#------------------------------------------------------------------------------
#$Date: 2016-04-03 04:17:27 +0300 (Sun, 03 Apr 2016) $
#$Revision: 181157 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/36/2223660.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2223660_Fobs
loop_
_publ_author_name
'Starosta, Wojciech'
'Leciejewicz, Janusz'
_publ_section_title
;
 Di-\m-aqua-bis(\m-pyridazine-4-carboxylato-\k^2^<i>N</i>:<i>N</i>')bis[triaqua(pyridazine-4-carboxylato-\k^2^<i>O</i>,<i>O</i>')lead(II)]
 dihydrate
;
_journal_coeditor_code           BV2128
_journal_issue                   11
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              m1291
_journal_volume                  65
_journal_year                    2009
_space_group_IT_number           2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                92.050
_cell_angle_beta                 105.128
_cell_angle_gamma                102.851
_cell_length_a                   7.0762
_cell_length_b                   9.2967
_cell_length_c                   12.8300
_exptl_crystal_F_000             516.00
_reflns_d_resolution_high        0.7076
_cod_data_source_file            bv2128Isup2.hkl
_cod_data_source_block           I
#BEGIN Tags that were not found in dictionaries:
_shelx_title                     ' Pbazyn1s4 in P-1'
_shelx_refln_list_code           4
_shelx_f_calc_maximum            189.95
_shelx_f_squared_multiplier      1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
1 0 0 10399.05 7260.23 39.22 o
2 0 0 2780.09 3334.53 39.69 o
3 0 0 7486.51 8079.95 72.58 o
4 0 0 4980.56 5469.31 74.69 o
5 0 0 6081.33 5924.97 89.49 o
6 0 0 663.26 736.10 32.88 o
7 0 0 310.98 278.56 19.73 o
8 0 0 1155.08 1179.31 45.57 o
9 0 0 949.35 900.98 35.94 o
-9 1 0 1244.84 1042.14 49.79 o
-8 1 0 886.34 721.07 37.58 o
-7 1 0 4.04 -36.41 115.56 o
-6 1 0 775.74 552.66 23.25 o
-4 1 0 6283.62 3782.67 66.47 o
-3 1 0 1681.21 1365.57 33.35 o
-2 1 0 20531.21 21367.79 75.16 o
-1 1 0 22084.77 27207.02 159.72 o
0 1 0 12305.89 13968.36 190.72 o
1 1 0 1717.16 2142.06 18.32 o
2 1 0 7426.66 5247.12 35.00 o
3 1 0 9103.05 9957.07 58.95 o
4 1 0 10651.50 11005.79 73.99 o
5 1 0 2704.17 2706.70 48.62 o
6 1 0 37.98 23.72 36.17 o
7 1 0 1081.94 1020.30 40.40 o
8 1 0 1650.14 1578.13 66.47 o
9 1 0 669.49 625.47 26.78 o
-9 2 0 948.50 608.56 29.36 o
-8 2 0 500.81 303.22 22.08 o
-7 2 0 209.22 146.56 16.44 o
