#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/37/2223735.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2223735_Fobs loop_ _publ_author_name 'Huang, Wei' _publ_section_title ; {\m-1,5-Bis[(E)-1-(2-pyridyl)ethylidene]carbonohydrazidato(1{-})}bis[chloridomethanolcopper(II)] perchlorate ; _journal_coeditor_code FI2081 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1347 _journal_volume 65 _journal_year 2009 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 8.0319 _cell_length_b 16.6784 _cell_length_c 37.3492 _exptl_crystal_F_000 2656.00 _reflns_d_resolution_high 0.7687 _[local]_cod_data_source_file fi2081Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' hw in Pbca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 516.53 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 65302.94 70256.26 2414.16 o 4 0 0 64244.47 57389.43 1982.40 o 6 0 0 113.57 231.86 45.27 o 8 0 0 28.05 -52.01 52.01 o 10 0 0 25.85 177.44 105.15 o 2 1 0 37834.12 37264.12 1011.49 o 4 1 0 26398.22 28758.98 710.76 o 6 1 0 1044.56 917.28 46.37 o 8 1 0 41.18 22.85 35.33 o 10 1 0 494.19 721.24 200.36 o 0 2 0 76349.73 67243.01 4415.83 o 2 2 0 2899.17 3121.44 97.21 o 4 2 0 4670.95 3897.79 103.46 o 6 2 0 3259.53 2874.12 89.84 o 8 2 0 2633.53 2666.17 156.63 o 10 2 0 36.92 119.61 67.73 o 2 3 0 21635.25 20889.22 575.55 o 4 3 0 7434.27 8488.53 251.48 o 6 3 0 202.46 150.65 41.05 o 8 3 0 2.20 -9.49 54.54 o 10 3 0 5.43 39.14 79.88 o 0 4 0 13938.90 13057.55 908.08 o 2 4 0 632.49 856.19 49.54 o 4 4 0 24170.01 24703.59 688.34 o 6 4 0 27.58 43.87 36.46 o 8 4 0 5559.63 5386.15 258.67 o 10 4 0 454.68 539.38 111.32 o 2 5 0 16472.59 15534.37 394.20 o 4 5 0 84.40 42.71 24.75 o 6 5 0 1742.60 2168.94 263.26 o 8 5 0 690.12 610.20 111.24 o 10 5 0 11.84 27.90 129.01 o 0 6 0 4294.03 6322.40 491.31 o 2 6 0 23468.01 25819.32 730.02 o 4 6 0 4322.44 4362.41 250.92 o 6 6 0 1728.77 1743.80 119.32 o 8 6 0 724.16 800.11 161.89 o 2 7 0 1112.03 1954.23 84.61 o 4 7 0 6332.94 7526.74 314.42 o 6 7 0 16602.89 17376.84 681.06 o 8 7 0 374.78 260.50 171.16 o 0 8 0 17049.31 14064.64 1025.93 o 2 8 0 13087.04 15349.72 496.15 o 4 8 0 1532.90 1465.62 125.51 o 6 8 0 4122.72 4496.25 225.84 o 8 8 0 175.37 188.95 76.39 o 2 9 0 3.74 12.29 20.35 o 4 9 0 1197.48 1247.55 98.89 o 6 9 0 5.80 1.21 63.01 o 8 9 0 20.67 66.70 79.24 o 0 10 0 37429.95 36940.62 1602.81 o 2 10 0 6211.71 6197.08 273.76 o 4 10 0 5523.26 6504.44 292.77 o 6 10 0 6843.67 7310.35 551.79 o 8 10 0 289.31 308.62 91.55 o 2 11 0 5.71 -36.03 36.03 o 4 11 0 5587.00 5928.72 274.18 o 6 11 0 3580.92 3602.90 206.92 o 8 11 0 474.35 448.03 102.79 o 0 12 0 1122.31 1517.44 276.06 o 2 12 0 71.38 56.25 52.82 o 4 12 0 22.38 40.23 52.83 o 6 12 0 153.49 217.43 73.61 o 8 12 0 60.25 177.86 92.05 o 2 13 0 44482.69 44507.29 1646.87 o 4 13 0 4092.10 4381.63 228.75 o 6 13 0 416.89 291.67 87.78 o 