#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/35/2223546.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2223546_Fobs loop_ _publ_author_name 'Kele\,so\(glu, Zeynep' 'B\"uy\"ukg\"ung\"or, Orhan' 'Albayrak, \,Ci\(gdem' 'Odaba\,so\(glu, Mustafa' _publ_section_title ; (E)-3-[(3-Bromophenyl)iminomethyl]benzene-1,2-diol: a combined X-ray and computational structural study ; _journal_coeditor_code SI2198 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2410 _journal_page_last o2411 _journal_volume 65 _journal_year 2009 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 4.7411 _cell_length_b 18.9447 _cell_length_c 26.1417 _exptl_crystal_F_000 1168.00 _reflns_d_resolution_high 0.8219 _[local]_cod_data_source_file si2198Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' zeynep3b in P b c a' _shelx_refln_list_code 4 _shelx_f_calc_maximum 261.69 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' '-x-1/2, y-1/2, z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 11953.31 12443.19 181.24 o 4 0 0 670.29 665.97 25.62 o 2 1 0 9616.87 9527.05 67.13 o 4 1 0 258.69 288.71 15.28 o 0 2 0 2408.71 2616.92 78.86 o 2 2 0 937.31 876.59 17.85 o 4 2 0 6.13 8.19 14.69 o 2 3 0 9632.81 10021.61 105.54 o 4 3 0 520.74 569.62 18.14 o 0 4 0 3848.02 3682.98 63.22 o 2 4 0 7254.64 6820.78 67.01 o 4 4 0 112.08 126.67 16.95 o 2 5 0 20120.98 20672.73 156.28 o 4 5 0 1896.85 1930.68 22.45 o 0 6 0 41248.33 40560.18 225.07 o 2 6 0 418.08 633.77 19.66 o 4 6 0 9.53 14.15 14.00 o 2 7 0 9039.27 9126.45 55.49 o 4 7 0 44.55 31.17 17.65 o 0 8 0 4318.76 3612.09 509.48 o 2 8 0 725.37 733.88 17.61 o 4 8 0 213.46 231.07 16.85 o 2 9 0 78.94 78.32 22.25 o 4 9 0 2042.85 1993.93 32.50 o 0 10 0 10706.19 10470.52 59.65 o 2 10 0 2541.36 2394.49 37.22 o 4 10 0 294.75 280.49 23.71 o 2 11 0 494.03 554.89 18.67 o 4 11 0 610.68 505.12 44.18 o 0 12 0 20191.76 21562.83 112.62 o 2 12 0 1565.85 1558.44 26.73 o 4 12 0 21.53 44.95 18.91 o 2 13 0 806.85 862.14 21.89 o 4 13 0 72.35 128.97 20.89 o 0 14 0 2379.48 2475.16 78.25 o 2 14 0 860.04 803.69 21.19 o 4 14 0 80.91 89.04 22.51 o 2 15 0 775.02 828.73 41.42 o 4 15 0 837.27 725.03 41.57 o 0 16 0 851.41 780.51 36.66 o 2 16 0 1888.20 1655.25 58.86 o 4 16 0 299.93 254.16 29.34 o 2 17 0 61.71 91.71 18.63 o 0 18 0 508.30 661.89 40.49 o 2 18 0 170.29 141.22 23.55 o 2 19 0 7.55 1.04 17.87 o 0 20 0 279.81 261.64 23.46 o 2 20 0 245.58 229.82 17.91 o 2 21 0 18.60 26.52 22.60 o 0 22 0 57.74 18.46 25.36 o 1 1 1 24.77 24.02 12.54 o 2 