#------------------------------------------------------------------------------ #$Date: 2009-12-10 09:06:56 +0200 (Thu, 10 Dec 2009) $ #$Revision: 927 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2223894.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2223894_Fobs loop_ _publ_author_name 'Lin, Cui-Hua' 'Liu, Nai-Sheng' 'Jian, Fang-Fang' _publ_section_title ; 2-Amino-4,6-dimethylpyrimidinium dihydrogenphosphate ; _journal_coeditor_code LH2909 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2639 _journal_volume 65 _journal_year 2009 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 95.554 _cell_angle_gamma 90.000 _cell_length_a 11.7427 _cell_length_b 4.8266 _cell_length_c 16.9398 _exptl_crystal_F_000 464.00 _reflns_d_resolution_high 0.7703 _[local]_cod_data_source_file lh2909Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' a in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 168.56 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 804.92 748.35 24.04 o 4 0 0 9.22 12.87 2.20 o 6 0 0 889.05 964.04 26.58 o 8 0 0 74.78 63.15 2.57 o 10 0 0 1131.59 1116.49 37.35 o 12 0 0 31.95 39.21 3.46 o 14 0 0 97.63 95.54 4.51 o 1 1 0 0.16 1.04 0.20 o 2 1 0 142.50 141.49 1.58 o 3 1 0 83.83 109.62 1.42 o 4 1 0 334.54 461.79 4.56 o 5 1 0 370.20 415.91 4.09 o 6 1 0 41.07 26.22 1.15 o 7 1 0 21.06 12.93 1.06 o 8 1 0 116.95 135.24 2.53 o 9 1 0 55.31 59.50 2.09 o 10 1 0 1657.73 1632.79 19.13 o 11 1 0 0.24 0.42 1.13 o 12 1 0 315.27 301.71 6.39 o 13 1 0 32.91 39.37 2.87 o 14 1 0 205.38 205.86 4.73 o 0 2 0 1924.27 1933.16 37.07 o 1 2 0 320.07 364.57 3.41 o 2 2 0 9.23 1.55 0.22 o 3 2 0 41.60 39.26 0.54 o 4 2 0 5027.42 5752.98 59.80 o 5 2 0 0.42 3.70 0.35 o 6 2 0 707.44 622.99 5.62 o 7 2 0 512.85 439.77 4.46 o 8 2 0 126.35 125.47 2.21 o 9 2 0 54.74 55.22 1.43 o 10 2 0 14.93 12.51 0.88 o 11 2 0 11.61 10.19 0.89 o 12 2 0 47.60 43.69 1.72 o 13 2 0 5.27 6.83 1.29 o 14 2 0 134.37 143.39 2.95 o 1 3 0 125.18 119.24 1.52 o 2 3 0 214.31 209.41 2.11 o 3 3 0 57.57 58.84 1.59 o 4 3 0 54.39 55.74 1.56 o 5 3 0 294.96 299.04 3.14 o 6 3 0 16.66 22.56 0.71 o 7 3 0 2.14 1.72 0.49 o 8 3 0 262.32 236.84 2.73 o 9 3 0 90.08 96.86 2.68 o 10 3 0 129.30 113.93 2.39 o 11 3 0 78.94 79.80 1.64 o 12 3 0 35.23 32.44 1.48 o 13 3 0 2.58 1.80 0.90 o 0 4 