#------------------------------------------------------------------------------ #$Date: 2009-12-10 09:06:56 +0200 (Thu, 10 Dec 2009) $ #$Revision: 927 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2223676.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2223676_Fobs loop_ _publ_author_name 'Portis, Bobby' 'Dey, Kalpana R.' 'Saeed, Musabbir A.' 'Powell, Douglas R.' 'Hossain, Md. Alamgir' _publ_section_title ; 1,3-Phenylenediammonium dinitrate ; _journal_coeditor_code CI2920 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2601 _journal_volume 65 _journal_year 2009 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 115.506 _cell_angle_gamma 90.000 _cell_length_a 16.2548 _cell_length_b 9.6212 _cell_length_c 7.1070 _exptl_crystal_F_000 488.00 _reflns_d_resolution_high 0.8228 _[local]_cod_data_source_file ci2920Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 09074a in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 279.62 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 89.10 91.47 3.87 o 4 0 0 8281.79 8127.12 171.05 o 6 0 0 3918.79 3699.76 87.11 o 8 0 0 306.42 363.07 22.58 o 10 0 0 251.15 241.30 21.31 o 12 0 0 107.54 124.80 7.62 o 14 0 0 666.41 651.24 21.50 o 16 0 0 603.63 605.71 26.99 o 1 1 0 452.12 411.30 6.52 o 3 1 0 6561.46 5941.44 77.94 o 5 1 0 174.33 188.52 5.26 o 7 1 0 315.62 333.00 11.93 o 9 1 0 1563.54 1544.38 30.41 o 11 1 0 428.59 441.12 13.49 o 13 1 0 316.90 329.38 9.64 o 15 1 0 0.08 1.56 1.62 o 17 1 0 76.55 72.65 4.11 o 0 2 0 17832.95 17207.58 273.43 o 2 2 0 2700.77 2487.25 32.47 o 4 2 0 1426.72 1252.54 16.95 o 6 2 0 1323.51 1133.55 21.61 o 8 2 0 2221.53 2270.41 46.57 o 10 2 0 349.27 340.58 16.85 o 12 2 0 196.77 223.90 8.80 o 14 2 0 31.01 29.19 2.98 o 16 2 0 4.00 3.60 1.52 o 1 3 0 5984.90 5600.94 68.63 o 3 3 0 2194.98 1881.99 27.06 o 5 3 0 285.17 276.30 7.87 o 7 3 0 933.87 980.66 19.65 o 9 3 0 2876.69 2775.91 58.08 o 11 3 0 337.16 310.45 8.12 o 13 3 0 9.02 12.05 1.98 o 15 3 0 383.27 382.58 9.90 o 17 3 0 76.73 77.48 4.22 o 0 4 0 7546.94 8013.39 182.09 o 2 4 0 531.07 532.33 12.39 o 4 4 0 1278.72 1349.18 22.10 o 6 4 0 82.97 81.74 5.64 o 8 4 0 429.07 396.70 14.35 o 10 4 0 513.87 518.27 9.67 o 12 4 0 695.24 735.44 15.12 o 14 4 0 10.22 12.30 1.86 o 16 4 0 1.26 4.36 1.21 o 1 5 0 130.37 165.14 6.67 o 3 5 0 169.86 243.02 8.52 o 5 5 0 45.46 68.07 6.67 o 7 5 0 61.34 61.75 6.18 o 9 5 0 675.57 686.72 11.98 o 11 5 0 90.17 93.37 3.48 o 13 5 0 829.90 761.32 15.15 o 15 5 0 221.33 195.05 5.07 o 0 6 0 2313.61 2206.17 