#------------------------------------------------------------------------------ #$Date: 2009-12-10 09:06:56 +0200 (Thu, 10 Dec 2009) $ #$Revision: 927 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2223965.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2223965_Fobs loop_ _publ_author_name 'Li, Chengjuan' 'Li, Da-Cheng' 'Wang, Da-Qi' _publ_section_title ; Bis[aqua(2,3-naphtho-15-crown-5)sodium] tetrakis(thiocyanato-\kN)cobaltate(II) ; _journal_coeditor_code PK2189 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1314 _journal_volume 65 _journal_year 2009 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 115.255 _cell_angle_gamma 90.000 _cell_length_a 23.0299 _cell_length_b 13.1703 _cell_length_c 17.4686 _exptl_crystal_F_000 2100.00 _reflns_d_resolution_high 0.8406 _[local]_cod_data_source_file pk2189Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 051127b in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 388.56 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 19489.97 18496.74 674.08 o 4 0 0 253.58 372.96 24.33 o 6 0 0 12377.15 13294.83 285.65 o 8 0 0 1779.14 1750.41 82.60 o 10 0 0 2674.43 2338.91 107.17 o 12 0 0 21103.79 22485.13 505.43 o 14 0 0 1222.94 1264.18 99.14 o 16 0 0 1356.60 1419.82 134.98 o 18 0 0 80.41 -4.72 83.34 o 20 0 0 1258.48 1619.34 254.31 o 22 0 0 827.06 1101.30 236.58 o 24 0 0 232.64 88.29 154.04 o 1 1 0 7844.40 7999.19 216.46 o 3 1 0 25539.12 26078.77 469.45 o 5 1 0 8487.22 8647.47 174.90 o 7 1 0 909.52 832.19 39.51 o 9 1 0 1092.43 1130.14 61.07 o 11 1 0 20074.79 20814.78 365.39 o 13 1 0 866.40 822.79 55.16 o 15 1 0 769.74 906.67 77.56 o 17 1 0 391.82 467.89 68.08 o 19 1 0 443.09 618.01 97.74 o 21 1 0 898.18 1444.60 187.82 o 23 1 0 17.07 -1.67 104.12 o 0 2 0 46.26 128.69 32.28 o 2 2 0 14722.09 14361.62 273.45 o 4 2 0 3272.49 3678.21 87.88 o 6 2 0 15149.85 14924.08 290.38 o 8 2 0 21250.24 20641.96 397.68 o 10 2 0 31.35 -27.99 27.99 o 12 2 0 7.09 12.97 32.93 o 14 2 0 11932.14 12261.11 278.66 o 16 2 0 131.94 188.09 70.68 o 18 2 0 2704.55 3167.72 235.31 o 20 2 0 10.99 -36.91 66.82 o 22 2 0 3.64 -2.25 102.50 o 24 2 0 194.77 121.56 121.09 o 1 3 0 20716.41 20441.91 555.02 o 3 3 0 67019.57 66581.15 1205.07 o 5 3 0 2272.52 1909.13 54.31 o 7 3 0 13651.44 13034.00 233.01 o 9 3 0 2827.21 2750.72 87.59 o 11 3 0 7.86 -14.23 29.93 o 13 3 0 936.48 1001.41 92.88 o 15 3 0 9849.73 10151.20 246.57 o 17 3 0 888.46 901.08 258.11 o 19 3 0 808.90 852.71 152.64 o 21 3 0 52.98 -25.66 93.53 o 23 3 0 37.37 30.84 112.62 o 0 4 0 8908.12 7640.34 340.44 o 2 4 0 5981.76 5735.40 290.39 o 4 4 0 23711.19 22861.18 441.19 o 6 4 0 10009.46 9788.47 211.17 o 8 4 0 4888.90 4693.36 105.41 o 10 4 0 111.20 69.59 35.49 o 12 4 0 3606.04 3441.17 112.86 o 14 4 0 4074.07 3748.48 142.49 o 16 4 0 386.10 287.33 75.68 o 18 4 0 122.18 205.83 93.86 o 20 4 0 169.38 188.02 233.49 o 22 4 0 545.13 634.29 148.81 o 1 5 0 1379.08 1159.11 73.86 o 3 5 0 4529.97 4095.09 186.96 o 5 5 0 5.58 -6.95 24.54 o 7 5 0 1178.07 980.94 96.56 o 9 5 0 6595.58 6442.49 140.47 o 11 5 0 5208.24 5235.50 