37.91 o 7 0 2 35.30 34.96 6.22 o 8 0 2 35.03 36.55 5.20 o 9 0 2 10.84 7.89 4.31 o 1 1 2 1924.58 1738.80 17.81 o 2 1 2 7438.57 7249.82 131.72 o 3 1 2 90.44 76.10 3.58 o 4 1 2 6.82 42.01 25.20 o 5 1 2 89.07 92.45 3.48 o 6 1 2 48.23 45.43 4.99 o 7 1 2 1.67 6.14 5.47 o 8 1 2 9.54 6.04 4.22 o 9 1 2 81.16 58.23 10.07 o 0 2 2 2056.77 1896.32 39.21 o 1 2 2 1567.62 1551.26 68.27 o 2 2 2 18.55 19.47 2.01 o 3 2 2 25.16 19.13 2.17 o 4 2 2 194.57 199.28 8.60 o 5 2 2 168.67 170.48 7.95 o 6 2 2 57.26 52.81 6.74 o 7 2 2 60.05 56.20 5.67 o 8 2 2 23.81 22.13 5.33 o 1 3 2 4955.24 4989.18 55.51 o 2 3 2 2724.97 2720.95 63.51 o 3 3 2 40.11 23.18 2.56 o 4 3 2 194.54 166.48 8.68 o 5 3 2 249.17 252.24 12.42 o 6 3 2 1.80 4.65 3.50 o 7 3 2 15.08 40.91 5.25 o 8 3 2 40.65 44.00 5.88 o 0 4 2 95.84 91.00 3.42 o 1 4 2 5.36 17.27 3.27 o 2 4 2 1677.93 1728.62 56.74 o 3 4 2 61.83 80.06 3.89 o 4 4 2 112.50 116.63 4.99 o 5 4 2 17.66 13.95 3.58 o 6 4 2 473.92 451.19 20.00 o 7 4 2 43.45 49.85 5.46 o 8 4 2 10.57 3.76 4.60 o 1 5 2 347.41 392.79 10.79 o 2 5 2 185.63 243.90 8.57 o 3 5 2 490.43 448.13 17.08 o 4 5 2 295.79 292.50 9.57 o 5 5 2 17.16 14.68 3.50 o 6 5 2 34.19 31.77 4.73 o 7 5 2 14.45 13.19 5.12 o 8 5 2 28.24 27.85 6.06 o 0 6 2 721.64 597.96 22.82 o 1 6 2 983.62 906.53 31.66 o 2 6 2 111.44 101.50 4.57 o 3 6 2 1.64 -1.49 2.19 o 4 6 2 122.23 117.70 6.04 o 5 6 2 218.80 209.72 11.40 o 6 6 2 223.49 240.65 12.36 o 7 6 2 109.60 128.72 7.73 o 8 6 2 0.15 3.21 4.36 o 1 7 2 164.85 170.64 6.27 o 2 7 2 67.07 63.34 4.31 o 3 7 2 179.81 190.06 10.17 o 4 7 2 22.96 40.42 4.34 o 5 7 2 8.80 8.73 3.50 o 6 7 2 3.10 0.08 5.28 o 7 7 2 20.23 13.32 5.02 o 0 8 2 3255.73 3263.01 100.90 o 1 8 2 10.95 9.51 2.37 o 2 8 2 2.85 11.50 3.27 o 3 8 2 244.59 227.84 9.28 o 4 8 2 429.04 444.51 19.35 o 5 8 2 89.71 84.63 6.74 o 6 8 2 7.05 2.66 4.91 o 7 8 2 53.68 44.94 7.19 o 1 9 2 472.27 457.40 12.84 o 2 9 2 227.95 236.61 9.46 o 3 9 2 539.52 562.98 23.17 o 4 9 2 270.43 269.79 9.57 o 5 9 2 161.45 154.00 8.34 o 6 9 2 26.36 23.78 5.57 o 0 10 2 34.67 35.95 4.70 o 1 10 2 60.29 59.20 3.72 o 2 10 2 8.50 5.56 3.79 o 3 10 