0 1748.36 1688.72 37.15 o 1 4 0 59.00 50.85 2.58 o 2 4 0 106.75 113.31 1.66 o 3 4 0 408.77 398.94 5.02 o 4 4 0 0.07 0.63 0.83 o 5 4 0 11.44 5.75 1.13 o 6 4 0 76.59 75.68 2.23 o 7 4 0 19.08 19.49 1.61 o 8 4 0 5.19 6.16 1.53 o 9 4 0 10.41 14.02 1.68 o 10 4 0 227.17 240.61 5.40 o 11 4 0 10.26 8.39 1.72 o 1 5 0 309.11 306.18 4.02 o 2 5 0 29.57 29.62 1.38 o 3 5 0 22.49 23.39 1.63 o 4 5 0 50.61 45.49 2.09 o 5 5 0 28.13 31.44 1.68 o 6 5 0 173.42 173.29 4.50 o 7 5 0 46.98 47.47 2.47 o 8 5 0 65.26 66.10 3.19 o 9 5 0 64.28 69.14 5.37 o 1 6 0 62.63 66.97 3.25 o 2 6 0 3.59 8.63 6.82 o 3 6 0 13.63 9.71 4.20 o 4 6 0 6.68 2.84 1.69 o -15 0 1 32.64 35.50 3.95 o -13 0 1 687.65 713.62 14.66 o -11 0 1 606.74 589.13 18.08 o -9 0 1 173.59 144.76 9.35 o -7 0 1 263.98 292.77 5.92 o -5 0 1 106.15 95.85 2.03 o -3 0 1 8484.41 7621.07 127.75 o 3 0 1 8731.65 6967.45 242.28 o 5 0 1 11.84 13.53 1.34 o 7 0 1 698.04 691.01 26.49 o 9 0 1 0.11 2.04 1.84 o 11 0 1 0.15 0.95 2.45 o 13 0 1 694.09 698.55 13.46 o 15 0 1 0.77 4.22 2.36 o -15 1 1 149.15 152.08 4.42 o -14 1 1 1.57 1.76 1.39 o -13 1 1 63.50 63.66 2.54 o -12 1 1 106.76 104.06 3.69 o -11 1 1 221.83 216.01 4.59 o -10 1 1 151.82 143.95 3.08 o -9 1 1 6.31 9.57 1.40 o -8 1 1 66.25 64.34 1.98 o -7 1 1 153.34 114.99 2.01 o -6 1 1 35.99 35.27 1.12 o -5 1 1 274.27 265.62 2.81 o -4 1 1 408.38 462.85 4.28 o -3 1 1 4109.02 4498.33 49.09 o -2 1 1 2359.23 2417.71 26.14 o -1 1 1 133.19 127.84 1.50 o 0 1 1 1678.79 1731.57 21.50 o 1 1 1 6728.16 6926.70 70.87 o 2 1 1 311.70 315.25 2.15 o 3 1 1 3511.27 3666.23 33.93 o 4 1 1 165.66 199.30 1.82 o 5 1 1 44.55 40.42 1.52 o 6 1 1 363.77 405.53 4.27 o 7 1 1 87.91 57.26 1.65 o 8 1 1 321.38 357.04 5.34 o 9 1 1 459.91 431.02 6.50 o 10 1 1 488.30 477.96 6.49 o 11 1 1 694.61 695.54 9.68 o 12 1 1 51.27 52.46 2.38 o 13 1 1 14.04 14.19 2.31 o 14 1 1 0.95 1.69 1.37 o -14 2 1 12.64 15.04 1.27 o -13 2 1 188.96 195.93 3.13 o -12 2 1 0.40 0.94 0.74 o -11 2 1 7.80 9.08 0.84 o -10 2 1 63.64 58.95 2.06 o -9 2 1 676.42 630.77 7.57 o -8 2 1 109.82 98.27 1.67 o -7 2 1 511.00 533.73 5.06 o -6 2 1 200.95 234.58 2.47 o -5 2 1 959.30 952.86 7.87 o -4 2 1 835.75 808.16 9.66 o -3 2 1 542.45 522.59 4.49 o -2 2 1 102.79 96.00 1.48 o -1 2 1 338.22 313.24 5.80 o 0 2 1 208.44 312.12 4.07 o 1 2 1 3108.52 