#------------------------------------------------------------------------------ #$Date: 2009-12-10 09:06:56 +0200 (Thu, 10 Dec 2009) $ #$Revision: 927 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2223806.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2223806_Fobs loop_ _publ_author_name 'Tahir, M. Nawaz' 'Acar, Nurcan' 'Yilmaz, Hamza' 'Tariq, Riaz H.' _publ_section_title ; Dimethyl (2-hydroxy-4-phenylbut-3-en-2-yl)phosphonate ; _journal_coeditor_code HB5172 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2922 _journal_volume 65 _journal_year 2009 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 103.771 _cell_angle_gamma 90.000 _cell_length_a 17.1522 _cell_length_b 8.1571 _cell_length_c 19.5230 _exptl_crystal_F_000 1088.00 _reflns_d_resolution_high 0.8263 _[local]_cod_data_source_file hb5172Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' NCAN4' _shelx_refln_list_code 4 _shelx_f_calc_maximum 308.90 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 8 0 0 12.62 33.22 18.58 o 10 0 0 442.53 419.11 53.13 o 12 0 0 10.22 32.09 12.03 o 14 0 0 360.49 332.20 17.46 o 16 0 0 3076.69 2958.54 63.69 o 18 0 0 942.35 1010.18 51.43 o 20 0 0 0.07 36.71 34.75 o 5 1 0 2318.36 2492.05 41.99 o 7 1 0 0.03 7.39 5.86 o 9 1 0 7905.24 8891.86 159.97 o 11 1 0 3.41 16.47 16.22 o 13 1 0 288.03 324.56 26.89 o 15 1 0 140.70 145.08 15.49 o 17 1 0 287.53 340.64 39.42 o 19 1 0 84.57 57.83 27.00 o 0 2 0 2705.60 2862.93 46.36 o 6 2 0 32.91 29.13 19.26 o 8 2 0 205.79 205.76 10.25 o 10 2 0 274.68 255.71 13.88 o 12 2 0 21.45 19.66 12.73 o 14 2 0 2081.21 2159.25 175.72 o 16 2 0 543.41 566.97 23.47 o 18 2 0 74.77 48.66 26.94 o 1 3 0 2413.70 2298.30 127.26 o 11 3 0 22.70 43.66 19.54 o 15 3 0 371.67 426.80 47.03 o 17 3 0 327.32 332.14 52.93 o 19 3 0 93.51 112.38 50.54 o 0 4 0 6394.13 5803.71 91.83 o 2 4 0 196.73 158.00 20.73 o 8 4 0 128.23 129.05 13.01 o 10 4 0 13.11 19.97 10.76 o 14 4 0 70.03 86.55 48.56 o 16 4 0 22.21 22.30 28.62 o 18 4 0 89.96 11.10 20.99 o 1 5 0 4374.52 3905.44 82.38 o 3 5 0 320.47 317.22 21.15 o 5 5 0 356.03 394.82 30.38 o 7 5 0 163.95 239.64 36.59 o 11 5 0 21.79 43.18 14.87 o 13 5 0 38.11 36.65 21.81 o 15 5 0 534.58 631.14 92.25 o 17 5 0 426.38 540.89 79.71 o 0 6 0 1132.30 1215.29 34.14 o 2 6 0 122.66 149.50 14.05 o 4 6 0 2222.33 2123.41 155.59 o 6 6 0 38.06 60.27 19.45 o 8 6 0 161.08 163.70 23.60 o 10 6 0 0.00 23.16 19.72 o 12 6 0 4.61 34.21 25.25 o 14 6 0 66.07 37.47 17.46 o 16 6 0 14.91 18.68 23.70 o 1 7 0 2320.35 