2 1.87 8.52 4.55 o 4 10 2 70.05 65.66 6.45 o 5 10 2 1.20 -1.31 4.96 o 1 11 2 89.36 100.76 5.35 o 2 11 2 119.89 122.58 7.53 o 3 11 2 4.22 -0.65 6.56 o 4 11 2 251.98 269.82 13.83 o 0 12 2 463.05 470.65 17.75 o 1 12 2 96.68 93.17 12.12 o 2 12 2 36.16 30.13 5.88 o 3 12 2 42.32 34.85 6.58 o 1 1 3 7811.23 7748.31 40.30 o 2 1 3 841.06 863.48 23.89 o 3 1 3 314.11 317.58 16.57 o 4 1 3 768.80 752.88 19.37 o 5 1 3 230.60 240.98 6.26 o 6 1 3 4.08 5.14 2.62 o 7 1 3 1.16 3.64 2.80 o 8 1 3 39.95 37.18 3.94 o 9 1 3 13.26 12.93 3.74 o 0 2 3 13608.98 14309.48 114.42 o 1 2 3 349.17 421.77 10.47 o 2 2 3 1076.44 975.41 36.81 o 3 2 3 15.35 16.38 2.33 o 4 2 3 2539.06 2498.75 77.68 o 5 2 3 1308.89 1332.01 66.93 o 6 2 3 9.66 9.88 3.63 o 7 2 3 144.74 138.47 8.57 o 8 2 3 2.86 6.04 4.76 o 1 3 3 6.03 7.57 1.23 o 2 3 3 169.03 176.32 5.78 o 3 3 3 70.80 74.11 3.61 o 4 3 3 873.57 947.27 32.10 o 5 3 3 116.71 131.86 5.64 o 6 3 3 369.70 356.09 14.04 o 7 3 3 1.43 1.20 3.66 o 8 3 3 14.81 16.56 4.73 o 0 4 3 1548.12 1329.94 44.71 o 1 4 3 3581.67 3771.33 54.85 o 2 4 3 43.69 36.29 2.77 o 3 4 3 238.54 253.76 12.50 o 4 4 3 26.68 19.99 3.50 o 5 4 3 456.04 470.08 19.45 o 6 4 3 389.97 416.02 17.54 o 7 4 3 30.49 36.84 5.28 o 8 4 3 0.57 -1.78 4.68 o 1 5 3 3323.54 3653.63 102.95 o 2 5 3 661.67 648.61 24.34 o 3 5 3 1012.79 1004.77 37.21 o 4 5 3 605.82 542.31 21.58 o 5 5 3 0.19 1.38 3.00 o 6 5 3 0.85 -0.16 3.32 o 7 5 3 71.24 78.88 6.90 o 8 5 3 272.19 248.47 16.44 o 0 6 3 1573.76 1785.32 64.78 o 1 6 3 3.63 5.60 1.96 o 2 6 3 855.65 834.06 29.32 o 3 6 3 1.30 3.03 2.93 o 4 6 3 105.28 97.76 5.44 o 5 6 3 0.31 7.47 3.58 o 6 6 3 25.30 29.63 4.60 o 7 6 3 2.06 -3.71 4.47 o 1 7 3 159.03 159.09 4.86 o 2 7 3 2242.91 2127.25 80.99 o 3 7 3 1462.56 1449.29 70.68 o 4 7 3 103.35 98.15 6.04 o 5 7 3 19.25 18.00 4.08 o 6 7 3 191.54 186.23 8.94 o 7 7 3 53.04 51.66 6.64 o 0 8 3 491.10 447.18 18.83 o 1 8 3 1282.06 1267.98 31.18 o 2 8 3 97.58 101.02 6.61 o 3 8 3 253.73 276.54 9.28 o 4 8 3 286.38 276.15 10.90 o 5 8 3 152.92 162.15 9.07 o 6 8 3 8.20 6.27 4.99 o 7 8 3 15.29 10.01 7.21 o 1 9 3 17.97 9.69 5.85 o 2 9 3 