-6 2 0 2767.63 2335.13 67.88 o
-5 2 0 5931.76 5061.33 72.58 o
-4 2 0 5463.14 5113.47 58.72 o
-3 2 0 87.81 90.19 5.17 o
-2 2 0 165.58 211.39 10.10 o
-1 2 0 19454.77 23826.70 173.10 o
0 2 0 11828.37 13586.41 161.12 o
1 2 0 1785.57 2157.10 22.31 o
2 2 0 16154.29 20797.98 214.44 o
3 2 0 7031.29 7765.45 54.73 o
4 2 0 3658.50 4099.28 49.32 o
5 2 0 761.85 742.91 35.23 o
6 2 0 286.67 303.93 15.03 o
7 2 0 1394.43 1427.10 57.78 o
8 2 0 1294.58 1247.19 53.79 o
-9 3 0 601.10 457.30 24.19 o
-8 3 0 36.81 86.90 60.13 o
-7 3 0 724.55 640.51 34.29 o
-6 3 0 4982.72 4872.49 80.80 o
-5 3 0 4972.81 4922.52 66.00 o
-4 3 0 4154.81 4652.65 54.02 o
-3 3 0 1941.48 1956.98 32.18 o
-2 3 0 9334.10 10011.09 52.85 o
-1 3 0 17843.94 22193.61 198.70 o
0 3 0 10684.89 11458.98 35.54 o
1 3 0 422.03 527.06 16.91 o
2 3 0 5725.16 6666.70 49.32 o
3 3 0 9610.40 10262.41 69.05 o
4 3 0 2441.88 2717.98 45.10 o
5 3 0 346.73 366.64 14.56 o
6 3 0 382.36 390.60 16.68 o
7 3 0 2195.86 2391.03 67.64 o
8 3 0 1432.26 1385.76 55.20 o
-9 4 0 230.27 186.26 21.37 o
-8 4 0 11.77 36.88 57.78 o
-7 4 0 1047.97 1026.88 40.87 o
-6 4 0 4204.98 4444.55 73.52 o
-5 4 0 3562.76 3735.46 59.89 o
-4 4 0 96.89 102.88 7.05 o
-3 4 0 3328.64 3439.51 41.57 o
-2 4 0 24349.40 30692.57 285.84 o
-1 4 0 13971.67 14743.36 66.00 o
0 4 0 2444.85 2523.14 50.62 o
1 4 0 1661.47 1770.02 29.12 o
2 4 0 10724.15 12229.96 72.11 o
3 4 0 11339.89 13530.23 85.02 o
4 4 0 2480.70 3332.41 52.38 o
5 4 0 411.11 469.52 20.67 o
6 4 0 1990.69 1988.69 59.42 o
7 4 0 2058.85 2024.39 67.64 o
8 4 0 486.79 501.69 23.49 o
-9 5 0 175.83 182.73 20.90 o
-8 5 0 140.44 136.70 17.15 o
-7 5 0 2053.83 2130.32 70.46 o
-6 5 0 3910.53 4681.77 76.57 o
-5 5 0 2148.02 2235.31 50.50 o
-4 5 0 1945.35 2023.92 41.57 o
-3 5 0 9027.07 9689.78 69.29 o
-2 5 0 8566.83 8918.92 61.77 o
-1 5 0 3509.29 3497.06 39.69 o
0 5 0 22.10 10.92 18.09 o
1 5 0 5442.00 5734.95 51.91 o
2 5 0 10392.23 10998.74 76.10 o
3 5 0 5161.96 5676.70 63.18 o
4 5 0 90.94 114.15 9.63 o
5 5 0 1259.76 1210.78 50.73 o
6 5 0 1615.39 1563.80 61.07 o
7 5 0 1016.53 1054.59 44.63 o
-9 6 0 8.96 118.61 67.41 o
-8 6 0 563.05 542.33 24.90 o
-7 6 0 2115.23 2557.79 72.11 o
-6 6 0 1901.13 2026.27 59.42 o
-5 6 0 120.76 134.35 9.86 o
-4 6 0 1823.97 1908.60 44.63 o
-3 6 0 5620.50 5649.46 59.89 o
-2 6 0 5098.72 5452.16 54.96 o
-1 6 0 687.97 710.26 27.25 o
0 6 0 195.35 186.00 6.38 o
1 6 0 6556.43 6710.15 62.48 o
2 6 0 7062.94 7656.47 71.17 o
