#------------------------------------------------------------------------------ #$Date: 2009-11-11 20:41:08 +0200 (Wed, 11 Nov 2009) $ #$Revision: 840 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2223405.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2223405_Fobs loop_ _publ_author_name 'Alizadeh, Robabeh' 'Kalateh, Khadijeh' 'Ebadi, Amin' 'Ahmadi, Roya' 'Amani, Vahid' _publ_section_title ; Dichlorido(6,6'-dimethyl-2,2'-bipyridine-\k^2^N,N')zinc(II) ; _journal_coeditor_code HB5106 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1250 _journal_volume 65 _journal_year 2009 _space_group_IT_number 11 _symmetry_space_group_name_Hall '-P 2yb' _symmetry_space_group_name_H-M 'P 1 21/m 1' _cell_angle_alpha 90.000 _cell_angle_beta 110.612 _cell_angle_gamma 90.000 _cell_length_a 7.6957 _cell_length_b 11.2664 _cell_length_c 8.1431 _exptl_crystal_F_000 324.00 _reflns_d_resolution_high 0.6989 _[local]_cod_data_source_file hb5106Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 11 IN P2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 59.03 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' '-x, -y, -z' 'x, -y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 829.07 849.90 31.04 o 3 0 0 900.90 897.99 35.70 o 4 0 0 125.41 202.26 9.99 o 5 0 0 166.19 144.03 7.07 o 6 0 0 661.36 651.46 29.32 o 7 0 0 97.61 90.03 2.02 o 8 0 0 4.16 6.81 1.14 o 9 0 0 209.96 185.45 13.44 o 10 0 0 132.61 109.83 1.66 o 2 1 0 251.21 233.71 4.15 o 3 1 0 767.60 766.39 18.69 o 4 1 0 784.88 953.96 26.59 o 5 1 0 56.61 58.92 1.66 o 6 1 0 619.58 621.85 19.52 o 7 1 0 562.07 550.27 13.41 o 8 1 0 62.94 63.24 2.41 o 9 1 0 1.61 2.49 0.91 o 10 1 0 17.14 15.77 1.06 o 1 2 0 1914.96 1956.28 21.38 o 2 2 0 1059.53 1138.72 29.84 o 3 2 0 401.93 413.40 6.44 o 4 2 0 82.37 132.50 3.94 o 5 2 0 544.27 566.74 16.66 o 6 2 0 140.53 130.07 3.78 o 7 2 0 34.35 34.95 0.87 o 8 2 0 29.67 36.22 0.99 o 9 2 0 85.40 79.56 2.58 o 10 2 0 42.87 38.85 1.14 o 1 3 0 1395.05 1485.13 5.17 o 2 3 0 803.96 841.52 5.09 o 3 3 0 1141.90 1109.06 20.56 o 4 3 0 2924.41 3328.42 6.50 o 5 3 0 1.16 4.23 0.68 o 6 3 0 1051.89 1060.92 30.86 o 7 3 0 493.83 488.39 11.50 o 8 3 0 21.67 20.22 1.47 o 9 3 0 9.79 9.60 0.87 o 10 3 0 0.41 1.21 0.94 o 2 4 0 279.85 288.43 1.53 o 3 4 0 462.88 473.84 5.70 o 4 4 0 289.44 320.75 6.04 o 5 4 