1295.67 1278.68 45.58 o 3 9 3 118.00 107.27 6.92 o 4 9 3 101.53 91.12 6.51 o 5 9 3 17.64 20.82 5.15 o 6 9 3 11.16 5.38 5.57 o 0 10 3 1189.08 1209.39 46.04 o 1 10 3 217.27 225.90 8.32 o 2 10 3 75.42 81.50 5.93 o 3 10 3 234.15 230.49 9.12 o 4 10 3 244.38 255.55 10.17 o 5 10 3 1.23 1.54 4.55 o 1 11 3 0.73 -1.14 3.04 o 2 11 3 247.59 240.32 10.35 o 3 11 3 265.52 255.71 13.64 o 4 11 3 40.06 48.62 6.82 o 0 12 3 3.64 6.09 4.57 o 1 12 3 19.69 19.52 3.59 o 2 12 3 9.25 13.51 4.52 o 3 12 3 20.16 24.53 5.70 o 0 0 4 278.65 303.72 9.61 o 1 0 4 5429.20 5705.57 50.88 o 2 0 4 10189.15 9714.58 111.32 o 3 0 4 649.06 645.68 24.43 o 4 0 4 1529.39 1460.68 57.51 o 5 0 4 1117.63 1148.59 41.53 o 6 0 4 416.28 431.56 19.24 o 7 0 4 146.94 159.28 9.22 o 8 0 4 6.84 1.41 3.71 o 1 1 4 920.31 847.39 15.08 o 2 1 4 100.58 129.34 2.66 o 3 1 4 1949.73 1962.29 41.51 o 4 1 4 2022.76 1944.76 56.83 o 5 1 4 2.01 0.04 1.93 o 6 1 4 4.50 5.11 2.40 o 7 1 4 208.04 199.55 10.36 o 8 1 4 79.35 59.11 4.50 o 0 2 4 1771.34 1632.20 41.07 o 1 2 4 3466.48 3401.13 45.32 o 2 2 4 223.37 220.92 8.63 o 3 2 4 331.50 339.87 12.95 o 4 2 4 44.51 54.69 3.66 o 5 2 4 348.24 374.97 10.75 o 6 2 4 66.05 61.95 5.15 o 7 2 4 14.01 25.37 5.02 o 8 2 4 60.38 48.10 5.98 o 1 3 4 5080.58 5229.40 60.31 o 2 3 4 122.97 112.49 3.82 o 3 3 4 5144.04 5109.43 101.89 o 4 3 4 49.68 56.75 3.81 o 5 3 4 1.02 -0.73 2.69 o 6 3 4 103.81 104.29 6.04 o 7 3 4 434.81 423.11 14.33 o 8 3 4 218.30 206.80 9.51 o 0 4 4 2048.66 2233.93 59.42 o 1 4 4 2572.34 2596.09 65.01 o 2 4 4 153.00 168.95 6.25 o 3 4 4 1000.38 986.61 33.58 o 4 4 4 1.79 3.40 2.43 o 5 4 4 167.49 164.49 7.71 o 6 4 4 1.39 7.03 3.58 o 7 4 4 37.13 43.61 6.27 o 8 4 4 44.29 40.21 5.93 o 1 5 4 2419.60 2594.48 51.68 o 2 5 4 68.96 81.53 4.00 o 3 5 4 775.93 766.30 25.33 o 4 5 4 212.49 235.71 10.85 o 5 5 4 0.22 5.59 3.27 o 6 5 4 5.03 1.49 3.11 o 7 5 4 5.21 12.78 5.15 o 8 5 4 0.57 1.88 4.89 o 0 6 4 53.75 71.15 3.95 o 1 6 4 5805.02 6182.31 86.36 o 2 6 4 10.88 12.33 2.64 o 3 6 4 377.27 462.32 19.87 o 4 6 4 19.78 22.18 3.81 o 5 6 4 1729.87 1650.27 56.46 o 6 6 4 0.17 -4.00 4.00 o 7 6 4 7.63 