3393.24 34.77 o 2 2 1 30.03 34.88 0.67 o 3 2 1 801.72 693.30 4.92 o 4 2 1 433.29 429.19 3.56 o 5 2 1 111.50 112.32 1.27 o 6 2 1 116.26 121.42 1.67 o 7 2 1 272.11 287.94 2.97 o 8 2 1 29.35 22.97 0.95 o 9 2 1 320.16 304.12 4.57 o 10 2 1 24.01 28.97 1.69 o 11 2 1 62.84 64.24 1.67 o 12 2 1 34.65 35.53 1.45 o 13 2 1 162.36 162.31 2.84 o 14 2 1 0.11 -0.57 0.89 o -13 3 1 3.73 3.51 0.71 o -12 3 1 2.11 1.83 0.63 o -11 3 1 77.64 75.33 1.57 o -10 3 1 8.48 9.74 0.95 o -9 3 1 2.53 3.35 0.58 o -8 3 1 327.76 307.04 3.18 o -7 3 1 293.36 265.12 2.86 o -6 3 1 0.37 1.24 0.63 o -5 3 1 676.01 649.42 8.55 o -4 3 1 73.27 70.04 1.72 o -3 3 1 286.58 322.64 4.30 o -2 3 1 32.65 46.07 0.56 o -1 3 1 250.61 243.87 2.68 o 0 3 1 725.34 785.98 10.85 o 1 3 1 597.12 568.63 5.15 o 2 3 1 1048.20 1196.13 11.58 o 3 3 1 535.46 572.36 5.44 o 4 3 1 96.44 78.06 2.14 o 5 3 1 139.21 129.86 1.78 o 6 3 1 484.12 488.49 4.86 o 7 3 1 80.84 74.67 1.17 o 8 3 1 9.75 9.24 0.75 o 9 3 1 21.21 21.24 0.79 o 10 3 1 2.51 2.99 0.73 o 11 3 1 205.80 209.12 2.94 o 12 3 1 31.74 35.27 1.25 o 13 3 1 33.11 37.68 2.16 o -11 4 1 83.99 86.84 3.69 o -10 4 1 130.04 136.36 4.29 o -9 4 1 14.13 13.82 1.70 o -8 4 1 3.05 3.33 1.38 o -7 4 1 12.12 8.18 1.38 o -6 4 1 71.89 71.18 2.20 o -5 4 1 30.09 28.94 1.56 o -4 4 1 9.97 6.63 1.26 o -3 4 1 388.66 369.39 4.68 o -2 4 1 153.84 132.98 1.34 o -1 4 1 160.57 182.28 2.17 o 0 4 1 569.77 574.32 8.30 o 1 4 1 211.13 238.09 2.77 o 2 4 1 592.98 580.89 6.04 o 3 4 1 397.87 379.27 3.63 o 4 4 1 1.10 2.33 0.97 o 5 4 1 335.59 310.05 5.41 o 6 4 1 51.43 53.56 2.00 o 7 4 1 147.14 153.70 5.65 o 8 4 1 99.58 104.13 3.26 o 9 4 1 32.36 33.60 2.23 o 10 4 1 25.99 24.36 3.36 o 11 4 1 84.64 79.21 2.95 o -9 5 1 123.25 126.80 4.81 o -8 5 1 109.75 109.10 5.12 o -7 5 1 70.62 67.54 3.33 o -6 5 1 7.00 7.37 1.67 o -5 5 1 242.32 239.67 4.13 o -4 5 1 53.15 51.17 2.47 o -3 5 1 16.24 7.72 6.12 o -2 5 1 95.98 98.65 3.52 o -1 5 1 93.84 93.08 1.21 o 0 5 1 0.10 0.02 0.29 o 1 5 1 9.09 6.08 4.45 o 2 5 1 340.27 342.18 4.58 o 3 5 1 15.05 11.56 8.08 o 4 5 1 160.45 168.13 3.87 o 5 5 1 0.15 0.88 0.91 o 6 5 1 48.86 49.23 2.71 o 7 5 1 0.16 1.72 1.21 o 8 5 1 45.25 51.80 2.92 o 9 5 1 132.69 131.98 3.91 o -4 6 1 184.72 194.29 4.97 o -3 6 1 0.03 -0.17 1.13 o -2 6 1 35.39 40.25 2.71 o -1 6 1 5.36 0.01 1.04 o 0 