#------------------------------------------------------------------------------ #$Date: 2009-12-10 09:06:56 +0200 (Thu, 10 Dec 2009) $ #$Revision: 927 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2223665.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2223665_Fobs loop_ _publ_author_name 'Tao, Xuquan' 'Cui, Hui' _publ_section_title ; N-(2-Thienylmethylene)naphthalen-1-amine ; _journal_coeditor_code BX2244 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2779 _journal_volume 65 _journal_year 2009 _space_group_IT_number 41 _symmetry_space_group_name_Hall 'A 2 -2ab' _symmetry_space_group_name_H-M 'A b a 2' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 10.7793 _cell_length_b 21.2599 _cell_length_c 10.7244 _exptl_crystal_F_000 992.00 _reflns_d_resolution_high 0.8405 _[local]_cod_data_source_file bx2244Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 090901f in Aba2' _shelx_refln_list_code 4 _shelx_f_calc_maximum 237.71 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z' 'x+1/2, -y+1/2, z' '-x+1/2, y+1/2, z' 'x, y+1/2, z+1/2' '-x, -y+1/2, z+1/2' 'x+1/2, -y+1, z+1/2' '-x+1/2, y+1, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 5 -11 166.58 193.92 41.67 o 5 5 -11 4.07 3.01 27.13 o 1 7 -11 71.00 55.76 29.34 o 2 7 -11 21.28 2.66 25.73 o 3 7 -11 70.70 64.14 31.49 o 4 7 -11 43.28 35.40 29.94 o 5 7 -11 64.68 98.09 37.36 o 1 9 -11 74.53 77.85 23.19 o 2 9 -11 34.15 49.14 31.79 o 3 9 -11 80.05 29.09 31.19 o 4 9 -11 236.68 298.98 52.35 o 1 11 -11 17.17 12.00 19.32 o 2 11 -11 131.24 175.89 29.54 o 3 11 -11 125.26 135.40 37.31 o 6 0 -10 7.29 -9.58 24.47 o 4 2 -10 153.15 158.12 35.10 o 5 2 -10 160.88 209.32 39.47 o 6 2 -10 2.41 -8.88 23.72 o 7 2 -10 100.03 91.57 38.16 o 1 4 -10 554.64 549.87 45.28 o 2 4 -10 423.06 476.80 43.98 o 3 4 -10 442.80 504.03 47.14 o 4 4 -10 36.34 19.71 25.58 o 5 4 -10 19.92 29.29 25.83 o 6 4 -10 60.09 64.89 33.30 o 7 4 -10 21.02 27.13 32.55 o 0 6 -10 688.29 704.32 52.05 o 1 6 -10 458.96 503.80 32.40 o 2 6 -10 114.56 140.26 31.94 o 3 6 -10 40.75 42.12 26.58 o 5 6 -10 12.72 -14.64 25.37 o 6 6 -10 39.90 19.06 26.03 o 7 6 -10 110.13 97.04 36.36 o 0 8 -10 216.91 212.43 38.91 o 1 8 -10 300.50 345.28 31.36 o 2 8 -10 62.91 58.39 19.51 o 3 8 -10 228.78 227.14 27.87 o 4 8 -10 179.75 211.90 28.99 o 5 8 -10 2.74 -19.91 25.17 o 6 8 -10 97.38 103.71 39.82 o 0 10 -10 314.44 280.43 42.83 o 1 10 -10 345.49 498.47 116.49 o 2 10 -10 0.46 -3.17 15.36 o 3 10 -10 54.57 72.90 21.33 o 4 10 -10 27.29 17.81 19.12 o 5 10 -10 114.57 87.79 24.56 o 6 10 -10 8.11 11.48 28.23 o 0 12 -10 110.60 114.94 35.86 o 1 12 -10 151.48 171.14 27.77 o 2 12 -10 185.37 203.68 29.64 o 3 12 -10 55.42 50.45 21.80 o 4 12 -10 179.67 179.81 47.11 o 5 12 -10 27.79 34.43 19.87 o 0 14 -10 169.42 218.84 46.24 o 1 14 -10 56.15 10.83 19.06 o 2 14 -10 54.80 46.13 20.51 o 3 14 -10 46.46 31.79 20.01 o 1 1 -9 107.72 86.25 23.17 o 2 1 -9 87.88 83.20 24.52 o 3 1 -9 461.36 465.52 28.06 o 4 1 -9 33.09 17.95 14.61 o 5 1 -9 561.83 627.35 35.92 o 6 1 -9 87.51 58.45 19.91 o 7 1 -9 242.46 218.49 43.83 o 8 1 -9 47.06 31.56 22.78 o 9 1 -9 24.95 18.24 24.48 o 1 3 -9 250.41 226.71 20.55 o 2 3 -9 321.09 370.79 37.16 o 3 3 -9 45.10 44.58 23.22 o 4 3 -9 314.80 306.20 36.36 o 5 3 -9 53.12 24.17 23.42 o 6 3 -9 277.28 317.73 33.24 o 7 3 -9 76.10 69.72 22.63 o 8 3 -9 110.80 86.46 26.03 o 1 5 -9 80.64 64.39 16.39 o 2 5 -9 631.74 653.08 32.94 o 3 5 -9 98.77 74.79 17.17 o 4 5 -9 20.39 15.66 13.51 o 5 5 -9 182.74 235.14 39.42 o 6 5 -9 12.83 7.67 23.07 o 7 5 -9 167.44 190.46 42.07 o 8 5 -9 92.53 134.40 44.23 o 1 7 -9 659.82 614.81 33.70 o 2 7 -9 79.46 52.37 19.06 o 3 7 -9 387.94 370.57 27.98 o 4 7 -9 30.74 41.45 17.71 o 5 7 -9 886.03 995.55 69.86 o 6 7 -9 4.67 3.19 15.81 o 7 7 -9 372.04 413.12 50.35 o 8 7 -9 18.87 11.13 32.65 o 1 9 -9 124.03 137.45 22.92 o 2 9 -9 59.58 32.27 21.74 o 3 9 -9 202.83 185.88 25.39 o 4 9 -9 10.58 0.19 14.86 o 5 9 -9 16.06 14.06 16.96 o 6 9 -9 165.60 199.34 28.94 o 7 9 -9 3.36 -3.82 17.62 o 1 11 -9 83.86 83.13 22.35 o 2 11 -9 331.18 351.93 33.47 o 3 11 -9 51.76 37.99 18.04 o 4 11 -9 165.56 199.99 28.75 o 5 11 -9 27.88 19.99 17.61 o 6 11 -9 179.31 209.67 31.32 o 7 11 -9 11.00 -21.44 18.10 o 1 13 -9 66.73 70.35 21.19 o 2 13 -9 0.83 -17.91 15.27 o 3 13 -9 127.06 159.75 26.22 o 4 13 -9 131.45 109.57 23.95 o 5 13 -9 206.33 255.02 33.07 o 6 13 -9 98.60 58.75 25.11 o 1 15 -9 12.74 2.07 18.83 o 2 15 -9 49.86 69.12 23.47 o 3 15 -9 27.67 34.24 21.05 o 4 15 -9 21.79 17.18 20.17 o 1 17 -9 57.68 44.68 22.90 o 2 17 -9 22.33 8.52 21.44 o 0 0 -8 1166.30 1158.56 49.95 o 2 0 -8 3631.42 4091.25 122.16 o 4 0 -8 889.61 910.88 54.56 o 6 0 -8 443.65 456.24 46.89 o 8 0 -8 84.19 73.02 33.35 o 0 2 -8 1981.54 1947.49 73.77 o 1 2 -8 708.77 663.07 22.81 o 2 2 -8 489.25 514.76 20.87 o 3 2 -8 692.10 731.07 25.73 o 4 2 -8 246.39 229.74 17.43 o 5 2 -8 131.95 117.67 21.12 o 6 2 -8 18.67 -5.07 13.80 o 7 2 -8 283.02 296.49 33.10 o 8 2 -8 79.77 52.67 22.78 o 9 2 -8 220.35 256.68 37.80 o 0 4 -8 832.92 820.92 47.94 o 1 4 -8 719.90 754.55 32.29 o 2 4 -8 584.29 590.92 29.11 o 3 4 -8 296.53 263.50 22.87 o 4 4 -8 193.20 199.23 18.27 o 5 4 -8 319.19 355.61 22.91 o 6 4 -8 291.10 301.22 30.83 o 7 4 -8 71.97 98.25 24.33 o 8 4 -8 185.15 232.00 34.60 o 9 4 -8 0.49 2.48 21.79 