4.18 4.47 o 1 7 4 908.18 910.84 22.66 o 2 7 4 85.64 85.63 5.25 o 3 7 4 1333.13 1354.88 48.35 o 4 7 4 79.02 79.57 5.64 o 5 7 4 4.34 5.96 4.31 o 6 7 4 39.40 39.30 5.17 o 7 7 4 93.80 90.91 8.54 o 0 8 4 1907.89 1882.64 80.52 o 1 8 4 45.20 44.35 3.06 o 2 8 4 462.19 479.34 19.53 o 3 8 4 68.51 68.67 5.46 o 4 8 4 238.73 212.44 8.42 o 5 8 4 228.94 228.29 9.30 o 6 8 4 150.51 126.03 7.89 o 1 9 4 794.83 832.15 27.60 o 2 9 4 139.70 127.34 7.60 o 3 9 4 809.46 848.09 34.03 o 4 9 4 252.76 240.32 10.40 o 5 9 4 14.56 19.26 4.76 o 6 9 4 2.25 6.90 4.99 o 0 10 4 101.02 97.60 6.22 o 1 10 4 237.19 232.30 6.67 o 2 10 4 0.07 1.15 3.84 o 3 10 4 13.18 6.19 4.62 o 4 10 4 78.42 77.60 7.21 o 5 10 4 312.14 282.26 16.31 o 1 11 4 52.64 49.15 4.89 o 2 11 4 50.40 42.80 5.23 o 3 11 4 8.41 5.72 4.36 o 4 11 4 7.92 14.37 5.56 o 0 12 4 188.44 192.63 10.51 o 1 12 4 168.16 183.41 7.12 o 2 12 4 1.95 7.66 4.70 o 1 1 5 154.48 152.76 2.56 o 2 1 5 9223.57 8997.06 80.52 o 3 1 5 210.45 219.19 4.96 o 4 1 5 2900.60 2862.64 58.80 o 5 1 5 130.79 148.50 7.11 o 6 1 5 349.57 348.51 24.56 o 7 1 5 54.70 50.44 9.50 o 8 1 5 209.68 197.50 13.42 o 0 2 5 12324.07 12043.77 121.86 o 1 2 5 1422.45 1474.57 30.76 o 2 2 5 1617.37 1762.60 51.86 o 3 2 5 51.64 55.13 3.27 o 4 2 5 241.62 246.95 10.30 o 5 2 5 226.83 248.47 9.44 o 6 2 5 1600.01 1519.09 52.76 o 7 2 5 119.44 127.21 7.40 o 8 2 5 21.75 24.90 6.87 o 1 3 5 3864.55 4006.27 64.17 o 2 3 5 617.09 709.28 24.03 o 3 3 5 8.60 10.76 2.43 o 4 3 5 1.76 5.04 2.64 o 5 3 5 166.06 173.82 7.79 o 6 3 5 20.28 6.32 4.26 o 7 3 5 0.01 5.30 4.91 o 8 3 5 14.88 15.96 5.17 o 0 4 5 261.47 191.11 7.11 o 1 4 5 191.44 195.35 5.26 o 2 4 5 654.34 589.95 22.87 o 3 4 5 353.56 357.63 11.90 o 4 4 5 238.84 218.26 9.36 o 5 4 5 32.13 37.18 4.21 o 6 4 5 493.62 504.64 23.38 o 7 4 5 70.57 72.33 6.24 o 8 4 5 5.71 11.37 4.55 o 1 5 5 195.97 245.15 6.67 o 2 5 5 889.18 757.10 27.99 o 3 5 5 1092.89 1084.65 36.58 o 4 5 5 412.97 403.69 14.90 o 5 5 5 308.15 280.38 13.23 o 6 5 5 8.05 11.18 3.68 o 7 5 5 41.31 47.27 6.11 o 8 5 5 87.65 76.53 7.34 o 0 6 5 492.21 560.24 23.12 o 1 6 5 16.27 11.37 1.98 o 2 6 