1 1 6421.02 6227.99 40.87 o 3 1 1 706.41 661.26 12.51 o 4 1 1 0.50 4.19 11.78 o 5 1 1 33.22 45.40 12.42 o 0 2 1 2060.46 1935.17 183.42 o 1 2 1 25305.16 25156.51 209.18 o 2 2 1 20.22 25.33 10.26 o 3 2 1 187.36 197.48 10.69 o 4 2 1 79.02 77.09 11.81 o 5 2 1 88.92 88.61 12.40 o 1 3 1 58065.36 56919.35 309.70 o 2 3 1 5.90 11.03 10.01 o 3 3 1 6063.33 6008.09 35.59 o 4 3 1 213.60 222.97 12.90 o 5 3 1 37.31 38.52 12.39 o 0 4 1 22224.44 21266.21 1305.36 o 1 4 1 41182.23 42034.38 165.95 o 2 4 1 2328.79 2434.67 23.78 o 3 4 1 260.00 262.12 10.47 o 4 4 1 11.82 14.41 11.64 o 5 4 1 23.03 39.88 13.66 o 1 5 1 200.27 253.21 14.07 o 2 5 1 2975.19 3286.82 28.20 o 3 5 1 166.04 169.59 11.01 o 4 5 1 32.66 37.00 11.08 o 5 5 1 5.93 16.25 12.61 o 0 6 1 49.41 48.88 26.36 o 1 6 1 4827.40 4626.59 23.73 o 2 6 1 701.70 641.90 12.74 o 3 6 1 20.86 44.16 11.87 o 4 6 1 0.49 -1.53 11.54 o 5 6 1 377.47 364.50 14.32 o 1 7 1 4108.95 4093.05 72.77 o 2 7 1 4144.95 4121.69 41.88 o 3 7 1 3461.93 3473.58 24.86 o 4 7 1 16.89 23.96 12.31 o 5 7 1 106.73 111.75 14.47 o 0 8 1 9952.57 9916.30 126.70 o 1 8 1 24906.17 24901.74 209.88 o 2 8 1 5045.08 5054.26 50.88 o 3 8 1 415.04 409.17 12.37 o 4 8 1 114.17 122.02 13.12 o 5 8 1 44.40 34.54 13.76 o 1 9 1 3103.39 3489.68 33.36 o 2 9 1 219.77 234.33 13.42 o 3 9 1 783.97 771.11 13.61 o 4 9 1 12.05 20.12 12.49 o 5 9 1 158.33 131.43 14.76 o 0 10 1 2152.98 2091.58 54.05 o 1 10 1 61.27 68.31 14.58 o 2 10 1 1.89 22.45 13.85 o 3 10 1 148.11 162.87 11.96 o 4 10 1 254.30 244.52 13.67 o 5 10 1 22.47 43.73 14.94 o 1 11 1 1208.20 1213.56 19.25 o 2 11 1 150.63 151.66 12.83 o 3 11 1 1580.90 1609.19 31.34 o 4 11 1 0.32 18.50 13.82 o 5 11 1 13.02 19.48 17.47 o 0 12 1 86.32 104.05 19.58 o 1 12 1 4234.57 4094.95 50.28 o 2 12 1 165.30 168.69 15.54 o 3 12 1 1752.44 1599.23 18.10 o 4 12 1 15.21 21.81 13.03 o 1 13 1 146.83 158.94 13.43 o 2 13 1 89.22 125.38 14.47 o 3 13 1 994.47 943.99 16.18 o 4 13 1 225.48 219.32 16.16 o 0 14 1 195.14 198.34 20.94 o 1 14 1 946.64 895.55 16.45 o 2 14 1 43.18 40.18 15.09 o 3 14 1 609.70 597.63 15.81 o 4 14 1 142.64 112.25 13.42 o 1 15 1 7.73 0.28 14.69 o 2 15 1 48.34 73.12 14.27 o 3 15 1 0.85 3.83 13.75 o 4 15 1 35.99 26.51 15.48 o 0 16 1 13.30 38.40 16.95 o 1 16 1 151.78 191.32 15.33 o 2 16 1 26.03 35.66 13.22 o 3 16 1 49.73 53.10 14.42 o 4 16 1 0.30 0.84 15.35 o 1 17 1 143.52 180.79 14.66 o 2 17 1 408.58 380.28 13.58 o 3 17 1 449.81 461.74 21.78 o 0 18 1 17.74 45.97 21.68 o 1 18 1 626.14 622.67 13.71 o 2 18 1 2.40 6.94 