o 0 6 -8 1177.71 1184.09 61.18 o 1 6 -8 288.04 265.29 21.92 o 2 6 -8 842.22 805.11 36.20 o 3 6 -8 25.98 16.71 12.83 o 4 6 -8 29.93 25.87 14.18 o 5 6 -8 215.68 215.85 25.67 o 6 6 -8 78.91 69.11 16.47 o 7 6 -8 161.69 178.17 23.20 o 8 6 -8 129.60 116.68 21.78 o 9 6 -8 36.92 14.56 22.87 o 0 8 -8 2003.29 2037.40 88.21 o 1 8 -8 1520.48 1511.20 52.28 o 2 8 -8 177.42 182.13 25.53 o 3 8 -8 260.03 286.30 27.80 o 4 8 -8 689.56 623.00 35.18 o 5 8 -8 401.28 371.45 29.39 o 6 8 -8 158.10 148.36 25.76 o 7 8 -8 126.19 97.83 24.06 o 8 8 -8 324.13 379.72 39.08 o 9 8 -8 10.19 -11.24 25.44 o 0 10 -8 148.75 171.30 34.10 o 1 10 -8 124.39 100.54 20.25 o 2 10 -8 210.44 227.46 26.65 o 3 10 -8 116.22 98.31 19.61 o 4 10 -8 213.06 225.82 31.09 o 5 10 -8 282.95 289.11 57.92 o 6 10 -8 63.63 55.65 19.99 o 7 10 -8 12.17 8.39 17.89 o 8 10 -8 0.64 -7.85 16.88 o 0 12 -8 278.91 301.74 39.01 o 1 12 -8 87.25 90.49 20.63 o 2 12 -8 282.11 275.38 29.56 o 3 12 -8 27.39 43.96 17.72 o 4 12 -8 315.00 286.61 30.84 o 5 12 -8 81.63 53.25 21.34 o 6 12 -8 145.78 120.64 24.37 o 7 12 -8 1.78 3.66 17.44 o 0 14 -8 233.58 239.46 42.48 o 1 14 -8 124.10 110.31 23.42 o 2 14 -8 219.88 226.48 29.16 o 3 14 -8 27.16 15.23 22.54 o 4 14 -8 24.00 10.78 16.89 o 5 14 -8 82.26 65.53 22.42 o 6 14 -8 23.78 0.79 17.87 o 7 14 -8 30.12 14.24 19.59 o 0 16 -8 300.44 307.51 47.54 o 1 16 -8 163.22 176.51 29.54 o 2 16 -8 44.83 38.96 21.22 o 3 16 -8 181.87 180.46 29.31 o 4 16 -8 35.79 27.05 25.37 o 5 16 -8 49.09 32.28 29.01 o 0 18 -8 39.99 22.42 24.72 o 1 18 -8 425.61 438.73 36.29 o 2 18 -8 37.75 42.64 21.76 o 3 18 -8 34.21 31.69 21.70 o 4 18 -8 18.18 -9.32 17.80 o 1 1 -7 230.48 212.95 10.85 o 2 1 -7 645.62 735.17 18.83 o 3 1 -7 525.03 545.22 20.68 o 4 1 -7 327.27 305.48 17.50 o 5 1 -7 425.10 422.55 21.80 o 6 1 -7 373.42 402.93 23.21 o 7 1 -7 440.98 455.41 34.01 o 8 1 -7 135.74 130.95 27.07 o 9 1 -7 112.85 101.23 26.79 o 10 1 -7 17.86 -2.02 23.60 o 1 3 -7 204.46 198.07 13.22 o 2 3 -7 388.64 379.61 17.34 o 3 3 -7 227.70 217.92 14.95 o 4 3 -7 1272.63 1302.91 44.85 o 5 3 -7 9.26 7.58 10.00 o 6 3 -7 1669.10 1779.74 49.16 o 7 3 -7 113.64 87.53 17.50 o 8 3 -7 594.96 620.93 32.69 o 9 3 -7 60.33 82.69 27.25 o 10 3 -7 36.64 50.50 27.86 o 1 5 -7 9.06 -2.35 9.44 o 2 5 -7 702.71 682.57 23.34 o 3 5 -7 66.68 69.04 11.47 o 4 5 -7 750.63 752.91 27.74 o 5 5 -7 183.58 178.40 18.90 o 6 5 -7 1379.13 1418.23 41.31 o 7 5 -7 154.35 159.02 20.62 o 8 5 -7 13.49 -3.53 14.16 o 9 5 -7 71.44 82.85 34.04 o 10 5 -7 65.91 59.75 22.71 o 1 7 -7 329.18 311.24 22.44 o 2 7 -7 63.28 68.71 15.44 o 3 7 -7 967.46 952.99 38.41 o 4 7 -7 49.17 38.16 11.61 o 5 7 -7 423.91 445.87 