#------------------------------------------------------------------------------ #$Date: 2009-11-11 20:41:08 +0200 (Wed, 11 Nov 2009) $ #$Revision: 840 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2223432.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2223432_Fobs loop_ _publ_author_name 'Zhu, Hui-Lan' 'Lai, Hui-Ling' 'Han, Lu' 'Luo, Yi-Fan' 'Zeng, Rong-Hua' _publ_section_title ; Poly[[aqua(\m~2~-oxalato)(\m~2~-2-oxidopyridinium-3-carboxylato)holmium(III)] monohydrate] ; _journal_coeditor_code HY2226 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1217 _journal_page_last m1218 _journal_volume 65 _journal_year 2009 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 71.810 _cell_angle_beta 78.862 _cell_angle_gamma 80.359 _cell_length_a 6.5391 _cell_length_b 9.5305 _cell_length_c 9.7391 _exptl_crystal_F_000 404.00 _reflns_d_resolution_high 0.8347 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1487.57 1581.81 74.47 o 1 8 9 935.00 1067.56 59.63 o 2 8 9 317.25 364.25 35.75 o 4 8 9 1190.84 1139.02 69.29 o 0 9 9 570.08 688.63 52.07 o 1 9 9 1131.85 1369.97 69.34 o 2 9 9 1284.42 1339.13 66.12 o 3 9 9 848.13 909.44 53.13 o 0 -2 10 2110.81 2303.50 107.32 o 1 -2 10 1944.67 2053.00 103.62 o 2 -2 10 810.66 835.77 68.08 o -1 -1 10 848.29 923.65 66.17 o 0 -1 10 208.96 184.11 36.86 o 1 -1 10 354.28 396.94 49.96 o 2 -1 10 1373.35 1749.86 95.27 o 3 -1 10 1598.16 1758.41 97.81 o -2 0 10 378.20 411.25 27.59 o -1 0 10 555.01 575.03 52.92 o 0 0 10 1592.10 1653.90 86.51 o 1 0 10 2399.58 2549.92 111.17 o 2 0 10 1041.92 1141.24 77.32 o 3 0 10 23.38 34.06 34.65 o 4 0 10 1343.28 1620.20 95.33 o -2 1 10 1742.34 1618.31 55.58 o -1 1 10 178.75 149.43 42.65 o 0 1 10 404.73 432.80 46.37 o 1 1 10 1542.14 1767.65 89.15 o 2 1 10 1825.53 1966.50 96.65 o 3 1 10 1951.08 2067.63 104.36 o 4 1 10 725.60 828.00 70.77 o -2 2 10 2166.34 1965.30 61.82 o -1 2 10 3122.11 3208.12 79.84 o 0 2 10 2242.98 2435.64 103.41 o 1 2 10 117.94 139.85 34.28 o 2 2 10 266.47 223.24 41.30 o 3 2 10 595.42 601.07 56.40 o 4 2 10 1147.32 1289.38 83.44 o 5 2 10 1373.77 1400.87 89.84 o -2 3 10 99.50 115.53 20.81 o -1 3 10 198.45 196.66 32.11 o 0 3 10 1733.12 1729.55 54.12 o 1 3 10 2542.89 2571.42 106.37 o 2 3 10 1901.95 2059.45 97.23 o 3 3 10 767.35 819.61 65.70 o 4 3 10 5.08 -27.78 29.31 o 5 3 10 213.46 160.50 43.73 o -2 4 10 1939.43 1976.11 88.15 o -1 4 10 1350.32 1407.11 99.47 o 0 4 10 715.99 780.40 78.90 o 1 4 10 0.23 -1.43 21.65 o 2 4 10 1067.68 1054.63 68.97 o 3 4 10 2860.36 3035.75 124.01 o 4 4 10 2291.25 2252.85 105.36 o 5 4 10 519.91 538.48 58.04 o -2 5 10 91.85 97.70 31.11 o -1 5 10 942.11 968.65 59.89 o 0 5 10 1903.35 2010.23 97.81 o 1 5 10 1463.74 1538.60 75.68 o 2 5 10 991.48 1117.10 68.92 o 3 5 10 130.69 95.38 35.02 o 4 5 10 454.71 477.27 55.14 o 5 5 10 1340.61 1310.29 82.23 o -1 6 10 415.62 451.34 44.68 o 0 6 10 32.40 42.73 23.34 o 1 6 10 442.88 446.32 31.79 o 2 6 10 1602.46 1719.54 83.97 o 3 6 10 1686.48 1828.50 91.95 o 4 6 10 984.44 978.73 70.77 o -1 7 10 1417.83 1704.91 83.23 o 0 7 10 1871.02 2185.88 90.47 o 1 7 10 804.37 969.23 56.25 o 3 7 10 186.88 204.28 39.61 o 4 7 10 880.10 835.77 68.82 o 0 8 10 207.05 180.94 32.48 o 1 8 10 1417.70 1719.12 77.42 o 2 8 10 1583.02 1711.73 74.62 o 1 0 11 1013.47 1121.80 75.79 o 2 0 11 1571.20 1833.72 100.08 o 0 1 11 1051.64 1130.94 72.83 o 1 1 11 296.42 333.94 45.68 o 2 1 11 3.58 32.00 30.21 o 3 1 11 608.05 701.20 66.28 o -1 2 11 153.07 191.50 35.97 o 0 2 11 1484.87 1599.44 85.29 o 1 2 11 2668.96 2832.16 118.83 o 2 2 11 1560.58 1693.08 92.85 o 3 2 11 298.52 316.72 50.07 o -1 3 11 1295.57 1381.27 54.50 o 0 3 11 480.72 528.98 50.17 o 1 3 11 122.93 126.75 33.48 o 2 3 11 903.02 1149.69 75.21 o 3 3 11 1682.96 1922.93 100.93 o -1 4 11 755.54 815.13 40.27 o 0 4 11 1534.62 1658.01 83.71 o 1 4 11 1455.43 1519.80 81.39 o 2 4 11 738.46 849.97 64.54 o 3 4 11 85.23 103.67 38.08 o 0 5 11 56.71 53.09 17.52 o 1 5 11 354.84 401.12 44.94 o 2 5 11 1397.31 1448.29 81.81 o 3 5 11 2455.73 2639.92 117.61 o 0 6 11 1448.61 1626.91 78.32 o 2 6 11 81.75 81.86 32.90 o 3 6 11 277.20 250.65 46.37 o