0 329.63 338.64 7.07 o 6 4 0 253.91 247.90 10.36 o 7 4 0 37.90 36.82 1.74 o 8 4 0 17.67 19.24 0.79 o 9 4 0 36.60 33.87 2.09 o 1 5 0 26.21 47.03 1.78 o 2 5 0 906.29 930.32 4.35 o 3 5 0 552.37 579.90 4.54 o 4 5 0 497.76 551.52 11.65 o 5 5 0 1.98 3.50 0.67 o 6 5 0 424.51 413.85 12.31 o 7 5 0 428.44 414.57 11.53 o 8 5 0 5.98 8.83 0.94 o 9 5 0 19.61 20.08 1.43 o 0 6 0 1786.94 1820.59 100.92 o 1 6 0 1185.71 1266.09 40.07 o 2 6 0 90.74 85.22 4.27 o 3 6 0 266.15 272.31 1.36 o 4 6 0 97.17 114.87 2.12 o 5 6 0 360.66 369.10 2.00 o 6 6 0 210.93 212.67 5.83 o 7 6 0 1.59 5.04 0.98 o 8 6 0 34.87 34.83 1.00 o 9 6 0 20.01 17.90 1.67 o 1 7 0 654.49 689.87 19.37 o 2 7 0 475.16 477.30 18.02 o 3 7 0 808.80 841.00 5.04 o 4 7 0 292.79 357.19 3.70 o 5 7 0 77.19 79.27 1.11 o 6 7 0 294.46 300.02 8.01 o 7 7 0 445.54 445.67 18.03 o 8 7 0 7.83 10.10 1.49 o 9 7 0 1.06 1.63 0.77 o 1 8 0 420.71 427.22 15.59 o 2 8 0 70.88 76.69 2.19 o 3 8 0 730.42 761.59 15.28 o 4 8 0 17.85 20.03 1.76 o 5 8 0 29.98 33.88 1.88 o 6 8 0 365.98 360.60 10.68 o 7 8 0 27.07 26.24 0.86 o 8 8 0 13.00 15.52 2.40 o 1 9 0 311.42 312.53 11.59 o 2 9 0 364.91 374.02 12.67 o 3 9 0 48.50 53.65 1.41 o 4 9 0 12.60 38.76 2.58 o 5 9 0 44.62 46.66 1.05 o 6 9 0 74.93 79.26 2.71 o 7 9 0 170.83 155.88 5.26 o 8 9 0 19.43 17.42 1.28 o 0 10 0 929.19 1006.03 70.47 o 1 10 0 457.67 431.98 17.94 o 2 10 0 60.76 66.18 1.69 o 3 10 0 74.08 70.23 1.05 o 4 10 0 19.92 20.83 1.37 o 5 10 0 190.54 196.54 3.51 o 6 10 0 58.11 66.18 3.50 o 7 10 0 8.22 8.76 0.68 o 8 10 0 10.78 8.82 3.64 o 1 11 0 7.60 11.82 1.09 o 2 11 0 171.62 163.80 5.08 o 3 11 0 175.24 184.44 4.93 o 4 11 0 159.16 170.53 3.74 o 5 11 0 0.01 1.77 0.72 o 6 11 0 77.48 79.58 2.10 o 7 11 0 93.41 74.22 2.68 o 0 12 0 237.23 269.49 23.71 o 1 12 0 69.46 70.54 2.96 o 2 12 0 7.09 11.37 0.70 o 3 12 0 25.50 23.26 0.89 o 4 12 0 23.97 27.44 1.16 o 5 12 0 27.05 29.05 0.78 o 6 12 0 15.25 17.21 1.53 o 1 13 0 95.36 94.20 2.84 o 2 13 0 32.38 33.12 1.54 o 3 13 0 29.19 27.60 0.77 o 4 13 0 96.26 109.97 2.35 o 5 13 0 2.25 3.40 0.75 o 6 13 0 62.23 47.52 6.50 o 0 14 0 147.74 146.89 7.37 o 1 14 0 53.11 51.36 2.47 o 2 14 0 0.20 -0.38 0.75 o 3 14 0 0.96 0.88 0.72 o 4 14 0 33.21 31.75 1.45 o 5 14 0 55.67 52.59 1.88 o 1 15 0 12.26 12.73 0.61 o 2 15 0 2.21 1.97 0.64 o 3 15 0 40.81 43.25 2.04 o 0 16 0 176.61 171.72 