#------------------------------------------------------------------------------
#$Date: 2009-11-11 20:41:08 +0200 (Wed, 11 Nov 2009) $
#$Revision: 840 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/2223583.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2223583_Fobs
loop_
_publ_author_name
'Ye, Chen'
'Wen, Ting Bin'
_publ_section_title
;
 Dichlorido(\h^4^-cycloocta-1,5-diene)bis(triphenylphosphine)osmium(II)
;
_journal_coeditor_code           WM2258
_journal_issue                   10
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              m1242
_journal_volume                  65
_journal_year                    2009
_space_group_IT_number           43
_symmetry_space_group_name_Hall  'F 2 -2d'
_symmetry_space_group_name_H-M   'F d d 2'
_cell_angle_alpha                90.000
_cell_angle_beta                 90.000
_cell_angle_gamma                90.000
_cell_length_a                   39.6505
_cell_length_b                   10.4393
_cell_length_c                   17.6248
_exptl_crystal_F_000             3568.00
_reflns_d_resolution_high        0.8109
_[local]_cod_data_source_file    wm2258Isup2.hkl
_[local]_cod_data_source_block   I
#BEGIN Tags that were not found in dictionaries:
_shelx_title                     ' OsCOD in Fdd2'
_shelx_refln_list_code           4
_shelx_f_calc_maximum            703.90
_shelx_f_squared_multiplier      1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, z'
'x+1/4, -y+1/4, z+1/4'
'-x+1/4, y+1/4, z+1/4'
'x, y+1/2, z+1/2'
'-x, -y+1/2, z+1/2'
'x+1/4, -y+3/4, z+3/4'
'-x+1/4, y+3/4, z+3/4'
'x+1/2, y, z+1/2'
'-x+1/2, -y, z+1/2'
'x+3/4, -y+1/4, z+3/4'
'-x+3/4, y+1/4, z+3/4'
'x+1/2, y+1/2, z'
'-x+1/2, -y+1/2, z'
'x+3/4, -y+3/4, z+1/4'
'-x+3/4, y+3/4, z+1/4'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
1 1 -21 29706.50 33719.76 2117.47 o
3 1 -21 29021.31 32832.84 1864.88 o
5 1 -21 19210.90 20902.86 1739.13 o
7 1 -21 13745.36 16374.11 1645.03 o
9 1 -21 8552.09 8928.60 1477.54 o
11 1 -21 17429.99 19442.43 1662.41 o
1 3 -21 8986.83 7428.51 1649.00 o
3 3 -21 20708.11 21676.66 2118.31 o
5 3 -21 6945.71 7233.32 1688.35 o
0 0 -20 52171.00 57452.33 4475.34 o
4 0 -20 49699.34 56688.75 4525.07 o
8 0 -20 31504.80 36167.16 2340.07 o
12 0 -20 34561.46 36487.66 1990.62 o
16 0 -20 51222.25 52570.60 2604.30 o
2 2 -20 44249.73 46050.09 1893.48 o
4 2 -20 5410.80 5861.11 1415.00 o
6 2 -20 42087.02 45790.90 1885.48 o
8 2 -20 330.84 1658.97 1204.86 o
10 2 -20 36094.77 39100.54 1774.80 o
12 2 -20 5809.34 6961.15 1554.36 o
14 2 -20 27129.33 30085.68 1944.39 o
16 2 -20 6070.85 7969.49 1591.69 o
0 4 -20 36298.05 38638.22 4110.68 o