13.84 o 3 18 1 81.79 103.31 16.24 o 1 19 1 0.22 11.18 13.70 o 2 19 1 3.09 -1.90 14.38 o 3 19 1 27.76 35.84 14.70 o 0 20 1 22.21 37.56 16.75 o 1 20 1 3.36 25.26 13.03 o 2 20 1 261.76 217.09 16.14 o 1 21 1 304.29 329.81 17.03 o 2 21 1 6.66 25.37 13.27 o 0 22 1 80.76 59.58 17.23 o 1 22 1 28.64 31.84 12.81 o 0 0 2 7375.29 8310.09 97.41 o 1 0 2 9170.77 9400.89 65.93 o 2 0 2 6923.67 6683.23 40.49 o 3 0 2 813.35 829.40 17.85 o 4 0 2 13.41 8.39 14.88 o 5 0 2 15.23 31.40 20.25 o 1 1 2 9201.83 9501.64 67.31 o 2 1 2 5977.07 5762.79 45.17 o 3 1 2 4165.37 4265.39 33.51 o 4 1 2 1075.74 1119.63 16.05 o 5 1 2 91.06 86.19 13.34 o 0 2 2 6808.57 7512.55 86.47 o 1 2 2 14.37 29.83 13.70 o 2 2 2 662.63 643.63 13.65 o 3 2 2 409.98 437.59 12.39 o 4 2 2 99.42 109.43 12.27 o 5 2 2 1.74 7.94 11.98 o 1 3 2 181.32 193.04 14.01 o 2 3 2 1814.72 1735.28 15.41 o 3 3 2 9.10 15.12 11.23 o 4 3 2 170.12 199.91 13.49 o 5 3 2 12.09 26.25 12.79 o 0 4 2 44905.48 43971.49 891.10 o 1 4 2 68481.54 67568.52 641.31 o 2 4 2 668.26 673.89 12.53 o 3 4 2 31.33 38.24 11.30 o 4 4 2 70.07 72.97 12.73 o 5 4 2 3.00 -1.49 12.34 o 1 5 2 3507.50 3780.27 27.49 o 2 5 2 5019.36 4641.76 37.22 o 3 5 2 416.63 393.35 12.63 o 4 5 2 1155.32 1184.65 14.10 o 5 5 2 183.12 188.75 13.79 o 0 6 2 18269.72 18218.40 139.15 o 1 6 2 483.15 452.86 14.45 o 2 6 2 10897.45 10784.08 52.60 o 3 6 2 106.13 100.07 11.03 o 4 6 2 47.40 72.89 12.73 o 5 6 2 5.05 7.47 13.01 o 1 7 2 272.13 283.80 13.94 o 2 7 2 1712.67 1626.59 15.22 o 3 7 2 22.32 41.52 12.15 o 4 7 2 177.30 171.31 11.65 o 5 7 2 26.71 39.16 14.25 o 0 8 2 1685.98 1700.48 31.11 o 1 8 2 5767.16 6387.02 64.60 o 2 8 2 504.19 503.54 13.92 o 3 8 2 300.13 297.22 13.17 o 4 8 2 224.78 240.22 13.08 o 5 8 2 7.37 -5.12 14.62 o 1 9 2 126.51 138.17 14.88 o 2 9 2 1483.40 1550.82 20.18 o 3 9 2 894.61 905.93 14.42 o 4 9 2 351.00 388.42 14.99 o 5 9 2 12.95 15.33 12.79 o 0 10 2 16155.76 15146.44 396.46 o 1 10 2 1074.17 965.52 15.47 o 2 10 2 2322.52 2193.52 24.37 o 3 10 2 2.22 -0.15 11.86 o 4 10 2 0.34 14.26 12.88 o 5 10 2 57.92 48.72 14.95 o 1 11 2 84.46 98.77 13.11 o 2 11 2 2497.18 2514.54 28.53 o 3 11 2 1672.74 1607.25 35.22 o 4 11 2 153.32 161.32 13.04 o 5 11 2 60.80 50.85 15.77 o 0 12 2 7.23 22.42 18.81 o 1 12 2 151.89 165.61 13.85 o 2 12 2 347.82 324.90 13.53 o 3 12 2 619.73 562.44 17.01 o 4 12 2 148.23 171.13 14.40 o 1 13 2 19.11 30.56 13.12 o 2 13 2 1103.38 1219.51 21.22 o 3 13 2 83.82 81.61 12.54 o 4 13 2 3.00 3.29 13.09 o 0 14 2 3086.64 3089.06 112.84 o 1 14 2 878.65 