8 13 0 555.90 744.51 129.66 o 0 14 0 469.88 260.45 168.16 o 2 14 0 1814.30 2211.59 158.33 o 4 14 0 3177.08 3260.60 190.85 o 6 14 0 47.77 0.33 73.37 o 2 15 0 2596.54 2593.22 170.24 o 4 15 0 244.43 260.57 75.98 o 6 15 0 1315.36 1534.07 196.01 o 0 16 0 3050.23 2283.52 374.80 o 2 16 0 1211.92 1461.88 131.89 o 4 16 0 2617.24 2629.01 177.90 o 6 16 0 111.86 166.77 94.45 o 2 17 0 116.72 -51.35 133.86 o 4 17 0 1213.67 1471.22 139.02 o 6 17 0 2742.19 3273.83 467.76 o 0 18 0 18002.35 17168.00 1383.78 o 2 18 0 1454.87 1528.55 303.10 o 4 18 0 3009.91 2925.48 334.98 o 2 19 0 1160.16 1494.86 267.20 o 4 19 0 5.84 -41.70 136.68 o 0 20 0 625.85 171.93 260.45 o 2 20 0 1585.31 1436.61 461.44 o 2 21 0 2925.77 4090.81 605.66 o 1 1 1 136.38 207.51 7.01 o 2 1 1 6361.15 5845.38 101.84 o 3 1 1 1506.43 1565.17 34.58 o 4 1 1 3192.13 2441.08 52.23 o 5 1 1 2579.11 2851.06 61.95 o 6 1 1 2519.96 2792.07 62.45 o 7 1 1 1390.89 1326.80 54.03 o 8 1 1 69.14 1.16 25.18 o 9 1 1 66.54 62.03 36.65 o 10 1 1 55.00 202.12 57.72 o 0 2 1 44232.48 40052.24 1219.37 o 1 2 1 103583.16 97883.63 2249.57 o 2 2 1 18817.33 18477.83 339.16 o 3 2 1 770.69 969.71 24.57 o 4 2 1 71.62 10.05 10.04 o 5 2 1 2423.74 2709.77 57.68 o 6 2 1 1454.15 1255.06 38.51 o 7 2 1 595.42 615.33 38.62 o 8 2 1 1523.28 1594.15 143.35 o 9 2 1 159.45 185.95 43.57 o 10 2 1 101.89 68.79 52.01 o 1 3 1 1985.15 2661.92 63.32 o 2 3 1 19.47 23.93 12.29 o 3 3 1 75.00 116.48 13.06 o 4 3 1 5077.12 4012.95 83.06 o 5 3 1 9107.20 9683.77 183.71 o 6 3 1 2784.51 3062.13 97.86 o 7 3 1 838.64 728.70 52.25 o 8 3 1 292.62 275.81 48.51 o 9 3 1 818.73 916.78 74.12 o 10 3 1 54.51 157.84 55.63 o 0 4 1 65226.39 65551.39 3062.15 o 1 4 1 1099.94 1123.45 39.90 o 2 4 1 3376.01 2931.02 71.82 o 3 4 1 3995.27 3710.60 110.49 o 4 4 1 1.95 64.84 18.68 o 5 4 1 3325.73 3391.91 92.03 o 6 4 1 26.97 63.33 28.60 o 7 4 1 5663.98 5606.84 179.34 o 8 4 1 392.82 440.66 59.33 o 9 4 1 237.55 275.42 55.28 o 10 4 1 67.35 69.00 60.50 o 1 5 1 5248.81 4472.48 120.18 o 2 5 1 21967.51 20287.06 396.65 o 3 5 1 65214.44 64626.11 1242.16 o 4 5 1 6746.92 6056.80 192.88 o 5 5 1 162.94 223.01 31.49 o 6 5 1 213.41 183.56 34.50 o 7 5 1 1783.48 1707.65 94.47 o 8 5 1 160.36 167.41 45.56 o 9 5 1 204.49 106.06 70.01 o 10 5 1 100.75 46.68 68.55 o 0 6 1 1104.12 953.12 61.48 o 1 6 1 11396.22 12013.88 322.53 o 2 6 1 13506.76 14833.96 314.01 o 3 6 1 7196.11 6700.89 152.90 o 4 6 1 3683.97 3719.83 114.97 o 5 6 1 3482.38 3028.28 142.15 o 6 6 1 1378.73 1093.12 74.56 o 7 6 1 5821.25 5719.49 295.12 o 8 6 1 1091.49 1208.87 93.18 o 9 6 1 475.32 492.39 92.26 o 1 7 1 6517.47 6394.75 185.89 o 2 7 1 5739.92 6304.59 139.52 o 3 7 1 433.24 495.31 42.32 o 4 7 1 2060.52 2263.66 75.77 o 5 7 1 8844.58 8544.63 233.58 o 6 7 1 128.48 190.00 41.20 o 7 7 1 704.94 559.67 57.98 o 8 7 1 422.81 342.29 76.51 o 9 7 1 361.73 430.58 69.67 o 0 8 1 31815.20 