6 1 1.61 -0.08 1.39 o 1 6 1 49.43 49.64 4.41 o 2 6 1 0.08 1.52 1.74 o 3 6 1 277.62 302.67 14.37 o 4 6 1 226.25 245.47 14.23 o -14 0 2 302.75 300.44 7.71 o -12 0 2 1965.71 1970.68 46.58 o -10 0 2 2.05 2.59 1.61 o -8 0 2 119.86 107.46 3.03 o -6 0 2 239.36 290.52 4.93 o -4 0 2 658.62 709.09 8.68 o -2 0 2 5645.54 5638.50 86.98 o 2 0 2 4387.75 4052.50 60.03 o 4 0 2 461.50 440.21 10.08 o 6 0 2 342.09 301.53 7.43 o 8 0 2 93.23 114.08 3.43 o 10 0 2 281.69 293.30 6.28 o 12 0 2 403.09 410.58 8.47 o 14 0 2 31.72 37.21 4.29 o -15 1 2 0.07 0.17 1.40 o -14 1 2 6.19 5.62 1.83 o -13 1 2 36.58 31.60 4.87 o -12 1 2 243.74 235.06 4.57 o -11 1 2 13.39 15.13 1.56 o -10 1 2 11.24 14.04 1.91 o -9 1 2 8.39 7.60 1.41 o -8 1 2 292.17 295.09 4.11 o -7 1 2 200.55 213.30 3.19 o -6 1 2 470.39 491.23 6.52 o -5 1 2 101.79 128.31 1.72 o -4 1 2 204.21 187.55 2.17 o -3 1 2 136.79 144.66 1.66 o -2 1 2 28414.00 23344.16 999.19 o -1 1 2 371.87 365.46 3.50 o 0 1 2 250.58 282.17 3.15 o 1 1 2 9.87 1.43 0.17 o 2 1 2 4410.44 4673.12 40.60 o 3 1 2 11.15 7.18 0.35 o 4 1 2 2.07 3.06 0.34 o 5 1 2 877.33 920.11 7.73 o 6 1 2 1489.42 1356.77 17.99 o 7 1 2 12.28 17.22 1.35 o 8 1 2 301.18 301.89 4.40 o 9 1 2 115.31 111.35 3.00 o 10 1 2 42.82 49.90 2.20 o 11 1 2 70.55 69.39 2.64 o 12 1 2 194.57 188.05 3.78 o 13 1 2 7.81 6.85 1.15 o 14 1 2 81.03 81.48 2.53 o -14 2 2 0.16 0.27 0.78 o -13 2 2 16.61 18.70 1.90 o -12 2 2 184.05 179.59 3.56 o -11 2 2 1.40 0.82 1.05 o -10 2 2 516.02 514.95 6.82 o -9 2 2 102.43 100.06 2.50 o -8 2 2 246.23 259.81 3.73 o -7 2 2 188.98 173.95 2.88 o -6 2 2 418.17 370.07 4.13 o -5 2 2 115.43 80.17 1.17 o -4 2 2 99.59 88.95 0.87 o -3 2 2 606.81 642.87 6.90 o -2 2 2 3691.74 4337.52 54.72 o -1 2 2 787.80 881.06 9.01 o 0 2 2 0.37 0.55 0.45 o 1 2 2 302.84 292.27 2.67 o 2 2 2 1207.06 1367.82 20.25 o 3 2 2 1443.04 1482.71 16.82 o 4 2 2 2626.22 2868.54 26.79 o 5 2 2 119.93 130.37 1.73 o 6 2 2 358.61 332.04 3.39 o 7 2 2 206.28 200.93 2.63 o 8 2 2 1635.97 1597.27 15.27 o 9 2 2 30.75 28.11 1.52 o 10 2 2 449.04 435.34 8.54 o 11 2 2 0.11 1.34 0.94 o 12 2 2 85.29 81.11 2.28 o 13 2 2 30.34 30.98 2.00 o 14 2 2 67.25 69.68 2.47 o -13 3 2 1.23 0.40 0.74 o -12 3 2 110.72 126.10 2.49 o -11 3 2 158.02 151.80 2.22 o -10 3 2 3.70 3.18 0.46 o -9 3 2 186.06 178.73 2.48 o -8 3 2 