2 4 -20 973.94 3707.63 2298.15 o
4 4 -20 30682.58 31000.96 2908.72 o
6 4 -20 4213.97 6755.70 2062.75 o
8 4 -20 39329.89 40598.02 2518.70 o
10 4 -20 2113.51 2887.82 1683.87 o
1 1 -19 17474.62 18867.68 1352.28 o
3 1 -19 28267.08 30125.87 1883.18 o
5 1 -19 22190.89 22075.22 1687.34 o
7 1 -19 19081.95 20105.83 1431.65 o
9 1 -19 30332.22 31564.08 1632.54 o
11 1 -19 15567.52 15926.47 1456.18 o
13 1 -19 39252.20 41891.64 1605.02 o
15 1 -19 14456.10 16691.16 1256.21 o
17 1 -19 29718.23 30568.04 1486.05 o
19 1 -19 21590.76 20400.39 1374.84 o
21 1 -19 19225.49 21329.76 1570.45 o
23 1 -19 22077.45 23149.50 1661.72 o
1 3 -19 44023.89 42768.41 2052.40 o
3 3 -19 17944.04 17708.68 1654.37 o
5 3 -19 40245.45 39772.32 2373.34 o
7 3 -19 13149.78 14330.25 1565.82 o
9 3 -19 25652.49 27884.50 1571.09 o
11 3 -19 34662.76 36010.23 1889.80 o
13 3 -19 12274.00 13020.54 1601.34 o
15 3 -19 39795.73 43156.70 2209.34 o
17 3 -19 15374.57 16266.73 1707.67 o
19 3 -19 10445.86 13795.86 1693.19 o
1 5 -19 18418.41 21320.81 2559.27 o
3 5 -19 10454.84 10235.87 2307.68 o
5 5 -19 12074.83 14256.22 2815.60 o
7 5 -19 34955.40 36716.47 3012.38 o
9 5 -19 12475.12 14646.04 2601.72 o
11 5 -19 36042.19 37471.43 3023.26 o
13 5 -19 7448.72 6707.76 2324.57 o
2 0 -18 20626.29 22737.16 2301.12 o
6 0 -18 30101.59 31831.70 2013.71 o
10 0 -18 76462.35 74464.41 2576.23 o
14 0 -18 56644.27 59358.11 2408.53 o
18 0 -18 46338.87 49219.72 2301.23 o
22 0 -18 74666.45 81730.77 3433.29 o
26 0 -18 37743.44 41204.08 4205.72 o
0 2 -18 34563.38 38431.73 2583.29 o
2 2 -18 2195.11 1898.05 1097.81 o
4 2 -18 68701.74 68811.31 1884.99 o
6 2 -18 3013.32 3415.69 1096.16 o
8 2 -18 77351.81 79530.18 2055.03 o
10 2 -18 3540.45 5309.08 1239.43 o
12 2 -18 60169.87 62498.73 2159.40 o
14 2 -18 29726.79 28312.05 1596.89 o
16 2 -18 44003.44 45616.66 1785.85 o
18 2 -18 1519.52 2090.86 1279.32 o
20 2 -18 25523.90 28371.18 1636.73 o
22 2 -18 1402.60 2858.97 1283.17 o
24 2 -18 29582.40 29929.93 1924.35 o
26 2 -18 4366.40 5554.31 1581.43 o
2 4 -18 69898.47 72011.45 3285.06 o
4 4 -18 1769.02 3016.52 1953.52 o
6 4 -18 56910.61 61401.19 2588.94 o
8 4 -18 1882.14 1538.62 1342.21 o
10 4 -18 60867.11 60818.64 2116.51 o
12 4 -18 2052.70 2811.28 1370.49 o
14 4 -18 44178.34 45169.19 1830.67 o
16 4 -18 282.08 276.99 1379.28 o
18 4 -18 37408.79 37623.65 1953.42 o
20 4 -18 504.23 1446.33 1654.19 o
22 4 -18 19240.40 20776.29 2079.14 o
0 6 -18 45645.07 46486.09 4455.45 o
2 6 -18 7666.17 7570.67 2098.20 o
4 6 -18 15792.40 17727.80 2495.85 o
6 6 -18 441.14 614.19 2058.27 o
8 6 -18 27859.29 30408.48 2917.39 o
10 6 -18 873.63 283.76 2180.53 o
12 6 -18 32556.12 36137.29 2948.19 o