29978.49 1098.13 o 1 8 1 15133.79 15522.31 418.07 o 2 8 1 5001.44 4718.40 129.65 o 3 8 1 9761.81 9490.53 269.83 o 4 8 1 4167.51 3840.13 132.97 o 5 8 1 2879.31 2607.53 110.80 o 6 8 1 2950.10 2896.37 165.14 o 7 8 1 3.87 69.74 42.36 o 8 8 1 50.42 15.43 47.61 o 9 8 1 2.67 6.27 53.53 o 1 9 1 21263.01 21935.17 581.42 o 2 9 1 6535.58 5775.94 147.12 o 3 9 1 1119.32 885.79 54.20 o 4 9 1 2957.54 2802.13 125.50 o 5 9 1 11446.18 11827.49 341.60 o 6 9 1 1389.74 1412.74 83.31 o 7 9 1 731.13 803.87 70.69 o 8 9 1 21.71 -73.50 73.50 o 9 9 1 340.07 398.22 75.21 o 0 10 1 4506.29 4860.79 177.67 o 1 10 1 6609.87 6581.42 199.69 o 2 10 1 12.42 78.38 22.29 o 3 10 1 16641.69 16269.96 443.90 o 4 10 1 2970.36 2869.41 113.34 o 5 10 1 254.76 337.55 48.99 o 6 10 1 189.83 336.98 58.04 o 7 10 1 786.81 757.84 73.62 o 8 10 1 252.59 238.69 60.16 o 9 10 1 352.39 171.99 133.72 o 1 11 1 15654.07 15129.77 418.37 o 2 11 1 670.82 858.33 85.61 o 3 11 1 1782.98 1705.15 98.29 o 4 11 1 649.95 702.89 57.94 o 5 11 1 1046.63 962.28 142.47 o 6 11 1 1256.95 1168.13 80.49 o 7 11 1 45.19 74.57 52.34 o 8 11 1 17.56 38.64 55.26 o 0 12 1 4121.62 4041.38 160.46 o 1 12 1 2838.09 3191.70 105.64 o 2 12 1 722.46 852.44 69.77 o 3 12 1 7154.67 7053.25 219.06 o 4 12 1 58.99 64.11 39.06 o 5 12 1 344.21 334.81 55.26 o 6 12 1 853.12 853.01 76.21 o 7 12 1 1151.08 1329.46 98.48 o 8 12 1 916.01 1008.33 96.31 o 1 13 1 7512.92 8187.02 299.28 o 2 13 1 2420.11 2982.80 124.87 o 3 13 1 1950.76 1963.49 91.21 o 4 13 1 1831.47 1722.82 92.31 o 5 13 1 2.68 21.15 46.45 o 6 13 1 9.27 0.06 47.44 o 7 13 1 13.47 47.84 56.92 o 8 13 1 81.01 143.50 67.81 o 0 14 1 1529.46 1467.68 113.43 o 1 14 1 1559.83 1564.37 85.15 o 2 14 1 5.95 42.42 38.86 o 3 14 1 915.68 779.57 62.52 o 4 14 1 53.66 101.14 48.98 o 5 14 1 281.63 282.68 57.94 o 6 14 1 29.35 4.48 54.13 o 7 14 1 186.88 278.81 68.46 o 1 15 1 3467.58 3728.82 285.25 o 2 15 1 2972.12 2953.60 185.70 o 3 15 1 2922.94 2898.55 119.19 o 4 15 1 1919.95 1668.39 96.80 o 5 15 1 699.50 833.68 100.32 o 6 15 1 229.92 315.34 69.20 o 7 15 1 279.31 410.51 77.50 o 0 16 1 2354.04 2019.78 247.07 o 1 16 1 483.58 803.49 120.48 o 2 16 1 547.56 429.09 74.86 o 3 16 1 839.40 952.11 98.10 o 4 16 1 26.03 11.64 49.99 o 5 16 1 1109.70 1301.61 101.31 o 6 16 1 229.35 173.63 69.18 o 1 17 1 545.63 477.90 115.13 o 2 17 1 870.88 905.33 137.42 o 3 17 1 819.53 653.25 68.19 o 4 17 1 25.80 14.70 51.38 o 5 17 1 222.86 248.68 67.81 o 6 17 1 124.49 257.12 74.70 o 0 18 1 3396.15 3912.07 568.80 o 1 18 1 485.60 438.88 123.32 o 2 18 1 174.69 257.69 115.37 o 3 18 1 319.22 273.07 98.20 o 4 18 1 192.79 67.24 60.51 o 5 18 1 148.58 192.78 69.29 o 1 19 1 261.48 198.32 114.46 o 2 19 1 121.70 199.60 119.74 o 3 19 1 468.47 485.75 127.64 o 4 19 1 936.04 980.09 167.24 o 0 20 1 22.11 89.65 165.50 o 1 20 1 759.01 586.10 151.16 o 2 20 1 10.38 -6.86 111.50 o 3 20 1 644.70 684.58 