#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/39/2223910.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2223910_Fobs loop_ _publ_author_name 'Loughrey, Bradley T.' 'Nadin, Kevin' 'Williams, Michael L.' 'Healy, Peter C.' _publ_section_title ; (\h^6^-Benzophenone)(\h^5^-pentamethylcyclopentadienyl)ruthenium(II) tetraphenylborate ; _journal_coeditor_code LH2927 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1486 _journal_volume 65 _journal_year 2009 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 91.250 _cell_angle_gamma 90.000 _cell_length_a 11.6754 _cell_length_b 20.5730 _cell_length_c 15.6245 _exptl_crystal_F_000 1536.00 _reflns_d_resolution_high 0.7696 _[local]_cod_data_source_file lh2927Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' xcalibur' _shelx_refln_list_code 4 _shelx_f_calc_maximum 306.74 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1654.74 2598.76 27.04 o 4 0 0 27755.90 28567.14 435.35 o 6 0 0 4274.80 3983.18 57.36 o 8 0 0 76.16 55.84 27.64 o 10 0 0 1463.97 1632.32 37.96 o 12 0 0 113.62 66.46 39.21 o 14 0 0 210.22 273.45 37.93 o 2 1 0 13486.91 14898.33 162.93 o 3 1 0 14266.21 15557.13 75.28 o 4 1 0 44.82 34.85 11.07 o 5 1 0 606.53 611.11 26.15 o 6 1 0 1256.56 1318.21 45.99 o 7 1 0 6907.06 6862.98 136.58 o 8 1 0 1795.45 1826.09 34.15 o 9 1 0 10.29 11.86 20.07 o 10 1 0 1433.01 1420.58 26.99 o 11 1 0 141.90 100.29 22.49 o 12 1 0 165.74 212.90 25.64 o 13 1 0 1903.59 2135.42 52.36 o 14 1 0 423.75 448.75 35.27 o 15 1 0 0.06 5.85 73.99 o 2 2 0 19516.54 22897.05 192.05 o 3 2 0 955.12 1083.86 22.27 o 4 2 0 602.14 811.56 34.85 o 5 2 0 10405.00 9839.92 67.55 o 6 2 0 28.63 23.51 11.41 o 7 2 0 3090.71 3109.33 89.82 o 8 2 0 81.65 65.90 18.52 o 9 2 0 5193.16 5103.98 100.31 o 10 2 0 499.02 500.82 24.71 o 11 2 0 1537.30 1586.50 40.56 o 12 2 0 1.26 18.60 26.97 o 13 2 0 67.89 95.24 26.55 o 14 2 0 18.79 40.95 36.31 o 15 2 0 345.11 352.67 44.13 o 1 3 0 83.93 281.45 12.33 o 2 3 0 28985.48 30938.71 335.75 o 3 3 0 862.59 878.34 14.85 o 4 3 0 1186.55 1173.34 28.87 o 5 3 0 400.41 469.19 13.77 o 6 3 0 2493.59 2436.36 43.40 o 7 3 0 131.37 130.41 11.96 o 8 3 0 3057.71 3006.54 29.90 o 9 3 0 310.06 283.15 21.78 o 10 3 0 6.00 7.05 27.17 o 11 3 0 280.70 277.69 26.66 o 12 3 0 1893.26 1956.31 49.55 