2319.52 58.05 o 3 7 0 641.93 672.37 45.95 o 5 7 0 121.76 117.28 24.80 o 7 7 0 209.46 245.29 44.00 o 9 7 0 15.42 34.60 23.24 o 11 7 0 72.28 79.25 16.28 o 13 7 0 46.71 34.48 19.95 o 0 8 0 4.68 10.37 12.74 o 2 8 0 61.86 68.53 12.12 o 4 8 0 219.80 240.53 35.75 o 6 8 0 66.14 49.93 13.91 o 8 8 0 48.63 50.27 30.95 o 10 8 0 23.49 49.83 17.85 o 1 9 0 645.90 722.87 26.12 o 3 9 0 6.17 20.09 15.67 o 5 9 0 11.81 28.58 16.65 o 7 9 0 8.29 21.14 18.54 o -19 1 1 312.56 326.22 36.06 o -17 1 1 950.29 947.05 38.25 o -15 1 1 7.10 7.15 13.30 o -13 1 1 307.78 295.67 23.32 o -11 1 1 13.42 9.08 18.05 o -9 1 1 138.98 139.89 13.81 o -7 1 1 11.06 4.06 7.36 o -5 1 1 5102.19 5621.51 79.08 o -3 1 1 32602.52 32580.83 142.78 o -1 1 1 22548.91 20101.47 85.45 o 1 1 1 1903.53 1914.11 31.31 o 3 1 1 1131.38 1257.68 30.72 o 5 1 1 119.61 196.34 13.72 o 7 1 1 262.24 312.09 16.64 o 9 1 1 3318.09 3575.66 103.61 o 11 1 1 55.17 45.97 14.81 o 13 1 1 900.55 903.51 30.57 o 15 1 1 479.84 479.76 28.88 o 17 1 1 8.52 25.67 32.44 o 19 1 1 269.37 243.77 38.81 o -18 2 1 66.41 40.04 26.22 o -16 2 1 19.21 11.37 39.18 o -14 2 1 60.60 17.64 25.79 o -12 2 1 2.91 73.76 32.03 o -10 2 1 106.62 83.09 14.76 o -8 2 1 130.36 162.09 11.99 o -6 2 1 182.53 177.30 10.53 o -4 2 1 478.74 507.38 14.42 o -2 2 1 3958.68 3634.46 54.50 o 0 2 1 24080.57 21668.94 121.98 o 2 2 1 3318.32 3371.44 56.87 o 4 2 1 611.64 718.25 20.19 o 6 2 1 2804.21 3573.41 85.56 o 8 2 1 24.48 30.04 14.66 o 10 2 1 332.87 399.30 24.09 o 12 2 1 2.23 39.33 25.28 o 14 2 1 1.79 2.75 21.97 o 16 2 1 64.38 55.90 25.35 o 18 2 1 2.58 10.74 34.96 o -19 3 1 369.43 388.09 37.10 o -17 3 1 77.35 49.61 24.67 o -15 3 1 159.17 104.58 20.42 o -13 3 1 224.76 207.04 18.43 o -11 3 1 921.33 976.25 27.07 o -9 3 1 111.67 70.87 13.00 o -7 3 1 784.29 853.28 25.31 o -5 3 1 5598.05 5397.85 88.56 o -3 3 1 16066.11 14208.19 125.72 o -1 3 1 8844.26 7613.66 88.74 o 1 3 1 10116.00 9528.64 102.95 o 3 3 1 5895.09 5763.60 88.65 o 5 3 1 3896.26 4384.97 89.79 o 7 3 1 4711.10 6003.40 122.58 o 9 3 1 68.14 78.02 18.30 o 11 3 1 256.27 244.95 21.81 o 13 3 1 229.41 319.45 25.58 o 15 3 1 231.99 311.42 31.24 o 17 3 1 1.22 40.76 28.38 o -18 4 1 35.36 0.00 97.12 o -16 4 1 71.42 34.53 22.35 o -14 4 1 9.01 8.63 28.38 o -12 4 1 391.21 394.05 20.19 o -10 4 1 2156.56 1892.75 54.08 o -8 4 1 173.66 139.00 14.66 o -6 4 1 3293.38 3245.78 79.40 o -4 4 1 2558.90 2475.91 65.60 o -2 4 1 2750.97 2213.37 60.25 o 0 4 1 696.08 464.22 14.61 o 2 4 1 5014.43 5641.30 96.19 o 4 4 1 2080.26 2301.05 