#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/34/2223427.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2223427_Fobs loop_ _publ_author_name 'Cui, Li-Jing' 'Xu, Hai-Jun' _publ_section_title ; 2,4,6-Trimethylanilinium bromide ; _journal_coeditor_code HK2763 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2376 _journal_volume 65 _journal_year 2009 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 10.3990 _cell_length_b 18.7200 _cell_length_c 10.2820 _exptl_crystal_F_000 879.83 _reflns_d_resolution_high 0.7701 _[local]_cod_data_source_file hk2763Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 1 in P-1 Pbca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 270.82 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' '-x-1/2, y-1/2, z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 12329.97 11197.89 343.16 o 4 0 0 38785.44 38343.42 1501.97 o 6 0 0 5551.85 5516.56 244.72 o 8 0 0 49.08 95.58 27.12 o 10 0 0 6767.93 7196.98 481.85 o 12 0 0 214.89 229.25 100.93 o 2 1 0 316.50 418.46 12.83 o 4 1 0 480.86 372.10 17.08 o 6 1 0 569.29 513.65 26.49 o 8 1 0 115.30 153.52 22.29 o 10 1 0 12.36 33.64 20.06 o 12 1 0 13.17 38.40 42.52 o 2 2 0 18048.58 17999.27 378.53 o 4 2 0 23559.26 24755.60 626.55 o 6 2 0 18186.07 19405.58 637.20 o 8 2 0 2143.64 2213.14 105.04 o 10 2 0 5124.53 5443.18 325.29 o 12 2 0 152.20 275.57 70.04 o 2 3 0 219.83 203.67 9.69 o 4 3 0 304.06 339.35 12.59 o 6 3 0 70.61 91.39 21.19 o 8 3 0 92.36 106.05 19.63 o 10 3 0 5.11 69.79 32.72 o 12 3 0 0.77 15.83 37.37 o 0 4 0 30559.76 22747.83 1713.32 o 2 4 0 2939.11 3026.00 75.20 o 4 4 0 18317.15 18959.54 425.15 o 6 4 0 8952.89 9181.69 268.51 o 8 4 0 699.47 654.02 40.00 o 10 4 0 3773.07 4156.17 258.62 o 12 4 0 127.67 150.81 51.31 o 2 5 0 3393.50 3204.56 85.63 o 4 5 0 1439.94 1589.50 53.47 o 6 5 0 6.85 4.93 10.80 o 8 5 0 68.39 90.89 44.53 o 10 5 0 190.97 220.86 48.08 o 12 5 0 540.29 563.45 83.09 o 0 6 0 39299.64 33394.97 3554.34 o 2 6 0 6140.36 6441.47 268.46 o 4 6 0 14743.07 14309.28 558.75 o 6 6 0 10494.63 10392.76 413.79 o 8 6 0 573.30 583.24 52.88 o 10 6 0 2358.95 2672.29 184.78 o 12 6 0 277.51 304.23 62.93 o 2 7 0 11073.56 11132.23 264.45 o 4 7 0 1080.89 1029.29 56.29 o 6 7 0 722.07 773.37 46.20 o 8 7 0 111.39 152.78 33.41 o 10 7 0 108.48 113.96 40.10 o 12 7 0 36.77 127.49 61.12 o 0 8 0 35088.45 32752.43 1714.32 o 