23.29 o 6 7 -7 176.56 189.18 21.51 o 7 7 -7 361.43 375.03 45.76 o 8 7 -7 205.53 213.13 38.59 o 9 7 -7 427.37 492.95 33.39 o 10 7 -7 6.07 14.01 25.21 o 1 9 -7 228.58 253.27 24.92 o 2 9 -7 1010.19 1005.66 42.83 o 3 9 -7 49.82 28.51 17.90 o 4 9 -7 908.24 931.71 41.68 o 5 9 -7 38.45 31.01 15.46 o 6 9 -7 289.20 286.13 28.56 o 7 9 -7 8.18 1.44 17.86 o 8 9 -7 39.13 15.41 18.11 o 9 9 -7 39.24 19.13 19.48 o 1 11 -7 1396.91 1391.73 51.43 o 2 11 -7 545.48 503.16 32.33 o 3 11 -7 66.20 67.81 18.36 o 4 11 -7 667.34 671.37 37.83 o 5 11 -7 212.72 196.56 35.76 o 6 11 -7 468.95 479.60 34.36 o 7 11 -7 11.65 -7.50 17.02 o 8 11 -7 358.41 399.50 36.58 o 9 11 -7 36.85 3.73 21.59 o 1 13 -7 61.63 42.84 17.56 o 2 13 -7 16.25 -14.22 12.74 o 3 13 -7 319.67 292.01 28.83 o 4 13 -7 123.41 94.91 21.24 o 5 13 -7 38.09 47.45 20.16 o 6 13 -7 95.24 73.17 22.05 o 7 13 -7 139.33 166.11 28.60 o 8 13 -7 22.72 11.91 18.69 o 1 15 -7 108.99 110.97 22.29 o 2 15 -7 8.09 6.39 15.36 o 3 15 -7 184.31 199.90 50.67 o 4 15 -7 31.61 1.87 16.87 o 5 15 -7 114.71 126.81 26.32 o 6 15 -7 84.46 73.63 23.94 o 7 15 -7 22.98 14.51 19.30 o 1 17 -7 22.76 33.04 18.55 o 2 17 -7 52.26 56.63 19.74 o 3 17 -7 39.02 30.36 18.55 o 4 17 -7 150.79 176.37 35.38 o 5 17 -7 23.40 10.05 19.86 o 6 17 -7 309.42 377.53 36.87 o 1 19 -7 12.60 5.02 18.56 o 2 19 -7 33.96 19.34 18.48 o 3 19 -7 65.94 96.12 24.51 o 4 19 -7 52.08 65.28 24.92 o 1 21 -7 46.05 48.29 22.34 o 0 0 -6 1295.29 1323.10 48.89 o 2 0 -6 193.13 192.01 17.73 o 4 0 -6 509.16 530.90 24.83 o 6 0 -6 23.83 12.24 11.55 o 8 0 -6 409.01 405.49 31.24 o 10 0 -6 70.36 101.45 44.73 o 0 2 -6 1407.96 1410.48 35.19 o 1 2 -6 6194.05 6388.91 90.85 o 2 2 -6 701.33 646.36 16.68 o 3 2 -6 1691.50 1898.98 33.65 o 4 2 -6 69.15 56.12 8.39 o 5 2 -6 307.08 296.30 14.79 o 6 2 -6 240.83 242.93 47.78 o 7 2 -6 1866.72 1949.60 50.17 o 8 2 -6 129.77 125.70 19.76 o 9 2 -6 79.63 69.66 18.54 o 10 2 -6 43.94 27.07 19.12 o 11 2 -6 49.26 24.67 29.74 o 0 4 -6 502.73 486.03 32.45 o 1 4 -6 3057.52 3142.05 38.27 o 2 4 -6 130.71 110.18 7.72 o 3 4 -6 2659.20 2801.43 53.72 o 4 4 -6 107.21 122.21 35.02 o 5 4 -6 405.25 390.69 20.03 o 6 4 -6 305.16 317.72 99.39 o 7 4 -6 173.95 199.00 38.68 o 8 4 -6 296.55 251.02 41.06 o 9 4 -6 472.74 532.16 56.89 o 10 4 -6 58.65 59.64 20.25 o 11 4 -6 108.40 136.18 27.15 o 0 6 -6 1744.37 1724.33 68.20 o 1 6 -6 261.26 247.68 12.80 o 2 6 -6 935.13 923.12 26.45 o 3 6 -6 2002.40 1973.62 40.30 o 4 6 -6 763.13 747.53 26.97 o 5 6 -6 408.66 406.36 21.88 o 6 6 -6 58.15 33.80 15.25 o 7 6 -6 409.80 367.79 34.45 o 8 6 -6 185.45 192.50 28.19 o 9 6 -6 247.37 306.12 42.15 o 10 6 -6 16.23 25.89 18.79 o 0 