151.61 o 1 21 1 401.26 272.28 138.64 o 2 21 1 56.39 116.88 116.51 o 1 0 2 165201.42 149103.41 3951.30 o 2 0 2 12670.73 12719.57 315.58 o 3 0 2 17336.15 18361.46 455.76 o 4 0 2 90.20 72.78 28.54 o 5 0 2 23374.94 20203.32 508.90 o 6 0 2 1128.01 1507.73 63.94 o 7 0 2 1188.43 1116.19 60.96 o 8 0 2 797.39 745.26 71.43 o 9 0 2 21.78 35.11 48.35 o 10 0 2 10.79 33.91 82.37 o 1 1 2 2682.17 2990.04 64.83 o 2 1 2 266798.13 253183.89 4147.15 o 3 1 2 10506.37 10084.95 174.15 o 4 1 2 12515.59 10968.66 191.25 o 5 1 2 13331.09 11542.04 203.77 o 6 1 2 2229.25 2234.15 60.08 o 7 1 2 1180.94 1502.16 52.00 o 8 1 2 53.41 46.13 29.27 o 9 1 2 377.28 381.96 42.85 o 10 1 2 381.43 345.50 70.75 o 0 2 2 22327.10 23094.11 693.78 o 1 2 2 86.62 136.24 12.97 o 2 2 2 2056.66 2191.75 48.03 o 3 2 2 12.75 39.88 9.30 o 4 2 2 9952.72 9901.17 167.99 o 5 2 2 2907.91 3195.56 67.82 o 6 2 2 5.29 -10.56 17.61 o 7 2 2 589.34 597.92 40.23 o 8 2 2 364.67 317.10 38.81 o 9 2 2 26.90 -1.76 40.92 o 10 2 2 13.26 50.61 52.50 o 1 3 2 36496.34 35844.92 776.30 o 2 3 2 213.48 120.92 20.37 o 3 3 2 27722.27 25208.88 463.86 o 4 3 2 1706.26 1670.18 44.56 o 5 3 2 3801.38 3800.93 91.26 o 6 3 2 4336.92 4267.24 110.60 o 7 3 2 935.00 930.67 54.81 o 8 3 2 61.84 105.92 41.82 o 9 3 2 10.40 43.81 43.85 o 10 3 2 363.31 402.87 69.07 o 0 4 2 50021.00 49940.34 1526.20 o 1 4 2 987.20 1364.34 59.98 o 2 4 2 5483.15 5159.22 123.83 o 3 4 2 21657.76 20539.55 427.45 o 4 4 2 6841.67 6538.11 149.50 o 5 4 2 3087.36 3746.95 114.99 o 6 4 2 258.01 185.83 33.23 o 7 4 2 3285.16 3605.61 133.74 o 8 4 2 239.86 207.27 47.61 o 9 4 2 2005.31 2021.48 190.22 o 10 4 2 92.47 153.23 64.59 o 1 5 2 5930.24 6882.56 176.13 o 2 5 2 51.43 35.07 10.48 o 3 5 2 267.79 217.30 20.24 o 4 5 2 3308.13 3222.54 126.00 o 5 5 2 262.00 297.35 33.19 o 6 5 2 2357.47 2086.55 84.23 o 7 5 2 0.11 -0.13 33.95 o 8 5 2 2.01 -7.98 41.32 o 9 5 2 40.87 139.04 53.97 o 10 5 2 15.52 6.43 60.59 o 0 6 2 2.88 14.65 19.88 o 1 6 2 15697.54 13850.10 338.50 o 2 6 2 322.81 190.96 14.79 o 3 6 2 1228.91 1246.60 45.77 o 4 6 2 5745.66 5475.72 194.14 o 5 6 2 419.65 466.66 55.12 o 6 6 2 921.39 1080.17 65.94 o 7 6 2 205.35 135.07 40.84 o 8 6 2 864.61 951.94 73.42 o 9 6 2 343.00 349.45 63.90 o 1 7 2 48.67 84.85 18.49 o 2 7 2 34.94 23.35 11.10 o 3 7 2 22525.00 21710.67 456.28 o 4 7 2 7659.19 7711.18 208.11 o 5 7 2 4311.07 3654.42 207.77 o 6 7 2 394.69 278.68 41.68 o 7 7 2 79.14 111.18 50.77 o 8 7 2 0.49 -15.44 44.30 o 9 7 2 12.48 33.60 50.53 o 0 8 2 2701.83 2470.95 186.16 o 1 8 2 31387.61 29183.78 759.14 o 2 8 2 1509.58 1344.38 48.44 o 3 8 2 124.95 108.75 25.01 o 4 8 2 1051.80 1175.24 88.65 o 5 8 2 2073.36 2084.88 86.30 o 6 8 2 303.86 380.08 49.27 o 7 8 2 133.01 110.46 44.76 o 8 8 2 384.24 292.25 58.93 o 9 8 2 1.59 -50.08 50.08 o 1 9 2 71.43 72.65 24.32 o 2 9 2 14.44 -0.75 21.30 o 3 9 2 115.90 135.09 43.00 o 4 9 2 364.38 