2 8 0 1009.05 854.37 27.94 o 4 8 0 9940.07 9596.81 331.80 o 6 8 0 9201.12 10311.14 445.34 o 8 8 0 1324.82 1403.02 99.48 o 10 8 0 3225.63 3147.41 209.11 o 12 8 0 5.90 -2.45 38.67 o 2 9 0 229.26 141.26 13.04 o 4 9 0 2090.72 1984.99 49.79 o 6 9 0 53.79 99.41 44.95 o 8 9 0 2770.05 2907.33 169.92 o 10 9 0 264.17 256.02 51.32 o 12 9 0 19.67 54.54 50.95 o 0 10 0 7664.62 7176.27 350.65 o 2 10 0 5824.44 6058.34 174.38 o 4 10 0 10405.91 11064.11 414.99 o 6 10 0 7081.12 7285.12 335.94 o 8 10 0 1748.38 1677.69 112.04 o 10 10 0 1414.88 1466.82 133.79 o 12 10 0 58.12 79.57 78.78 o 2 11 0 769.20 740.21 39.30 o 4 11 0 777.67 742.90 33.70 o 6 11 0 698.26 667.87 66.70 o 8 11 0 61.13 64.18 48.68 o 10 11 0 97.73 102.57 37.60 o 12 11 0 70.37 99.48 76.64 o 0 12 0 12701.66 13148.43 638.06 o 2 12 0 1876.84 1860.61 85.90 o 4 12 0 6789.85 6610.87 287.61 o 6 12 0 3079.78 3178.54 169.47 o 8 12 0 38.24 73.79 31.16 o 10 12 0 1622.08 1507.64 155.55 o 2 13 0 1824.90 1995.19 82.89 o 4 13 0 758.38 868.68 41.58 o 6 13 0 174.56 150.97 30.92 o 8 13 0 328.55 367.78 53.95 o 10 13 0 26.94 99.59 71.14 o 0 14 0 10623.45 10429.61 672.07 o 2 14 0 19.24 38.08 15.59 o 4 14 0 2533.45 2480.23 102.47 o 6 14 0 1702.37 1724.00 110.70 o 8 14 0 180.37 158.58 40.70 o 10 14 0 989.24 1170.75 197.99 o 2 15 0 287.99 278.06 27.40 o 4 15 0 1847.15 1950.10 114.95 o 6 15 0 450.09 478.56 51.08 o 8 15 0 700.86 658.80 102.18 o 10 15 0 10.57 -71.11 93.73 o 0 16 0 4607.82 4762.37 291.04 o 2 16 0 144.18 163.98 25.95 o 4 16 0 1920.49 2049.40 131.63 o 6 16 0 665.80 696.35 71.04 o 8 16 0 43.88 75.95 61.60 o 10 16 0 489.40 536.89 139.74 o 2 17 0 2482.11 2538.39 128.95 o 4 17 0 7.73 25.41 29.37 o 6 17 0 26.84 20.57 35.44 o 8 17 0 416.51 479.08 114.23 o 0 18 0 2254.37 2427.58 189.16 o 2 18 0 345.91 353.90 37.79 o 4 18 0 1383.54 1226.15 90.86 o 6 18 0 681.51 663.28 100.52 o 8 18 0 63.17 76.73 66.86 o 2 19 0 761.48 830.09 59.97 o 4 19 0 497.29 402.82 67.31 o 6 19 0 158.07 117.53 55.31 o 8 19 0 146.81 173.96 74.86 o 0 20 0 1158.68 1203.69 113.33 o 2 20 0 72.52 126.48 29.89 o 4 20 0 660.35 663.88 99.85 o 6 20 0 284.19 379.48 121.89 o 2 21 0 575.47 585.01 93.98 o 4 21 0 83.65 168.15 58.67 o 6 21 0 39.57 -17.65 47.63 o 0 22 0 724.43 796.38 126.06 o 2 22 0 9.46 -20.41 35.39 o 4 22 0 236.14 269.42 89.84 o 2 23 0 274.27 283.55 78.33 o 4 23 0 52.26 -15.05 77.40 o 0 24 0 62.03 26.35 