o 13 3 0 107.69 100.33 33.37 o 14 3 0 316.57 369.44 33.00 o 15 3 0 0.37 28.28 47.64 o 0 4 0 94086.84 98491.91 1025.39 o 1 4 0 3799.12 4228.13 50.96 o 2 4 0 858.93 939.14 37.40 o 3 4 0 4393.93 5058.01 19.48 o 4 4 0 11364.43 11788.28 97.15 o 5 4 0 893.27 622.31 28.48 o 6 4 0 3644.80 3609.56 62.14 o 7 4 0 1992.33 2040.61 23.67 o 8 4 0 29.94 62.05 11.99 o 9 4 0 10.92 -3.00 22.05 o 10 4 0 890.69 864.33 31.79 o 11 4 0 291.61 274.80 26.73 o 12 4 0 7.84 35.81 34.80 o 13 4 0 125.19 125.79 29.84 o 14 4 0 75.92 114.00 38.90 o 1 5 0 76.87 81.59 11.73 o 2 5 0 4032.20 4116.92 27.48 o 3 5 0 22751.72 23452.40 89.11 o 4 5 0 277.26 284.88 16.35 o 5 5 0 2236.30 2389.49 34.22 o 6 5 0 191.45 173.19 13.11 o 7 5 0 9890.01 10493.93 44.40 o 8 5 0 452.19 414.86 22.38 o 9 5 0 1220.07 1238.28 34.63 o 10 5 0 758.92 745.00 34.13 o 11 5 0 425.17 473.72 29.48 o 12 5 0 72.30 79.23 28.61 o 13 5 0 1127.47 1226.63 38.21 o 14 5 0 61.09 85.44 39.51 o 0 6 0 244.57 263.77 19.39 o 1 6 0 8400.04 8642.95 84.99 o 2 6 0 367.32 573.85 13.82 o 3 6 0 32.94 26.35 8.13 o 4 6 0 6491.36 5705.55 53.70 o 5 6 0 88.09 147.17 9.67 o 6 6 0 4725.37 4865.72 27.88 o 7 6 0 539.08 458.51 17.48 o 8 6 0 428.14 483.96 15.90 o 9 6 0 769.09 722.82 23.35 o 10 6 0 3760.66 3722.44 88.16 o 11 6 0 107.47 125.03 30.06 o 12 6 0 34.89 24.54 30.15 o 13 6 0 1.04 51.20 36.73 o 14 6 0 228.03 295.19 48.05 o 1 7 0 1973.18 2613.74 70.25 o 2 7 0 18282.95 17724.16 125.78 o 3 7 0 6086.01 5712.69 60.22 o 4 7 0 1567.09 1635.46 30.19 o 5 7 0 113.15 128.59 10.06 o 6 7 0 2205.27 2148.25 18.02 o 7 7 0 551.84 551.40 17.80 o 8 7 0 1584.97 1572.68 20.73 o 9 7 0 299.08 244.63 19.00 o 10 7 0 6.16 37.45 23.48 o 11 7 0 70.80 112.52 29.24 o 12 7 0 1067.52 1119.34 48.26 o 13 7 0 79.91 68.89 35.52 o 14 7 0 195.13 247.63 44.42 o 0 8 0 4780.78 4899.79 55.85 o 1 8 0 6123.68 5832.50 49.58 o 2 8 0 54.31 56.29 14.65 o 3 8 0 610.13 537.31 15.71 o 4 8 0 356.56 396.92 11.44 o 5 8 0 7796.13 7802.25 57.10 o 6 8 0 14.26 5.90 10.15 o 7 8 0 532.16 543.46 12.89 o 8 8 0 324.03 330.49 18.54 o 9 8 0 302.76 344.56 20.46 o 10 8 0 21.90 35.43 28.26 o 11 8 0 1155.46 1119.06 33.82 o 12 8 0 95.61 84.33 46.18 o 13 8 0 20.68 9.10 42.61 o 14 8 0 20.02 28.40 50.84 o 1 9 0 820.80 656.04 18.25 o 2 9 0 9875.62 9632.97 76.44 o 3 9 0 8603.47 8504.45 