306.40 40.04 o 5 9 2 1442.12 1451.25 78.98 o 6 9 2 802.25 740.99 68.92 o 7 9 2 94.31 31.10 53.80 o 8 9 2 55.11 43.82 48.45 o 9 9 2 0.83 -2.53 56.49 o 0 10 2 2026.62 2051.62 219.12 o 1 10 2 23003.79 22598.02 602.52 o 2 10 2 1950.96 2133.75 78.45 o 3 10 2 1220.58 1520.69 92.89 o 4 10 2 2173.76 2204.03 96.75 o 5 10 2 4573.90 4301.34 153.68 o 6 10 2 103.63 85.17 44.09 o 7 10 2 1711.08 1814.71 103.91 o 8 10 2 380.31 484.39 71.44 o 9 10 2 193.39 218.09 147.18 o 1 11 2 326.28 464.18 35.11 o 2 11 2 1701.98 1792.36 99.83 o 3 11 2 3547.13 3545.70 122.75 o 4 11 2 762.25 812.08 62.01 o 5 11 2 1699.92 1667.53 160.68 o 6 11 2 35.91 81.43 46.04 o 7 11 2 19.86 0.65 48.50 o 8 11 2 7.14 -6.66 56.91 o 0 12 2 8119.60 8493.12 292.25 o 1 12 2 95.07 121.23 50.13 o 2 12 2 4.22 24.31 38.55 o 3 12 2 3.32 48.69 34.01 o 4 12 2 6237.64 6457.34 210.49 o 5 12 2 26.02 11.55 41.93 o 6 12 2 89.86 125.40 52.58 o 7 12 2 97.25 109.50 56.53 o 8 12 2 795.22 665.39 132.24 o 1 13 2 2496.60 2161.65 120.53 o 2 13 2 101.54 67.64 39.59 o 3 13 2 9447.84 9561.44 269.70 o 4 13 2 653.05 535.54 69.09 o 5 13 2 2112.93 2177.79 152.25 o 6 13 2 1036.82 1155.38 94.58 o 7 13 2 15.53 -40.30 52.12 o 8 13 2 202.34 169.08 69.48 o 0 14 2 24771.76 23873.40 915.13 o 1 14 2 37.77 -14.55 34.75 o 2 14 2 2249.74 2316.40 144.69 o 3 14 2 2748.08 2832.49 114.77 o 4 14 2 3938.51 3578.90 143.79 o 5 14 2 39.67 -5.48 45.78 o 6 14 2 152.76 100.60 53.90 o 7 14 2 1224.71 1081.03 98.83 o 1 15 2 222.48 169.21 106.04 o 2 15 2 2191.95 2141.40 107.63 o 3 15 2 174.54 199.72 49.07 o 4 15 2 520.28 571.56 64.44 o 5 15 2 47.82 65.64 51.32 o 6 15 2 2365.75 2531.12 171.69 o 7 15 2 89.78 79.41 65.50 o 0 16 2 667.78 522.52 150.87 o 1 16 2 3360.75 3727.10 237.53 o 2 16 2 2.02 -33.63 57.10 o 3 16 2 6.38 -30.29 45.42 o 4 16 2 1385.17 1271.16 93.70 o 5 16 2 115.02 106.20 56.23 o 6 16 2 14.30 16.54 60.55 o 1 17 2 0.00 29.12 86.71 o 2 17 2 3412.64 3770.70 252.26 o 3 17 2 613.65 489.73 77.35 o 4 17 2 180.11 220.65 59.11 o 5 17 2 2150.62 2450.63 255.93 o 6 17 2 991.75 1073.37 103.49 o 0 18 2 1176.43 1037.84 218.21 o 1 18 2 3804.02 3553.57 247.49 o 2 18 2 42.38 49.70 97.16 o 3 18 2 17.81 21.57 89.29 o 4 18 2 780.64 835.29 153.36 o 5 18 2 718.63 800.50 133.76 o 1 19 2 217.59 262.35 120.53 o 2 19 2 3004.69 3570.46 263.43 o 3 19 2 8.55 102.32 116.16 o 4 19 2 103.27 89.65 115.97 o 0 20 2 2150.77 1650.64 274.88 o 1 20 2 426.04 445.85 137.31 o 2 20 2 49.03 -42.49 97.89 o 3 20 2 89.89 94.18 105.08 o 1 21 2 285.04 330.72 138.06 o 2 21 2 1370.49 1664.64 223.03 o 1 1 3 58152.03 58790.18 1125.27 o 2 1 3 132.33 215.83 13.29 o 3 1 3 33546.63 35798.31 647.76 o 4 1 3 7081.03 7126.23 139.72 o 5 1 3 3038.38 3762.58 83.65 o 6 1 3 1157.66 1176.80 41.42 o 7 1 3 1746.55 1728.54 54.36 o 8 1 3 76.65 32.10 30.50 o 9 1 3 165.69 184.86 38.02 o 10 1 3 11.35 123.95 63.84 o 0 2 3 22017.80 25676.99 785.14 