82.22 o 2 24 0 73.27 175.14 128.31 o 1 1 1 4031.47 2815.45 115.43 o 2 1 1 18227.58 19711.60 417.01 o 3 1 1 3622.46 3647.96 89.16 o 4 1 1 15987.83 16344.46 304.00 o 5 1 1 200.65 184.99 10.76 o 6 1 1 8047.99 8579.01 185.88 o 7 1 1 553.56 505.20 21.38 o 8 1 1 7646.34 8059.62 222.40 o 9 1 1 420.40 450.67 29.32 o 10 1 1 12.09 10.71 18.40 o 11 1 1 170.60 199.96 33.13 o 12 1 1 1391.74 1351.75 107.91 o 13 1 1 3.30 19.95 34.26 o 1 2 1 6799.08 6202.28 137.48 o 2 2 1 82.97 81.54 2.17 o 3 2 1 6.40 16.41 3.34 o 4 2 1 360.16 303.85 9.48 o 5 2 1 303.97 252.62 12.88 o 6 2 1 98.26 80.76 10.13 o 7 2 1 5.50 24.44 10.74 o 8 2 1 221.20 191.70 18.19 o 9 2 1 45.48 49.26 13.61 o 10 2 1 49.21 64.38 19.87 o 11 2 1 21.03 86.42 24.86 o 12 2 1 8.13 -11.91 27.03 o 13 2 1 16.50 -20.40 36.55 o 1 3 1 6947.40 6506.81 166.16 o 2 3 1 73340.84 71181.20 1063.91 o 3 3 1 483.05 446.96 8.98 o 4 3 1 10992.81 11058.92 202.26 o 5 3 1 4434.55 4389.82 84.67 o 6 3 1 4621.01 4667.98 99.15 o 7 3 1 8.24 41.88 12.70 o 8 3 1 7962.81 8442.12 230.84 o 9 3 1 193.39 203.33 20.99 o 10 3 1 4.15 1.14 18.88 o 11 3 1 551.20 578.99 54.48 o 12 3 1 968.90 924.54 78.83 o 13 3 1 113.06 50.17 36.25 o 0 4 1 3237.92 3338.89 99.10 o 1 4 1 1693.80 1596.53 21.97 o 2 4 1 2560.35 2237.77 32.74 o 3 4 1 176.84 232.08 9.26 o 4 4 1 935.85 1028.79 22.10 o 5 4 1 76.53 95.01 8.22 o 6 4 1 520.06 459.68 22.46 o 7 4 1 58.51 64.78 13.80 o 8 4 1 4.53 -8.35 11.56 o 9 4 1 134.31 161.68 25.03 o 10 4 1 1.22 29.48 27.74 o 11 4 1 61.81 49.95 27.00 o 12 4 1 61.60 69.96 34.67 o 13 4 1 1.50 26.26 38.01 o 1 5 1 4121.43 4087.08 92.95 o 2 5 1 32720.61 31136.84 517.74 o 3 5 1 75.73 94.83 6.94 o 4 5 1 7324.82 7559.00 146.11 o 5 5 1 4440.03 4132.58 89.74 o 6 5 1 5687.27 5590.76 152.50 o 7 5 1 83.53 117.47 13.10 o 8 5 1 8176.22 8011.00 240.76 o 9 5 1 796.14 844.02 54.30 o 10 5 1 46.25 29.27 20.20 o 11 5 1 165.17 219.37 36.99 o 12 5 1 1514.99 1445.41 105.77 o 13 5 1 17.74 7.97 33.27 o 0 6 1 292.33 262.38 13.52 o 1 6 1 307.27 279.74 13.07 o 2 6 1 47.23 25.48 5.83 o 3 6 1 810.38 943.46 21.00 o 4 6 1 6.48 29.66 8.81 o 5 6 1 867.14 896.91 25.18 o 6 6 1 1221.17 1199.29 38.17 o 7 6 1 111.60 90.03 11.32 o 8 6 1 40.56 63.23 27.09 o 9 6 1 1.93 30.00 19.44 o 10 6 1 232.12 250.13 34.21 o 11 6 1 63.21 52.04 27.19 o 12 6 1 0.75 18.41 30.43 o 13 6 1 37.74 18.35 42.00 o 1 7 1 3085.62 3153.48 61.76 o 2 7 1 24854.87 