307.24 299.78 3.29 o -7 3 2 309.67 267.72 2.81 o -6 3 2 46.11 58.52 2.46 o -5 3 2 5.83 3.35 0.95 o -4 3 2 281.66 269.77 3.95 o -3 3 2 6.12 10.14 0.89 o -2 3 2 1636.60 1643.84 16.56 o -1 3 2 6.18 1.91 0.84 o 0 3 2 35.59 40.04 1.49 o 1 3 2 503.54 436.53 4.11 o 2 3 2 1913.40 1971.72 19.96 o 3 3 2 259.18 249.33 2.63 o 4 3 2 196.52 183.21 2.95 o 5 3 2 301.96 279.24 3.08 o 6 3 2 82.34 94.38 1.61 o 7 3 2 79.91 64.34 1.17 o 8 3 2 55.97 48.10 1.21 o 9 3 2 4.60 6.73 0.84 o 10 3 2 6.54 8.87 0.76 o 11 3 2 17.07 15.58 1.15 o 12 3 2 153.35 154.84 2.88 o 13 3 2 66.92 68.49 1.91 o -11 4 2 137.51 144.12 4.06 o -10 4 2 64.71 68.06 3.24 o -9 4 2 24.82 22.49 4.05 o -8 4 2 61.72 61.88 3.10 o -7 4 2 20.28 13.05 1.47 o -6 4 2 21.25 16.00 1.61 o -5 4 2 146.36 141.84 3.61 o -4 4 2 38.52 49.03 1.74 o -3 4 2 155.37 152.72 2.46 o -2 4 2 298.39 310.97 4.86 o -1 4 2 528.76 529.52 5.32 o 0 4 2 212.73 184.21 2.67 o 1 4 2 6.87 8.93 0.60 o 2 4 2 254.17 259.77 2.90 o 3 4 2 724.65 736.51 6.72 o 4 4 2 110.67 117.55 3.08 o 5 4 2 27.15 26.67 2.41 o 6 4 2 98.23 97.14 3.43 o 7 4 2 132.19 141.11 3.42 o 8 4 2 0.14 0.34 1.31 o 9 4 2 1.34 1.82 0.47 o 10 4 2 49.45 41.41 3.46 o 11 4 2 60.83 63.63 2.53 o -9 5 2 39.81 44.70 2.83 o -8 5 2 145.39 145.88 4.28 o -7 5 2 22.71 25.26 1.93 o -6 5 2 4.94 2.95 1.08 o -5 5 2 121.35 116.04 2.56 o -4 5 2 35.71 31.99 2.21 o -3 5 2 5.24 2.53 1.46 o -2 5 2 260.07 262.33 5.83 o -1 5 2 99.87 95.59 3.59 o 0 5 2 0.00 0.06 0.27 o 1 5 2 71.87 75.53 1.39 o 2 5 2 0.92 0.57 0.60 o 3 5 2 0.27 0.46 0.40 o 4 5 2 18.05 18.77 1.63 o 5 5 2 333.76 340.90 5.16 o 6 5 2 30.34 33.24 2.03 o 7 5 2 4.35 6.08 1.47 o 8 5 2 153.09 160.04 4.51 o -4 6 2 16.87 13.22 4.08 o -3 6 2 45.72 46.21 2.76 o -2 6 2 1.24 20.81 15.01 o -1 6 2 40.62 44.69 2.19 o 0 6 2 27.18 29.30 2.31 o 1 6 2 0.17 0.61 1.22 o 2 6 2 6.39 4.24 2.31 o 3 6 2 204.03 211.86 4.77 o 4 6 2 77.97 93.82 12.33 o -15 0 3 108.47 115.18 5.09 o -13 0 3 210.20 211.53 6.08 o -11 0 3 75.11 72.47 5.09 o -9 0 3 67.83 61.76 2.97 o -7 0 3 87.39 94.38 4.08 o -5 0 3 8.88 6.43 0.97 o -3 0 3 1840.03 1833.77 23.46 o -1 0 3 4946.46 5221.51 76.52 o 1 0 3 1578.35 1726.14 14.71 o 3 0 3 604.29 452.17 5.79 o 5 0 3 383.05 527.28 7.80 o 7 0 3 1068.30 1184.28 17.87 o 9 0 3 170.01 159.37 6.48 o 11 0 3 26.28 27.83 2.51 o 13 0 3 261.40 