o 1 2 3 32824.22 35858.97 688.48 o 2 2 3 47709.66 47891.73 912.99 o 3 2 3 117.86 201.35 16.38 o 4 2 3 3.23 22.53 13.04 o 5 2 3 757.56 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341.07 68.25 o 7 6 27 1425.69 1342.68 106.39 o 8 6 27 521.60 523.53 163.42 o 1 7 27 26.99 84.59 33.91 o 2 7 27 24.59 18.63 31.07 o 3 7 27 5.33 -24.49 32.96 o 4 7 27 703.99 842.63 85.81 o 5 7 27 1231.56 1157.51 89.64 o 6 7 27 582.42 522.72 71.71 o 7 7 27 146.54 185.90 75.72 o 0 8 27 1824.58 1900.93 246.00 o 1 8 27 8447.75 8063.87 251.01 o 2 8 27 1037.15 963.52 79.54 o 3 8 27 620.38 626.17 89.08 o 4 8 27 701.99 556.90 58.82 o 5 8 27 701.80 813.23 70.91 o 6 8 27 620.25 693.26 104.74 o 7 8 27 4.09 14.65 54.54 o 1 9 27 1644.02 1450.20 106.36 o 2 9 27 3232.98 3168.72 135.75 o 3 9 27 870.41 837.05 78.93 o 4 9 27 172.22 116.13 49.77 o 5 9 27 6327.77 6729.46 347.54 o 6 9 27 1050.59 976.12 187.96 o 7 9 27 605.13 473.98 155.26 o 0 10 27 6134.12 6267.20 257.22 o 1 10 27 3954.22 3855.14 154.39 o 2 10 27 79.16 72.36 43.60 o 3 10 27 4793.21 4609.92 194.74 o 4 10 27 456.31 468.88 62.25 o 5 10 27 35.28 134.26 54.53 o 6 10 27 279.70 333.14 75.16 o 7 10 27 7.53 15.01 97.83 o 1 11 27 3884.47 3527.81 137.28 o 2 11 27 1268.96 1235.40 101.13 o 3 11 27 271.91 301.09 61.07 o 4 11 27 3.07 10.24 52.96 o 5 11 27 121.31 122.60 60.29 o 6 11 27 42.58 102.14 76.20 o 0 12 27 162.41 278.18 83.13 o 1 12 27 167.18 167.47 49.92 o 2 12 27 775.93 703.40 134.84 o 3 12 27 3645.41 3795.45 158.19 o 4 12 27 114.99 96.55 64.10 o 5 12 27 12.46 9.25 60.73 o 6 12 27 212.53 204.58 86.67 o 1 13 27 1075.43 1190.85 98.82 o 2 13 27 2826.17 2451.36 147.85 o 3 13 27 548.39 436.51 84.74 o 4 13 27 464.87 524.49 96.53 o 5 13 27 1.23 50.19 60.68 o 0 14 27 224.48 283.10 288.43 o 1 14 27 161.27 100.55 68.95 o 2 14 27 33.48 -25.65 55.04 o 3 14 27 23.52 39.76 74.86 o 4 14 27 30.27 -25.88 123.55 o 5 14 27 159.44 281.42 130.07 o 1 15 27 311.80 404.46 85.11 o 2 15 27 521.31 185.98 110.47 o 3 15 27 356.99 305.45 78.82 o 4 15 27 817.89 970.80 156.56 o 0 16 27 491.45 471.52 413.95 o 1 16 27 641.78 299.99 83.34 o 2 16 27 346.98 254.58 146.93 o 3 16 27 239.99 124.61 99.26 o 4 16 27 69.55 -52.74 336.60 o 1 17 27 253.88 220.39 133.55 o 2 17 27 9.66 33.95 103.31 o 0 0 28 70145.92 75137.81 4464.27 o 1 0 28 2039.65 2330.20 134.66 o 2 0 28 65.05 25.77 41.97 o 3 0 28 50.20 97.88 50.31 o 4 0 28 6270.23 6343.32 240.39 o 5 0 28 133.94 8.94 58.74 o 6 0 28 13.00 39.62 65.68 o 7 0 28 51.40 75.04 108.13 o 8 0 28 46.77 15.98 115.12 o 1 1 28 2655.66 2686.09 103.61 o 2 1 28 5580.88 5128.10 165.42 o 3 1 28 693.03 753.89 51.40 o 4 1 28 1392.40 1436.19 65.46 o 5 1 28 1074.47 1135.23 69.47 o 6 1 28 1294.86 1395.46 106.83 o 7 1 28 300.09 222.32 69.70 o 8 1 28 40.53 14.97 83.65 o 0 2 28 3219.61 3173.91 164.46 o 1 2 28 225.99 313.57 42.96 o 2 2 28 2912.47 2863.08 113.85 o 3 2 28 1.58 