25824.85 514.47 o 3 7 1 122.96 147.17 6.33 o 4 7 1 4779.86 4291.67 83.52 o 5 7 1 3399.70 3361.28 114.06 o 6 7 1 4115.99 4363.19 110.95 o 7 7 1 8.13 38.40 17.53 o 8 7 1 4249.96 4062.31 151.72 o 9 7 1 661.43 663.34 46.18 o 10 7 1 18.11 87.37 26.76 o 11 7 1 3.05 -4.93 24.76 o 12 7 1 1288.32 1189.37 95.02 o 0 8 1 107.93 152.46 17.38 o 1 8 1 899.74 917.69 23.15 o 2 8 1 698.11 728.97 18.36 o 3 8 1 1279.83 1479.42 30.20 o 4 8 1 1016.02 1001.59 25.34 o 5 8 1 364.92 403.30 16.43 o 6 8 1 185.00 209.90 20.91 o 7 8 1 9.93 0.92 18.53 o 8 8 1 41.03 72.86 21.32 o 9 8 1 224.22 278.80 30.90 o 10 8 1 86.93 151.13 29.06 o 11 8 1 51.57 56.32 31.60 o 12 8 1 48.99 9.08 28.31 o 1 9 1 437.64 391.94 15.07 o 2 9 1 22470.24 22377.67 471.27 o 3 9 1 3.80 11.67 10.32 o 4 9 1 3847.83 3770.63 90.42 o 5 9 1 683.03 676.07 41.85 o 6 9 1 2011.27 2018.19 79.48 o 7 9 1 530.42 520.30 37.83 o 8 9 1 3644.22 3768.12 162.27 o 9 9 1 357.32 321.14 38.61 o 10 9 1 62.54 64.91 25.12 o 11 9 1 114.41 94.79 34.97 o 12 9 1 798.14 783.47 87.50 o 0 10 1 8390.86 8457.21 269.72 o 1 10 1 313.19 388.47 16.13 o 2 10 1 20.07 42.37 9.33 o 3 10 1 890.64 937.85 27.37 o 4 10 1 1347.02 1348.18 41.20 o 5 10 1 12.88 12.54 9.82 o 6 10 1 289.23 305.80 27.38 o 7 10 1 565.82 491.79 36.30 o 8 10 1 104.46 119.61 25.04 o 9 10 1 123.96 137.25 32.70 o 10 10 1 258.05 322.03 41.99 o 11 10 1 13.33 -33.78 33.78 o 12 10 1 45.10 10.17 32.84 o 1 11 1 652.76 581.46 21.81 o 2 11 1 9771.30 9640.72 211.61 o 3 11 1 16.71 44.38 13.28 o 4 11 1 2393.68 2494.92 71.11 o 5 11 1 1716.66 1667.09 67.11 o 6 11 1 1788.31 1744.76 77.89 o 7 11 1 147.67 131.75 23.45 o 8 11 1 3503.91 3573.20 161.59 o 9 11 1 5.67 18.48 22.18 o 10 11 1 57.12 21.71 23.39 o 11 11 1 82.09 101.12 38.80 o 12 11 1 505.91 478.38 99.17 o 0 12 1 1723.55 1603.01 72.20 o 1 12 1 7.86 37.02 11.89 o 2 12 1 344.72 287.91 15.91 o 3 12 1 476.31 498.69 21.15 o 4 12 1 680.17 574.34 26.24 o 5 12 1 4.92 7.86 14.69 o 6 12 1 1170.57 1185.80 62.62 o 7 12 1 193.73 212.62 27.99 o 8 12 1 55.39 84.24 18.94 o 9 12 1 21.50 37.33 24.11 o 10 12 1 367.30 380.07 56.36 o 11 12 1 23.76 38.46 32.20 o 1 13 1 472.88 450.06 20.65 o 2 13 1 7647.69 7935.50 212.02 o 3 13 1 5.06 3.98 8.10 o 4 13 1 1349.53 1401.25 47.46 o 5 13 1 733.96 687.16 42.59 o 6 13 1 1495.62 1487.36 75.59 o 7 13 1 80.75 57.02 22.54 o 8 13 1 1390.43 1356.67 80.05 o 9 13 1 372.44 352.11 