161.80 o 13 5 0 5051.58 4911.03 147.74 o 15 5 0 1678.73 1852.49 178.44 o 17 5 0 957.74 1117.19 149.19 o 19 5 0 245.89 219.72 103.56 o 21 5 0 565.61 812.40 159.16 o 23 5 0 601.94 818.73 172.08 o 0 6 0 6994.15 6466.89 326.78 o 2 6 0 578.27 530.70 73.69 o 4 6 0 504.24 573.14 62.89 o 6 6 0 471.88 347.52 95.92 o 8 6 0 935.23 1043.63 106.63 o 10 6 0 894.48 1013.87 103.57 o 12 6 0 6347.99 5976.12 299.40 o 14 6 0 484.97 527.27 92.19 o 16 6 0 3706.79 3518.34 166.34 o 18 6 0 915.19 788.03 142.38 o 20 6 0 17.93 -9.76 155.74 o 22 6 0 360.34 528.08 149.57 o 1 7 0 201.12 139.37 77.83 o 3 7 0 466.99 561.37 84.68 o 5 7 0 20683.19 21252.35 508.63 o 7 7 0 191.98 107.61 48.67 o 9 7 0 1264.51 1321.34 109.86 o 11 7 0 615.30 1009.62 168.13 o 13 7 0 35.18 17.37 60.15 o 15 7 0 744.59 723.79 107.16 o 17 7 0 551.90 512.64 99.45 o 19 7 0 96.96 9.83 76.45 o 21 7 0 314.73 262.52 121.03 o 0 8 0 1165.53 1152.80 169.09 o 2 8 0 3008.18 2979.30 153.46 o 4 8 0 1678.55 1828.92 112.84 o 6 8 0 92.11 93.80 51.63 o 8 8 0 4888.98 4945.45 174.98 o 10 8 0 522.06 440.74 106.41 o 12 8 0 319.99 280.79 77.77 o 14 8 0 176.08 60.14 73.25 o 16 8 0 1179.23 1432.37 162.79 o 18 8 0 36.94 -18.05 77.70 o 20 8 0 701.30 1005.76 207.40 o 1 9 0 85.54 -36.03 61.91 o 3 9 0 7036.57 6956.18 277.00 o 5 9 0 200.26 223.56 64.94 o 7 9 0 646.18 1000.78 102.06 o 9 9 0 3325.95 2972.24 212.47 o 11 9 0 1312.60 1594.48 181.94 o 13 9 0 351.08 324.41 91.41 o 15 9 0 0.88 -71.40 71.40 o 17 9 0 17.08 -30.74 73.73 o 19 9 0 151.54 188.14 94.51 o 0 10 0 170.65 329.60 138.41 o 2 10 0 1691.00 2406.53 352.59 o 4 10 0 15.78 -50.24 50.24 o 6 10 0 471.07 501.68 87.77 o 8 10 0 1.25 -7.72 77.45 o 10 10 0 860.59 918.14 148.11 o 12 10 0 597.29 516.98 129.44 o 14 10 0 110.33 172.71 120.46 o 16 10 0 0.94 -55.15 77.97 o 18 10 0 1.62 -84.46 84.58 o 1 11 0 3370.46 3138.90 188.21 o 3 11 0 4813.30 4208.69 328.99 o 5 11 0 2259.75 2445.87 153.52 o 7 11 0 29.37 -20.25 87.65 o 9 11 0 491.10 276.03 114.64 o 11 11 0 85.98 61.67 101.32 o 13 11 0 106.76 0.64 101.00 o 15 11 0 125.31 -3.07 106.10 o 17 11 0 38.75 -32.39 119.86 o 0 12 0 54.55 0.15 125.44 o 2 12 0 247.19 209.55 99.44 o 4 12 0 550.84 534.93 162.19 o 6 12 0 189.58 148.96 103.40 o 8 12 0 8.16 -78.76 88.58 o 10 12 0 2.83 -15.74 105.45 o 12 12 0 151.33 65.10 122.05 o 14 12 0 37.05 -113.55 113.55 o 1 13 0 0.58 -27.75 82.49 o 3 13 0 201.08 89.67 86.57 o 5 13 0 3.22 -15.81 104.76 o 7 13 0 2.03 -131.35 131.35 o 9 13 0 20.34 35.32 117.08 o 11 13 0 0.20 -35.25 116.67 o 13 13 0 0.21 -113.56 163.78 o 0 14 0 65.93 178.66 161.70 o 2 14 0 35.49 -92.86 92.86 o 4 14 0 43.98 52.96 89.76 o 6 14 0 9.45 89.22 107.34 o 8 14 0 2.69 14.72 122.08 o 10 14 0 66.06 41.80 130.14 o 1 15 0 4.85 -41.09 104.97 o 3 15 0 4.48 -45.93 94.85 o 5 15 0 29.95 27.33 129.44 o 7 15 0 6.06 -120.99 120.99 o -25 1 1 12.22 18.27 112.98 o -23 1 1 71.65 0.58 101.68 o -21 1 1 465.60 565.76 101.55 o -19 1 1 386.20 346.21 70.62 o -17 1 1 120.42 106.80 56.05 o -15 1 1 122.75 77.00 38.58 o -13 1 1 25.18 -25.78 25.78 o -11 1 1 685.54 704.43 39.88 o -9 1 1 4895.99 4987.59 