55.42 o 2 6 0 2478.01 2617.25 48.35 o 4 6 0 0.00 -3.39 3.61 o 6 6 0 3483.85 3287.81 40.10 o 8 6 0 25.89 29.80 2.35 o 10 6 0 60.68 81.74 7.18 o 12 6 0 1.02 1.81 1.32 o 14 6 0 6.44 9.15 1.45 o 1 7 0 82.44 97.94 7.74 o 3 7 0 118.88 131.15 4.60 o 5 7 0 119.70 124.68 4.02 o 7 7 0 4.39 4.32 1.42 o 9 7 0 843.91 882.40 14.99 o 11 7 0 34.56 45.04 2.55 o 13 7 0 88.25 88.10 3.52 o 0 8 0 116.90 162.99 5.55 o 2 8 0 590.17 585.34 10.01 o 4 8 0 0.50 4.77 1.18 o 6 8 0 3557.83 3501.46 52.93 o 8 8 0 32.34 33.47 2.30 o 10 8 0 41.92 40.62 2.39 o 12 8 0 392.70 395.66 9.34 o 1 9 0 3.19 2.92 1.08 o 3 9 0 37.60 33.41 2.16 o 5 9 0 34.72 44.35 2.52 o 7 9 0 35.38 46.44 5.25 o 9 9 0 0.13 1.48 1.28 o 11 9 0 219.77 203.12 6.38 o 0 10 0 0.37 2.02 1.44 o 2 10 0 34.75 32.76 1.96 o 4 10 0 440.77 468.78 8.97 o 6 10 0 39.45 35.02 2.21 o 8 10 0 31.66 32.32 2.01 o 1 11 0 7.98 2.92 1.21 o 3 11 0 124.48 105.28 3.59 o 5 11 0 7.01 3.22 1.34 o -17 1 1 1222.34 1131.07 43.64 o -15 1 1 951.22 978.24 23.89 o -13 1 1 1167.33 1130.21 20.81 o -11 1 1 110.54 112.42 12.73 o -9 1 1 8.42 9.74 3.70 o -7 1 1 6055.15 5857.51 73.21 o -5 1 1 23072.53 24160.58 259.10 o -3 1 1 2338.63 1995.20 26.03 o -1 1 1 320.35 262.80 3.98 o 1 1 1 8077.25 8553.88 89.04 o 3 1 1 1707.28 1714.87 21.17 o 5 1 1 2.34 3.14 1.74 o 7 1 1 136.37 172.44 7.18 o 9 1 1 213.10 210.30 11.15 o 11 1 1 575.81 606.11 19.27 o 13 1 1 3405.50 3444.40 56.70 o 15 1 1 34.05 39.53 2.89 o -18 2 1 2.18 4.09 2.59 o -16 2 1 0.00 -0.94 2.85 o -14 2 1 118.61 123.18 5.22 o -12 2 1 190.08 174.25 6.21 o -10 2 1 538.89 507.74 22.44 o -8 2 1 186.89 185.04 9.95 o -6 2 1 1166.10 1163.33 24.88 o -4 2 1 0.64 6.20 1.14 o -2 2 1 4045.84 4133.37 46.07 o 0 2 1 8.89 13.78 0.92 o 2 2 1 465.68 429.16 8.70 o 4 2 1 13195.66 14208.74 168.04 o 6 2 1 27.40 42.50 4.29 o 8 2 1 1983.79 1803.62 44.40 o 10 2 1 458.13 447.78 9.48 o 12 2 1 2.61 10.47 4.61 o 14 2 1 63.26 71.79 3.54 o 16 2 1 484.20 457.55 12.54 o -17 3 1 76.12 73.71 4.05 o -15 3 1 332.15 328.51 10.32 o -13 3 1 184.21 196.75 6.80 o -11 3 1 483.46 451.04 10.24 o -9 3 1 78.04 75.30 7.53 o -7 3 1 904.20 953.24 31.12 o -5 3 1 143.89 174.02 8.21 o -3 3 1 84.28 116.33 4.67 o -1 3 1 1.11 2.50 1.44 o 1 3 1 169.52 141.11 4.34 o 3 3 1 1769.35 1818.16 30.16 o 5 3 1 1283.97 1318.29 32.83 o 7 3 1 1599.52 1502.63 62.80 o 9 3 1 120.60 128.32 4.92 o 11 3 1 420.69 444.13 10.52 o 13 3 1 19.32 25.32 2.38 o 15 3 1 0.10 0.57 1.00 o -16 4 1 38.84 39.44 2.89 o -14 4 1 4.58 3.74 2.19 o -12 4 1 59.77 74.94 4.14 o -10 4 1 601.23 