3 6 0 2169.52 2401.37 50.73 o
4 6 0 91.70 101.23 10.57 o
5 6 0 1021.48 1065.39 45.80 o
6 6 0 1636.81 1642.25 67.41 o
7 6 0 711.07 783.54 34.06 o
-9 7 0 35.26 9.63 69.52 o
-8 7 0 805.82 745.96 33.59 o
-7 7 0 1627.95 1629.10 67.17 o
-6 7 0 1158.67 1168.50 53.08 o
-5 7 0 21.51 30.06 10.33 o
-4 7 0 3208.18 3313.39 57.07 o
-3 7 0 6020.02 6008.82 66.94 o
-2 7 0 2674.37 2697.31 46.74 o
-1 7 0 17.59 -15.27 24.43 o
0 7 0 1529.39 1457.18 26.57 o
1 7 0 4181.95 4261.34 57.78 o
2 7 0 3946.55 4185.01 61.07 o
3 7 0 966.77 1022.65 41.57 o
4 7 0 223.66 204.11 12.45 o
5 7 0 2270.52 2387.74 67.41 o
6 7 0 1910.01 2121.63 74.46 o
-8 8 0 1087.40 1019.83 43.45 o
-7 8 0 1545.35 1427.10 66.70 o
-6 8 0 114.97 43.92 47.21 o
-5 8 0 750.03 826.53 36.88 o
-4 8 0 2366.57 2432.37 56.14 o
-3 8 0 4774.70 4751.29 66.94 o
-2 8 0 1115.46 1018.18 39.22 o
-1 8 0 50.80 47.68 29.36 o
0 8 0 2044.56 2043.85 33.55 o
1 8 0 4892.77 4903.49 68.11 o
2 8 0 4108.49 4190.65 68.82 o
3 8 0 1.79 46.98 40.40 o
4 8 0 1757.22 1774.72 64.83 o
5 8 0 1634.39 1768.14 71.40 o
-8 9 0 666.45 670.33 33.12 o
-7 9 0 307.22 309.57 17.38 o
-6 9 0 9.34 42.75 48.62 o
-5 9 0 958.42 984.36 45.33 o
-4 9 0 2960.05 2943.46 64.36 o
-3 9 0 4482.90 4467.56 71.40 o
-2 9 0 322.00 314.26 13.15 o
-1 9 0 1929.67 1830.15 49.56 o
0 9 0 4130.47 3932.08 47.41 o
1 9 0 3309.64 3134.18 64.36 o
2 9 0 509.49 544.21 21.14 o
3 9 0 61.29 49.79 47.68 o
4 9 0 1307.19 1302.38 57.78 o
5 9 0 1550.75 1626.75 64.36 o
-7 10 0 269.30 257.66 18.32 o
-6 10 0 155.57 151.51 11.38 o
-5 10 0 1555.61 1625.10 65.77 o
-4 10 0 1956.06 1948.53 64.36 o
-3 10 0 307.03 280.44 12.92 o
-2 10 0 0.37 13.86 39.93 o
-1 10 0 2376.37 2247.99 61.30 o
0 10 0 2850.61 2633.29 45.91 o
1 10 0 1493.15 1655.87 60.13 o
2 10 0 89.08 82.91 51.44 o
3 10 0 595.98 609.03 25.37 o
4 10 0 1058.79 1163.81 50.97 o
-7 11 0 31.51 -67.41 67.41 o
-6 11 0 264.57 282.56 18.09 o
-5 11 0 712.01 729.05 33.82 o
-4 11 0 1411.47 1335.03 55.67 o
-3 11 0 381.64 356.78 15.03 o
-2 11 0 329.44 328.36 14.33 o
-1 11 0 1748.86 1595.74 61.77 o
0 11 0 1942.87 1910.58 61.77 o
1 11 0 167.14 159.25 15.50 o
2 11 0 2.24 -1.17 55.43 o
3 11 0 641.30 736.80 27.48 o
-5 12 0 1326.17 1324.93 55.20 o
-4 12 0 598.88 566.99 22.78 o
-3 12 0 48.04 1.17 53.79 o
-2 12 0 611.65 590.95 23.25 o
-1 12 0 1207.17 1091.00 45.33 o
0 12 0 1228.13 1101.43 34.68 o
1 12 0 135.73 151.96 17.62 o
-3 13 0 68.90 28.65 64.59 o
-2 13 0 832.77 832.16 27.95 o
