#------------------------------------------------------------------------------ #$Date: 2009-12-10 09:06:56 +0200 (Thu, 10 Dec 2009) $ #$Revision: 927 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2223675.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2223675_Fobs loop_ _publ_author_name 'Fun, Hoong-Kun' 'Surasit, Chanasuk' 'Chanawanno, Kullapa' 'Chantrapromma, Suchada' _publ_section_title ; Bis[(E)-1-methyl-4-styrylpyridinium] 4-chlorobenzenesulfonate iodide ; _journal_coeditor_code CI2919 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2633 _journal_page_last o2634 _journal_volume 65 _journal_year 2009 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _cell_angle_alpha 90.000 _cell_angle_beta 101.799 _cell_angle_gamma 90.000 _cell_length_a 8.1103 _cell_length_b 20.5054 _cell_length_c 9.5549 _exptl_crystal_F_000 720.00 _reflns_d_resolution_high 0.6196 _[local]_cod_data_source_file ci2919Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' pr7cl_0m in P2(1) (100K)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 176.10 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 -32 0 438.69 436.36 26.38 o 3 -32 0 285.21 282.11 21.30 o 2 -31 0 129.97 156.94 16.42 o 3 -31 0 175.03 189.81 17.71 o 4 -31 0 358.51 353.17 22.93 o 2 -30 0 625.63 648.50 31.61 o 3 -30 0 517.56 474.58 26.67 o 4 -30 0 228.58 222.62 18.16 o 5 -30 0 452.07 519.04 26.43 o 1 -29 0 33.75 20.60 8.83 o 2 -29 0 45.65 39.87 9.99 o 3 -29 0 24.22 25.04 8.52 o 4 -29 0 90.25 104.78 13.30 o 5 -29 0 230.93 221.10 17.06 o 6 -29 0 244.79 277.68 40.22 o 1 -28 0 1110.47 1088.56 42.42 o 2 -28 0 636.42 628.59 29.98 o 3 -28 0 1156.71 1152.80 43.65 o 4 -28 0 172.41 182.06 15.75 o 5 -28 0 169.15 178.75 11.81 o 6 -28 0 92.91 87.01 8.78 o 1 -27 0 3.76 14.72 7.07 o 2 -27 0 261.84 287.61 19.47 o 3 -27 0 376.64 372.38 21.94 o 4 -27 0 227.26 210.38 16.71 o 5 -27 0 580.46 575.05 20.39 o 6 -27 0 509.25 493.09 23.57 o 1 -26 0 485.17 517.78 25.52 o 2 -26 0 468.38 456.87 24.56 o 3 -26 0 377.92 375.98 21.59 o 4 -26 0 447.52 462.00 32.10 o 5 -26 0 190.44 196.71 11.76 o 6 -26 0 187.26 168.61 10.59 o 7 -26 0 86.29 85.74 12.61 o 1 -25 0 90.26 79.15 10.68 o 2 -25 0 132.92 127.77 13.07 o 3 -25 0 91.07 71.83 10.62 o 4 -25 0 416.35 406.84 16.57 o 5 -25 0 117.10 124.54 9.49 o 6 -25 0 