14 6 -18 2996.96 5355.00 2167.33 o
1 1 -17 11081.10 10209.08 1352.78 o
3 1 -17 11185.64 11669.51 1092.40 o
5 1 -17 21378.71 23478.01 1368.93 o
7 1 -17 27269.35 26902.84 1431.13 o
9 1 -17 42035.04 43356.41 1383.44 o
11 1 -17 45811.84 46753.59 1424.52 o
13 1 -17 41114.67 41282.57 1375.60 o
15 1 -17 54963.98 56581.07 1613.59 o
17 1 -17 28186.59 30972.74 1533.51 o
19 1 -17 19931.97 21621.25 1405.55 o
21 1 -17 26333.76 27911.03 1489.56 o
23 1 -17 23692.07 24494.29 1736.92 o
25 1 -17 32025.95 35465.98 2201.80 o
27 1 -17 17741.94 21078.89 1998.72 o
29 1 -17 22901.17 27508.24 2933.90 o
1 3 -17 59630.28 62826.96 2009.17 o
3 3 -17 89432.60 89047.98 2004.57 o
5 3 -17 39651.61 39951.14 1594.15 o
7 3 -17 34634.36 37875.17 2176.49 o
9 3 -17 31524.81 32628.15 1719.25 o
11 3 -17 16711.92 17220.30 1379.13 o
13 3 -17 48392.27 50889.26 1933.48 o
15 3 -17 8154.70 9527.42 1391.69 o
17 3 -17 31430.73 32766.20 1594.83 o
19 3 -17 29491.71 30586.37 1587.09 o
21 3 -17 9674.75 12144.33 1331.87 o
23 3 -17 20051.90 20054.61 1708.15 o
25 3 -17 3361.65 4085.24 1480.95 o
27 3 -17 13042.33 13112.64 1714.15 o
1 5 -17 36254.25 40618.02 3052.07 o
3 5 -17 33476.56 33516.47 2524.17 o
5 5 -17 16634.62 21273.43 2386.04 o
7 5 -17 17229.16 17316.24 2140.70 o
9 5 -17 20800.09 23021.09 1832.48 o
11 5 -17 20697.93 23387.99 1922.04 o
13 5 -17 23408.30 25235.37 1960.65 o
15 5 -17 17917.40 18519.00 1862.92 o
17 5 -17 28873.61 30609.59 1791.99 o
19 5 -17 24989.06 26909.67 2115.50 o
21 5 -17 27279.56 31192.58 2238.97 o
23 5 -17 28148.60 30659.82 2311.48 o
1 7 -17 13025.42 11515.57 2366.52 o
3 7 -17 6602.87 7185.07 1977.63 o
5 7 -17 16619.40 15920.58 2431.19 o
7 7 -17 29362.67 34796.61 2716.24 o
9 7 -17 15697.61 16458.60 2456.53 o
11 7 -17 21925.60 24010.73 2606.60 o
13 7 -17 11257.26 13057.54 2423.47 o
0 0 -16 10256.74 9493.30 1812.76 o
4 0 -16 37186.57 36136.23 1799.74 o
8 0 -16 79839.45 82009.39 2408.73 o
12 0 -16 63958.23 64771.38 2258.09 o
16 0 -16 94165.05 94556.48 2678.95 o
20 0 -16 46522.74 49007.45 2210.92 o
24 0 -16 91098.01 93540.17 3397.56 o
28 0 -16 85120.56 84571.80 5288.64 o
32 0 -16 37949.64 38684.63 4583.63 o
2 2 -16 82017.44 82352.13 1876.33 o
4 2 -16 6622.75 6591.43 1025.23 o
6 2 -16 74371.77 79933.98 1883.81 o
8 2 -16 193.83 498.00 1027.34 o
10 2 -16 116317.95 114763.68 2012.22 o
12 2 -16 13878.04 14436.08 1119.81 o
14 2 -16 55301.81 58134.66 2206.67 o
16 2 -16 3879.08 4614.06 1138.65 o
18 2 -16 36844.96 37211.21 1596.70 o
20 2 -16 2933.64 2963.87 997.86 o
22 2 -16 51566.98 54059.61 1800.42 o
24 2 -16 7916.31 8651.31 1238.47 o
26 2 -16 38222.66 40231.02 1944.73 o
28 2 -16 1123.20 1650.81 1621.05 o