1 -13 1 745.86 752.54 27.48 o
2 -13 1 15.54 80.09 62.48 o
3 -13 1 650.28 609.03 22.55 o
-1 -12 1 1873.67 1839.54 76.57 o
0 -12 1 709.17 715.30 21.75 o
1 -12 1 40.20 23.02 55.67 o
2 -12 1 165.97 159.01 16.21 o
3 -12 1 1348.46 1314.60 47.44 o
4 -12 1 1109.50 1093.34 38.75 o
5 -12 1 463.00 466.93 19.49 o
-3 -11 1 66.30 -28.89 63.18 o
-2 -11 1 1117.23 1069.62 43.69 o
-1 -11 1 1208.54 1225.81 54.49 o
0 -11 1 1089.36 1021.34 31.89 o
1 -11 1 100.82 114.17 9.80 o
2 -11 1 871.81 832.63 39.22 o
3 -11 1 2267.91 2104.48 69.29 o
4 -11 1 1009.32 963.69 41.10 o
5 -11 1 3.57 8.46 54.96 o
6 -11 1 268.50 253.90 18.79 o
-4 -10 1 50.63 -7.52 61.07 o
-3 -10 1 265.34 303.69 18.32 o
-2 -10 1 3074.42 2955.20 76.33 o
-1 -10 1 2279.76 2234.60 65.53 o
0 -10 1 202.96 210.26 9.86 o
1 -10 1 332.27 307.92 12.68 o
2 -10 1 1242.71 1335.03 53.32 o
3 -10 1 955.96 892.53 42.04 o
4 -10 1 1075.01 1018.18 43.45 o
5 -10 1 34.33 20.35 34.63 o
6 -10 1 771.47 716.60 34.29 o
7 -10 1 731.99 683.96 28.42 o
-5 -9 1 652.57 701.34 26.54 o
-4 -9 1 17.06 85.73 51.44 o
-3 -9 1 2653.83 2640.23 71.87 o
-2 -9 1 3831.30 3724.42 73.75 o
-1 -9 1 2489.50 2394.79 60.13 o
0 -9 1 4.71 20.65 24.83 o
1 -9 1 616.06 561.12 26.07 o
2 -9 1 3615.16 3593.83 65.77 o
3 -9 1 2734.81 2721.03 62.24 o
4 -9 1 461.77 469.05 22.08 o
5 -9 1 58.03 52.85 46.04 o
6 -9 1 1284.18 1273.49 57.31 o
7 -9 1 875.68 802.80 40.16 o
8 -9 1 188.76 206.46 20.20 o
-6 -8 1 1422.94 1267.62 59.89 o
-5 -8 1 60.88 71.17 15.74 o
-4 -8 1 686.05 744.55 27.95 o
-3 -8 1 4197.56 4255.94 74.93 o
-2 -8 1 3310.27 3291.54 63.89 o
-1 -8 1 816.16 856.12 35.94 o
0 -8 1 791.51 731.58 20.99 o
1 -8 1 6205.82 6196.25 71.64 o
2 -8 1 3861.74 3569.17 59.42 o
3 -8 1 2600.34 2512.46 54.96 o
4 -8 1 62.07 59.19 10.57 o
5 -8 1 764.02 733.28 35.00 o
6 -8 1 2623.11 2652.21 71.87 o
7 -8 1 1173.71 1189.17 54.02 o
8 -8 1 31.45 -13.15 66.94 o
-6 -7 1 604.40 617.72 27.48 o
-5 -7 1 16.76 39.22 47.44 o
-4 -7 1 1019.72 1062.11 42.51 o
-3 -7 1 4016.24 4372.91 69.52 o
-2 -7 1 3541.83 3700.93 59.42 o
-1 -7 1 126.78 131.30 8.46 o
0 -7 1 2209.35 2133.42 30.39 o
1 -7 1 3893.04 3983.96 53.55 o
2 -7 1 4321.70 4309.73 56.37 o
3 -7 1 800.79 783.07 32.41 o
4 -7 1 339.63 358.65 14.80 o
5 -7 1 3317.48 3451.02 68.35 o
6 -7 1 2600.91 2602.65 69.29 o
7 -7 1 686.62 694.76 29.36 o
8 -7 1 26.67 104.52 65.53 o
9 -7 1 333.40 319.20 23.25 o
-7 -6 1 1149.48 1079.72 49.79 o
-6 -6 1 460.64 451.20 23.25 o
-5 -6 1 371.68 376.51 17.15 o