613.30 12.65 o -8 4 1 23.69 11.51 3.85 o -6 4 1 0.68 0.43 2.21 o -4 4 1 533.34 522.64 11.00 o -2 4 1 3253.10 3477.15 47.31 o 0 4 1 1690.42 1758.37 26.22 o 2 4 1 2230.28 2332.27 34.16 o 4 4 1 1406.99 1542.04 37.07 o 6 4 1 294.80 336.33 13.31 o 8 4 1 29.63 33.05 2.32 o 10 4 1 222.22 192.02 5.58 o 12 4 1 45.16 38.30 2.90 o 14 4 1 564.76 556.39 12.64 o -15 5 1 137.30 132.24 4.33 o -13 5 1 398.01 409.40 9.65 o -11 5 1 103.15 113.11 10.09 o -9 5 1 831.66 800.19 10.82 o -7 5 1 1390.97 1320.88 29.36 o -5 5 1 1345.51 1249.13 23.36 o -3 5 1 858.52 918.58 18.28 o -1 5 1 557.68 634.91 17.53 o 1 5 1 39.31 40.92 4.01 o 3 5 1 50.38 53.10 5.13 o 5 5 1 1733.16 1721.80 35.40 o 7 5 1 236.71 248.97 5.26 o 9 5 1 62.72 65.42 3.38 o 11 5 1 0.07 5.58 2.10 o 13 5 1 71.07 75.74 3.21 o 15 5 1 100.17 87.64 6.50 o -16 6 1 0.01 2.32 1.42 o -14 6 1 384.99 385.40 7.95 o -12 6 1 141.76 144.64 4.66 o -10 6 1 253.80 271.32 6.07 o -8 6 1 384.63 404.93 8.41 o -6 6 1 260.41 281.46 14.10 o -4 6 1 26.38 21.55 4.37 o -2 6 1 1857.26 1949.85 35.71 o 0 6 1 16.71 32.64 4.62 o 2 6 1 355.92 392.41 14.46 o 4 6 1 1886.17 1829.26 46.82 o 6 6 1 38.28 43.86 2.82 o 8 6 1 152.14 151.38 4.39 o 10 6 1 148.03 172.09 5.03 o 12 6 1 6.58 5.91 1.19 o 14 6 1 19.38 12.97 2.23 o -15 7 1 77.90 67.70 4.55 o -13 7 1 217.76 214.65 5.24 o -11 7 1 3567.75 3712.74 52.13 o -9 7 1 2376.55 2417.28 38.56 o -7 7 1 909.22 904.35 15.37 o -5 7 1 261.88 279.72 6.45 o -3 7 1 0.11 2.48 2.40 o -1 7 1 48.44 52.08 3.23 o 1 7 1 501.35 512.44 9.52 o 3 7 1 62.34 77.40 10.36 o 5 7 1 1599.19 1582.51 26.29 o 7 7 1 3236.60 3253.73 50.36 o 9 7 1 67.23 64.94 2.92 o 11 7 1 417.52 443.69 9.18 o 13 7 1 73.35 67.15 5.55 o -12 8 1 201.14 195.59 5.18 o -10 8 1 348.90 335.94 7.67 o -8 8 1 3.80 7.18 1.92 o -6 8 1 476.51 474.60 9.45 o -4 8 1 15.79 16.30 1.62 o -2 8 1 436.47 429.17 8.01 o 0 8 1 100.19 104.01 3.38 o 2 8 1 1602.17 1560.95 23.92 o 4 8 1 375.74 378.82 7.88 o 6 8 1 23.33 23.47 2.02 o 8 8 1 214.21 208.84 6.37 o 10 8 1 114.65 118.77 5.22 o -11 9 1 539.46 530.57 9.37 o -9 9 1 5.84 8.12 1.31 o -7 9 1 66.58 67.37 2.87 o -5 9 1 15.67 19.29 1.79 o -3 9 1 120.03 102.84 3.29 o -1 9 1 858.69 808.43 12.19 o 1 9 1 313.66 326.01 6.86 o 3 9 1 3.32 7.24 1.49 o 5 9 1 204.20 203.39 5.77 o 7 9 1 1097.90 1096.86 18.84 o 9 9 1 288.66 303.34 6.94 o -8 10 1 70.64 70.79 2.98 o -6 10 1 63.70 65.75 2.29 o -4 10 1 7.07 4.34 1.39 o -2 10 1 1357.87 1244.06 19.32 o 0 10 1 58.57 55.86 2.85 o 2 10 1 280.74 275.24 6.63 o 4 10 1 241.89 246.84 6.03 o 6 10 1 