2.69 o 1 16 0 1.72 2.63 1.76 o -10 0 1 0.43 1.68 2.78 o -9 0 1 3.33 3.51 2.16 o -8 0 1 67.28 71.44 1.32 o -7 0 1 503.84 499.09 14.58 o -6 0 1 770.41 743.16 21.63 o -5 0 1 3.33 4.78 0.84 o -4 0 1 1710.10 2115.03 6.39 o -3 0 1 48.05 37.86 1.01 o -1 0 1 1423.18 1364.87 3.96 o 1 0 1 2.58 4.41 1.74 o 3 0 1 1725.51 1719.52 51.17 o 4 0 1 735.04 733.92 37.52 o 5 0 1 0.80 2.49 0.98 o 6 0 1 96.43 94.00 4.34 o 7 0 1 500.54 505.50 33.16 o 8 0 1 237.93 231.58 14.45 o 9 0 1 23.69 23.51 2.02 o -10 1 1 142.32 129.46 1.50 o -9 1 1 5.87 3.85 0.74 o -8 1 1 1.11 29.34 2.49 o -7 1 1 18.13 19.83 0.72 o -6 1 1 0.91 7.71 2.48 o -5 1 1 797.38 776.25 19.73 o -4 1 1 1295.28 1244.34 25.65 o -3 1 1 1161.44 1159.08 23.43 o -2 1 1 266.14 266.03 4.29 o 1 1 1 2077.74 2172.65 5.56 o 2 1 1 660.42 750.65 14.29 o 3 1 1 628.03 677.81 11.93 o 4 1 1 4.81 30.90 1.31 o 5 1 1 78.77 74.77 2.62 o 6 1 1 754.73 756.38 27.27 o 7 1 1 348.03 355.63 11.34 o 8 1 1 131.99 131.66 5.18 o 9 1 1 178.78 168.21 5.90 o -10 2 1 18.02 15.47 0.84 o -9 2 1 1.15 0.55 0.72 o -8 2 1 11.66 13.38 0.66 o -7 2 1 710.61 689.80 14.56 o -6 2 1 1089.95 1052.01 19.03 o -5 2 1 91.97 94.79 1.95 o -4 2 1 1535.17 1533.94 31.18 o -3 2 1 875.69 794.47 13.87 o -2 2 1 1680.67 1816.18 35.76 o -1 2 1 666.47 647.28 8.54 o 1 2 1 39.39 40.94 2.62 o 4 2 1 15.24 46.03 3.62 o 5 2 1 50.31 51.86 1.36 o 6 2 1 199.35 197.82 7.38 o 7 2 1 273.81 270.24 13.50 o 8 2 1 9.84 8.74 0.89 o 9 2 1 0.17 -0.94 0.98 o -10 3 1 64.74 57.61 2.11 o -9 3 1 12.15 10.03 0.77 o -8 3 1 6.93 21.38 0.95 o -7 3 1 80.44 81.85 1.25 o -6 3 1 263.89 253.73 5.16 o -5 3 1 1080.71 1049.08 22.38 o -4 3 1 896.43 867.43 15.48 o -3 3 1 453.52 460.15 4.70 o -2 3 1 20.16 22.84 0.73 o -1 3 1 1600.27 1595.17 8.88 o 2 3 1 298.23 344.17 6.26 o 3 3 1 907.30 975.29 18.26 o 4 3 1 586.66 679.20 10.20 o 5 3 1 46.62 42.94 0.83 o 6 3 1 519.29 505.40 13.57 o 7 3 1 172.97 175.66 6.32 o 8 3 1 15.67 16.14 1.33 o 9 3 1 142.57 137.66 4.69 o -10 4 1 7.48 7.55 1.01 o -9 4 1 1.06 1.04 0.92 o -8 4 1 33.52 35.24 1.70 o -7 4 1 478.13 468.39 16.24 o -6 4 1 917.55 908.06 25.53 o -5 4 1 11.11 13.86 1.05 o -4 4 1 1562.37 1750.63 23.39 o -3 4 1 964.59 1038.43 14.77 o -2 4 1 18.82 22.21 0.80 o -1 4 1 1003.79 1036.36 14.70 o 0 4 1 2142.08 2351.12 7.50 o 1 4 1 144.33 146.38 5.34 o 3 4 1 2127.09 2213.03 3.68 o 4 