8 -6 1239.03 1191.36 59.83 o 1 8 -6 145.36 155.45 18.95 o 2 8 -6 1418.04 1447.21 35.46 o 3 8 -6 857.07 905.83 37.29 o 4 8 -6 138.71 159.78 20.94 o 5 8 -6 392.87 387.14 27.52 o 6 8 -6 47.69 27.79 16.24 o 7 8 -6 186.58 174.88 40.54 o 8 8 -6 73.06 78.98 22.99 o 9 8 -6 256.84 307.07 36.47 o 10 8 -6 47.58 74.68 32.85 o 0 10 -6 21.28 17.10 17.25 o 1 10 -6 879.37 877.10 37.61 o 2 10 -6 254.09 226.04 23.84 o 3 10 -6 789.10 719.68 35.15 o 4 10 -6 251.97 242.57 27.02 o 5 10 -6 832.37 770.15 55.69 o 6 10 -6 93.90 84.82 21.29 o 7 10 -6 132.79 128.32 24.78 o 8 10 -6 10.12 34.24 18.71 o 9 10 -6 69.50 99.38 50.50 o 10 10 -6 24.18 22.68 21.80 o 0 12 -6 1929.81 1815.90 82.29 o 1 12 -6 1057.26 990.19 42.87 o 2 12 -6 1796.69 1678.80 79.84 o 3 12 -6 298.63 283.58 26.79 o 4 12 -6 37.46 48.23 17.12 o 5 12 -6 111.76 115.46 23.95 o 6 12 -6 11.24 11.22 16.11 o 7 12 -6 141.41 151.76 25.66 o 8 12 -6 25.53 9.79 18.65 o 9 12 -6 79.75 77.94 34.98 o 0 14 -6 2447.89 2415.72 102.30 o 1 14 -6 28.54 32.68 16.88 o 2 14 -6 35.65 32.62 16.63 o 3 14 -6 306.97 306.90 29.93 o 4 14 -6 119.83 108.41 21.93 o 5 14 -6 78.24 60.03 21.12 o 6 14 -6 20.67 13.50 17.98 o 7 14 -6 6.89 8.90 18.81 o 8 14 -6 18.55 3.75 18.18 o 0 16 -6 603.47 554.98 49.35 o 1 16 -6 296.96 263.86 29.66 o 2 16 -6 185.10 194.61 26.67 o 3 16 -6 112.22 72.61 39.42 o 4 16 -6 22.26 23.80 16.50 o 5 16 -6 59.14 64.77 29.61 o 6 16 -6 36.28 13.31 19.11 o 7 16 -6 36.28 51.60 22.56 o 0 18 -6 261.58 288.80 46.64 o 1 18 -6 262.08 281.16 31.33 o 2 18 -6 77.28 51.74 19.35 o 3 18 -6 37.87 37.08 18.69 o 4 18 -6 98.45 109.55 24.55 o 5 18 -6 18.62 6.48 19.46 o 6 18 -6 33.14 18.50 20.31 o 0 20 -6 290.21 367.28 53.26 o 1 20 -6 49.99 59.67 21.16 o 2 20 -6 54.51 44.44 19.35 o 3 20 -6 20.42 33.98 20.33 o 4 20 -6 38.06 24.76 19.85 o 5 20 -6 1.25 -10.65 18.83 o 0 22 -6 28.11 30.19 30.44 o 1 22 -6 148.31 138.37 27.72 o 1 1 -5 400.06 389.90 11.30 o 2 1 -5 2274.79 2428.26 36.77 o 3 1 -5 2392.43 2518.74 39.41 o 4 1 -5 527.02 491.18 16.35 o 5 1 -5 2009.13 1950.40 36.10 o 6 1 -5 700.44 718.62 22.57 o 7 1 -5 1970.99 1971.94 41.99 o 8 1 -5 553.88 568.09 70.96 o 9 1 -5 463.75 468.55 29.60 o 10 1 -5 45.75 20.58 14.19 o 11 1 -5 18.73 12.09 20.14 o 1 3 -5 1.33 -1.32 3.08 o 2 3 -5 2861.52 2942.14 42.02 o 3 3 -5 270.12 253.93 10.64 o 4 3 -5 2175.03 2173.24 35.99 o 5 3 -5 53.81 47.10 8.91 o 6 3 -5 625.26 643.66 22.59 o 7 3 -5 50.23 33.53 11.09 o 8 3 -5 557.66 555.03 25.41 o 9 3 -5 19.34 4.64 15.61 o 10 3 -5 152.73 190.59 36.10 o 11 3 -5 8.35 5.83 19.87 o 1 5 -5 262.99 247.70 12.08 o 2 5 -5 3439.04 3767.86 57.17 o 3 5 -5 465.02 419.50 34.42 o 4 5 -5 554.78 525.13 19.04 o 5 