5 206.91 210.15 8.73 o 3 6 5 150.21 176.82 7.94 o 4 6 5 0.74 2.87 3.34 o 5 6 5 623.54 655.32 26.07 o 6 6 5 57.77 57.74 6.53 o 7 6 5 131.06 123.34 8.07 o 1 7 5 0.63 3.71 2.20 o 2 7 5 93.36 87.64 5.07 o 3 7 5 3.10 8.49 3.50 o 4 7 5 331.10 323.21 10.61 o 5 7 5 18.06 24.38 4.99 o 6 7 5 27.08 19.52 5.72 o 7 7 5 49.24 53.04 7.79 o 0 8 5 110.21 118.40 5.93 o 1 8 5 95.47 115.13 4.06 o 2 8 5 280.14 270.54 11.40 o 3 8 5 91.37 100.52 5.77 o 4 8 5 73.39 71.70 5.67 o 5 8 5 5.32 11.86 3.97 o 6 8 5 376.54 379.71 13.91 o 1 9 5 334.60 363.35 22.05 o 2 9 5 286.61 260.00 11.08 o 3 9 5 13.70 28.06 4.89 o 4 9 5 188.82 180.30 8.42 o 5 9 5 32.48 37.70 5.43 o 6 9 5 16.59 8.54 6.51 o 0 10 5 613.06 649.75 28.66 o 1 10 5 1.21 4.80 5.29 o 2 10 5 216.64 197.55 8.60 o 3 10 5 28.88 26.23 5.02 o 4 10 5 113.39 125.69 8.13 o 5 10 5 1.51 10.01 4.60 o 1 11 5 14.19 17.59 3.33 o 2 11 5 756.34 783.41 30.99 o 3 11 5 22.19 10.40 5.57 o 4 11 5 67.78 55.63 6.87 o 0 12 5 0.88 2.19 4.05 o 1 12 5 2.78 10.87 4.08 o 2 12 5 13.07 14.71 4.44 o 0 0 6 10620.53 10637.46 111.99 o 1 0 6 2870.77 2823.45 104.28 o 2 0 6 69.27 69.38 3.42 o 3 0 6 2345.79 2595.79 71.14 o 4 0 6 1917.45 1883.96 67.81 o 5 0 6 52.53 49.10 4.05 o 6 0 6 20.09 20.14 3.68 o 7 0 6 29.45 36.37 6.53 o 8 0 6 50.31 33.21 5.17 o 1 1 6 2100.70 2085.82 26.57 o 2 1 6 721.02 671.00 15.71 o 3 1 6 140.41 142.67 4.17 o 4 1 6 82.61 100.07 3.31 o 5 1 6 16.74 18.18 3.61 o 6 1 6 5.05 3.83 2.62 o 7 1 6 5.04 6.33 3.83 o 8 1 6 64.71 53.49 4.27 o 0 2 6 607.83 530.41 18.12 o 1 2 6 3313.74 3324.83 48.64 o 2 2 6 352.34 374.96 14.99 o 3 2 6 198.60 180.73 7.08 o 4 2 6 140.78 153.59 6.27 o 5 2 6 350.19 337.73 14.20 o 6 2 6 180.06 179.46 7.63 o 7 2 6 12.73 13.06 4.28 o 8 2 6 0.08 -5.09 5.88 o 1 3 6 127.96 118.61 5.95 o 2 3 6 0.52 15.34 2.25 o 3 3 6 2783.36 2614.00 79.42 o 4 3 6 1102.34 1076.68 38.26 o 5 3 6 0.35 1.54 3.03 o 6 3 6 2.72 5.96 3.50 o 7 3 6 73.92 80.24 6.11 o 8 3 6 194.25 170.65 8.91 o 0 4 6 8.22 4.83 1.88 o 1 4 6 181.39 219.44 6.55 o 2 4 6 52.48 55.45 3.50 o 3 4 6 273.20 295.44 8.76 o 4 4 6 90.69 84.17 4.73 o 5 4 6 112.99 120.96 6.11 o 6 