48.79 o 6 4 1 6110.59 7282.10 131.79 o 8 4 1 1536.17 1874.76 55.45 o 10 4 1 164.82 161.61 19.63 o 12 4 1 1024.12 1231.10 34.36 o 14 4 1 422.41 575.71 34.34 o 16 4 1 28.81 42.22 29.86 o 18 4 1 0.10 15.64 36.56 o -17 5 1 8.63 34.53 42.94 o -15 5 1 4.18 33.87 33.54 o -13 5 1 58.52 44.20 16.28 o -11 5 1 16.65 23.79 12.49 o -9 5 1 84.13 101.53 13.28 o -7 5 1 939.02 971.55 31.70 o -5 5 1 1368.74 1350.15 41.52 o -3 5 1 8.95 32.35 10.07 o -1 5 1 468.41 439.40 16.58 o 1 5 1 650.31 610.57 18.61 o 3 5 1 381.70 433.89 18.83 o 5 5 1 1353.87 1310.31 46.36 o 7 5 1 150.97 146.20 14.57 o 9 5 1 0.59 12.54 24.14 o 11 5 1 183.28 200.05 20.78 o 13 5 1 17.52 21.29 31.98 o 15 5 1 14.68 21.64 25.06 o 17 5 1 3.35 1.45 49.07 o -16 6 1 43.15 43.45 24.08 o -14 6 1 169.16 196.34 26.92 o -12 6 1 278.83 307.45 22.46 o -10 6 1 282.72 259.91 19.43 o -8 6 1 127.22 94.81 13.94 o -6 6 1 63.88 78.35 13.00 o -4 6 1 2578.95 2489.04 58.26 o -2 6 1 5679.59 5320.64 115.40 o 0 6 1 1881.87 1837.44 51.67 o 2 6 1 1068.43 1215.29 35.45 o 4 6 1 1655.22 1618.34 43.94 o 6 6 1 849.08 993.98 28.50 o 8 6 1 298.65 388.83 20.80 o 10 6 1 0.69 57.32 32.51 o 12 6 1 307.00 362.55 29.41 o 14 6 1 507.46 617.10 43.04 o -13 7 1 170.99 164.98 25.64 o -11 7 1 123.58 147.11 23.30 o -9 7 1 54.51 51.22 16.71 o -7 7 1 29.70 51.22 29.11 o -5 7 1 0.21 5.37 25.07 o -3 7 1 244.48 161.61 15.80 o -1 7 1 391.14 377.77 18.30 o 1 7 1 11.30 55.62 12.64 o 3 7 1 446.11 459.36 20.99 o 5 7 1 88.86 92.62 15.59 o 7 7 1 28.57 27.61 33.85 o 9 7 1 118.97 200.59 22.94 o 11 7 1 5.63 0.00 41.89 o 13 7 1 106.59 162.09 31.17 o -10 8 1 5.08 18.28 25.77 o -8 8 1 16.17 24.91 29.52 o -6 8 1 25.93 40.76 17.80 o -4 8 1 360.39 389.58 23.05 o -2 8 1 248.25 258.69 19.99 o 0 8 1 37.35 21.82 13.90 o 2 8 1 32.40 16.70 31.10 o 4 8 1 23.50 9.31 26.15 o 6 8 1 131.22 136.79 23.79 o 8 8 1 55.40 13.91 30.40 o 10 8 1 0.11 27.61 36.81 o -7 9 1 0.07 3.84 47.22 o -5 9 1 192.92 223.62 25.91 o -3 9 1 80.10 68.05 21.44 o -1 9 1 15.79 6.95 42.58 o 1 9 1 0.47 24.53 30.60 o 3 9 1 0.70 67.74 37.51 o 5 9 1 295.22 355.42 31.96 o 7 9 1 142.49 224.18 29.89 o -20 0 2 426.13 511.63 42.60 o -18 0 2 5.29 33.21 45.15 o -16 0 2 1805.36 2031.21 54.32 o -14 0 2 2910.72 3220.08 83.36 o -12 0 2 100.85 87.62 19.39 o -10 0 2 359.14 386.61 20.74 o -8 0 2 1901.19 1710.54 43.62 o -6 0 2 350.91 253.87 12.60 o -4 0 2 21261.12 25948.10 157.76 o -2 0 2 40.98 54.78 8.09 o 2 0 2 79902.80 64043.22 200.18 o 4 0 2 1587.85 1133.98 32.98 o 6 0 2 7440.02 6804.82 105.65 o 8 