1.10 26.93 o 4 2 28 330.44 359.59 48.64 o 5 2 28 1268.02 1307.54 90.21 o 6 2 28 1650.65 1821.62 118.83 o 7 2 28 44.78 44.14 58.25 o 8 2 28 374.22 313.48 81.81 o 1 3 28 1766.41 1900.17 86.68 o 2 3 28 19755.25 20110.51 537.39 o 3 3 28 22.89 21.31 27.09 o 4 3 28 5431.41 5694.52 191.24 o 5 3 28 1227.35 1228.47 68.09 o 6 3 28 16.99 34.00 40.27 o 7 3 28 387.05 360.76 79.14 o 8 3 28 33.01 -20.95 69.23 o 0 4 28 854.15 800.54 83.19 o 1 4 28 1700.90 1582.46 81.24 o 2 4 28 1954.90 1956.11 78.93 o 3 4 28 1.80 34.91 40.58 o 4 4 28 1255.46 1224.95 81.62 o 5 4 28 724.66 843.41 77.18 o 6 4 28 452.97 411.75 54.68 o 7 4 28 41.73 70.23 62.11 o 8 4 28 1588.59 1730.04 137.51 o 1 5 28 56.14 32.06 31.50 o 2 5 28 3190.54 3065.51 143.34 o 3 5 28 18.00 111.52 35.12 o 4 5 28 405.43 582.68 59.80 o 5 5 28 107.52 18.36 41.83 o 6 5 28 797.91 1071.51 75.83 o 7 5 28 393.03 376.35 57.61 o 8 5 28 75.46 171.73 87.90 o 0 6 28 503.76 428.33 68.88 o 1 6 28 2715.46 2686.31 113.42 o 2 6 28 5903.36 5493.87 183.19 o 3 6 28 4.84 -26.53 34.69 o 4 6 28 334.26 237.45 44.82 o 5 6 28 10.32 -29.34 42.10 o 6 6 28 285.28 314.22 54.42 o 7 6 28 29.79 -0.77 52.25 o 8 6 28 77.96 8.61 119.46 o 1 7 28 13.76 -32.80 32.80 o 2 7 28 34.81 -34.73 34.73 o 3 7 28 318.86 238.09 50.36 o 4 7 28 2231.16 2052.45 112.32 o 5 7 28 60.43 132.73 47.12 o 6 7 28 3240.62 3718.04 373.37 o 7 7 28 0.19 49.28 59.61 o 0 8 28 1084.59 1457.42 121.26 o 1 8 28 2771.56 2359.34 108.17 o 2 8 28 1752.25 1511.78 89.88 o 3 8 28 406.07 248.93 61.96 o 4 8 28 581.40 615.65 65.26 o 5 8 28 51.64 67.13 58.22 o 6 8 28 383.15 405.52 68.47 o 7 8 28 55.16 64.58 58.20 o 1 9 28 121.14 93.88 41.26 o 2 9 28 254.20 282.44 51.54 o 3 9 28 5.30 20.31 46.91 o 4 9 28 457.12 583.83 67.06 o 5 9 28 47.88 21.68 52.22 o 6 9 28 200.65 235.23 96.44 o 7 9 28 20.19 113.17 66.42 o 0 10 28 3979.39 3835.04 184.26 o 1 10 28 124.15 156.31 55.25 o 2 10 28 2588.00 2691.03 149.31 o 3 10 28 1765.43 1867.48 116.38 o 4 10 28 2.07 -47.05 47.05 o 5 10 28 233.40 165.24 59.38 o 6 10 28 564.12 640.51 122.25 o 7 10 28 0.28 47.89 95.25 o 1 11 28 149.97 68.80 64.68 o 2 11 28 125.28 152.89 66.88 o 3 11 28 277.67 260.26 60.83 o 4 11 28 1916.19 1711.04 121.92 o 5 11 28 17.85 -1.01 61.97 o 6 11 28 1200.92 1150.98 157.89 o 0 12 28 267.86 218.15 92.13 o 1 12 28 298.82 173.49 55.74 o 2 12 28 119.99 201.33 56.15 o 3 12 28 22.90 0.95 56.47 o 4 12 28 41.16 90.20 64.10 o 5 12 28 0.41 -34.75 62.36 o 6 12 28 90.74 151.75 131.57 o 1 13 28 10.68 69.79 54.19 o 2 13 28 6209.17 6229.57 224.53 o 3 13 28 280.76 133.13 79.91 o 4 13 28 1368.87 1281.91 114.28 o 5 13 28 11.15 -39.15 65.13 o 0 14 28 440.77 404.37 143.41 o 1 14 28 491.60 398.45 174.95 o 2 14 28 247.68 193.18 64.59 o 3 14 28 53.90 88.43 83.99 o 4 14 28 1338.53 1320.31 143.30 o 5 14 28 436.07 230.61 126.16 o 1 15 28 1.63 106.24 76.23 o 2 15 28 1181.76 1300.39 246.89 o 3 15 