4 6 0.35 1.44 3.19 o 7 4 6 2.20 8.62 3.71 o 8 4 6 0.34 1.91 4.55 o 1 5 6 89.66 98.16 3.37 o 2 5 6 13.85 8.67 2.51 o 3 5 6 1748.69 1715.18 73.26 o 4 5 6 285.71 292.33 10.38 o 5 5 6 73.66 81.32 5.57 o 6 5 6 5.35 -3.24 4.44 o 7 5 6 134.73 144.35 8.39 o 8 5 6 15.20 19.93 5.77 o 0 6 6 189.03 158.52 6.82 o 1 6 6 1978.65 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9 8 126.23 136.48 5.89 o 2 9 8 403.15 443.95 18.59 o 3 9 8 168.85 151.65 7.84 o 4 9 8 370.83 381.10 14.98 o 5 9 8 5.64 -2.01 7.11 o 0 10 8 11.26 10.45 3.92 o 1 10 8 167.36 154.49 5.58 o 2 10 8 103.70 99.58 8.54 o 3 10 8 57.74 50.09 6.11 o 4 10 8 32.18 26.73 5.62 o 1 11 8 76.02 67.46 4.90 o 2 11 8 0.62 7.42 4.42 o 3 11 8 1.18 -1.31 6.17 o 0 12 8 466.91 516.99 21.93 o 1 12 8 7.90 9.47 3.69 o 1 1 9 1173.24 1107.90 23.73 o 2 1 9 1831.31 1879.79 46.70 o 3 1 9 2667.94 2675.31 57.97 o 4 1 9 67.37 77.79 8.19 o 5 1 9 11.21 17.68 2.80 o 6 1 9 1.02 0.50 4.40 o 7 1 9 122.67 126.95 5.10 o 8 1 9 21.22 19.29 3.65 o 0 2 9 5.85 6.22 1.93 o 1 2 9 3563.44 3685.11 69.93 o 2 2 9 256.74 273.77 9.70 o 3 2 9 68.20 88.48 4.63 o 4 2 9 115.91 121.88 6.06 o 5 2 9 1328.58 1233.72 45.80 o 6 2 9 107.98 105.12 7.00 o 7 2 9 72.98 77.24 6.45 o 8 2 9 9.20 14.74 5.09 o 1 3 9 159.48 164.26 5.04 o 2 3 9 105.63 120.60 4.81 o 3 3 9 844.42 853.65 32.25 o 4 3 9 243.13 252.47 10.80 o 5 3 9 132.16 134.32 6.98 o 6 3 9 75.48 73.92 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52.43 55.98 4.39 o 2 9 9 0.01 -3.27 3.27 o 3 9 9 62.41 59.57 5.59 o 4 9 9 77.07 66.26 6.51 o 5 9 9 0.13 -0.13 4.65 o 0 10 9 139.30 155.69 8.62 o 1 10 9 333.51 335.51 18.91 o 2 10 9 7.10 7.76 4.13 o 3 10 9 25.22 16.33 7.29 o 4 10 9 20.54 19.70 5.46 o 1 11 9 141.58 113.27 5.62 o 2 11 9 2.03 -3.84 3.84 o 3 11 9 196.65 187.56 9.96 o 0 0 10 5437.73 5641.83 104.12 o 1 0 10 2374.80 2513.97 51.11 o 2 0 10 799.51 805.23 29.29 o 3 0 10 85.75 83.75 4.73 o 4 0 10 1597.08 1568.18 71.81 o 5 0 10 169.56 170.84 7.27 o 6 0 10 159.94 154.08 7.37 o 7 0 10 68.75 73.42 6.64 o 8 0 10 2.53 4.21 3.97 o 1 1 10 1042.97 1161.27 25.55 o 2 1 10 1.43 8.75 1.73 o 3 1 10 220.05 