929.95 21.05 o 2 14 2 56.43 44.48 13.82 o 3 14 2 384.90 360.32 13.44 o 4 14 2 71.69 88.17 16.33 o 1 15 2 3.99 31.41 15.20 o 2 15 2 683.28 730.72 16.30 o 3 15 2 30.55 42.69 14.53 o 4 15 2 326.61 277.42 20.48 o 0 16 2 1324.43 1285.74 29.38 o 1 16 2 750.47 726.15 15.52 o 2 16 2 410.38 410.25 16.03 o 3 16 2 143.49 142.55 14.94 o 4 16 2 0.83 19.78 16.40 o 1 17 2 613.44 624.36 23.31 o 2 17 2 4.86 17.78 13.99 o 3 17 2 111.67 96.70 15.43 o 0 18 2 52.84 94.13 18.54 o 1 18 2 63.64 77.97 12.39 o 2 18 2 9.44 10.33 15.48 o 3 18 2 5.40 4.97 13.98 o 1 19 2 36.01 68.43 11.94 o 2 19 2 448.25 473.21 15.28 o 3 19 2 72.90 85.43 17.77 o 0 20 2 497.49 514.85 23.22 o 1 20 2 258.48 264.28 15.69 o 2 20 2 126.03 120.09 14.05 o 1 21 2 38.21 50.61 13.17 o 2 21 2 0.47 22.08 13.90 o 0 22 2 16.95 29.94 20.29 o 1 22 2 38.91 20.93 11.99 o 1 1 3 3854.31 3867.68 26.36 o 2 1 3 754.73 755.59 13.12 o 3 1 3 1348.97 1359.20 14.32 o 4 1 3 232.30 252.43 12.19 o 5 1 3 197.46 213.97 12.93 o 0 2 3 6224.55 6612.22 46.50 o 1 2 3 27365.88 26792.97 303.03 o 2 2 3 7144.49 7196.18 46.45 o 3 2 3 1791.71 1893.53 14.95 o 4 2 3 0.38 8.89 12.27 o 5 2 3 86.44 76.15 12.90 o 1 3 3 10143.59 10521.12 72.54 o 2 3 3 3938.83 4045.39 22.36 o 3 3 3 2470.03 2445.14 16.94 o 4 3 3 55.15 60.39 11.42 o 5 3 3 176.01 172.82 12.35 o 0 4 3 15370.94 16229.05 181.42 o 1 4 3 2104.14 2302.71 20.97 o 2 4 3 560.56 573.38 13.93 o 3 4 3 608.69 618.98 12.33 o 4 4 3 2.78 13.02 12.47 o 5 4 3 2.45 3.53 13.30 o 1 5 3 103.48 114.00 13.12 o 2 5 3 833.18 973.97 14.53 o 3 5 3 16.70 30.78 11.57 o 4 5 3 81.42 79.05 12.46 o 5 5 3 112.07 102.29 13.38 o 0 6 3 9333.18 8965.02 95.92 o 1 6 3 5073.10 4816.04 34.30 o 2 6 3 351.85 369.62 12.88 o 3 6 3 2.73 9.29 11.55 o 4 6 3 124.15 150.77 12.78 o 5 6 3 64.05 41.00 14.41 o 1 7 3 6210.94 5941.35 50.66 o 2 7 3 8929.43 8995.69 34.80 o 3 7 3 1519.97 1533.02 14.74 o 4 7 3 538.00 538.81 13.13 o 5 7 3 15.69 30.28 13.14 o 0 8 3 2691.40 2713.97 44.29 o 1 8 3 5323.59 4848.04 43.37 o 2 8 3 5061.05 5167.64 33.31 o 3 8 3 167.12 179.22 12.41 o 4 8 3 141.59 136.73 12.13 o 5 8 3 3.32 -0.17 15.94 o 1 9 3 1448.25 1517.93 17.99 o 2 9 3 162.07 164.79 13.41 o 3 9 3 363.26 350.67 14.81 o 4 9 3 73.71 69.31 13.97 o 5 9 3 23.21 28.50 16.65 o 0 10 3 148.69 180.71 22.21 o 1 10 3 28.08 46.17 13.28 o 2 10 3 214.80 198.27 12.77 o 3 10 3 2386.02 2337.40 16.55 o 4 10 3 109.36 130.02 13.83 o 5 10 3 28.66 35.44 16.40 o 1 11 3 1595.19 1567.71 21.21 o 2 11 3 1150.22 1190.31 17.68 o 3 11 3 721.12 755.24 15.58 o 4 11 