114.76 119.09 3.61 o -5 11 1 112.28 98.84 3.79 o -3 11 1 173.56 164.67 4.05 o -1 11 1 448.00 434.97 11.28 o 1 11 1 285.14 263.35 6.17 o 3 11 1 68.35 64.86 2.51 o -16 0 2 0.67 4.09 3.18 o -14 0 2 240.81 259.70 11.08 o -12 0 2 647.47 629.15 36.50 o -10 0 2 2970.17 2691.47 75.90 o -8 0 2 2737.64 2518.70 71.73 o -6 0 2 1242.03 1345.95 30.69 o -4 0 2 78185.59 85533.98 1480.64 o -2 0 2 3.63 19.62 1.82 o 0 0 2 5153.51 4816.20 78.36 o 2 0 2 302.47 172.09 8.69 o 4 0 2 384.63 402.39 15.01 o 6 0 2 457.98 502.44 19.77 o 8 0 2 3566.56 3352.89 81.66 o 10 0 2 1342.20 1365.40 27.94 o 12 0 2 87.92 87.22 5.14 o 14 0 2 1527.39 1609.02 57.63 o -17 1 2 284.14 281.02 10.87 o -15 1 2 38.36 45.88 3.58 o -13 1 2 183.68 200.63 6.70 o -11 1 2 1096.72 1076.44 31.02 o -9 1 2 483.96 478.74 16.13 o -7 1 2 4573.88 4485.39 106.65 o -5 1 2 1647.60 1573.25 35.17 o -3 1 2 678.71 695.17 11.51 o -1 1 2 327.70 259.21 5.89 o 1 1 2 33.77 52.99 2.98 o 3 1 2 0.04 0.94 1.50 o 5 1 2 1263.14 1312.94 25.19 o 7 1 2 409.91 406.56 13.41 o 9 1 2 52.00 56.74 3.22 o 11 1 2 252.88 265.67 8.44 o 13 1 2 26.71 27.57 2.26 o 15 1 2 152.60 143.92 4.27 o -18 2 2 8.48 10.70 2.30 o -16 2 2 20.06 23.74 2.63 o -14 2 2 25.32 37.71 3.30 o -12 2 2 1408.79 1353.30 22.85 o -10 2 2 328.06 288.76 12.64 o -8 2 2 168.28 184.72 17.16 o -6 2 2 254.99 218.94 6.76 o -4 2 2 5508.08 5358.88 57.83 o -2 2 2 1585.67 1358.45 16.23 o 0 2 2 1884.22 1888.77 23.67 o 2 2 2 863.04 689.08 13.30 o 4 2 2 968.65 1060.95 20.37 o 6 2 2 1843.38 1904.61 43.88 o 8 2 2 1031.86 1059.55 15.87 o 10 2 2 177.39 178.20 5.42 o 12 2 2 154.27 157.45 5.92 o 14 2 2 98.31 105.04 3.55 o -17 3 2 13.08 14.53 2.25 o -15 3 2 9.21 14.34 2.06 o -13 3 2 307.50 334.53 10.86 o -11 3 2 2563.03 2509.00 36.55 o -9 3 2 163.07 203.33 24.68 o -7 3 2 1605.12 1552.85 30.95 o -5 3 2 12361.48 12174.61 162.49 o -3 3 2 438.54 459.31 7.85 o -1 3 2 24.36 54.58 3.02 o 1 3 2 1532.81 1590.39 23.44 o 3 3 2 148.87 190.03 6.63 o 5 3 2 2133.96 2125.73 54.66 o 7 3 2 271.95 285.52 6.58 o 9 3 2 472.27 434.48 9.40 o 11 3 2 2.89 3.61 1.36 o 13 3 2 8.28 9.83 1.47 o -18 4 2 18.62 18.45 2.44 o -16 4 2 322.45 337.65 9.04 o -14 4 2 236.47 262.55 7.32 o -12 4 2 113.46 109.02 4.05 o -10 4 2 99.94 104.60 4.20 o -8 4 2 2048.99 1842.31 40.78 o -6 4 2 2.37 1.25 2.53 o -4 4 2 1811.98 1919.13 32.75 o -2 4 2 107.69 118.29 4.05 o 0 4 2 36.15 32.44 2.22 o 2 4 2 1318.59 1250.85 25.21 o 4 4 2 1041.09 1004.81 22.96 o 6 4 2 70.20 83.92 3.93 o 8 4 2 76.17 95.47 3.68 o 10 4 2 2.70 8.49 1.53 o 12 4 2 205.85 