365.32 364.82 33.72 o 7 -25 0 520.92 536.37 15.86 o 1 -24 0 2075.44 2128.86 63.29 o 2 -24 0 1726.95 1802.37 54.99 o 3 -24 0 723.84 733.24 30.48 o 4 -24 0 560.19 573.75 23.27 o 5 -24 0 314.96 314.71 13.90 o 6 -24 0 78.44 87.91 7.84 o 7 -24 0 28.63 23.44 5.75 o 8 -24 0 47.73 52.74 7.37 o 1 -23 0 313.83 348.08 18.93 o 2 -23 0 42.16 48.42 8.42 o 3 -23 0 523.59 536.64 18.07 o 4 -23 0 596.92 598.95 19.54 o 5 -23 0 180.12 181.68 13.72 o 6 -23 0 280.79 266.13 9.99 o 7 -23 0 607.07 595.24 26.19 o 8 -23 0 242.46 222.36 12.96 o 9 -23 0 81.23 95.15 12.27 o 0 -22 0 1287.92 1236.23 53.05 o 1 -22 0 1082.74 1081.86 37.75 o 2 -22 0 937.76 974.09 35.10 o 3 -22 0 818.15 757.73 22.29 o 4 -22 0 391.72 373.74 14.52 o 5 -22 0 820.82 815.78 23.00 o 6 -22 0 104.04 104.03 7.77 o 7 -22 0 101.15 87.40 8.17 o 8 -22 0 66.68 64.34 7.54 o 9 -22 0 86.53 95.32 11.95 o 1 -21 0 484.81 501.82 17.21 o 2 -21 0 306.21 314.96 22.68 o 3 -21 0 260.79 259.77 11.86 o 4 -21 0 1044.26 1020.21 26.13 o 5 -21 0 1349.38 1356.09 26.12 o 6 -21 0 567.37 560.67 19.12 o 7 -21 0 1076.35 1066.41 37.88 o 8 -21 0 1074.84 1065.76 61.17 o 9 -21 0 333.16 310.26 13.94 o 0 -20 0 4347.00 4407.60 89.23 o 1 -20 0 3363.22 3205.53 67.80 o 2 -20 0 1376.78 1383.98 55.40 o 3 -20 0 1510.21 1502.65 33.98 o 4 -20 0 463.74 489.05 12.80 o 5 -20 0 385.23 373.07 17.92 o 6 -20 0 838.39 882.14 18.53 o 7 -20 0 167.30 182.47 14.87 o 8 -20 0 157.68 162.22 10.01 o 9 -20 0 1.82 2.98 3.66 o 10 -20 0 114.40 117.00 12.65 o 1 -19 0 435.39 454.50 14.51 o 2 -19 0 645.22 633.18 15.66 o 3 -19 0 363.24 365.70 10.70 o 4 -19 0 106.29 97.79 6.91 o 5 -19 0 653.21 651.08 15.20 o 6 -19 0 541.89 551.81 13.37 o 7 -19 0 71.95 90.08 12.03 o 8 -19 0 414.91 398.16 27.09 o 9 -19 0 399.64 408.11 15.27 o 10 -19 0 48.60 36.89 5.40 o 0 -18 0 7962.83 7502.36 144.60 o 1 -18 0 4504.02 4373.24 62.90 o 2 -18 0 2826.57 2765.32 46.51 o 3 -18 0 1997.38 1971.12 29.87 o 4 -18 0 1276.84 1293.76 35.37 o 5 -18 0 493.71 479.30 12.33 o 6 -18 0 649.10 628.26 14.09 o 7 -18 0 127.88 124.25 15.27 o 8 -18 0 264.30 256.06 11.66 o 9 -18 0 122.51 124.65 16.30 o 10 -18 0 53.29 66.00 9.76 o 1 -17 0 1152.93 1076.81 19.28 o 2 -17 0 1094.22 1050.14 18.07 o 3 -17 0 211.47 223.93 6.73 o 4 -17 0 471.36 475.28 10.97 o 5 -17 0 2443.03 2351.07 37.77 o 6 -17 0 1956.59 1932.91 31.74 