3 108.41 129.02 13.60 o 5 11 3 1.24 18.36 14.59 o 0 12 3 3846.91 3794.59 28.77 o 1 12 3 2457.95 2463.55 21.76 o 2 12 3 892.37 881.96 23.54 o 3 12 3 434.97 400.77 13.51 o 4 12 3 74.19 71.19 12.69 o 1 13 3 659.11 755.81 17.63 o 2 13 3 195.89 241.93 13.59 o 3 13 3 522.93 511.52 14.22 o 4 13 3 167.42 146.29 15.28 o 0 14 3 6.30 24.07 16.84 o 1 14 3 1311.97 1261.51 17.82 o 2 14 3 938.62 931.33 16.22 o 3 14 3 80.07 81.79 13.54 o 4 14 3 26.21 24.64 12.90 o 1 15 3 536.49 584.37 14.88 o 2 15 3 85.37 109.30 13.44 o 3 15 3 172.44 179.86 15.08 o 4 15 3 7.30 16.19 15.34 o 0 16 3 116.90 118.19 17.44 o 1 16 3 1274.30 1333.91 23.79 o 2 16 3 201.91 230.04 18.28 o 3 16 3 16.91 19.91 14.47 o 4 16 3 10.08 12.52 14.17 o 1 17 3 275.46 292.96 12.70 o 2 17 3 306.61 307.05 17.50 o 3 17 3 69.64 88.20 14.85 o 0 18 3 297.76 288.86 16.55 o 1 18 3 472.76 437.20 15.01 o 2 18 3 107.55 122.69 16.50 o 3 18 3 45.53 39.85 14.76 o 1 19 3 36.85 42.18 13.36 o 2 19 3 73.27 79.17 19.37 o 3 19 3 22.93 -3.11 16.17 o 0 20 3 79.57 124.05 22.34 o 1 20 3 11.17 -0.32 13.28 o 2 20 3 77.41 69.68 12.30 o 1 21 3 4.60 22.66 13.91 o 2 21 3 68.84 59.51 14.03 o 0 22 3 73.49 115.94 26.34 o 1 22 3 200.92 174.80 13.22 o 0 0 4 20720.36 19482.54 1940.07 o 1 0 4 15724.97 16480.62 175.01 o 2 0 4 1698.49 1671.28 25.58 o 3 0 4 390.14 386.75 15.90 o 4 0 4 9.11 8.44 13.30 o 5 0 4 291.65 298.15 18.98 o 1 1 4 2579.46 2634.83 30.49 o 2 1 4 1536.69 1468.60 15.41 o 3 1 4 1732.03 1659.94 15.11 o 4 1 4 393.35 387.42 11.71 o 5 1 4 54.56 67.66 12.05 o 0 2 4 543.59 531.31 17.76 o 1 2 4 6686.75 6900.95 65.15 o 2 2 4 1314.16 1267.67 15.48 o 3 2 4 700.13 718.93 13.03 o 4 2 4 7.99 22.02 11.78 o 5 2 4 16.20 18.80 13.29 o 1 3 4 7549.30 7171.64 83.07 o 2 3 4 13.18 30.05 10.41 o 3 3 4 1095.88 1136.75 14.24 o 4 3 4 332.26 310.94 11.82 o 5 3 4 5.53 15.53 12.83 o 0 4 4 14494.80 14332.46 137.22 o 1 4 4 6358.99 6385.96 28.52 o 2 4 4 3801.52 3705.83 22.21 o 3 4 4 78.79 84.94 11.77 o 4 4 4 49.89 56.76 12.22 o 5 4 4 98.27 105.60 13.55 o 1 5 4 683.98 676.16 14.93 o 2 5 4 1465.21 1376.63 15.77 o 3 5 4 2085.86 2106.11 26.46 o 4 5 4 484.45 474.30 12.95 o 5 5 4 201.08 192.75 13.92 o 0 6 4 1899.86 1916.40 29.57 o 1 6 4 12309.31 12169.09 71.98 o 2 6 4 6032.29 6218.76 44.61 o 3 6 4 534.32 526.50 13.25 o 4 6 4 58.81 55.81 14.29 o 5 6 4 1.24 21.83 14.89 o 1 7 4 338.30 404.63 15.28 o 2 7 4 256.42 304.72 12.08 o 3 7 4 2.36 -1.39 12.54 o 4 7 4 34.34 42.41 12.30 o 5 7 4 25.34 32.06 14.28 o 0 8 4 881.68 783.97 24.33 o 1 8 4 2910.89 