234.28 12.56 o 4 1 10 966.25 977.87 25.08 o 5 1 10 154.57 153.21 5.55 o 6 1 10 15.41 14.79 4.23 o 7 1 10 32.96 32.98 4.31 o 8 1 10 22.97 21.08 5.06 o 0 2 10 5083.11 5266.45 105.74 o 1 2 10 14.37 21.89 2.09 o 2 2 10 40.26 53.88 3.48 o 3 2 10 176.93 196.99 10.43 o 4 2 10 573.77 604.70 24.90 o 5 2 10 20.17 22.68 4.05 o 6 2 10 19.68 36.66 4.76 o 7 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6 7 10 9.13 1.93 4.73 o 0 8 10 4.28 8.02 3.71 o 1 8 10 73.61 70.23 3.92 o 2 8 10 204.00 199.30 10.35 o 3 8 10 60.05 52.05 5.59 o 4 8 10 9.26 19.07 4.10 o 5 8 10 31.58 27.83 5.64 o 1 9 10 70.51 70.19 4.17 o 2 9 10 452.68 450.82 17.80 o 3 9 10 66.58 54.92 6.32 o 4 9 10 227.86 221.99 11.50 o 5 9 10 1.43 2.43 4.91 o 0 10 10 60.54 50.69 6.66 o 1 10 10 5.75 3.68 8.33 o 2 10 10 43.50 36.34 5.93 o 3 10 10 2.83 0.34 4.39 o 4 10 10 70.30 56.54 7.60 o 1 11 10 3.68 7.05 3.28 o 2 11 10 486.49 541.45 17.99 o 1 1 11 112.50 84.57 2.17 o 2 1 11 1237.74 1196.85 40.44 o 3 1 11 714.55 682.76 18.22 o 4 1 11 0.18 1.61 2.13 o 5 1 11 76.92 75.32 5.07 o 6 1 11 99.62 90.50 4.45 o 7 1 11 131.22 134.65 9.81 o 8 1 11 2.11 -1.50 2.78 o 0 2 11 0.85 -0.71 2.30 o 1 2 11 339.95 295.98 8.10 o 2 2 11 0.63 1.54 2.30 o 3 2 11 0.13 3.32 3.50 o 4 2 11 11.19 12.93 4.52 o 5 2 11 276.26 288.28 12.62 o 6 2 11 63.93 66.47 6.66 o 7 2 11 2.10 5.88 5.20 o 1 3 11 55.34 76.98 3.12 o 2 3 11 9.01 12.65 2.77 o 3 3 11 216.77 230.79 11.58 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4 18 67.17 56.75 6.19 o 3 4 18 21.28 27.02 5.46 o 4 4 18 33.36 34.15 5.43 o 5 4 18 13.06 16.46 6.87 o 1 5 18 0.14 -0.70 2.55 o 2 5 18 176.71 191.74 9.77 o 3 5 18 10.56 5.80 5.54 o 4 5 18 117.34 124.72 7.94 o 0 6 18 815.62 870.27 35.28 o 1 6 18 11.80 17.80 6.09 o 2 6 18 251.84 263.81 12.10 o 3 6 18 1.22 5.02 4.73 o 1 7 18 0.98 0.08 2.88 o 2 7 18 421.34 423.09 16.49 o 3 7 18 19.57 32.42 5.67 o 0 8 18 36.79 37.23 5.41 o 1 8 18 2.68 6.16 3.13 o 1 1 19 333.01 322.76 6.67 o 2 1 19 0.07 -1.01 3.73 o 3 1 19 80.43 90.78 5.24 o 4 1 19 11.48 13.63 3.36 o 5 1 19 36.12 40.29 5.33 o 0 2 19 18.02 12.02 3.87 o 1 2 19 291.08 