4 1 112.63 132.95 2.37 o 5 4 1 11.46 11.54 0.75 o 6 4 1 196.73 194.18 3.68 o 7 4 1 159.82 154.59 2.66 o 8 4 1 43.81 42.53 1.12 o 9 4 1 9.96 8.18 0.77 o -10 5 1 32.89 28.81 1.93 o -9 5 1 20.54 21.00 1.27 o -8 5 1 1.72 6.53 0.85 o -7 5 1 30.49 32.40 1.76 o -6 5 1 2.36 1.58 0.75 o -5 5 1 548.83 546.42 15.17 o -4 5 1 1143.58 1174.75 14.47 o -3 5 1 12.28 9.38 0.86 o -2 5 1 51.29 59.00 1.00 o -1 5 1 152.21 208.78 2.75 o 1 5 1 1621.29 1698.83 74.39 o 2 5 1 175.32 188.50 3.08 o 3 5 1 520.41 538.46 10.23 o 4 5 1 9.01 17.12 1.50 o 5 5 1 54.82 53.82 1.88 o 6 5 1 305.16 325.23 10.85 o 7 5 1 51.74 52.20 2.90 o 8 5 1 5.58 7.10 0.83 o 9 5 1 83.45 73.43 3.13 o -9 6 1 8.15 7.62 1.83 o -8 6 1 38.75 37.16 1.54 o -7 6 1 440.98 428.28 19.82 o -6 6 1 487.31 491.80 14.25 o -5 6 1 14.02 11.55 0.75 o -4 6 1 929.71 971.58 10.82 o -3 6 1 687.73 690.46 2.94 o -2 6 1 117.95 150.87 2.79 o -1 6 1 467.14 480.69 7.79 o 0 6 1 1607.82 1819.28 43.40 o 1 6 1 120.91 133.54 4.84 o 2 6 1 1793.93 1856.69 27.34 o 3 6 1 1585.10 1630.14 27.30 o 4 6 1 109.26 141.82 6.74 o 5 6 1 60.98 62.19 2.62 o 6 6 1 200.99 207.48 5.80 o 7 6 1 84.89 82.93 3.60 o 8 6 1 10.12 13.63 2.60 o 9 6 1 8.63 7.69 0.87 o -9 7 1 25.33 24.35 1.95 o -8 7 1 5.25 11.04 1.16 o -7 7 1 7.87 11.83 0.92 o -6 7 1 3.39 5.73 0.99 o -5 7 1 510.17 506.06 11.95 o -4 7 1 670.05 695.15 8.86 o -3 7 1 131.74 139.18 2.47 o -2 7 1 0.06 1.87 0.62 o -1 7 1 939.91 947.22 15.42 o 0 7 1 1868.77 1925.60 37.63 o 1 7 1 1710.88 1649.19 55.04 o 2 7 1 41.08 45.71 1.44 o 3 7 1 178.16 183.52 6.31 o 4 7 1 15.50 23.25 1.59 o 5 7 1 287.43 299.11 3.64 o 6 7 1 208.88 216.23 7.79 o 7 7 1 81.03 80.68 1.75 o 8 7 1 12.34 13.92 1.98 o -9 8 1 0.04 2.29 1.38 o -8 8 1 82.53 70.77 1.15 o -7 8 1 37.92 36.84 1.43 o -6 8 1 96.18 92.66 2.74 o -5 8 1 181.23 207.36 3.29 o -4 8 1 439.67 514.12 7.92 o -3 8 1 247.45 259.54 5.61 o -2 8 1 186.85 200.40 2.74 o -1 8 1 256.45 264.87 5.21 o 0 8 1 288.34 284.60 8.21 o 1 8 1 291.69 300.32 11.57 o 2 8 1 1116.05 1137.04 43.75 o 3 8 1 3.75 5.06 1.07 o 4 8 1 317.26 339.17 6.36 o 5 8 1 23.94 28.89 2.81 o 6 8 1 132.59 125.87 3.83 o 7 8 1 100.96 95.17 3.11 o 8 8 1 35.59 28.95 0.99 o -8 9 1 0.31 6.27 0.73 o -7 9 1 1.11 2.74 0.81 o -6 9 1 13.34 11.45 2.14 o -5 9 1 61.46 58.93 2.55 o -4 9 1 506.70 507.16 2.93 o -3 9 1 162.45 156.25 5.11 o -2 9 1 