o 7 -17 0 1155.94 1163.49 28.18 o 8 -17 0 1384.72 1326.77 31.28 o 9 -17 0 418.04 424.36 22.17 o 10 -17 0 994.05 974.68 36.83 o 0 -16 0 4197.88 4335.69 67.60 o 1 -16 0 3697.46 3671.57 45.55 o 2 -16 0 3335.23 3199.00 43.86 o 3 -16 0 1809.48 1824.51 27.38 o 4 -16 0 364.01 345.38 8.39 o 5 -16 0 1427.38 1409.25 22.23 o 6 -16 0 396.69 384.71 9.60 o 7 -16 0 45.81 53.13 5.52 o 8 -16 0 433.96 436.23 14.66 o 9 -16 0 104.28 114.30 7.49 o 10 -16 0 109.23 122.12 11.77 o 11 -16 0 52.49 51.88 9.13 o 1 -15 0 204.66 225.44 5.38 o 2 -15 0 1066.19 1063.39 15.64 o 3 -15 0 795.62 815.48 14.41 o 4 -15 0 3303.61 3284.60 44.31 o 5 -15 0 557.15 514.09 10.38 o 6 -15 0 554.36 529.12 9.91 o 7 -15 0 1306.21 1276.93 44.05 o 8 -15 0 296.63 272.78 11.63 o 9 -15 0 651.38 661.00 17.92 o 10 -15 0 181.59 164.32 13.09 o 11 -15 0 50.51 50.74 8.60 o 0 -14 0 2112.27 2196.15 31.24 o 1 -14 0 4545.25 4689.13 46.76 o 2 -14 0 5551.77 5548.89 64.46 o 3 -14 0 3792.99 3858.34 46.55 o 4 -14 0 4249.61 4218.01 55.55 o 5 -14 0 912.71 975.04 15.87 o 6 -14 0 162.53 160.74 5.96 o 7 -14 0 226.14 210.46 14.33 o 8 -14 0 60.29 56.24 5.29 o 9 -14 0 158.66 155.30 7.60 o 10 -14 0 121.43 131.44 11.46 o 11 -14 0 21.02 23.83 6.73 o 1 -13 0 650.31 671.24 8.96 o 2 -13 0 538.20 545.51 9.25 o 3 -13 0 483.89 535.43 9.24 o 4 -13 0 1765.70 1719.36 24.99 o 5 -13 0 952.06 984.66 15.52 o 6 -13 0 1733.50 1677.29 29.14 o 7 -13 0 1818.21 1815.43 36.55 o 8 -13 0 663.26 643.19 17.08 o 9 -13 0 479.17 487.63 21.41 o 10 -13 0 911.55 938.81 33.29 o 11 -13 0 256.46 260.95 15.91 o 0 -12 0 5291.26 5109.13 66.56 o 1 -12 0 4474.94 4457.52 54.18 o 2 -12 0 2254.15 2131.70 26.26 o 3 -12 0 2114.50 2176.71 27.37 o 4 -12 0 1829.03 1737.56 22.43 o 5 -12 0 970.80 907.47 13.24 o 6 -12 0 81.70 79.43 5.32 o 7 -12 0 34.00 41.55 4.83 o 8 -12 0 292.69 298.41 10.21 o 9 -12 0 40.71 36.35 6.26 o 10 -12 0 26.99 22.14 5.84 o 11 -12 0 5.25 8.32 4.85 o 1 -11 0 713.75 776.15 10.26 o 2 -11 0 1518.24 1509.78 28.49 o 3 -11 0 1034.60 1064.90 13.17 o 4 -11 0 1178.70 1196.68 13.85 o 5 -11 0 2088.25 1987.11 27.43 o 6 -11 0 893.47 898.95 17.92 o 7 -11 0 1886.67 1773.70 35.08 o 8 -11 0 1377.31 1357.40 27.95 o 9 -11 0 935.28 909.75 30.87 o 10 -11 0 316.68 297.51 15.75 o 11 -11 0 775.26 805.38 30.34 o 12 -11 0 73.94 75.71 9.07 o 0 -10 0 5860.16 5785.29 