#------------------------------------------------------------------------------ #$Date: 2016-04-03 04:16:45 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181156 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/35/2223517.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2223517_Fobs loop_ _publ_author_name 'Choi, Hong Dae' 'Seo, Pil Ja' 'Son, Byeng Wha' 'Lee, Uk' _publ_section_title ; 5-(4-Bromophenyl)-2-(3,4-methylenedioxyphenyl)-3-methylsulfanyl-1-benzofuran ; _journal_coeditor_code PB2008 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2530 _journal_volume 65 _journal_year 2009 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 84.078 _cell_angle_beta 88.657 _cell_angle_gamma 68.055 _cell_length_a 12.3757 _cell_length_b 16.0670 _cell_length_c 19.5870 _exptl_crystal_F_000 1776.00 _reflns_d_resolution_high 0.8409 _cod_data_source_file pb2008Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 09ZB IN P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 777.64 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 63.19 363.46 46.52 o 2 0 0 138913.83 133660.70 7660.09 o 3 0 0 1219.61 1391.60 179.42 o 4 0 0 5862.27 5834.63 165.34 o 5 0 0 122.27 -35.64 75.18 o 6 0 0 1014.11 1110.10 148.09 o 7 0 0 174.11 175.34 105.65 o 8 0 0 4795.10 4641.25 220.66 o 9 0 0 4.21 -184.82 203.94 o 10 0 0 3751.82 4009.08 277.05 o 11 0 0 61.77 49.26 158.89 o 12 0 0 962.70 930.48 257.77 o 13 0 0 133.42 32.95 260.66 o -13 1 0 157.97 -111.74 246.91 o -12 1 0 2.47 -43.83 192.21 o -11 1 0 54.76 -129.50 207.12 o -10 1 0 75.40 -196.91 193.33 o -9 1 0 2453.65 2630.67 256.79 o -8 1 0 401.47 412.98 261.30 o -7 1 0 1659.79 1805.21 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