0.06 0.64 0.60 o -1 9 1 279.70 287.40 9.65 o 0 9 1 956.24 1023.68 26.21 o 1 9 1 215.33 231.81 8.05 o 2 9 1 241.93 244.89 11.33 o 3 9 1 25.50 22.16 1.05 o 4 9 1 11.07 15.77 0.81 o 5 9 1 58.41 60.73 1.36 o 6 9 1 168.02 176.09 3.58 o 7 9 1 39.71 37.53 0.90 o 8 9 1 21.48 18.45 1.65 o -8 10 1 12.40 11.34 1.04 o -7 10 1 147.84 137.59 1.19 o -6 10 1 130.37 129.63 1.04 o -5 10 1 7.94 10.10 0.92 o -4 10 1 133.98 153.33 6.36 o -3 10 1 303.90 301.88 8.04 o -2 10 1 33.52 39.30 0.74 o -1 10 1 210.59 208.83 5.21 o 0 10 1 143.32 144.45 3.94 o 1 10 1 101.98 101.08 3.45 o 2 10 1 346.48 343.75 10.22 o 3 10 1 609.37 624.46 5.15 o 4 10 1 32.90 38.81 1.39 o 5 10 1 3.85 4.23 1.01 o 6 10 1 46.00 46.45 1.99 o 7 10 1 62.30 59.31 1.08 o -7 11 1 4.30 5.53 2.31 o -6 11 1 21.95 19.00 1.77 o -5 11 1 152.34 154.09 5.35 o -4 11 1 154.03 152.09 4.65 o -3 11 1 0.86 3.47 0.74 o -2 11 1 9.94 9.17 0.94 o -1 11 1 3.84 9.02 1.77 o 0 11 1 497.46 503.67 21.61 o 1 11 1 391.86 380.92 11.76 o 2 11 1 4.07 6.70 0.70 o 3 11 1 76.73 80.86 0.84 o 4 11 1 29.35 27.28 0.71 o 5 11 1 33.90 36.04 1.34 o 6 11 1 71.77 71.79 1.76 o 7 11 1 4.14 3.91 0.95 o -7 12 1 40.48 32.83 8.80 o -6 12 1 78.99 84.68 4.45 o -5 12 1 0.07 -0.47 1.00 o -4 12 1 78.40 86.07 4.71 o -3 12 1 38.90 39.83 1.09 o -2 12 1 1.54 1.81 0.67 o -1 12 1 42.25 43.14 2.16 o 0 12 1 89.97 87.61 3.16 o 1 12 1 8.07 9.21 0.73 o 2 12 1 186.94 190.75 5.47 o 3 12 1 95.18 97.63 1.84 o 4 12 1 3.85 6.39 0.74 o 5 12 1 1.89 4.43 0.75 o 6 12 1 17.48 15.01 0.70 o -6 13 1 21.90 20.28 0.92 o -5 13 1 51.37 45.50 1.17 o -4 13 1 31.89 31.32 2.32 o -3 13 1 37.83 37.10 1.35 o -2 13 1 0.02 0.04 1.27 o -1 13 1 88.68 84.90 3.55 o 0 13 1 134.04 146.72 6.52 o 1 13 1 48.66 46.66 1.38 o 2 13 1 14.34 16.18 0.84 o 3 13 1 32.04 32.56 0.83 o 4 13 1 53.96 50.13 1.36 o 5 13 1 1.56 2.61 0.76 o -5 14 1 5.20 4.48 0.94 o -4 14 1 59.36 65.31 1.54 o -3 14 1 31.34 33.15 1.41 o -2 14 1 11.16 9.98 0.85 o -1 14 1 32.22 32.12 1.01 o 0 14 1 33.18 36.99 1.73 o 1 14 1 2.31 2.49 0.68 o 2 14 1 135.01 133.89 4.31 o 3 14 1 140.25 133.42 2.11 o 4 14 1 2.77 3.62 0.71 o -3 15 1 0.94 0.55 0.66 o -2 15 1 1.76 3.24 0.88 o -1 15 1 14.48 16.34 0.62 o 0 15 1 17.58 16.39 0.95 o 1 15 1 62.90 61.35 2.14 o 2 15 1 2.40 2.06 0.75 o 3 15 1 13.56 12.65 0.80 o 0 16 1 5.96 8.43 1.80 o -10 0 2 51.94 46.30 3.44 o -9 0 