109.60 o 4 9 0 71.72 113.32 9.51 o 5 9 0 3.41 10.54 10.45 o 6 9 0 1050.67 1122.56 25.85 o 7 9 0 2166.02 2011.86 30.19 o 8 9 0 2864.30 2967.97 43.29 o 9 9 0 440.63 460.30 23.26 o 10 9 0 233.51 239.36 28.47 o 11 9 0 12.57 39.76 29.36 o 12 9 0 771.94 731.87 42.35 o 13 9 0 1063.40 1190.92 65.08 o 14 9 0 5.62 48.88 48.48 o 0 10 0 61.67 263.15 24.29 o 1 10 0 603.48 777.40 24.42 o 2 10 0 201.47 221.78 23.67 o 3 10 0 469.70 527.94 15.21 o 4 10 0 656.44 672.65 27.32 o 5 10 0 3757.64 3921.20 40.44 o 6 10 0 6776.80 6410.34 58.69 o 7 10 0 845.41 803.43 36.68 o 8 10 0 695.30 775.36 37.73 o 9 10 0 27.48 30.25 21.02 o 10 10 0 2400.54 2353.09 58.01 o 11 10 0 227.11 235.18 38.61 o 12 10 0 50.25 66.77 32.65 o 13 10 0 7.77 51.34 52.35 o 14 10 0 297.16 350.43 57.90 o 1 11 0 926.74 731.12 23.54 o 2 11 0 284.85 235.19 14.92 o 3 11 0 4399.40 4315.97 28.19 o 4 11 0 3968.20 3700.98 93.63 o 5 11 0 420.75 335.90 24.98 o 6 11 0 923.04 772.06 41.34 o 7 11 0 1963.72 1957.24 34.79 o 8 11 0 49.41 37.10 23.31 o 9 11 0 1532.31 1451.04 131.13 o 10 11 0 48.90 30.94 31.06 o 11 11 0 583.33 489.69 41.58 o 12 11 0 229.99 234.61 38.29 o 13 11 0 806.54 804.51 48.26 o 0 12 0 5183.95 4996.02 117.47 o 1 12 0 1722.73 1580.36 25.61 o 2 12 0 1297.39 1448.69 35.63 o 3 12 0 985.08 1038.86 19.33 o 4 12 0 2634.27 2702.67 25.13 o 5 12 0 1976.79 1862.31 28.88 o 6 12 0 940.75 904.48 25.48 o 7 12 0 1730.28 1748.93 28.08 o 8 12 0 300.30 321.43 31.52 o 9 12 0 1394.02 1373.40 145.22 o 10 12 0 119.68 98.22 34.33 o 11 12 0 832.48 916.53 43.50 o 12 12 0 2.59 18.68 34.95 o 13 12 0 49.51 87.04 40.27 o 1 13 0 1389.30 1456.18 39.55 o 2 13 0 6950.31 6872.38 35.18 o 3 13 0 2487.75 2447.45 31.48 o 4 13 0 2646.24 2605.30 25.80 o 5 13 0 17.12 28.13 11.40 o 6 13 0 1328.68 1329.89 28.92 o 7 13 0 149.70 113.49 20.89 o 8 13 0 3399.95 3256.58 75.68 o 9 13 0 54.28 40.55 24.20 o 10 13 0 2.82 -6.66 33.13 o 11 13 0 31.01 44.14 45.92 o 12 13 0 348.67 454.15 44.19 o 13 13 0 13.11 50.04 36.92 o 0 14 0 3223.44 2933.57 87.53 o 1 14 0 1777.22 1761.04 22.90 o 2 14 0 168.89 154.93 17.24 o 3 14 0 1024.84 999.86 22.46 o 4 14 0 208.48 206.06 16.86 o 5 14 0 5954.08 5854.33 53.31 o 6 14 0 2966.67 2749.24 36.23 o 7 14 0 56.24 84.00 20.88 o 8 14 0 95.07 107.39 26.53 o 9 14 0 1216.08 1268.52 36.86 o 10 14 0 993.55 