50.49 o 10 13 1 1.09 41.43 33.51 o 11 13 1 12.73 49.09 45.68 o 0 14 1 3105.59 3126.15 142.96 o 1 14 1 24.46 29.96 11.02 o 2 14 1 2.84 -11.76 14.85 o 3 14 1 308.84 282.88 17.70 o 4 14 1 671.65 642.78 29.58 o 5 14 1 6.82 41.37 16.63 o 6 14 1 242.28 267.69 30.22 o 7 14 1 56.35 110.40 23.16 o 8 14 1 0.69 21.18 23.53 o 9 14 1 7.28 52.41 38.70 o 10 14 1 271.62 289.23 68.20 o 1 15 1 1298.46 1222.42 45.82 o 2 15 1 3227.64 3408.57 100.96 o 3 15 1 1101.80 1102.32 40.83 o 4 15 1 2691.79 2685.89 90.29 o 5 15 1 23.27 87.23 26.54 o 6 15 1 1358.58 1287.74 72.03 o 7 15 1 81.72 122.60 31.24 o 8 15 1 1040.96 1056.14 87.74 o 9 15 1 69.49 91.78 38.36 o 10 15 1 1.64 24.72 45.18 o 0 16 1 968.98 1009.25 70.69 o 1 16 1 30.31 83.90 21.10 o 2 16 1 449.03 489.50 27.98 o 3 16 1 15.12 32.44 12.47 o 4 16 1 709.59 656.94 39.18 o 5 16 1 101.20 126.35 28.40 o 6 16 1 546.85 544.22 46.51 o 7 16 1 75.13 111.60 35.18 o 8 16 1 3.34 23.27 26.81 o 9 16 1 39.02 79.23 46.08 o 10 16 1 93.86 159.33 60.78 o 1 17 1 167.04 193.00 20.21 o 2 17 1 2024.70 2088.45 74.91 o 3 17 1 4.98 20.94 16.59 o 4 17 1 465.95 485.76 43.63 o 5 17 1 269.31 293.02 34.68 o 6 17 1 418.25 475.74 47.90 o 7 17 1 3.64 15.63 24.66 o 8 17 1 822.33 919.46 102.90 o 9 17 1 16.94 5.29 35.21 o 0 18 1 734.44 711.53 72.25 o 1 18 1 75.93 98.24 19.11 o 2 18 1 111.57 116.24 19.78 o 3 18 1 71.84 104.55 22.20 o 4 18 1 305.34 270.25 38.31 o 5 18 1 3.88 7.28 21.58 o 6 18 1 447.32 444.71 54.19 o 7 18 1 14.66 10.56 30.25 o 8 18 1 9.89 -1.27 34.75 o 9 18 1 1.34 -2.68 42.20 o 1 19 1 69.49 72.59 17.66 o 2 19 1 1146.54 1126.18 58.54 o 3 19 1 2.36 9.48 19.89 o 4 19 1 251.47 332.11 41.42 o 5 19 1 115.09 104.13 31.51 o 6 19 1 304.23 342.37 59.77 o 7 19 1 2.74 -30.00 36.63 o 8 19 1 198.54 158.58 56.37 o 0 20 1 608.51 586.00 61.40 o 1 20 1 35.26 79.21 23.69 o 2 20 1 51.27 45.84 20.00 o 3 20 1 81.67 114.80 31.56 o 4 20 1 249.86 306.26 40.09 o 5 20 1 20.54 77.12 38.37 o 6 20 1 246.06 285.87 59.97 o 7 20 1 0.81 -8.39 47.51 o 1 21 1 64.80 87.61 22.73 o 2 21 1 572.74 498.02 50.50 o 3 21 1 14.31 -7.01 22.88 o 4 21 1 168.81 248.57 51.80 o 5 21 1 57.45 80.58 38.11 o 6 21 1 84.53 155.34 55.10 o 0 22 1 359.78 432.90 62.22 o 1 22 1 78.92 76.15 26.83 o 2 22 1 83.79 86.50 34.36 o 3 22 1 14.76 10.80 30.57 o 4 22 1 168.80 146.16 54.51 o 5 22 1 0.61 34.45 43.90 o 1 23 1 30.99 34.24 31.60 o 2 23 1 254.70 291.55 