211.78 5.34 o 14 4 2 113.13 94.24 3.43 o -17 5 2 487.09 490.84 10.62 o -15 5 2 14.24 17.01 3.53 o -13 5 2 614.12 631.65 12.14 o -11 5 2 4.73 6.62 1.56 o -9 5 2 34.67 45.26 2.73 o -7 5 2 386.24 371.51 13.37 o -5 5 2 1880.80 1972.09 38.27 o -3 5 2 521.68 482.03 12.69 o -1 5 2 104.00 81.63 5.88 o 1 5 2 917.22 907.31 23.74 o 3 5 2 143.66 150.14 25.32 o 5 5 2 932.19 913.99 14.22 o 7 5 2 13.10 21.99 2.07 o 9 5 2 839.36 755.74 13.95 o 11 5 2 400.20 361.24 7.63 o 13 5 2 47.28 55.04 3.18 o -16 6 2 9.78 10.16 1.34 o -14 6 2 607.99 617.03 11.39 o -12 6 2 0.15 2.59 1.48 o -10 6 2 1321.01 1370.54 21.45 o -8 6 2 86.07 110.40 6.49 o -6 6 2 269.52 308.57 10.45 o -4 6 2 279.89 317.66 14.49 o -2 6 2 1495.54 1525.69 33.99 o 0 6 2 194.13 166.04 9.23 o 2 6 2 3213.29 3092.90 66.01 o 4 6 2 552.88 544.23 10.28 o 6 6 2 824.28 814.52 15.98 o 8 6 2 190.75 205.95 5.34 o 10 6 2 89.32 103.92 4.16 o 12 6 2 663.89 599.64 11.58 o -15 7 2 37.25 33.32 2.14 o -13 7 2 301.41 320.59 6.55 o -11 7 2 33.12 45.63 2.51 o -9 7 2 0.25 6.02 2.13 o -7 7 2 66.03 84.84 3.65 o -5 7 2 303.55 300.10 7.27 o -3 7 2 210.18 179.34 4.85 o -1 7 2 206.96 204.34 7.23 o 1 7 2 5.06 4.19 1.76 o 3 7 2 6.00 8.68 2.27 o 5 7 2 706.90 731.17 15.57 o 7 7 2 254.14 293.03 10.32 o 9 7 2 47.61 54.81 3.45 o 11 7 2 0.90 1.21 1.15 o -14 8 2 138.02 131.39 5.58 o -12 8 2 25.69 26.48 1.79 o -10 8 2 860.60 912.97 15.05 o -8 8 2 113.25 123.20 4.00 o -6 8 2 592.68 575.93 10.68 o -4 8 2 33.53 45.27 2.40 o -2 8 2 215.97 236.64 7.46 o 0 8 2 19.83 19.06 2.72 o 2 8 2 5330.05 5442.27 83.03 o 4 8 2 100.11 100.65 4.37 o 6 8 2 573.90 542.67 12.13 o 8 8 2 304.70 281.20 9.22 o 10 8 2 27.98 43.68 3.38 o -11 9 2 1.61 2.21 1.03 o -9 9 2 50.01 52.05 2.86 o -7 9 2 160.64 162.18 5.25 o -5 9 2 589.06 588.94 11.96 o -3 9 2 623.72 680.08 13.68 o -1 9 2 24.73 20.20 2.96 o 1 9 2 206.37 226.47 6.87 o 3 9 2 20.79 23.84 2.42 o 5 9 2 13.81 20.01 2.13 o 7 9 2 285.37 286.32 7.87 o -10 10 2 0.66 2.23 1.59 o -8 10 2 25.35 28.60 1.98 o -6 10 2 669.24 646.93 13.39 o -4 10 2 39.29 48.35 3.13 o -2 10 2 34.31 37.41 2.89 o 0 10 2 907.09 894.43 17.39 o 2 10 2 98.76 97.08 4.52 o 4 10 2 139.38 147.06 4.52 o 6 10 2 3.94 3.50 2.18 o -5 11 2 93.41 74.71 2.95 o -3 11 2 1.07 3.45 1.15 o -1 11 2 20.42 18.02 2.03 o 1 11 2 176.10 216.18 5.90 o -19 1 3 302.36 305.31 10.33 o -17 1 3 643.03 630.94 14.02 o -15 1 3 201.52 214.66 8.04 o -13 1 3 381.10 421.78 10.71 o -11 1 3 736.76 751.59 20.47 o -9 1 3 7638.02 8261.53 115.05 o -7 1 3 2516.49 2701.64 39.32 o -5 1 3 105.22 