990.50 52.48 o 11 14 0 490.52 471.00 39.14 o 12 14 0 51.14 45.64 36.07 o 1 15 0 2852.01 2726.07 67.15 o 2 15 0 198.83 204.83 18.69 o 3 15 0 5466.80 5537.17 53.10 o 4 15 0 1087.54 1052.00 33.10 o 5 15 0 675.99 605.23 26.68 o 6 15 0 19.74 17.75 22.80 o 7 15 0 653.23 705.55 26.70 o 8 15 0 65.77 81.04 27.76 o 9 15 0 686.40 718.42 32.66 o 10 15 0 52.02 56.04 36.54 o 11 15 0 241.96 225.45 45.11 o 12 15 0 0.48 10.37 37.82 o 0 16 0 4339.00 4204.79 157.49 o 1 16 0 1226.52 1253.34 37.44 o 2 16 0 171.20 173.64 19.28 o 3 16 0 1550.66 1481.22 44.23 o 4 16 0 3400.02 3598.91 70.76 o 5 16 0 1793.07 1712.45 32.78 o 6 16 0 580.29 580.56 29.13 o 7 16 0 106.00 91.81 24.99 o 8 16 0 118.99 136.18 29.03 o 9 16 0 345.50 363.33 32.38 o 10 16 0 591.79 677.56 44.52 o 11 16 0 198.59 175.65 39.75 o 12 16 0 71.09 68.18 41.95 o 1 17 0 2.86 21.82 25.78 o 2 17 0 2361.89 2495.34 41.81 o 3 17 0 97.98 140.58 24.54 o 4 17 0 918.75 924.68 37.77 o 5 17 0 54.53 71.28 30.47 o 6 17 0 117.47 142.47 32.05 o 7 17 0 608.70 627.29 33.21 o 8 17 0 928.28 938.29 43.79 o 9 17 0 139.14 137.94 34.24 o 10 17 0 32.03 71.11 46.26 o 11 17 0 241.43 266.22 67.50 o 0 18 0 869.91 803.97 43.08 o 1 18 0 2985.67 3017.47 66.47 o 2 18 0 76.20 99.72 25.07 o 3 18 0 51.51 62.20 24.19 o 4 18 0 138.12 161.75 33.32 o 5 18 0 2631.23 2489.96 46.70 o 6 18 0 230.82 244.56 31.22 o 7 18 0 0.54 17.69 29.02 o 8 18 0 23.82 54.80 32.00 o 9 18 0 659.35 665.59 39.13 o 10 18 0 42.27 52.57 48.65 o 11 18 0 512.68 583.96 56.46 o 1 19 0 457.32 479.01 28.80 o 2 19 0 2065.80 2107.10 43.33 o 3 19 0 316.78 345.78 34.39 o 4 19 0 170.44 158.74 33.23 o 5 19 0 97.08 101.89 32.55 o 6 19 0 33.57 44.48 29.53 o 7 19 0 399.52 437.95 33.81 o 8 19 0 793.10 813.16 43.17 o 9 19 0 479.10 493.29 42.20 o 10 19 0 74.44 102.03 44.17 o 0 20 0 1526.36 1583.92 50.50 o 1 20 0 24.76 67.94 27.76 o 2 20 0 28.93 57.21 34.48 o 3 20 0 87.31 78.11 33.49 o 4 20 0 1477.36 1499.73 55.13 o 5 20 0 163.77 156.45 36.01 o 6 20 0 394.28 361.73 41.73 o 7 20 0 101.57 92.53 32.81 o 8 20 0 52.05 84.81 35.21 o 9 20 0 3.56 46.89 35.22 o 10 20 0 517.00 609.83 68.11 o 1 21 0 553.35 567.03 30.28 o 2 21 0 318.24 307.72 36.23 o 3 21 0 803.69 838.44 40.30 o 4 21 0 53.97 75.45 34.83 o 5 21 0 0.76 29.66 46.18 o 6 21 0 19.14 39.69 36.01 o 7 21 0 1308.03 1264.93 