5 -5 987.81 936.24 28.41 o 6 5 -5 1402.32 1386.40 49.83 o 7 5 -5 846.14 808.62 39.88 o 8 5 -5 1658.00 1748.85 63.74 o 9 5 -5 271.54 275.92 33.22 o 10 5 -5 100.19 103.77 25.60 o 11 5 -5 19.42 -14.20 20.43 o 1 7 -5 67.33 63.12 21.84 o 2 7 -5 255.09 226.61 18.49 o 3 7 -5 3988.09 3832.57 84.57 o 4 7 -5 626.10 615.47 30.51 o 5 7 -5 1182.26 1185.52 44.63 o 6 7 -5 41.07 24.47 14.92 o 7 7 -5 451.53 500.34 36.81 o 8 7 -5 94.27 83.83 21.45 o 9 7 -5 131.00 185.57 29.04 o 10 7 -5 83.10 67.49 23.08 o 11 7 -5 0.37 -11.60 20.86 o 1 9 -5 771.98 768.79 32.43 o 2 9 -5 1039.50 1065.16 39.23 o 3 9 -5 975.85 977.13 38.39 o 4 9 -5 226.06 227.37 23.23 o 5 9 -5 712.68 730.13 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2519.99 2542.95 39.58 o 6 1 3 169.62 209.07 12.14 o 7 1 3 1521.87 1547.79 31.35 o 8 1 3 2570.30 2543.85 109.42 o 9 1 3 1264.26 1183.79 80.74 o 10 1 3 53.29 76.93 36.26 o 1 3 3 8131.90 8169.02 67.39 o 2 3 3 5411.60 5375.10 55.01 o 3 3 3 1214.71 1240.08 16.50 o 4 3 3 4133.59 4229.05 47.73 o 5 3 3 447.03 416.14 17.51 o 6 3 3 1229.58 1137.93 30.30 o 7 3 3 714.85 710.84 25.20 o 8 3 3 1030.08 1067.73 70.22 o 9 3 3 437.93 408.67 32.12 o 11 3 3 49.69 48.54 34.55 o 12 3 3 48.24 27.83 35.30 o 1 5 3 3512.20 3519.87 54.20 o 2 5 3 5494.51 5501.65 56.56 o 3 5 3 5370.71 5639.96 59.45 o 4 5 3 1796.08 1685.83 28.76 o 5 5 3 852.07 800.22 19.95 o 6 5 3 2426.38 2420.01 46.62 o 7 5 3 628.71 653.61 24.01 o 8 5 3 68.88 46.00 13.26 o 9 5 3 346.46 453.54 64.77 o 10 5 3 43.50 13.99 21.09 o 11 5 3 14.99 4.16 29.14 o 12 5 3 42.87 42.83 35.55 o 1 7 3 1481.59 1540.35 20.96 o 2 7 3 520.28 529.95 11.59 o 3 7 3 2539.92 2795.42 35.11 o 4 7 3 3101.02 3303.75 41.24 o 5 7 3 4071.93 4081.41 50.10 o 6 7 3 55.10 70.53 9.09 o 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316.48 363.28 24.64 o 6 4 8 291.33 343.86 23.93 o 7 4 8 70.54 86.19 16.53 o 8 4 8 184.77 219.00 24.41 o 9 4 8 0.21 0.15 15.54 o 0 6 8 1213.45 1124.16 31.64 o 1 6 8 277.40 275.99 20.27 o 2 6 8 847.96 838.29 17.84 o 3 6 8 24.04 8.25 7.70 o 4 6 8 33.31 22.10 10.45 o 5 6 8 217.09 261.20 23.81 o 6 6 8 78.74 45.02 17.92 o 7 6 8 161.50 167.57 22.14 o 8 6 8 128.91 150.25 22.45 o 9 6 8 37.95 59.67 18.11 o 0 8 8 2039.62 2008.92 44.45 o 1 8 8 1499.70 1475.97 28.90 o 2 8 8 186.32 191.21 14.18 o 3 8 8 262.56 293.76 46.85 o 4 8 8 673.52 668.04 26.93 o 5 8 8 400.30 401.30 23.51 o 6 8 8 158.34 143.51 26.32 o 7 8 8 126.33 85.05 18.70 o 8 8 8 323.55 286.33 28.93 o 9 8 8 10.54 -4.92 15.20 o 0 10 8 146.68 134.48 30.92 o 1 10 8 109.41 102.08 14.24 o 2 10 8 210.89 215.99 20.95 o 3 10 8 113.58 135.34 20.04 o 4 10 8 213.79 226.86 24.62 o 5 10 8 289.75 