2901.16 38.05 o 2 8 4 542.63 557.44 13.50 o 3 8 4 25.58 17.36 12.38 o 4 8 4 154.62 158.70 12.53 o 5 8 4 87.14 89.90 14.02 o 1 9 4 814.95 753.23 16.34 o 2 9 4 6999.93 7142.69 63.45 o 3 9 4 1583.28 1599.96 25.27 o 4 9 4 16.18 17.34 13.16 o 5 9 4 2.21 6.99 14.57 o 0 10 4 3540.06 3259.81 106.46 o 1 10 4 6802.37 6703.55 49.57 o 2 10 4 1110.28 1063.89 14.85 o 3 10 4 163.24 165.49 12.39 o 4 10 4 47.04 44.74 14.62 o 5 10 4 0.45 7.14 16.70 o 1 11 4 7.01 23.13 14.46 o 2 11 4 145.04 160.07 12.88 o 3 11 4 99.42 102.79 13.16 o 4 11 4 124.52 104.60 13.12 o 5 11 4 67.61 46.84 19.55 o 0 12 4 723.34 860.07 25.49 o 1 12 4 194.19 187.75 12.42 o 2 12 4 476.88 449.10 15.04 o 3 12 4 7.89 29.73 12.96 o 4 12 4 110.21 106.86 14.05 o 1 13 4 28.58 43.61 13.32 o 2 13 4 373.70 417.83 12.89 o 3 13 4 5.43 38.24 12.64 o 4 13 4 39.73 42.56 13.05 o 0 14 4 1391.24 1421.06 41.91 o 1 14 4 871.21 882.54 21.04 o 2 14 4 76.97 86.91 14.52 o 3 14 4 1.16 15.78 14.39 o 4 14 4 47.48 70.85 15.40 o 1 15 4 497.19 531.09 14.73 o 2 15 4 611.77 640.21 17.04 o 3 15 4 994.29 970.78 24.50 o 4 15 4 58.37 49.91 13.30 o 0 16 4 812.83 749.83 36.85 o 1 16 4 634.99 586.46 15.99 o 2 16 4 72.52 51.65 15.66 o 3 16 4 211.43 187.01 14.24 o 4 16 4 3.79 22.29 14.94 o 1 17 4 84.99 123.51 13.38 o 2 17 4 0.16 13.43 14.20 o 3 17 4 37.44 42.18 14.74 o 0 18 4 363.85 437.26 21.67 o 1 18 4 5.86 29.54 13.36 o 2 18 4 17.88 38.23 13.65 o 3 18 4 77.91 74.61 15.42 o 1 19 4 30.92 49.67 13.43 o 2 19 4 306.09 298.99 15.84 o 3 19 4 138.37 145.41 15.61 o 0 20 4 99.06 154.50 19.95 o 1 20 4 183.72 200.27 13.38 o 2 20 4 44.46 51.84 13.34 o 1 21 4 68.35 77.59 13.79 o 2 21 4 40.41 25.00 14.32 o 0 22 4 18.52 44.34 20.09 o 1 22 4 0.51 8.05 13.90 o 1 1 5 25.08 41.95 12.54 o 2 1 5 4449.83 4383.70 49.32 o 3 1 5 2627.05 2547.39 24.36 o 4 1 5 601.70 616.64 13.74 o 5 1 5 58.48 63.43 13.50 o 0 2 5 46405.77 47229.54 195.72 o 1 2 5 4613.86 4484.61 60.10 o 2 2 5 4961.05 4873.53 34.98 o 3 2 5 15.15 21.73 11.44 o 4 2 5 19.44 31.62 12.03 o 5 2 5 12.14 15.06 13.14 o 1 3 5 667.59 647.42 15.22 o 2 3 5 4809.18 4704.44 31.25 o 3 3 5 612.99 558.99 12.44 o 4 3 5 299.27 307.36 11.71 o 5 3 5 33.64 39.71 13.21 o 0 4 5 17929.73 18211.64 349.41 o 1 4 5 6420.78 6385.82 27.77 o 2 4 5 1073.35 1026.63 14.71 o 3 4 5 1.08 0.79 10.98 o 4 4 5 17.23 40.07 12.64 o 5 4 5 45.11 54.47 14.54 o 1 5 5 2564.02 2494.56 27.42 o 2 5 5 110.78 113.33 10.98 o 3 5 5 11.53 15.78 12.97 o 4 5 5 415.94 448.78 14.99 o 5 5 5 7.51 31.20 13.95 o 0 6 5 5785.30 5401.43 87.14 o 1 