299.56 15.43 o 2 2 19 62.04 66.47 7.11 o 3 2 19 41.75 39.40 5.23 o 4 2 19 19.31 29.29 4.76 o 5 2 19 208.77 198.09 13.88 o 1 3 19 182.83 174.02 6.35 o 2 3 19 49.80 45.15 6.01 o 3 3 19 34.99 31.48 4.91 o 4 3 19 23.86 21.95 4.83 o 0 4 19 128.36 141.87 8.31 o 1 4 19 51.37 58.13 4.52 o 2 4 19 6.56 6.87 4.78 o 3 4 19 15.57 6.69 4.00 o 4 4 19 19.96 23.54 5.04 o 1 5 19 57.87 58.93 4.37 o 2 5 19 81.66 78.75 6.64 o 3 5 19 267.48 276.93 10.87 o 0 6 19 288.81 292.78 12.21 o 1 6 19 18.50 22.05 4.31 o 2 6 19 14.63 15.23 4.99 o 3 6 19 35.23 43.76 6.38 o 1 7 19 157.69 149.37 6.33 o 0 0 20 283.38 267.10 13.17 o 1 0 20 194.95 176.66 5.82 o 2 0 20 43.01 30.33 4.86 o 3 0 20 37.88 43.19 5.83 o 4 0 20 186.77 174.31 9.33 o 1 1 20 1.58 1.46 2.35 o 2 1 20 86.44 69.00 5.05 o 3 1 20 163.17 145.92 5.86 o 4 1 20 17.69 16.11 3.86 o 0 2 20 42.29 34.78 4.86 o 1 2 20 6.88 5.56 7.89 o 2 2 20 114.83 98.83 6.74 o 3 2 20 0.21 1.49 4.23 o 4 2 20 50.49 45.15 6.27 o 1 3 20 52.38 51.57 6.53 o 2 3 20 287.03 257.24 10.56 o 3 3 20 36.85 41.67 6.43 o 4 3 20 37.32 41.96 6.48 o 0 4 20 33.74 30.07 5.30 o 1 4 20 174.72 160.59 8.70 o 2 4 20 2.35 -4.81 4.81 o 3 4 20 88.88 86.04 7.21 o 1 5 20 17.26 19.47 4.19 o 2 5 20 264.52 258.64 11.16 o 3 5 20 3.69 13.01 5.02 o 0 6 20 561.33 671.81 29.75 o 1 6 20 69.90 76.78 10.91 o 2 6 20 34.44 38.56 5.70 o 1 1 21 99.48 103.53 3.57 o 2 1 21 109.75 103.09 5.24 o 3 1 21 211.25 204.11 7.25 o 0 2 21 128.82 125.35 7.50 o 1 2 21 132.35 139.80 13.48 o 2 2 21 9.24 5.83 4.42 o 3 2 21 24.75 31.59 5.15 o 1 3 21 86.53 75.99 6.78 o 2 3 21 19.12 22.68 5.09 o 3 3 21 0.25 1.41 4.86 o 0 4 21 759.85 718.37 32.98 o 1 4 21 49.81 49.47 4.67 o 2 4 21 1.65 -1.67 5.64 o 1 5 21 1.05 -3.14 3.14 o 0 0 22 11.49 17.17 4.81 o 1 0 22 711.62 723.28 21.58 o 2 0 22 2.42 3.00 4.10 o 3 0 22 22.06 22.31 5.90 o 1 1 22 5.48 6.48 3.00 o 2 1 22 12.17 10.40 3.23 o 0 2 22 20.92 25.66 5.02 o 1 2 22 143.67 145.36 6.08 o 2 2 22 0.02 0.13 3.89 o 1 3 22 85.12 89.79 5.26 o 2 3 22 27.89 26.65 6.19 o 0 4 22 2.13 14.81 4.83 o 1 4 22 39.79 44.69 9.25 o 1 1 23 129.91 133.46 5.57 o 0 2 23 425.33 438.22 20.96 o