57.58 o 3 23 1 18.93 43.33 37.39 o 4 23 1 66.23 40.62 44.12 o 0 24 1 182.42 224.53 123.21 o 1 24 1 2.00 -15.67 39.82 o 0 0 2 7026.33 7489.31 601.79 o 1 0 2 5812.63 5582.77 174.70 o 2 0 2 19497.96 20714.91 423.64 o 3 0 2 54925.56 61383.05 1922.41 o 4 0 2 9460.61 9022.53 284.76 o 5 0 2 87.46 114.10 16.47 o 6 0 2 12593.28 12122.87 381.96 o 7 0 2 11555.74 11846.93 414.70 o 8 0 2 610.78 654.26 41.56 o 9 0 2 181.55 194.50 26.55 o 10 0 2 1960.56 2044.76 115.00 o 11 0 2 295.99 282.14 44.58 o 12 0 2 142.56 155.08 56.35 o 13 0 2 383.66 466.78 123.37 o 1 1 2 475.72 533.29 16.85 o 2 1 2 21601.01 22279.05 413.43 o 3 1 2 2468.77 2458.69 38.92 o 4 1 2 1911.53 1963.97 37.04 o 5 1 2 494.31 586.97 18.11 o 6 1 2 123.24 116.46 11.95 o 7 1 2 1.79 37.05 15.92 o 8 1 2 42.45 66.05 13.68 o 9 1 2 0.97 15.50 14.40 o 10 1 2 176.58 217.35 28.99 o 11 1 2 0.05 53.69 25.26 o 12 1 2 9.22 6.66 24.04 o 13 1 2 0.44 -9.35 41.65 o 0 2 2 36651.32 34543.46 1182.02 o 1 2 2 17838.92 18373.69 418.96 o 2 2 2 652.16 603.35 10.33 o 3 2 2 9003.68 8661.21 209.94 o 4 2 2 13217.30 14083.49 247.89 o 5 2 2 27.78 53.32 6.87 o 6 2 2 5975.77 5980.17 138.54 o 7 2 2 4451.30 4595.83 120.80 o 8 2 2 771.28 843.69 33.66 o 9 2 2 895.86 896.13 44.29 o 10 2 2 2342.87 2246.29 93.32 o 11 2 2 522.21 571.55 49.49 o 12 2 2 86.37 124.31 42.30 o 13 2 2 266.65 272.37 67.32 o 1 3 2 236.62 190.75 4.59 o 2 3 2 228.37 187.58 4.35 o 3 3 2 256.96 313.86 7.35 o 4 3 2 2463.52 3037.01 58.44 o 5 3 2 187.42 217.29 9.99 o 6 3 2 437.59 487.83 17.76 o 7 3 2 17.95 40.53 10.30 o 8 3 2 178.93 195.67 19.70 o 9 3 2 32.31 45.06 17.61 o 10 3 2 0.26 9.42 14.20 o 11 3 2 8.27 18.89 20.40 o 12 3 2 43.93 80.99 33.22 o 13 3 2 8.37 -14.20 37.75 o 0 4 2 40519.77 38323.17 1047.38 o 1 4 2 4253.22 4472.19 87.72 o 2 4 2 330.27 199.07 4.64 o 3 4 2 8989.37 9218.09 131.34 o 4 4 2 9507.75 10231.48 181.70 o 5 4 2 20.19 18.24 6.17 o 6 4 2 5885.66 5705.03 135.01 o 7 4 2 3906.47 4368.89 122.75 o 8 4 2 333.30 332.10 25.30 o 9 4 2 477.74 465.38 34.19 o 10 4 2 3171.41 3307.30 146.11 o 11 4 2 181.27 190.68 31.64 o 12 4 2 50.81 97.22 33.26 o 13 4 2 316.23 341.11 74.60 o 1 5 2 259.65 240.30 9.99 o 2 5 2 4.65 10.60 7.41 o 3 5 2 811.20 937.18 19.78 o 4 5 2 201.71 261.30 10.69 o 5 5 2 520.68 551.24 25.36 o 6 5 2 182.79 165.26 13.26 o 7 5 2 6.17 16.70 11.15 o 8 5 2 314.38 363.49 24.60 o 9 5 2 259.86 259.72 27.26 o 10 5 2 