-4 -6 1 3986.46 4330.87 69.52 o
-3 -6 1 4404.67 4815.18 65.06 o
-2 -6 1 2272.32 2355.33 44.63 o
-1 -6 1 194.91 185.32 8.46 o
0 -6 1 5576.20 5480.81 132.23 o
1 -6 1 5625.55 5672.94 55.67 o
2 -6 1 3395.09 3543.33 47.21 o
3 -6 1 21.58 46.04 25.60 o
4 -6 1 956.15 988.59 38.52 o
5 -6 1 3642.29 3777.27 66.94 o
6 -6 1 1861.04 1922.92 60.36 o
7 -6 1 249.27 254.84 15.97 o
8 -6 1 203.03 204.81 19.26 o
9 -6 1 524.74 480.79 24.19 o
-7 -5 1 841.79 862.23 37.11 o
-6 -5 1 3.84 35.23 44.39 o
-5 -5 1 1429.73 1570.38 50.50 o
-4 -5 1 5859.79 6420.55 74.22 o
-3 -5 1 5516.26 6526.25 67.17 o
-2 -5 1 954.09 1020.53 31.71 o
-1 -5 1 983.85 1065.39 28.89 o
0 -5 1 7867.37 7499.92 179.44 o
1 -5 1 13636.59 13862.81 75.39 o
2 -5 1 3273.71 3595.00 43.45 o
3 -5 1 24.99 -14.09 23.49 o
4 -5 1 3230.74 3578.80 53.55 o
5 -5 1 4290.04 4169.04 67.41 o
6 -5 1 1815.85 1598.56 59.42 o
7 -5 1 28.17 -8.46 50.73 o
8 -5 1 406.00 366.41 20.20 o
9 -5 1 821.16 699.69 27.48 o
-8 -4 1 1127.71 1121.53 51.44 o
-7 -4 1 562.23 533.87 26.31 o
-6 -4 1 311.55 339.39 16.21 o
-5 -4 1 3063.78 3329.59 59.66 o
-4 -4 1 7093.92 7919.06 74.46 o
-3 -4 1 2242.31 2522.33 42.04 o
-2 -4 1 203.65 207.86 7.52 o
-1 -4 1 6885.85 7431.93 53.08 o
0 -4 1 21272.89 23765.39 175.55 o
1 -4 1 16656.79 17546.13 74.93 o
2 -4 1 80.06 105.22 5.17 o
3 -4 1 2223.53 2379.05 38.75 o
4 -4 1 5017.87 5261.21 62.01 o
5 -4 1 4889.64 4893.63 70.46 o
6 -4 1 1304.21 1144.78 54.26 o
7 -4 1 280.52 293.36 16.21 o
8 -4 1 999.29 815.02 31.24 o
9 -4 1 974.80 757.24 27.95 o
-8 -3 1 1179.34 1224.64 50.73 o
-7 -3 1 4.49 -24.90 45.10 o
-6 -3 1 1281.69 1524.34 50.26 o
-5 -3 1 4420.96 4944.83 63.42 o
-4 -3 1 5767.20 6248.39 62.95 o
-3 -3 1 803.96 886.18 27.01 o
-2 -3 1 4805.51 5929.90 46.98 o
-1 -3 1 7247.14 8091.22 48.15 o
0 -3 1 12519.17 12682.30 96.18 o
1 -3 1 9976.70 10046.32 50.73 o
2 -3 1 420.15 484.08 18.56 o
3 -3 1 8800.88 8922.68 66.23 o
4 -3 1 7242.61 7204.57 72.11 o
5 -3 1 1983.39 1845.89 51.44 o
6 -3 1 341.94 257.89 14.09 o
7 -3 1 456.59 366.17 17.85 o
8 -3 1 1436.26 984.60 44.39 o
9 -3 1 886.28 508.74 29.36 o
-9 -2 1 799.51 763.58 35.70 o
-8 -2 1 599.14 635.57 26.31 o
-7 -2 1 235.72 247.09 14.80 o
-6 -2 1 2133.60 2375.76 53.08 o
-5 -2 1 4322.49 4748.71 59.89 o
-4 -2 1 1987.25 2073.48 38.05 o
-3 -2 1 1317.93 1476.90 29.12 o
-2 -2 1 4836.35 5700.42 41.57 o
-1 -2 1 12631.97 15667.36 163.47 o
0 -2 1 8576.70 8489.06 117.67 o
1 -2 1 5554.97 5494.91 34.76 o