44.26 o 8 21 0 25.59 85.37 41.07 o 9 21 0 393.32 463.73 52.91 o 0 22 0 862.36 831.12 55.90 o 1 22 0 400.54 392.93 35.40 o 2 22 0 117.63 123.19 37.76 o 3 22 0 111.48 120.63 33.93 o 4 22 0 239.13 283.24 37.15 o 5 22 0 964.10 1012.40 43.64 o 6 22 0 12.94 28.16 34.94 o 7 22 0 99.44 106.10 31.56 o 8 22 0 2.91 21.20 35.41 o 1 23 0 0.21 11.60 32.80 o 2 23 0 1833.48 1871.29 51.27 o 3 23 0 6.28 23.15 33.54 o 4 23 0 53.95 56.25 34.43 o 5 23 0 8.14 15.66 45.22 o 6 23 0 335.41 334.60 36.01 o 7 23 0 2.38 33.73 35.93 o 0 24 0 254.69 257.38 62.53 o 1 24 0 171.44 180.52 34.04 o 2 24 0 178.58 213.83 39.20 o 3 24 0 3.65 31.68 43.74 o 4 24 0 234.12 238.97 37.80 o 5 24 0 626.58 696.36 45.25 o 6 24 0 180.80 186.14 39.88 o 1 25 0 482.85 570.70 49.55 o 2 25 0 204.92 241.45 39.97 o 3 25 0 329.32 385.75 42.62 o 4 25 0 1.86 22.86 38.54 o 5 25 0 0.86 19.77 51.37 o 0 26 0 284.65 239.56 65.93 o 1 26 0 9.50 46.77 49.86 o 2 26 0 129.24 121.04 51.51 o 3 26 0 12.58 13.32 40.14 o -15 0 1 1442.33 1429.39 102.30 o -13 0 1 99.62 107.07 52.02 o -11 0 1 1.37 22.22 33.63 o -9 0 1 58.65 54.88 26.29 o -7 0 1 126.44 186.41 28.47 o -5 0 1 16526.99 15795.50 1384.58 o -3 0 1 1833.72 2074.23 17.81 o 3 0 1 17566.74 19967.32 302.34 o 5 0 1 8303.42 8619.88 1269.00 o 7 0 1 9529.16 9825.46 151.84 o 9 0 1 6.24 -2.46 31.92 o 11 0 1 728.36 824.52 36.45 o 13 0 1 6.87 19.71 34.77 o 15 0 1 726.24 600.67 87.18 o -15 1 1 7.42 96.07 76.58 o -14 1 1 0.62 33.16 36.85 o -13 1 1 168.79 166.88 30.96 o -12 1 1 1853.29 1888.68 45.49 o -11 1 1 464.73 459.32 27.48 o -10 1 1 1372.26 1367.59 29.24 o -9 1 1 6.80 4.68 21.10 o -8 1 1 6039.51 6018.31 57.42 o -7 1 1 4230.83 4456.65 41.41 o -6 1 1 6461.20 6271.35 77.06 o -5 1 1 4529.72 4427.55 40.26 o -4 1 1 672.59 449.93 15.50 o -3 1 1 6563.38 6928.74 36.91 o -2 1 1 93211.09 102808.38 610.48 o 2 1 1 10550.48 11407.15 133.72 o 3 1 1 5045.26 4929.95 35.74 o 4 1 1 908.18 907.36 23.69 o 5 1 1 1.20 6.91 6.31 o 6 1 1 363.55 303.54 30.63 o 7 1 1 1014.32 1051.50 32.35 o 8 1 1 3963.79 4130.49 85.25 o 9 1 1 1444.51 1458.81 27.18 o 10 1 1 179.02 183.96 21.39 o 11 1 1 39.36 27.53 22.20 o 12 1 1 395.30 383.22 22.33 o 13 1 1 205.01 214.31 29.03 o 14 1 1 289.05 244.44 39.35 o 15 1 1 55.61 39.20 52.74 o -15 2 1 98.44 100.58 34.98 o -14 2 1 795.27 890.76 