30 2 -16 38722.42 44965.38 2446.27 o
32 2 -16 6750.05 7605.49 2458.43 o
0 4 -16 121489.59 127059.93 5383.67 o
2 4 -16 3759.50 5323.54 1826.29 o
4 4 -16 94940.88 91789.08 2217.32 o
6 4 -16 2590.75 2416.96 1132.02 o
8 4 -16 59859.52 59294.25 1941.51 o
10 4 -16 3021.86 4257.99 1214.18 o
12 4 -16 64572.20 64551.69 2666.34 o
14 4 -16 6885.43 6790.41 1361.55 o
16 4 -16 54044.43 54818.35 1822.23 o
18 4 -16 510.98 1700.80 1282.10 o
20 4 -16 53125.84 52465.03 2417.86 o
22 4 -16 1112.94 2745.52 1439.55 o
24 4 -16 20648.48 22240.30 1745.82 o
26 4 -16 2291.38 1758.22 1460.87 o
28 4 -16 24120.09 24035.89 1841.25 o
2 6 -16 36910.57 36562.65 2586.40 o
4 6 -16 1205.67 1819.79 1971.36 o
6 6 -16 34900.23 38584.76 2570.69 o
8 6 -16 549.28 1467.27 1834.07 o
10 6 -16 30314.45 29769.56 1947.14 o
12 6 -16 90.51 895.09 1508.84 o
14 6 -16 57052.25 57149.63 2591.03 o
16 6 -16 1204.05 2750.68 1605.21 o
18 6 -16 61237.27 64996.88 2661.35 o
20 6 -16 114.63 1563.79 1398.26 o
22 6 -16 45316.59 47102.51 2458.92 o
24 6 -16 3036.00 4563.30 1841.87 o
0 8 -16 40558.09 42536.73 4278.65 o
2 8 -16 2566.59 4324.99 2112.81 o
4 8 -16 30303.94 34535.17 2905.80 o
6 8 -16 2473.88 3290.33 2019.90 o
8 8 -16 48287.05 46027.20 3173.08 o
10 8 -16 3646.16 5134.00 2325.35 o
12 8 -16 40965.76 44646.04 3049.71 o
1 1 -15 26537.54 25984.79 1280.33 o
3 1 -15 51209.17 50401.20 1501.48 o
5 1 -15 37439.17 37416.27 1188.19 o
7 1 -15 50076.29 50733.48 1211.01 o
9 1 -15 23142.79 23856.62 1177.33 o
11 1 -15 73410.81 73656.42 1614.33 o
13 1 -15 11787.40 13143.15 1042.86 o
15 1 -15 42315.29 44054.02 1394.21 o
17 1 -15 28654.91 29178.32 1382.46 o
19 1 -15 32479.85 32886.56 1439.27 o
21 1 -15 26899.53 28961.98 1400.78 o
23 1 -15 57687.72 59912.02 1749.59 o
25 1 -15 35726.01 35230.04 2018.24 o
27 1 -15 28214.27 30334.27 2042.26 o
29 1 -15 47845.30 51628.43 2313.46 o
31 1 -15 13599.29 15172.84 2467.61 o
33 1 -15 27959.95 30522.62 2941.85 o
35 1 -15 5700.98 11047.84 2435.28 o
1 3 -15 87304.58 87210.95 1594.95 o
3 3 -15 45353.82 45832.85 1265.74 o
5 3 -15 55759.41 56841.15 1594.78 o
7 3 -15 21100.61 21670.40 1365.49 o
9 3 -15 32747.15 33944.05 1588.06 o
11 3 -15 48386.20 48339.02 1730.13 o
13 3 -15 23947.60 24005.56 1336.33 o
15 3 -15 40356.92 41256.50 1563.80 o
17 3 -15 34495.88 36126.32 1498.16 o
19 3 -15 32086.76 35647.12 1523.39 o
21 3 -15 48617.11 49597.23 1698.64 o
23 3 -15 19957.81 20212.81 1561.00 o
25 3 -15 23597.39 25046.97 1721.37 o
27 3 -15 13390.67 13023.10 1563.62 o
29 3 -15 14790.94 14415.98 1618.70 o
31 3 -15 22858.87 23192.65 2025.66 o
33 3 -15 15600.53 17547.44 2034.45 o
1 5 -15 50144.53 47207.05 3669.78 o