115.16 88.21 26.82 o 11 5 2 63.05 82.51 32.89 o 12 5 2 1.95 24.03 38.28 o 13 5 2 42.30 -30.99 39.22 o 0 6 2 33245.59 31305.73 766.37 o 1 6 2 6380.37 5922.71 171.70 o 2 6 2 5272.65 5666.26 112.23 o 3 6 2 6896.22 6991.85 106.96 o 4 6 2 12600.51 13525.89 279.79 o 5 6 2 19.93 51.37 13.01 o 6 6 2 6437.09 6688.54 165.78 o 7 6 2 2238.34 2433.83 86.61 o 8 6 2 480.64 474.62 28.13 o 9 6 2 1359.09 1326.28 67.58 o 10 6 2 1428.01 1498.27 83.95 o 11 6 2 466.40 408.69 47.93 o 12 6 2 157.04 165.82 37.10 o 1 7 2 1036.10 897.02 30.00 o 2 7 2 805.81 777.12 15.18 o 3 7 2 6.46 12.21 6.29 o 4 7 2 742.47 672.99 20.49 o 5 7 2 908.13 783.83 33.87 o 6 7 2 14.72 27.56 13.77 o 7 7 2 217.54 233.44 18.56 o 8 7 2 129.61 175.24 23.10 o 9 7 2 336.29 300.43 32.35 o 10 7 2 69.15 84.67 27.59 o 11 7 2 8.56 35.05 26.47 o 12 7 2 12.36 -17.09 28.58 o 0 8 2 7849.86 7514.13 210.60 o 1 8 2 4222.25 3889.00 105.71 o 2 8 2 1484.62 1634.89 30.85 o 3 8 2 10480.92 10642.37 193.08 o 4 8 2 4966.76 4703.87 100.94 o 5 8 2 612.59 572.32 20.98 o 6 8 2 4705.85 4401.77 146.65 o 7 8 2 1988.53 1855.58 72.82 o 8 8 2 404.24 351.18 31.04 o 9 8 2 417.47 422.64 36.74 o 10 8 2 2134.24 2242.67 129.48 o 11 8 2 134.76 123.32 34.05 o 12 8 2 9.18 73.35 39.57 o 1 9 2 1229.02 1126.63 32.64 o 2 9 2 1790.43 1795.06 36.22 o 3 9 2 350.09 374.04 14.39 o 4 9 2 17.98 17.36 7.90 o 5 9 2 823.85 775.80 27.87 o 6 9 2 56.67 62.03 11.19 o 7 9 2 87.24 108.19 22.61 o 8 9 2 164.07 168.37 23.63 o 9 9 2 51.12 54.26 23.74 o 10 9 2 83.18 65.19 26.95 o 11 9 2 260.52 292.31 52.95 o 12 9 2 109.61 122.60 41.20 o 0 10 2 15401.75 15839.46 751.42 o 1 10 2 6534.87 7296.23 184.31 o 2 10 2 64.22 96.41 10.73 o 3 10 2 3589.24 3167.48 78.84 o 4 10 2 5328.73 5344.25 129.59 o 5 10 2 5.83 4.96 9.46 o 6 10 2 974.27 923.31 43.15 o 7 10 2 1772.71 1715.05 69.88 o 8 10 2 40.07 65.90 30.84 o 9 10 2 615.27 595.00 52.06 o 10 10 2 852.05 897.72 81.50 o 11 10 2 466.14 428.64 64.73 o 12 10 2 117.83 135.29 46.10 o 1 11 2 526.91 535.80 21.73 o 2 11 2 510.28 514.02 19.27 o 3 11 2 382.06 411.27 18.71 o 4 11 2 509.68 481.78 21.32 o 5 11 2 12.47 13.94 10.56 o 6 11 2 318.52 333.45 25.14 o 7 11 2 403.24 401.60 30.04 o 8 11 2 372.57 374.71 37.57 o 9 11 2 101.81 103.88 34.22 o 10 11 2 29.80 72.49 40.82 o 11 11 2 87.50 120.95 40.99 o 0 12 2 8499.01 8459.04 279.64 o 1 12 2 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