6 5 2514.67 2405.34 33.22 o 2 6 5 678.41 665.04 14.06 o 3 6 5 169.66 187.53 13.62 o 4 6 5 258.79 271.48 13.49 o 5 6 5 1.23 4.03 14.39 o 1 7 5 183.69 202.71 13.23 o 2 7 5 3669.96 3596.50 30.79 o 3 7 5 909.94 894.71 15.21 o 4 7 5 197.27 203.64 12.84 o 5 7 5 29.55 23.66 15.62 o 0 8 5 13506.38 13540.76 178.66 o 1 8 5 2847.19 2616.80 40.61 o 2 8 5 336.74 307.72 13.40 o 3 8 5 201.08 198.31 12.56 o 4 8 5 0.19 0.51 11.66 o 5 8 5 0.97 8.22 13.02 o 1 9 5 5.90 7.66 11.48 o 2 9 5 767.29 825.53 14.10 o 3 9 5 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575.37 19.26 o 1 2 25 246.65 231.93 10.84 o 2 2 25 357.42 370.20 11.75 o 3 2 25 44.70 39.85 12.50 o 1 3 25 78.57 74.25 9.51 o 2 3 25 665.28 712.77 12.12 o 3 3 25 169.35 151.18 11.87 o 0 4 25 423.73 481.45 14.38 o 1 4 25 359.68 376.24 10.50 o 2 4 25 83.46 102.64 11.73 o 3 4 25 154.65 135.99 13.16 o 1 5 25 189.84 184.32 10.93 o 2 5 25 3.88 16.05 10.47 o 3 5 25 25.30 72.82 12.79 o 0 6 25 309.81 351.78 17.11 o 1 6 25 450.04 440.92 11.34 o 2 6 25 8.08 17.29 11.05 o 3 6 25 4.72 7.79 13.83 o 1 7 25 88.33 89.42 10.98 o 2 7 25 389.53 393.07 12.71 o 3 7 25 118.20 114.68 13.78 o 0 8 25 294.14 337.18 14.07 o 1 8 25 810.89 825.73 17.69 o 2 8 25 280.28 288.46 11.66 o 1 9 25 0.46 22.75 12.02 o 2 9 25 116.07 108.54 11.50 o 0 10 25 84.40 93.88 16.26 o 1 10 25 142.74 111.59 11.54 o 2 10 25 217.09 199.64 12.42 o 1 11 25 168.72 145.82 11.79 o 2 11 25 228.03 227.66 13.59 o 0 12 25 236.25 249.68 19.16 o 1 12 25 221.44 196.90 15.36 o 1 13 25 1.57 -0.82 12.48 o 0 14 25 7.78 43.13 17.33 o 0 0 26 2593.70 2618.54 72.27 o 1 0 26 162.25 212.22 15.29 o 2 0 26 376.15 388.06 19.84 o 3 0 26 92.56 70.11 16.04 o 1 1 26 199.22 198.21 10.56 o 2 1 26 276.20 283.74 11.19 o 3 1 26 266.74 225.86 11.94 o 0 2 26 191.35 221.61 18.32 o 1 2 26 6.30 10.62 9.96 o 2 2 26 2.43 15.67 11.86 o 3 2 26 1.58 1.08 12.55 o 1 3 26 0.51 12.15 9.20 o 2 3 26 110.33 109.41 11.85 o 3 3 26 0.99 19.01 12.73 o 0 4 26 1570.59 1581.04 25.05 o 1 4 26 269.92 284.61 10.53 o 2 4 26 149.78 166.77 12.22 o 3 4 26 12.04 24.72 11.90 o 1 5 26 18.23 45.91 9.43 o 2 5 26 251.94 249.09 12.46 o 3 5 26 100.09 102.23 14.53 o 0 6 26 726.98 736.48 15.20 o 1 6 26 1121.71 1149.12 20.64 o 2 6 26 233.05 240.63 12.95 o 1 7 26 1.96 26.18 10.87 o 2 7 26 33.99 32.98 12.81 o 0 8 26 98.19 103.66 13.34 o 1 8 26 1.08 22.50 14.00 o 2 8 26 31.15 20.60 12.15 o 1 9 26 18.62 32.06 11.61 o 2 9 26 16.82 27.73 10.78 o 0 10 26 659.40 591.94 21.26 o 1 10 26 52.89 77.68 11.22 o 2 10 26 61.65 