3 5 -15 32843.96 29746.79 2316.62 o
5 5 -15 49179.77 49785.63 2401.94 o
7 5 -15 19797.94 19460.05 1651.18 o
9 5 -15 35903.86 39382.70 2000.06 o
11 5 -15 5573.41 6576.29 1438.85 o
13 5 -15 41110.37 43525.29 2147.58 o
15 5 -15 18963.48 20120.94 1811.66 o
17 5 -15 45756.08 47909.42 2268.20 o
19 5 -15 45279.90 47187.05 1982.82 o
21 5 -15 42437.09 47167.56 2298.78 o
23 5 -15 26689.01 27577.12 2049.00 o
25 5 -15 21439.45 21291.83 1957.52 o
27 5 -15 14075.56 16788.28 1949.11 o
29 5 -15 2949.66 3176.28 1885.56 o
1 7 -15 28345.26 29737.23 2656.47 o
3 7 -15 26919.63 26351.27 2415.94 o
5 7 -15 20354.56 19885.09 2423.47 o
7 7 -15 11737.37 13054.22 1999.45 o
9 7 -15 28561.45 27796.52 2483.26 o
11 7 -15 9466.21 10871.88 1726.06 o
13 7 -15 39761.94 41691.83 2176.48 o
15 7 -15 12327.80 14728.90 1783.91 o
17 7 -15 35034.08 37800.85 2162.14 o
19 7 -15 26858.81 28061.46 2093.69 o
21 7 -15 22899.96 23524.86 2120.44 o
23 7 -15 32759.36 35967.45 3005.02 o
1 9 -15 29696.98 28663.54 2829.89 o
3 9 -15 17276.28 18582.82 2350.01 o
5 9 -15 26960.62 29925.00 2755.18 o
7 9 -15 31686.40 34186.43 2721.26 o
9 9 -15 15731.06 16448.58 2566.02 o
2 0 -14 140101.73 137237.11 2330.88 o
6 0 -14 91148.63 91183.41 2304.69 o
10 0 -14 140817.88 140083.75 2775.62 o
14 0 -14 87773.48 86238.45 2363.59 o
18 0 -14 42460.34 42423.07 1902.84 o
22 0 -14 64981.12 66206.45 2679.36 o
26 0 -14 94514.68 99817.31 3992.45 o
30 0 -14 91213.54 95487.21 5365.99 o
34 0 -14 29046.43 36090.04 4316.22 o
0 2 -14 77059.68 77508.08 2027.39 o
2 2 -14 7220.78 6621.29 841.78 o
4 2 -14 97187.01 96017.41 1852.93 o
6 2 -14 14423.98 13791.15 1112.34 o
8 2 -14 104403.88 102451.70 1742.28 o
10 2 -14 14552.89 15493.12 1040.34 o
12 2 -14 83670.01 80883.18 1788.32 o
14 2 -14 7780.23 8388.25 935.80 o
16 2 -14 66035.83 66401.75 1527.13 o
18 2 -14 4555.19 5553.06 915.87 o
20 2 -14 65626.18 64403.46 1700.77 o
22 2 -14 4074.20 4757.41 1068.72 o
24 2 -14 70858.73 71019.91 2140.15 o
26 2 -14 1105.99 1428.92 1285.91 o
28 2 -14 68237.11 70990.70 2554.80 o
30 2 -14 5258.81 5217.88 1593.97 o
32 2 -14 48115.12 44387.28 2278.39 o
34 2 -14 9898.96 10289.77 2454.72 o
36 2 -14 32238.29 32138.01 3068.59 o
2 4 -14 92169.47 90030.49 1815.07 o
4 4 -14 2226.08 3125.33 1234.93 o
6 4 -14 59298.19 59442.64 1779.96 o
8 4 -14 10239.01 10291.00 1172.75 o
10 4 -14 70332.91 69395.02 1952.44 o
12 4 -14 6348.92 6708.91 1127.42 o
14 4 -14 77119.00 74551.26 2024.60 o
16 4 -14 4442.51 4946.56 1236.77 o
18 4 -14 103760.70 103896.09 2100.78 o
20 4 -14 1913.65 2853.52 1080.86 o
22 4 -14 75348.86 75267.65 2186.87 o
24 4 -14 1753.75 1930.21 1292.43 o
26 4 -14 36883.13 37396.96 1827.73 o