56.42 o -13 2 1 38.31 61.95 27.38 o -12 2 1 115.78 117.52 28.79 o -11 2 1 29.64 39.95 23.56 o -10 2 1 305.20 303.52 25.41 o -9 2 1 2998.82 3030.87 35.96 o -8 2 1 2737.78 2364.87 148.52 o -7 2 1 53.85 73.19 16.15 o -6 2 1 1468.19 1395.61 33.34 o -5 2 1 10282.27 10956.54 64.42 o -4 2 1 18030.63 17978.62 150.68 o -3 2 1 3551.56 3479.03 38.78 o -2 2 1 4569.26 5554.53 54.43 o -1 2 1 7044.91 8750.59 117.33 o 1 2 1 1522.30 1289.99 18.73 o 2 2 1 35885.95 39041.79 236.67 o 3 2 1 3779.83 4074.05 70.74 o 4 2 1 16503.09 17043.11 170.28 o 5 2 1 1143.24 1147.53 32.28 o 6 2 1 10104.25 10188.70 144.79 o 7 2 1 334.14 344.12 12.58 o 8 2 1 139.56 176.20 20.01 o 9 2 1 494.38 490.45 22.31 o 10 2 1 574.49 655.99 25.02 o 11 2 1 323.34 311.38 23.49 o 12 2 1 348.56 370.78 22.40 o 13 2 1 0.01 18.07 30.98 o 14 2 1 133.18 104.56 37.48 o 15 2 1 108.74 56.95 81.11 o -15 3 1 1.29 52.42 43.90 o -14 3 1 6.54 33.82 33.97 o -13 3 1 772.30 857.00 43.21 o -12 3 1 368.08 330.73 30.27 o -11 3 1 777.56 779.02 29.29 o -10 3 1 392.32 354.57 25.24 o -9 3 1 656.18 744.43 26.59 o -8 3 1 289.78 297.79 19.41 o -7 3 1 10503.60 10628.70 100.71 o -6 3 1 2274.56 2475.03 81.82 o -5 3 1 1482.20 1475.34 22.01 o -4 3 1 61.57 47.32 10.91 o -3 3 1 7670.85 7972.68 54.35 o -2 3 1 5136.14 5703.62 53.41 o -1 3 1 26769.79 29019.91 308.90 o 0 3 1 7.66 128.79 24.93 o 1 3 1 6090.83 7153.82 32.08 o 2 3 1 5781.87 6372.89 93.89 o 3 3 1 4878.01 4438.94 21.82 o 4 3 1 4709.57 4927.79 86.69 o 5 3 1 2088.61 1866.20 28.57 o 6 3 1 648.63 785.12 19.29 o 7 3 1 1688.36 1607.67 43.53 o 8 3 1 707.29 586.02 16.13 o 9 3 1 4711.13 4776.15 55.32 o 10 3 1 920.14 884.75 26.16 o 11 3 1 108.74 103.23 20.59 o 12 3 1 20.07 19.24 29.64 o 13 3 1 1055.03 1104.16 39.18 o 14 3 1 96.75 82.44 32.83 o 15 3 1 165.02 134.75 55.98 o -14 4 1 513.90 534.81 42.25 o -13 4 1 66.32 59.59 37.21 o -12 4 1 13.03 23.75 25.63 o -11 4 1 180.04 170.55 26.09 o -10 4 1 485.38 480.94 26.27 o -9 4 1 3.20 -1.39 22.47 o -8 4 1 1356.36 1396.48 29.41 o -7 4 1 136.64 99.58 9.05 o -6 4 1 1764.91 1885.50 40.06 o -5 4 1 11052.58 11685.27 31.88 o -4 4 1 23125.72 25113.99 142.74 o -3 4 1 1063.77 1053.83 13.73 o -2 4 1 4878.77 5906.45 28.08 o -1 4 1 11567.67 11760.91 211.68 o 0 4 1 59472.00 66947.82 891.24 o 1 4 1 39569.11 44896.47 216.37 o 2 4 