2 9.06 10.84 1.23 o -8 0 2 7.08 27.26 2.32 o -7 0 2 132.91 134.12 3.83 o -6 0 2 41.84 51.24 1.62 o -5 0 2 476.83 433.60 11.04 o -3 0 2 2256.03 2063.23 6.08 o -1 0 2 835.62 738.14 14.01 o 1 0 2 896.52 920.52 4.73 o 2 0 2 1562.82 1656.11 5.60 o 3 0 2 8.33 11.94 1.04 o 4 0 2 227.43 230.30 14.57 o 5 0 2 588.04 565.97 33.01 o 6 0 2 1467.96 1446.72 65.39 o 7 0 2 12.19 11.30 1.69 o 8 0 2 80.04 82.77 1.94 o 9 0 2 76.37 68.05 2.11 o -10 1 2 28.16 29.40 1.23 o -9 1 2 9.81 10.77 0.70 o -8 1 2 141.35 152.74 2.45 o -7 1 2 248.79 235.25 4.51 o -6 1 2 333.42 301.02 5.89 o -5 1 2 174.27 173.55 3.62 o -4 1 2 68.78 114.10 1.25 o -2 1 2 121.92 119.65 0.98 o -1 1 2 76.86 59.68 0.97 o 0 1 2 2447.38 2378.63 7.81 o 1 1 2 35.13 36.52 1.23 o 4 1 2 94.17 101.15 3.57 o 5 1 2 55.44 55.47 2.99 o 6 1 2 162.60 169.14 8.11 o 7 1 2 60.13 58.38 3.27 o 8 1 2 13.41 13.73 1.21 o 9 1 2 51.34 48.28 1.45 o -10 2 2 44.34 41.60 0.99 o -9 2 2 28.09 24.82 0.79 o -8 2 2 20.56 33.75 0.67 o -7 2 2 15.50 14.61 0.63 o -6 2 2 56.29 56.71 1.09 o -5 2 2 839.28 765.11 9.39 o -4 2 2 2385.72 2294.69 38.82 o -3 2 2 433.75 389.59 7.46 o -2 2 2 71.57 60.54 0.90 o -1 2 2 1224.19 1107.38 6.11 o 0 2 2 15.59 12.88 0.90 o 1 2 2 1760.61 1798.21 82.28 o 2 2 2 126.65 113.75 1.18 o 3 2 2 169.86 207.55 4.33 o 4 2 2 85.62 89.03 1.07 o 5 2 2 353.39 371.23 11.27 o 6 2 2 223.67 224.90 7.85 o 7 2 2 90.06 89.24 5.65 o 8 2 2 14.17 17.49 1.34 o 9 2 2 105.71 91.21 4.89 o -10 3 2 41.47 39.37 1.03 o -9 3 2 0.38 0.85 0.72 o -8 3 2 319.99 320.91 7.53 o -7 3 2 404.90 394.64 8.39 o -6 3 2 108.66 93.87 1.52 o -5 3 2 70.94 74.42 1.26 o -4 3 2 462.49 474.90 8.32 o -3 3 2 1244.33 1127.57 22.96 o -2 3 2 532.43 473.87 5.82 o -1 3 2 615.60 587.59 9.18 o 1 3 2 0.79 5.77 3.34 o 3 3 2 2247.57 2291.95 37.34 o 4 3 2 14.03 28.37 1.18 o 5 3 2 131.90 135.81 3.70 o 6 3 2 23.83 23.05 0.90 o 7 3 2 23.29 22.73 0.89 o 8 3 2 87.55 81.69 2.78 o 9 3 2 46.24 40.79 2.55 o -10 4 2 46.85 45.48 2.75 o -9 4 2 16.28 16.26 1.20 o -8 4 2 9.03 20.53 0.87 o -7 4 2 35.04 33.55 0.73 o -6 4 2 4.89 6.09 0.60 o -5 4 2 837.35 853.56 12.96 o -4 4 2 2699.12 2752.10 29.62 o -3 4 2 381.78 365.07 3.92 o -2 4 2 626.74 643.24 6.28 o -1 4 2 1313.55 1264.50 20.68 o 0 4 2 1174.83 1195.03 32.55 o 1 4 2 1567.58 1561.61 51.64 o 2 4 2 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