295.11 39.36 o 6 10 8 63.86 36.07 17.14 o 7 10 8 12.21 4.97 20.48 o 8 10 8 0.68 3.67 21.50 o 0 12 8 280.03 212.88 37.26 o 1 12 8 93.37 77.77 17.12 o 2 12 8 290.64 284.92 36.00 o 3 12 8 27.54 35.00 15.80 o 4 12 8 307.32 293.85 51.23 o 5 12 8 80.15 71.40 19.73 o 6 12 8 144.39 129.78 22.60 o 7 12 8 1.63 -1.81 16.16 o 0 14 8 249.94 265.88 50.85 o 1 14 8 124.06 116.79 30.04 o 2 14 8 217.67 177.38 22.08 o 3 14 8 28.13 28.40 16.08 o 4 14 8 22.18 16.58 15.23 o 5 14 8 83.56 50.81 18.94 o 6 14 8 23.43 7.88 17.30 o 7 14 8 30.48 30.50 19.18 o 0 16 8 298.90 191.46 51.75 o 1 16 8 159.01 138.78 30.03 o 2 16 8 44.78 30.53 26.22 o 3 16 8 181.21 188.05 61.81 o 4 16 8 36.59 29.65 37.49 o 5 16 8 47.34 36.62 26.47 o 0 18 8 39.85 22.92 39.97 o 1 18 8 426.05 434.73 95.05 o 2 18 8 38.57 0.42 22.84 o 3 18 8 33.71 14.14 26.03 o 4 18 8 19.02 0.83 25.14 o 1 1 9 111.41 102.93 9.79 o 2 1 9 90.28 89.15 10.41 o 3 1 9 463.01 470.31 16.20 o 4 1 9 32.03 19.47 12.89 o 5 1 9 561.44 583.24 24.67 o 6 1 9 92.02 86.43 17.49 o 7 1 9 245.21 227.28 23.18 o 8 1 9 44.50 32.29 15.68 o 9 1 9 24.36 23.90 16.37 o 1 3 9 249.76 291.87 29.79 o 2 3 9 325.49 333.11 13.11 o 3 3 9 43.80 18.83 10.36 o 4 3 9 305.94 313.73 22.43 o 5 3 9 54.53 29.56 15.17 o 6 3 9 280.90 289.11 24.31 o 7 3 9 77.58 75.04 17.87 o 8 3 9 110.09 112.74 20.35 o 1 5 9 82.51 84.99 10.65 o 2 5 9 618.52 620.63 16.37 o 3 5 9 97.11 100.51 15.64 o 4 5 9 19.08 22.87 13.01 o 5 5 9 180.80 216.64 20.98 o 6 5 9 10.88 3.41 13.22 o 7 5 9 168.81 172.41 23.16 o 8 5 9 94.44 108.20 26.74 o 1 7 9 657.31 621.03 18.12 o 2 7 9 79.90 74.02 10.44 o 3 7 9 379.74 374.78 17.50 o 4 7 9 31.12 31.45 12.97 o 5 7 9 888.13 900.07 35.20 o 6 7 9 4.77 4.27 13.83 o 7 7 9 378.63 355.17 31.02 o 8 7 9 18.79 2.99 16.70 o 1 9 9 122.94 107.65 13.14 o 2 9 9 57.65 44.58 11.57 o 3 9 9 205.61 230.62 20.00 o 4 9 9 10.93 0.91 12.07 o 5 9 9 18.04 12.20 14.50 o 6 9 9 168.48 187.62 23.52 o 7 9 9 3.51 -3.77 15.29 o 1 11 9 83.02 53.02 11.32 o 2 11 9 327.89 345.77 25.52 o 3 11 9 50.65 49.13 17.10 o 4 11 9 164.82 225.83 43.48 o 5 11 9 26.34 33.01 17.26 o 6 11 9 186.74 154.20 29.95 o 7 11 9 11.14 0.29 21.64 o 1 13 9 68.04 76.71 18.60 o 2 13 9 0.89 -10.33 19.96 o 3 13 9 127.64 147.71 22.04 o 4 13 9 131.59 154.39 51.73 o 5 13 9 206.32 231.14 68.13 o 6 13 9 97.26 78.01 28.68 o 1 15 9 13.10 2.85 25.72 o 2 15 9 51.12 52.05 40.95 o 3 15 9 27.15 44.94 19.02 o 4 15 9 22.25 -0.05 16.60 o 1 17 9 57.51 70.43 27.18 o 2 17 9 21.82 17.63 28.95 o 0 0 10 634.08 629.25 45.89 o 2 0 10 643.91 644.56 27.19 o 4 0 10 63.63 96.95 24.75 o 6 0 10 7.79 22.34 20.79 o 0 2 10 11.05 -9.95 10.76 o 1 2 10 355.21 340.72 16.26 