0 2 645.03 700.20 20.93 o 10 0 2 359.73 312.09 21.96 o 12 0 2 11.02 21.64 29.44 o 14 0 2 16.98 52.85 19.17 o 16 0 2 360.76 339.96 31.95 o 18 0 2 2131.54 2068.73 65.10 o -19 1 2 50.26 19.59 25.17 o -17 1 2 460.93 543.64 32.50 o -15 1 2 0.80 26.05 27.68 o -13 1 2 279.63 382.18 23.56 o -11 1 2 549.76 551.57 23.00 o -9 1 2 286.23 294.38 14.22 o -7 1 2 821.97 941.26 25.42 o -5 1 2 533.93 541.01 17.52 o -3 1 2 4637.09 4942.93 60.91 o -1 1 2 299.42 269.09 8.65 o 1 1 2 42325.76 38875.77 133.68 o 3 1 2 8444.47 8033.41 91.15 o 5 1 2 8975.55 7989.58 114.47 o 7 1 2 87.81 97.77 14.53 o 9 1 2 44.85 75.06 18.60 o 11 1 2 564.92 550.69 22.10 o 13 1 2 18.54 0.00 65.13 o 15 1 2 4.43 16.70 27.71 o 17 1 2 270.85 222.49 37.64 o 19 1 2 20.62 15.20 34.65 o -20 2 2 51.84 10.25 60.49 o -18 2 2 5.13 21.99 38.86 o -16 2 2 578.08 522.76 29.28 o -14 2 2 778.36 822.75 27.01 o -12 2 2 235.02 264.17 20.82 o -10 2 2 528.91 500.61 20.23 o -8 2 2 762.32 804.49 24.57 o -6 2 2 4608.44 4508.04 78.40 o -4 2 2 2590.01 2599.23 53.77 o -2 2 2 2432.41 2129.12 43.45 o 0 2 2 1431.09 1404.67 36.70 o 2 2 2 4518.47 3949.85 61.55 o 4 2 2 22937.38 26142.62 182.71 o 6 2 2 2897.35 2868.98 80.70 o 8 2 2 424.28 478.12 22.24 o 10 2 2 1.46 9.08 40.86 o 12 2 2 386.13 381.44 25.75 o 14 2 2 208.34 288.59 26.24 o 16 2 2 992.35 1021.49 44.54 o 18 2 2 202.20 45.46 65.02 o -19 3 2 356.07 311.42 35.23 o -17 3 2 30.98 4.94 16.61 o -15 3 2 92.32 81.04 19.67 o -13 3 2 677.39 565.82 23.30 o -11 3 2 1673.23 1659.52 52.17 o -9 3 2 165.01 131.99 14.71 o -7 3 2 3012.38 2751.18 71.13 o -5 3 2 5474.20 4911.20 84.47 o -3 3 2 1811.11 1759.17 48.98 o -1 3 2 2105.19 2097.95 50.03 o 1 3 2 1818.27 1615.32 31.79 o 3 3 2 19552.74 20407.03 161.43 o 5 3 2 559.55 624.61 18.83 o 7 3 2 6.63 18.12 12.67 o 9 3 2 675.69 790.66 28.60 o 11 3 2 13.48 32.35 15.64 o 13 3 2 22.02 49.61 30.25 o 15 3 2 237.76 280.33 32.79 o 17 3 2 8.81 24.72 31.84 o -18 4 2 242.99 202.73 29.50 o -16 4 2 18.72 6.56 14.30 o -14 4 2 0.62 54.51 33.37 o -12 4 2 21.86 4.94 27.53 o -10 4 2 68.26 75.71 15.08 o -8 4 2 386.56 318.10 17.47 o -6 4 2 84.59 66.50 11.67 o -4 4 2 824.03 950.53 31.36 o -2 4 2 0.03 16.24 16.85 o 0 4 2 592.62 653.17 18.29 o 2 4 2 4349.68 4384.97 84.81 o 4 4 2 1536.04 1564.25 41.71 o 6 4 2 357.09 419.11 20.05 o 8 4 2 81.38 128.97 14.12 o 10 4 2 49.11 37.93 15.54 o 12 4 2 235.20 279.07 25.17 o 14 4 2 17.85 27.81 46.08 o 16 4 2 2.86 19.26 18.84 o -17 5 2 277.56 268.48 32.09 o -15 5 2 261.16 316.76 27.49 o -13 5 2 616.26 618.04 