74.30 o 1 -10 0 9111.73 9579.26 102.26 o 2 -10 0 6433.96 6705.86 85.72 o 3 -10 0 10541.68 10829.42 111.63 o 4 -10 0 2988.00 3064.46 33.12 o 5 -10 0 1302.04 1339.64 17.14 o 6 -10 0 1168.17 1147.98 22.29 o 7 -10 0 168.97 163.39 6.88 o 8 -10 0 303.97 294.69 9.15 o 9 -10 0 29.10 39.62 5.90 o 10 -10 0 137.00 138.88 10.50 o 11 -10 0 287.30 285.41 15.67 o 12 -10 0 147.59 169.80 12.41 o 1 -9 0 820.60 891.71 11.25 o 2 -9 0 1671.70 1751.22 26.11 o 3 -9 0 1156.25 1158.09 12.97 o 4 -9 0 884.69 878.27 11.11 o 5 -9 0 2636.23 2633.32 35.71 o 6 -9 0 835.68 847.20 16.37 o 7 -9 0 460.33 463.76 10.70 o 8 -9 0 1052.29 1050.15 31.75 o 9 -9 0 660.10 662.86 23.53 o 10 -9 0 315.51 340.91 15.93 o 11 -9 0 156.62 179.09 11.79 o 12 -9 0 221.52 230.84 13.99 o 0 -8 0 7232.99 7231.64 109.73 o 1 -8 0 2176.33 2193.28 24.81 o 2 -8 0 3815.04 3901.27 45.98 o 3 -8 0 3945.22 3783.94 39.79 o 4 -8 0 1055.18 1063.82 11.73 o 5 -8 0 296.70 281.19 6.37 o 6 -8 0 516.08 525.96 10.79 o 7 -8 0 19.45 25.48 3.42 o 8 -8 0 278.94 252.99 12.05 o 9 -8 0 146.96 157.07 9.87 o 10 -8 0 6.62 2.98 2.97 o 11 -8 0 26.16 30.05 5.79 o 12 -8 0 57.23 51.14 7.14 o 1 -7 0 1234.11 1288.55 16.66 o 2 -7 0 747.96 819.24 10.37 o 3 -7 0 2982.66 3185.76 33.93 o 4 -7 0 4009.31 4157.25 39.83 o 5 -7 0 3230.67 3288.11 43.50 o 6 -7 0 2400.86 2406.42 33.51 o 7 -7 0 3766.23 3826.90 74.83 o 8 -7 0 1178.34 1179.98 37.13 o 9 -7 0 2005.46 2031.38 53.08 o 10 -7 0 837.02 818.80 27.04 o 11 -7 0 527.30 525.40 20.63 o 12 -7 0 359.93 357.10 16.93 o 0 -6 0 12410.46 12260.29 242.40 o 1 -6 0 13473.45 13244.80 159.69 o 2 -6 0 8772.70 8930.09 92.20 o 3 -6 0 10657.56 11033.57 126.84 o 4 -6 0 4940.49 5040.78 58.88 o 5 -6 0 3556.01 3596.38 47.61 o 6 -6 0 225.92 211.01 7.20 o 7 -6 0 67.29 81.90 4.46 o 8 -6 0 177.86 186.01 18.16 o 9 -6 0 422.53 422.04 15.96 o 10 -6 0 270.47 286.29 13.13 o 11 -6 0 46.97 37.69 5.61 o 12 -6 0 205.27 206.11 12.26 o 1 -5 0 1783.46 1898.01 26.07 o 2 -5 0 2072.48 2232.95 29.83 o 3 -5 0 1956.39 2111.35 27.79 o 4 -5 0 335.06 312.06 4.93 o 5 -5 0 566.46 566.95 9.95 o 6 -5 0 763.25 736.55 14.79 o 7 -5 0 1377.23 1373.99 25.07 o 8 -5 0 331.17 345.24 9.72 o 9 -5 0 105.27 117.42 6.75 o 10 -5 0 775.87 793.23 25.47 o 11 -5 0 31.05 33.28 5.22 o 12 -5 0 107.45 117.87 8.94 o 0 -4 0 20590.63 19902.63 421.09 o 1 -4 0 20358.45 