28 4 -14 2726.33 3378.86 1390.44 o
30 4 -14 26625.86 25079.65 1754.94 o
32 4 -14 3305.13 4248.42 1741.67 o
34 4 -14 48643.22 50530.14 2643.36 o
0 6 -14 134764.67 132585.03 5379.25 o
2 6 -14 5318.61 4500.93 1863.35 o
4 6 -14 62227.54 64474.73 2985.61 o
6 6 -14 383.28 1120.57 1329.16 o
8 6 -14 52001.30 51413.03 2081.21 o
10 6 -14 788.46 1736.01 1419.41 o
12 6 -14 52303.87 54426.29 2219.18 o
14 6 -14 1510.21 2360.15 1402.74 o
16 6 -14 70027.30 70147.00 2681.10 o
18 6 -14 1275.82 2388.14 1492.70 o
20 6 -14 77233.91 81347.32 2668.49 o
22 6 -14 0.81 2555.91 1568.92 o
24 6 -14 46592.17 47867.50 2802.04 o
26 6 -14 4274.44 7883.23 3155.94 o
28 6 -14 26440.68 28452.12 3955.98 o
2 8 -14 48301.07 50753.10 2854.94 o
4 8 -14 2598.81 4307.01 1943.28 o
6 8 -14 61839.71 65634.15 5045.53 o
8 8 -14 4374.02 5788.92 2125.03 o
10 8 -14 44460.41 47146.52 2807.82 o
12 8 -14 2814.31 3381.16 1893.71 o
14 8 -14 39748.63 41633.65 2241.20 o
16 8 -14 5796.12 6524.84 1798.53 o
18 8 -14 38300.54 42311.73 2754.32 o
20 8 -14 335.12 3211.53 2016.93 o
1 1 -13 68866.65 65998.52 1476.12 o
3 1 -13 56314.86 55501.97 1280.49 o
5 1 -13 90353.08 86644.73 1408.01 o
7 1 -13 58212.18 57321.89 1226.39 o
9 1 -13 152013.50 145655.61 1936.85 o
11 1 -13 52333.31 51095.91 1311.25 o
13 1 -13 48712.36 47765.60 1298.45 o
15 1 -13 33691.89 33598.70 1211.40 o
17 1 -13 38494.81 38656.02 1365.11 o
19 1 -13 9191.40 9784.13 1033.84 o
21 1 -13 21289.26 21880.61 1206.34 o
23 1 -13 49966.25 50596.46 1535.43 o
25 1 -13 31654.42 32094.33 1529.46 o
27 1 -13 27395.41 28141.25 1886.57 o
29 1 -13 45694.43 46193.74 2192.60 o
31 1 -13 44416.77 44805.49 2386.07 o
33 1 -13 14187.34 14520.02 2554.43 o
35 1 -13 38932.21 36432.32 3380.26 o
37 1 -13 8990.56 12252.30 2665.91 o
39 1 -13 23347.84 27992.70 4536.12 o
1 3 -13 32081.58 31464.40 1042.53 o
3 3 -13 82390.16 78910.56 1389.63 o
5 3 -13 26708.98 26532.06 975.26 o
7 3 -13 34402.05 33171.34 1650.79 o
9 3 -13 14383.80 12516.17 1198.21 o
11 3 -13 25895.20 25480.53 1405.11 o
13 3 -13 37743.71 37911.09 1376.79 o
15 3 -13 38238.30 38515.15 1263.89 o
17 3 -13 73616.88 72002.60 2144.47 o
19 3 -13 93801.68 92099.00 1918.09 o
21 3 -13 67088.24 64684.71 1707.84 o
23 3 -13 80811.40 80690.18 1858.16 o
25 3 -13 51985.49 52424.77 1911.24 o
27 3 -13 29834.41 31751.63 1686.12 o
29 3 -13 27460.18 28473.79 1965.48 o
31 3 -13 13682.73 15615.91 1779.19 o
33 3 -13 16517.15 18487.51 1940.15 o
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10 10 8 79889.35 81528.56 4380.31 o
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13 7 9 122095.73 123732.07 2937.95 o
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