26.22 o -11 5 2 57.39 48.82 13.16 o -9 5 2 631.71 548.04 20.28 o -7 5 2 53.53 8.52 26.15 o -5 5 2 646.57 583.88 19.11 o -3 5 2 212.72 195.82 13.70 o -1 5 2 839.11 795.96 22.32 o 1 5 2 1430.15 1328.10 39.81 o 3 5 2 1305.89 1097.49 31.20 o 5 5 2 594.53 601.30 18.47 o 7 5 2 228.51 259.91 17.61 o 9 5 2 59.89 62.57 15.49 o 11 5 2 73.00 26.24 37.63 o 13 5 2 2.82 90.10 41.48 o 15 5 2 0.07 30.87 50.02 o -16 6 2 14.81 17.48 18.74 o -14 6 2 24.85 26.63 36.35 o -12 6 2 203.66 144.83 20.40 o -10 6 2 40.26 20.60 25.82 o -8 6 2 553.17 532.28 19.99 o -6 6 2 671.71 638.81 20.94 o -4 6 2 46.35 2.16 38.84 o -2 6 2 2.66 19.26 24.63 o 0 6 2 436.51 426.86 15.56 o 2 6 2 148.80 128.55 14.52 o 4 6 2 1603.91 1695.00 52.73 o 6 6 2 19.48 17.01 26.41 o 8 6 2 39.58 13.21 23.00 o 10 6 2 68.56 33.43 40.94 o 12 6 2 3.24 5.37 22.73 o 14 6 2 83.46 117.68 31.46 o -13 7 2 173.93 200.05 25.57 o -11 7 2 1.36 27.61 17.42 o -9 7 2 7.58 12.27 23.49 o -7 7 2 230.10 257.48 20.55 o -5 7 2 1245.80 1283.19 39.13 o -3 7 2 0.59 33.21 24.10 o -1 7 2 195.23 195.29 15.27 o 1 7 2 1793.10 1775.01 57.13 o 3 7 2 979.37 1145.42 30.60 o 5 7 2 372.45 345.54 20.31 o 7 7 2 17.92 23.61 16.11 o 9 7 2 3.06 1.89 17.26 o 11 7 2 124.78 154.04 27.12 o 13 7 2 92.46 62.57 29.20 o -12 8 2 54.80 77.03 24.46 o -10 8 2 0.53 7.25 14.51 o -8 8 2 11.13 68.05 38.53 o -6 8 2 30.26 12.80 24.53 o -4 8 2 130.13 139.45 19.57 o -2 8 2 167.39 174.30 18.90 o 0 8 2 0.44 20.95 27.41 o 2 8 2 0.81 15.79 13.17 o 4 8 2 286.65 332.37 24.03 o 6 8 2 37.61 34.53 21.03 o 8 8 2 0.85 16.70 30.48 o 10 8 2 59.65 91.54 27.03 o -7 9 2 65.33 101.15 22.35 o -5 9 2 99.22 118.09 24.97 o -3 9 2 178.92 182.86 25.47 o -1 9 2 84.09 95.54 21.72 o 1 9 2 352.41 444.15 31.75 o 3 9 2 229.18 258.09 27.23 o 5 9 2 53.65 102.29 25.14 o 7 9 2 19.48 58.47 40.90 o -19 1 3 463.21 448.92 38.31 o -17 1 3 1389.79 1319.88 43.79 o -15 1 3 9.25 28.41 34.33 o -13 1 3 1279.88 1235.07 38.39 o -11 1 3 1733.96 1781.36 54.05 o -9 1 3 122.57 113.23 12.83 o -7 1 3 116.77 118.09 11.46 o -5 1 3 9.05 5.37 19.31 o -3 1 3 4103.87 4266.06 59.05 o -1 1 3 13278.66 13692.14 88.15 o 1 1 3 23301.82 21624.61 110.78 o 3 1 3 677.17 754.02 20.69 o 5 1 3 1315.06 1001.12 30.99 o 7 1 3 4.39 50.15 21.87 o 9 1 3 438.95 648.37 26.86 o 11 1 3 64.67 65.59 17.39 o 13 1 3 612.87 584.79 29.15 o 15 1 3 1492.71 1492.11 46.56 o 17 1 3 371.02 392.55 41.05 o 19 1 3 6.29 23.61 55.22 o -20 2 3 151.02 0.00 118.09 o -18 2 3 11.02 75.71 23.60 o -16 2 3 105.21 103.05 21.41 o -14 2 3 59.19 53.40 