28 7.66 38.71 66.95 o 4 15 28 318.09 -41.95 135.06 o 0 16 28 1684.79 1384.83 610.10 o 1 16 28 5.35 -25.42 68.25 o 2 16 28 429.75 501.55 254.50 o 3 16 28 28.59 32.64 100.07 o 1 17 28 25.91 -162.82 190.31 o 2 17 28 88.47 3.49 202.47 o 1 1 29 81.41 55.26 47.61 o 2 1 29 551.52 690.90 54.31 o 3 1 29 59.90 49.74 31.05 o 4 1 29 2181.82 2164.33 100.54 o 5 1 29 705.27 772.72 60.21 o 6 1 29 623.68 660.60 81.03 o 7 1 29 578.69 629.27 127.47 o 8 1 29 114.76 165.78 79.07 o 0 2 29 2059.93 1936.93 123.03 o 1 2 29 5963.12 5589.84 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1462.14 1432.89 137.22 o 1 3 42 460.34 663.62 76.98 o 2 3 42 158.01 231.19 63.35 o 3 3 42 444.25 535.25 97.23 o 4 3 42 1680.76 1578.18 185.53 o 0 4 42 2484.27 2690.73 201.35 o 1 4 42 7.25 -43.36 48.13 o 2 4 42 409.68 592.61 91.78 o 3 4 42 1.76 -7.74 83.79 o 4 4 42 177.17 143.10 68.64 o 1 5 42 292.56 250.39 69.98 o 2 5 42 601.93 465.60 115.32 o 3 5 42 61.15 61.34 73.65 o 4 5 42 351.21 378.77 80.88 o 0 6 42 11.31 107.86 85.92 o 1 6 42 1276.22 1422.31 380.86 o 2 6 42 543.03 531.03 94.08 o 3 6 42 180.96 212.85 66.40 o 4 6 42 177.07 150.25 76.38 o 1 7 42 66.36 106.16 71.35 o 2 7 42 1403.89 1658.02 246.27 o 3 7 42 246.86 376.54 81.49 o 0 8 42 300.04 438.84 137.22 o 1 8 42 14.41 -53.62 66.18 o 2 8 42 136.56 114.75 67.47 o 3 8 42 5.20 -26.25 90.56 o 1 9 42 23.58 -62.31 62.31 o 2 9 42 36.70 -16.83 76.12 o 1 10 42 45.88 12.38 111.39 o 1 1 43 25.23 11.31 48.19 o 2 1 43 363.36 321.98 80.16 o 3 1 43 2.30 -68.98 70.93 o 4 1 43 809.22 865.14 173.68 o 0 2 43 2304.28 2672.86 195.32 o 1 2 43 1.65 -14.29 51.77 o 2 2 43 486.63 468.58 69.62 o 3 2 43 903.47 847.28 119.54 o 4 2 43 73.05 -33.87 79.18 o 1 3 43 954.77 1104.49 92.57 o 2 3 43 51.18 20.34 64.14 o 3 3 43 597.40 712.74 104.54 o 4 3 43 540.36 550.93 116.73 o 0 4 43 1.98 -74.92 74.92 o 1 4 43 344.14 390.22 72.84 o 2 4 43 457.27 435.41 85.95 o 3 4 43 205.98 109.44 77.80 o 4 4 43 96.54 179.21 76.59 o 1 5 43 190.00 75.18 103.92 o 2 5 43 1115.59 1177.96 247.39 o 3 5 43 139.85 102.71 82.76 o 4 5 43 350.78 277.26 99.73 o 0 6 43 43.09 -86.23 237.58 o 1 6 43 747.66 869.09 104.90 o 2 6 43 218.98 82.41 99.58 o 3 6 43 392.65 493.85 124.70 o 1 7 43 1247.74 1121.33 218.83 o 2 7 43 126.29 175.94 76.59 o 3 7 43 1127.03 1015.08 108.64 o 0 8 43 989.80 1109.88 191.57 o 1 8 43 29.83 -17.58 102.82 o 2 8 43 156.81 74.09 75.79 o 2 9 43 51.31 45.15 105.69 o 0 0 44 1387.94 1962.26 231.93 o 1 0 44 2443.63 2779.45 329.33 o 2 0 44 315.38 221.42 94.03 o 3 0 44 417.57 415.79 192.51 o 1 1 44 168.50 184.20 86.02 o 2 1 44 429.21 356.27 66.97 o 3 1 44 110.05 25.49 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159.40 281.98 130.49 o 0 4 47 35.42 232.20 147.18 o 1 4 47 166.09 272.56 188.61 o 0 0 48 0.34 217.94 126.19 o 1 0 48 1398.62 1523.16 209.06 o 1 1 48 136.78 99.39 97.27 o 0 2 48 409.71 454.44 160.90 o