o 2 2 10 80.53 93.74 11.59 o 3 2 10 245.08 280.31 29.28 o 4 2 10 151.57 193.46 22.16 o 5 2 10 157.39 164.39 21.08 o 6 2 10 2.28 -1.56 14.14 o 7 2 10 101.12 103.99 19.69 o 0 4 10 644.69 638.54 26.95 o 1 4 10 567.29 565.73 18.10 o 2 4 10 418.56 402.63 17.56 o 3 4 10 443.43 448.19 19.11 o 4 4 10 37.49 31.58 14.51 o 5 4 10 18.73 6.54 14.10 o 6 4 10 60.33 54.46 17.39 o 7 4 10 20.36 5.32 15.72 o 0 6 10 657.27 641.02 29.55 o 1 6 10 465.29 462.94 17.21 o 2 6 10 118.35 161.36 16.40 o 3 6 10 41.68 40.20 12.91 o 4 6 10 250.08 269.90 33.11 o 5 6 10 12.53 5.44 14.83 o 6 6 10 39.15 28.09 16.75 o 7 6 10 109.50 65.99 20.20 o 0 8 10 228.69 210.61 22.10 o 1 8 10 306.17 328.11 17.81 o 2 8 10 65.96 73.37 13.06 o 3 8 10 230.37 261.01 32.21 o 4 8 10 179.95 169.36 38.00 o 5 8 10 3.06 5.34 15.38 o 6 8 10 97.11 78.12 19.84 o 0 10 10 317.06 262.14 23.66 o 1 10 10 351.59 308.48 18.68 o 2 10 10 0.45 10.65 14.19 o 3 10 10 58.36 54.32 15.61 o 4 10 10 27.27 40.66 15.87 o 5 10 10 112.25 94.50 20.43 o 6 10 10 8.03 19.26 16.49 o 0 12 10 113.90 92.23 18.10 o 1 12 10 153.94 148.67 23.21 o 2 12 10 186.27 188.75 20.54 o 3 12 10 52.69 34.89 14.58 o 4 12 10 182.07 218.39 31.50 o 5 12 10 28.34 49.08 18.99 o 0 14 10 169.86 149.34 45.94 o 1 14 10 56.36 76.85 31.02 o 2 14 10 53.90 64.90 21.25 o 3 14 10 47.40 51.49 21.90 o 1 1 11 273.26 279.85 20.14 o 2 1 11 59.69 49.40 13.49 o 3 1 11 206.80 256.24 22.89 o 4 1 11 5.23 14.64 14.42 o 5 1 11 61.98 68.25 18.93 o 6 1 11 17.72 10.49 15.93 o 1 3 11 176.04 186.70 25.38 o 2 3 11 287.34 329.16 29.14 o 3 3 11 61.84 58.61 17.86 o 4 3 11 193.97 276.12 24.32 o 5 3 11 3.08 -11.03 14.87 o 6 3 11 273.83 340.02 30.41 o 1 5 11 48.48 43.75 11.98 o 2 5 11 154.49 158.35 18.13 o 3 5 11 22.01 13.59 12.47 o 4 5 11 166.17 131.80 21.40 o 5 5 11 3.54 -0.53 15.68 o 1 7 11 71.87 54.70 13.07 o 2 7 11 21.17 1.99 11.85 o 3 7 11 73.85 82.98 16.17 o 4 7 11 43.58 10.72 15.65 o 5 7 11 68.68 52.31 19.51 o 1 9 11 73.81 60.86 13.91 o 2 9 11 34.07 37.07 12.75 o 3 9 11 77.26 46.81 17.48 o 4 9 11 234.84 239.83 27.25 o 1 11 11 17.36 22.59 12.22 o 2 11 11 130.56 134.16 20.42 o 3 11 11 126.83 113.11 19.84 o 0 0 12 21.97 -18.25 22.27 o 2 0 12 62.99 68.80 29.44 o 4 0 12 110.67 72.80 26.68 o 0 2 12 95.21 90.44 22.03 o 1 2 12 51.92 24.79 13.04 o 2 2 12 198.70 219.75 30.16 o 3 2 12 109.13 124.39 23.03 o 4 2 12 21.00 14.14 17.64 o 0 4 12 140.33 142.12 24.45 o 1 4 12 12.47 -16.61 12.89 o 2 4 12 76.61 53.14 15.58 o 3 4 12 55.36 57.84 19.50 o 0 6 12 374.64 379.58 32.04 o 1 6 12 74.80 58.40 15.36 o 2 6 12 257.85 246.28 22.20 o 3 6 12 31.95 45.58 20.85 o 0 8 12 181.43 164.28 22.90 o 1 8 12 37.37 35.02 14.53 o