255.67 6.59 o -15 1 3 148.49 156.72 4.95 o -14 1 3 32.80 30.34 2.27 o -13 1 3 63.39 60.72 2.68 o -12 1 3 24.07 26.71 1.91 o -11 1 3 448.41 452.71 6.19 o -10 1 3 13.76 14.04 1.46 o -9 1 3 208.75 206.56 3.33 o -8 1 3 149.78 138.73 2.56 o -7 1 3 5.54 9.26 0.90 o -6 1 3 98.88 111.70 1.89 o -5 1 3 1776.41 1695.53 16.62 o -4 1 3 1447.64 1656.66 31.16 o -3 1 3 123.82 102.99 1.51 o -2 1 3 8270.03 8494.55 189.52 o -1 1 3 3513.98 3693.38 32.63 o 0 1 3 2356.46 2479.16 22.92 o 1 1 3 6122.63 6132.02 56.01 o 2 1 3 2161.12 2399.45 18.66 o 3 1 3 142.20 118.30 1.01 o 4 1 3 1249.67 1304.99 10.63 o 5 1 3 107.15 116.87 2.37 o 6 1 3 33.51 46.29 1.25 o 7 1 3 14.27 4.16 0.65 o 8 1 3 299.59 304.91 4.13 o 9 1 3 75.49 65.01 1.74 o 10 1 3 39.24 44.34 1.67 o 11 1 3 534.87 538.87 6.02 o 12 1 3 1.31 0.78 0.83 o 13 1 3 38.15 35.57 1.64 o 14 1 3 40.19 46.24 2.42 o -14 2 3 3.13 1.66 1.37 o -13 2 3 14.29 12.81 1.86 o -12 2 3 0.17 0.57 1.09 o -11 2 3 50.74 49.27 2.13 o -10 2 3 138.16 118.64 3.47 o -9 2 3 860.99 792.75 9.12 o -8 2 3 60.68 43.16 1.68 o -7 2 3 1200.10 1229.82 12.91 o -6 2 3 83.77 95.85 1.97 o -5 2 3 366.86 365.65 3.85 o -4 2 3 144.12 108.03 1.09 o -3 2 3 116.66 157.55 2.13 o -2 2 3 433.20 473.78 5.10 o -1 2 3 767.12 783.34 12.69 o 0 2 3 6.74 2.53 0.32 o 1 2 3 1095.45 1170.46 10.56 o 2 2 3 297.33 333.50 2.61 o 3 2 3 60.60 34.42 0.79 o 4 2 3 1311.32 1346.23 11.58 o 5 2 3 73.96 77.65 1.06 o 6 2 3 514.19 496.37 4.66 o 7 2 3 897.76 858.73 8.52 o 8 2 3 567.29 545.02 5.53 o 9 2 3 845.05 828.39 10.61 o 10 2 3 93.01 89.89 1.79 o 11 2 3 3.41 4.09 0.79 o 12 2 3 0.00 0.01 0.66 o 13 2 3 19.98 20.29 2.30 o 14 2 3 1.14 1.52 0.93 o -13 3 3 44.57 48.52 2.67 o -12 3 3 190.68 196.00 2.86 o -11 3 3 85.68 80.98 1.55 o -10 3 3 146.87 138.42 2.09 o -9 3 3 26.95 30.15 1.22 o -8 3 3 318.02 324.92 3.41 o -7 3 3 0.01 1.44 0.99 o -6 3 3 135.64 132.27 3.37 o -5 3 3 472.51 508.61 6.45 o -4 3 3 32.89 41.63 1.60 o -3 3 3 31.22 38.92 1.41 o -2 3 3 88.81 70.35 1.39 o -1 3 3 1261.33 1397.83 22.52 o 0 3 3 252.41 315.48 4.66 o 1 3 3 364.31 304.29 3.02 o 2 3 3 0.24 0.08 0.38 o 3 3 3 123.83 132.08 1.66 o 4 3 3 31.33 33.51 1.05 o 5 3 3 1252.21 1252.77 13.00 o 6 3 3 147.09 163.43 2.12 o 7 3 3 40.50 33.01 0.89 o 8 3 3 282.59 280.02 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