57.40 12.59 o 1 11 26 47.56 54.18 10.73 o 0 12 26 46.12 47.70 15.42 o 1 12 26 48.99 58.66 12.38 o 1 1 27 175.91 163.78 11.24 o 2 1 27 88.38 104.67 12.14 o 3 1 27 40.53 46.24 12.46 o 0 2 27 293.68 356.69 37.33 o 1 2 27 1465.70 1491.54 24.17 o 2 2 27 7.35 17.41 11.10 o 3 2 27 49.62 33.86 25.11 o 1 3 27 374.47 384.90 11.40 o 2 3 27 171.33 184.24 12.45 o 0 4 27 110.15 144.18 14.46 o 1 4 27 375.33 389.64 14.46 o 2 4 27 1.55 21.51 11.09 o 1 5 27 32.51 33.90 10.73 o 2 5 27 3.16 19.94 11.60 o 0 6 27 0.39 24.26 15.30 o 1 6 27 75.11 69.48 11.15 o 2 6 27 0.75 -7.15 13.33 o 1 7 27 464.64 440.21 15.21 o 2 7 27 41.12 38.01 11.61 o 0 8 27 297.39 312.10 22.11 o 1 8 27 568.69 522.50 16.15 o 2 8 27 2.49 11.30 12.18 o 1 9 27 46.89 47.01 11.48 o 2 9 27 115.08 82.93 12.89 o 0 10 27 70.98 75.13 16.46 o 1 10 27 0.87 14.58 11.41 o 1 11 27 33.21 47.17 12.14 o 0 12 27 1.20 -0.70 14.63 o 0 0 28 2774.95 2668.51 61.06 o 1 0 28 23.06 64.32 16.03 o 2 0 28 303.10 331.23 27.33 o 1 1 28 60.06 85.65 9.82 o 2 1 28 257.38 263.01 12.18 o 0 2 28 238.09 215.76 14.61 o 1 2 28 0.33 7.46 11.07 o 2 2 28 163.70 170.61 11.44 o 1 3 28 1.45 10.98 9.76 o 2 3 28 46.79 34.22 10.34 o 0 4 28 1073.91 1087.25 24.80 o 1 4 28 5.66 17.43 13.15 o 2 4 28 78.35 66.16 11.83 o 1 5 28 107.55 95.15 10.98 o 2 5 28 323.25 320.30 14.37 o 0 6 28 852.13 917.51 37.63 o 1 6 28 9.25 20.12 10.59 o 2 6 28 137.03 144.53 13.64 o 1 7 28 69.81 81.43 9.89 o 2 7 28 1.91 8.43 12.37 o 0 8 28 86.25 56.80 15.08 o 1 8 28 57.84 48.62 10.87 o 1 9 28 2.05 21.17 11.06 o 0 10 28 734.04 771.92 34.20 o 1 10 28 0.38 -4.22 11.45 o 1 1 29 13.92 18.36 10.72 o 2 1 29 14.60 36.64 12.16 o 0 2 29 13.10 39.89 13.25 o 1 2 29 535.73 503.55 12.99 o 2 2 29 90.16 78.70 11.26 o 1 3 29 174.09 171.77 11.05 o 2 3 29 6.89 19.79 10.56 o 0 4 29 106.86 130.43 14.87 o 1 4 29 341.83 341.12 12.79 o 2 4 29 48.60 54.80 12.67 o 1 5 29 38.01 31.03 10.33 o 2 5 29 1.02 28.53 27.68 o 0 6 29 54.37 55.72 14.73 o 1 6 29 154.19 126.07 10.67 o 1 7 29 128.48 124.38 10.74 o 0 8 29 32.07 29.60 16.05 o 1 8 29 444.03 439.90 13.84 o 0 0 30 723.43 769.69 49.07 o 1 0 30 202.50 179.47 14.02 o 1 1 30 54.06 72.52 11.31 o 0 2 30 21.63 40.92 20.20 o 1 2 30 5.66 7.69 11.54 o 1 3 30 28.02 38.27 10.69 o 0 4 30 260.97 279.50 17.13 o 1 4 30 208.84 180.72 12.56 o 1 5 30 0.83 19.18 11.70 o 0 6 30 158.38 156.86 16.22 o 1 6 30 5.29 5.12 11.85 o 1 1 31 11.44 16.71 10.31 o 0 2 31 90.08 81.01 17.39 o 1 2 31 304.36 308.57 12.52 o 1 3 31 47.28 52.70 15.83 o 0 4 31 160.01 163.46 15.32 o