16.79 o -12 2 3 37.68 40.04 15.73 o -10 2 3 1135.41 1042.05 31.61 o -8 2 3 735.49 704.19 24.99 o -6 2 3 2498.54 2605.00 63.44 o -4 2 3 10447.03 10160.17 102.51 o -2 2 3 309.34 315.42 9.37 o 0 2 3 592.06 598.53 20.27 o 2 2 3 5630.61 5192.28 70.57 o 4 2 3 1746.28 1701.21 37.29 o 6 2 3 58.36 61.09 12.66 o 8 2 3 29.37 51.76 17.34 o 10 2 3 17.52 1.94 34.96 o 12 2 3 754.73 798.09 31.92 o 14 2 3 36.34 71.51 21.66 o 16 2 3 0.43 9.66 31.58 o 18 2 3 111.53 193.19 36.12 o -19 3 3 230.79 257.48 33.24 o -17 3 3 24.52 8.09 49.07 o -15 3 3 409.54 433.89 25.89 o -13 3 3 84.01 75.06 15.34 o -11 3 3 1006.96 927.45 30.97 o -9 3 3 6408.48 5950.98 116.23 o -7 3 3 2818.64 2639.72 69.67 o -5 3 3 226.65 229.86 11.42 o -3 3 3 4844.00 4422.46 75.15 o -1 3 3 12331.85 11585.13 113.52 o 1 3 3 1237.33 1147.97 29.35 o 3 3 3 9003.40 9106.90 111.43 o 5 3 3 136.79 120.15 11.97 o 7 3 3 1412.70 1528.70 48.60 o 9 3 3 868.60 1154.36 35.83 o 11 3 3 247.32 230.43 21.73 o 13 3 3 644.59 724.32 32.44 o 15 3 3 306.66 455.33 34.56 o 17 3 3 179.43 274.68 40.58 o -18 4 3 404.45 414.50 34.51 o -16 4 3 273.52 290.51 28.89 o -14 4 3 669.41 569.41 26.07 o -12 4 3 240.99 231.00 16.60 o -10 4 3 2419.16 2279.42 59.35 o -8 4 3 1643.14 1576.19 44.86 o -6 4 3 5.28 3.27 7.24 o -4 4 3 2837.67 3168.99 72.09 o -2 4 3 7242.45 6088.33 96.99 o 0 4 3 649.37 546.28 14.09 o 2 4 3 1875.93 2012.58 42.25 o 4 4 3 1.32 49.61 11.41 o 6 4 3 438.44 484.73 19.90 o 8 4 3 2948.63 3156.28 71.95 o 10 4 3 0.19 8.20 9.81 o 12 4 3 81.89 116.46 19.92 o 14 4 3 389.52 359.69 33.58 o 16 4 3 288.02 306.79 41.56 o -17 5 3 35.78 76.70 24.74 o -15 5 3 15.06 11.62 15.41 o -13 5 3 2.14 43.70 15.44 o -11 5 3 83.12 100.39 14.34 o -9 5 3 809.88 770.66 23.00 o -7 5 3 283.58 213.05 15.94 o -5 5 3 169.77 174.80 13.94 o -3 5 3 241.98 211.40 13.69 o -1 5 3 2.04 6.85 20.26 o 1 5 3 704.08 639.77 19.05 o 3 5 3 27.47 55.34 12.61 o 5 5 3 567.98 557.78 17.79 o 7 5 3 49.19 97.39 14.13 o 9 5 3 11.77 2.50 37.85 o 11 5 3 26.77 18.76 32.14 o 13 5 3 113.35 140.78 26.82 o 15 5 3 8.75 10.37 22.23 o -16 6 3 650.82 626.50 37.71 o -14 6 3 0.36 24.16 34.62 o -12 6 3 174.38 211.95 20.29 o -10 6 3 297.00 305.47 21.73 o -8 6 3 975.01 909.18 27.26 o -6 6 3 494.76 422.20 17.80 o -4 6 3 158.62 155.45 15.50 o -2 6 3 3139.24 2956.39 61.44 o 0 6 3 6416.04 5757.89 125.76 o 2 6 3 505.33 506.53 19.50 o 4 6 3 835.73 784.32 22.15 o 6 6 3 639.55 653.17 23.10 o 8 6 3 89.60 123.89 17.61 o 10 6 3 412.24 523.63 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