20040.77 267.92 o 2 -4 0 24058.05 23795.68 247.79 o 3 -4 0 4513.88 4571.41 55.16 o 4 -4 0 2386.72 2335.57 25.86 o 5 -4 0 3302.30 3309.51 43.81 o 6 -4 0 25.11 33.51 2.74 o 7 -4 0 337.05 338.06 9.97 o 8 -4 0 289.06 301.31 8.68 o 9 -4 0 39.57 41.20 4.63 o 10 -4 0 88.68 95.27 7.19 o 11 -4 0 247.38 265.46 12.36 o 12 -4 0 535.35 574.94 21.06 o 1 -3 0 890.64 930.98 16.52 o 2 -3 0 2542.49 2719.79 32.15 o 3 -3 0 5579.04 5616.37 101.75 o 4 -3 0 7468.14 7262.35 95.67 o 5 -3 0 5421.80 5390.32 82.83 o 6 -3 0 2779.63 2835.19 45.43 o 7 -3 0 4291.30 4355.10 80.11 o 8 -3 0 2263.42 2306.70 49.31 o 9 -3 0 1414.24 1458.93 37.59 o 10 -3 0 849.09 880.19 26.04 o 11 -3 0 397.28 403.93 15.54 o 12 -3 0 169.32 199.75 10.75 o 0 -2 0 1200.16 1146.41 32.08 o 1 -2 0 1791.21 1878.81 20.84 o 2 -2 0 8515.22 8839.62 126.34 o 3 -2 0 4284.72 4227.78 65.39 o 4 -2 0 2021.95 1999.21 34.72 o 5 -2 0 3404.16 3512.52 54.08 o 6 -2 0 1594.11 1626.13 24.57 o 7 -2 0 785.66 771.51 12.68 o 8 -2 0 41.65 52.03 11.37 o 9 -2 0 75.53 82.15 5.57 o 10 -2 0 170.10 163.77 8.45 o 11 -2 0 51.39 58.42 5.43 o 12 -2 0 92.69 100.15 7.67 o 1 -1 0 169.12 167.90 3.23 o 2 -1 0 3294.70 3296.46 43.59 o 3 -1 0 932.56 874.37 16.87 o 4 -1 0 394.11 394.48 15.36 o 5 -1 0 4271.98 4404.56 73.46 o 6 -1 0 3016.30 2980.47 44.04 o 7 -1 0 1163.98 1162.11 28.79 o 8 -1 0 2215.57 2241.52 32.49 o 9 -1 0 1453.12 1470.75 37.27 o 10 -1 0 813.56 890.05 25.04 o 11 -1 0 432.52 439.96 15.69 o 12 -1 0 350.86 390.87 14.86 o 1 0 0 15604.45 14812.92 626.00 o 2 0 0 28959.91 28594.83 449.92 o 3 0 0 13689.98 13747.00 182.14 o 4 0 0 2430.60 2501.44 42.63 o 5 0 0 619.86 628.29 14.35 o 6 0 0 2094.91 2016.15 31.04 o 7 0 0 20.05 19.62 2.24 o 8 0 0 79.31 81.59 6.16 o 9 0 0 370.33 385.56 9.12 o 10 0 0 209.15 230.55 9.06 o 11 0 0 642.53 692.78 20.82 o 12 0 0 288.86 342.54 13.25 o 1 1 0 173.68 169.16 3.83 o 2 1 0 3284.64 3344.91 53.22 o 3 1 0 960.32 938.13 17.16 o 4 1 0 409.86 400.24 9.73 o 5 1 0 4314.36 4510.40 73.80 o 6 1 0 3094.33 3018.51 44.31 o 7 1 0 1189.77 1183.23 23.33 o 8 1 0 2229.61 2229.33 41.13 o 9 1 0 1513.48 1458.43 43.95 o 10 1 0 821.16 884.84 23.75 o 11 1 0 445.91 471.26 14.84 o 12 1 0 354.62 398.14 14.10 o 0 2 0 1312.50 1321.48 34.53 o 1 2 0 1763.56 1846.18 30.75 o 2 2 0 8346.02 8680.90 137.24 o 3 2 0 4283.77 4286.20 68.52 