2 -2 1 4360.32 4601.68 41.34 o
3 -2 1 11275.26 10350.96 77.27 o
4 -2 1 5834.96 4487.06 67.88 o
5 -2 1 2110.78 1454.58 58.95 o
6 -2 1 11.60 64.36 53.08 o
7 -2 1 1450.29 1244.37 41.81 o
8 -2 1 2097.55 2405.83 100.76 o
9 -2 1 311.18 349.49 38.28 o
-9 -1 1 798.52 738.45 29.12 o
-8 -1 1 213.55 219.61 16.91 o
-7 -1 1 572.88 617.49 27.95 o
-6 -1 1 3891.60 3727.94 63.89 o
-5 -1 1 5732.92 5798.84 63.65 o
-4 -1 1 2758.59 2894.60 39.69 o
-3 -1 1 56.97 66.00 4.70 o
-2 -1 1 2693.62 4032.58 31.71 o
-1 -1 1 24503.30 30773.37 199.88 o
0 -1 1 12358.12 11633.50 232.06 o
1 -1 1 0.87 33.12 18.56 o
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3 -1 1 17587.63 18056.98 176.86 o
4 -1 1 4230.79 3156.96 93.01 o
5 -1 1 470.58 410.09 20.20 o
6 -1 1 811.08 790.83 30.53 o
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8 -1 1 1712.26 1848.70 67.41 o
9 -1 1 529.47 516.49 39.93 o
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-8 0 1 5.64 -45.33 95.36 o
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0 0 1 6868.66 6290.02 42.16 o
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2 0 1 2686.22 2466.66 30.77 o
3 0 1 18873.79 17489.76 93.48 o
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5 0 1 3.71 11.98 35.23 o
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7 0 1 2940.39 2774.58 89.72 o
8 0 1 1446.20 1428.75 60.60 o
9 0 1 16.89 89.02 85.02 o
-9 1 1 294.00 171.46 35.00 o
-8 1 1 275.76 116.97 23.02 o
-6 1 1 4546.78 2954.26 75.16 o
-5 1 1 2903.26 2451.63 54.73 o
-4 1 1 2703.19 2980.10 46.74 o
-3 1 1 10550.52 11352.47 69.76 o
-2 1 1 17770.81 24555.98 194.01 o
-1 1 1 10647.09 14335.38 109.69 o
0 1 1 333.35 338.63 5.98 o
1 1 1 7615.45 9079.58 106.16 o
2 1 1 15944.71 20253.30 201.52 o
3 1 1 6784.78 7310.73 53.32 o
4 1 1 4216.55 4624.23 52.14 o
5 1 1 1141.44 1253.06 39.46 o
6 1 1 2871.39 2820.15 62.48 o
7 1 1 1962.11 1823.57 65.77 o
8 1 1 472.53 496.29 19.49 o
9 1 1 0.69 -11.04 70.70 o
-9 2 1 8.60 -39.93 75.39 o
-8 2 1 434.87 389.19 19.02 o
-7 2 1 3194.95 2703.18 78.92 o
-6 2 1 3216.00 3055.96 66.23 o
-5 2 1 435.31 511.09 20.67 o
-4 2 1 1860.05 2085.46 40.16 o
-3 2 1 11682.26 13426.42 67.17 o
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-1 2 1 4628.95 5120.28 28.42 o
0 2 1 1986.46 2000.11 13.45 o
1 2 1 1308.67 1359.46 19.49 o
2 2 1 24757.29 31441.59 270.58 o
3 2 1 5070.21 5428.20 49.09 o
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