89.07 4.03 o -3 1 3 27.57 46.83 2.70 o -1 1 3 1684.04 1650.38 26.98 o 1 1 3 1721.64 1735.97 27.64 o 3 1 3 74.47 123.52 6.44 o 5 1 3 263.31 247.25 10.08 o 7 1 3 84.13 92.84 3.04 o 9 1 3 4841.26 4967.03 60.08 o 11 1 3 294.34 310.46 7.09 o 13 1 3 478.57 468.90 9.07 o -18 2 3 53.66 61.23 3.07 o -16 2 3 385.64 412.82 11.83 o -14 2 3 178.33 192.67 6.07 o -12 2 3 796.56 803.34 13.47 o -10 2 3 2846.91 2549.18 53.57 o -8 2 3 273.82 256.08 8.85 o -6 2 3 636.75 598.35 12.22 o -4 2 3 232.35 257.91 5.95 o -2 2 3 34.54 37.73 2.99 o 0 2 3 12794.08 14175.37 174.76 o 2 2 3 167.89 179.64 6.84 o 4 2 3 1070.00 1001.58 21.55 o 6 2 3 3.46 2.04 2.01 o 8 2 3 413.15 400.03 7.68 o 10 2 3 2.48 3.64 1.25 o 12 2 3 504.52 469.30 8.82 o -17 3 3 138.17 134.79 4.46 o -15 3 3 20.43 23.27 2.33 o -13 3 3 54.72 65.33 3.66 o -11 3 3 335.54 350.78 7.10 o -9 3 3 193.08 193.81 9.86 o -7 3 3 18.81 24.31 4.31 o -5 3 3 14.90 13.60 2.86 o -3 3 3 661.64 591.28 17.71 o -1 3 3 1579.93 1620.68 25.56 o 1 3 3 1580.37 1648.95 29.97 o 3 3 3 1004.29 1067.08 25.24 o 5 3 3 4.18 5.17 1.72 o 7 3 3 299.02 311.44 6.79 o 9 3 3 25.52 33.64 9.38 o 11 3 3 8.07 10.64 1.44 o 13 3 3 0.79 1.37 1.57 o -18 4 3 292.61 287.06 7.02 o -16 4 3 427.75 452.00 9.87 o -14 4 3 275.01 293.78 7.77 o -12 4 3 489.01 496.80 10.24 o -10 4 3 1240.69 1211.38 20.69 o -8 4 3 15.84 32.11 5.94 o -6 4 3 812.40 905.62 27.00 o -4 4 3 1137.36 1014.03 36.66 o -2 4 3 797.06 823.85 24.09 o 0 4 3 840.61 901.26 21.46 o 2 4 3 38.23 63.45 8.13 o 4 4 3 10.77 11.73 1.24 o 6 4 3 190.87 152.84 4.18 o 8 4 3 416.74 365.93 7.96 o 10 4 3 56.05 50.57 3.08 o 12 4 3 13.50 12.12 1.46 o -17 5 3 168.66 168.13 4.48 o -15 5 3 447.60 439.58 9.70 o -13 5 3 0.70 3.18 1.40 o -11 5 3 252.61 262.80 7.56 o -9 5 3 260.22 271.76 6.51 o -7 5 3 155.57 144.70 9.88 o -5 5 3 187.24 200.83 13.76 o -3 5 3 564.46 590.99 20.69 o -1 5 3 1941.50 1783.14 49.85 o 1 5 3 63.97 91.12 11.19 o 3 5 3 267.34 305.49 7.86 o 5 5 3 17.17 25.13 2.61 o 7 5 3 199.08 196.12 6.19 o 9 5 3 302.89 305.50 7.89 o 11 5 3 351.15 347.41 7.68 o -16 6 3 1.13 5.19 1.72 o -14 6 3 90.99 94.90 3.48 o -12 6 3 125.63 141.03 4.99 o -10 6 3 68.04 62.60 3.04 o -8 6 3 6.71 15.16 2.00 o -6 6 3 94.73 106.17 5.02 o -4 6 3 542.60 565.31 12.98 o -2 6 3 433.17 425.21 10.39 o 0 6 3 3115.08 2961.14 45.91 o 2 6 3 52.17 59.14 4.34 o 4 6 3 19.34 17.90 2.74 o 6 6 3 7.24 4.79 2.97 o 8 6 3 3.92 2.83 1.50 o 10 6 3 26.92 36.95 2.24 o -15 7 3 2189.66 2253.63 46.57 o -13 7 3 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