o 4 2 0 2041.60 2008.93 35.09 o 5 2 0 3349.71 3426.97 58.67 o 6 2 0 1613.24 1660.83 26.41 o 7 2 0 790.02 776.97 17.06 o 8 2 0 39.84 49.60 8.02 o 9 2 0 74.69 80.97 6.61 o 10 2 0 169.25 177.12 9.95 o 11 2 0 54.87 58.99 4.55 o 12 2 0 86.98 104.66 6.44 o 1 3 0 878.26 888.88 15.75 o 2 3 0 2492.34 2649.57 31.49 o 3 3 0 5603.00 5885.19 114.81 o 4 3 0 7508.37 7525.83 117.70 o 5 3 0 5462.84 5504.00 115.52 o 6 3 0 2758.47 2813.93 42.28 o 7 3 0 4250.31 4283.61 73.52 o 8 3 0 2260.83 2279.35 52.93 o 9 3 0 1385.97 1361.58 44.04 o 10 3 0 842.39 873.44 30.42 o 0 4 0 20751.51 20809.26 876.82 o 1 4 0 20529.49 20069.91 301.12 o 2 4 0 24223.40 24306.33 365.02 o 3 4 0 4623.80 4846.43 85.92 o 4 4 0 2382.60 2354.51 59.04 o 5 4 0 3333.95 3400.78 48.90 o 6 4 0 22.86 28.48 3.18 o 7 4 0 334.59 318.27 9.73 o 8 4 0 286.87 281.23 11.63 o 9 4 0 41.02 57.32 6.43 o 10 4 0 88.42 95.22 8.28 o 11 4 0 250.18 256.36 14.10 o 1 5 0 1776.61 1890.83 32.60 o 2 5 0 2043.46 2175.47 30.10 o 3 5 0 1927.71 2075.56 27.71 o 4 5 0 308.51 308.34 8.42 o 5 5 0 563.10 568.55 11.50 o 6 5 0 769.34 730.55 16.47 o 7 5 0 1389.23 1367.04 30.01 o 8 5 0 331.91 346.11 13.44 o 9 5 0 100.85 118.04 9.21 o 10 5 0 789.07 816.87 30.35 o 11 5 0 38.41 43.37 6.66 o 0 6 0 12275.17 12212.28 193.90 o 1 6 0 13420.04 13306.39 171.27 o 2 6 0 8775.89 8928.60 196.20 o 3 6 0 10551.31 10873.26 123.93 o 4 6 0 4964.63 5140.40 83.28 o 5 6 0 3551.54 3649.76 59.02 o 6 6 0 221.47 212.85 7.74 o 7 6 0 67.61 77.96 6.68 o 8 6 0 182.60 191.79 11.81 o 9 6 0 422.55 404.72 19.16 o 10 6 0 266.82 263.95 15.39 o 11 6 0 50.25 47.06 7.29 o 1 7 0 1239.73 1276.31 17.02 o 2 7 0 777.04 862.62 11.69 o 3 7 0 3044.21 3238.84 32.24 o 4 7 0 4094.30 4241.81 53.85 o 5 7 0 3261.59 3242.30 44.09 o 6 7 0 2448.28 2458.56 44.32 o 7 7 0 3794.75 3780.05 72.78 o 8 7 0 1184.16 1211.84 41.31 o 9 7 0 1998.00 1887.16 61.98 o 10 7 0 851.87 809.33 31.97 o 11 7 0 514.19 517.27 23.96 o 0 8 0 7215.52 7326.12 95.04 o 1 8 0 2171.83 2212.83 27.92 o 2 8 0 3901.21 4024.22 48.63 o 3 8 0 3944.15 3787.65 58.57 o 4 8 0 1092.83 1094.94 12.89 o 5 8 0 307.24 289.72 6.23 o 6 8 0 502.92 483.58 9.52 o 7 8 0 22.30 29.73 2.10 o 8 8 0 282.29 250.01 14.77 o 9 8 0 148.06 154.31 11.89 o 10 8 0 7.46 8.85 4.84 o 11 8 0 26.86 27.69 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