1 5762.38 5685.90 43.22 o 3 4 1 5036.93 5478.90 84.72 o 4 4 1 6541.27 6974.89 30.26 o 5 4 1 3248.04 3155.20 44.06 o 6 4 1 2831.77 2637.74 71.50 o 7 4 1 2917.08 2891.49 37.95 o 8 4 1 4.59 17.62 10.96 o 9 4 1 94.24 65.63 19.26 o 10 4 1 389.45 383.12 21.23 o 11 4 1 1372.75 1413.91 29.21 o 12 4 1 206.29 124.35 35.93 o 13 4 1 39.32 53.65 37.34 o 14 4 1 294.35 337.30 35.27 o -14 5 1 175.17 157.39 34.95 o -13 5 1 165.37 124.59 42.28 o -12 5 1 1990.97 1989.80 47.04 o -11 5 1 252.19 262.87 30.78 o -10 5 1 14.86 14.23 25.04 o -9 5 1 92.82 107.18 20.45 o -8 5 1 3613.86 3539.65 73.02 o -7 5 1 133.45 140.11 10.44 o -6 5 1 9855.39 9633.75 68.48 o -5 5 1 905.40 1026.06 24.32 o -4 5 1 137.02 102.11 9.59 o -3 5 1 10266.38 11338.64 112.28 o -2 5 1 20424.21 22145.54 249.62 o -1 5 1 1441.06 1523.83 31.59 o 0 5 1 2248.86 2404.93 39.52 o 1 5 1 9089.50 9950.29 145.19 o 2 5 1 4743.87 4555.07 59.84 o 3 5 1 5215.85 5069.33 75.42 o 4 5 1 6084.14 5660.16 77.66 o 5 5 1 3.93 50.12 15.48 o 6 5 1 1844.08 1955.37 19.62 o 7 5 1 396.22 419.10 26.73 o 8 5 1 7738.65 7262.67 47.98 o 9 5 1 3.23 18.38 17.43 o 10 5 1 3.93 20.17 21.56 o 11 5 1 847.39 878.71 48.49 o 12 5 1 317.42 315.01 36.81 o 13 5 1 55.30 74.40 36.91 o 14 5 1 982.32 1047.71 52.57 o -14 6 1 324.45 362.51 66.55 o -13 6 1 142.73 234.07 42.53 o -12 6 1 7.90 43.26 35.86 o -11 6 1 1004.84 1030.18 44.59 o -10 6 1 76.56 110.98 21.80 o -9 6 1 9109.10 9492.10 133.76 o -8 6 1 471.63 474.84 16.31 o -7 6 1 13.23 24.26 9.26 o -6 6 1 2650.48 2764.93 71.69 o -5 6 1 19284.63 19693.71 107.42 o -4 6 1 4063.83 4033.95 39.98 o -3 6 1 4819.80 5039.07 88.46 o -2 6 1 137.53 120.57 11.39 o -1 6 1 993.38 1043.92 17.03 o 0 6 1 661.98 537.86 12.12 o 1 6 1 7552.74 7385.24 75.81 o 2 6 1 258.19 358.85 24.99 o 3 6 1 7337.92 7409.53 39.89 o 4 6 1 922.72 1013.50 11.25 o 5 6 1 1879.47 1803.11 35.03 o 6 6 1 5189.64 5618.13 76.57 o 7 6 1 982.57 879.49 32.90 o 8 6 1 178.51 152.01 13.40 o 9 6 1 881.26 755.20 23.34 o 10 6 1 1154.80 1270.65 33.27 o 11 6 1 1143.32 1297.45 43.79 o 12 6 1 58.56 83.11 33.97 o 13 6 1 0.01 69.16 49.47 o 14 6 1 149.72 204.65 34.30 o -14 7 1 0.03 88.70 46.87 o -13 7 1 368.61 417.33 42.27 o -12 7 1 235.32 266.25 52.98 o -11 7 1 1214.18 1304.39 41.85 o -10 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