105.37 o -7 1 1 1136.26 1122.01 77.88 o -5 1 1 5951.99 5940.66 125.84 o -3 1 1 455.55 414.07 21.81 o -1 1 1 8399.85 8592.52 225.39 o 1 1 1 41934.57 42512.79 767.15 o 3 1 1 19135.70 21022.71 391.75 o 5 1 1 1855.27 1821.04 47.82 o 7 1 1 717.55 612.06 33.18 o 9 1 1 3.91 -7.29 17.42 o 11 1 1 12807.00 13440.17 201.65 o 13 1 1 9992.54 10441.34 248.35 o 15 1 1 333.49 361.59 71.48 o 17 1 1 1097.00 1123.29 115.49 o 19 1 1 686.54 810.45 138.76 o 21 1 1 393.26 452.75 137.45 o 23 1 1 0.03 74.16 103.72 o -24 2 1 137.32 155.86 111.79 o -22 2 1 1174.85 1435.70 198.83 o -20 2 1 62.15 -5.69 68.84 o -18 2 1 660.37 806.42 102.78 o -16 2 1 980.95 1345.20 94.77 o -14 2 1 21.59 51.30 41.35 o -12 2 1 89.90 -2.67 35.17 o -10 2 1 2198.99 1909.26 72.50 o -8 2 1 621.60 768.84 52.68 o -6 2 1 2619.32 2592.47 73.15 o -4 2 1 1396.98 1441.91 46.60 o -2 2 1 8997.15 9199.55 200.29 o 0 2 1 2509.08 2549.21 70.32 o 2 2 1 24987.17 25841.89 548.89 o 4 2 1 21558.75 22124.61 357.31 o 6 2 1 3.06 -12.35 13.91 o 8 2 1 1344.45 1383.58 41.74 o 10 2 1 77.99 106.17 26.60 o 12 2 1 9.99 28.13 21.87 o 14 2 1 193.12 192.44 50.40 o 16 2 1 1390.76 1716.77 173.33 o 18 2 1 154.21 142.66 135.91 o 20 2 1 529.63 498.21 130.33 o 22 2 1 14.86 52.82 102.92 o -23 3 1 1.13 -45.45 104.90 o -21 3 1 93.15 62.98 93.90 o -19 3 1 163.42 106.42 205.04 o -17 3 1 205.59 217.27 62.80 o -15 3 1 888.04 1077.66 84.72 o -13 3 1 36.76 24.33 37.68 o -11 3 1 135.99 149.57 40.02 o -9 3 1 9715.55 9846.66 227.61 o -7 3 1 391.88 320.21 36.13 o -5 3 1 45767.83 45222.16 731.17 o -3 3 1 3953.67 4039.71 137.72 o -1 3 1 12252.42 11761.17 260.76 o 1 3 1 6377.13 6759.25 164.72 o 3 3 1 12951.53 12900.74 225.76 o 5 3 1 31431.38 33670.42 495.87 o 7 3 1 7962.17 8495.01 146.88 o 9 3 1 3564.92 3207.24 80.68 o 11 3 1 2120.94 2021.65 82.76 o 13 3 1 7700.18 7163.10 308.41 o 15 3 1 49.08 -49.13 49.13 o 17 3 1 1999.63 2459.61 215.56 o 19 3 1 4.47 -82.64 82.64 o 21 3 1 228.04 269.96 125.57 o 23 3 1 8.16 -25.34 112.65 o -24 4 1 732.55 898.32 168.03 o -22 4 1 19.95 -99.64 99.64 o -20 4 1 114.30 24.47 85.14 o -18 4 1 293.34 370.61 103.97 o -16 4 1 166.04 51.34 54.01 o -14 4 1 400.85 305.49 75.96 o -12 4 1 334.11 361.42 52.59 o -10 4 1 3940.13 3501.12 139.91 o -8 4 1 15911.91 15920.74 284.23 o -6 4 1 302.02 265.16 29.26 o -4 4 1 7.14 20.47 25.02 o -2 4 1 15827.29 15211.52 434.93 o 0 4 1 684.80 778.79 78.80 o 2 4 1 19839.94 19858.19 449.33 o 4 4 1 5468.59 5435.92 131.74 o 6 4 1 15774.82 16538.59 336.20 o 8 4 1 1569.04 1351.08 74.97 o 10 4 1 17752.47 17599.18 317.32 o 12 4 1 2349.31 2294.61 91.93 o 14 4 1 52.62 -48.51 48.51 o 16 4 1 151.20 91.07 69.95 o 18 4 1 185.56 309.90 105.24 o 20 4 1 104.22 141.35 105.29 o 22 4 1 99.39 93.51 114.80 o -23 5 1 119.79 111.99 127.55 o -21 5 1 11.98 12.64 99.45 o -19 5 1 1761.30 1967.21 196.39 o -17 5 1 3083.59 2832.66 163.40 o -15 5 1 1.09 -34.92 45.70 o -13 5 1 7.59 -18.00 43.50 o -11 5 1 7511.43 7608.31 190.06 o -9 5 1 2511.78 2453.34 73.23 o -7 5 1 36527.86 37410.93 811.63 o -5 5 1 1211.09 1323.63 114.31 o -3 5 1 1431.15 1616.16 87.93 o -1 5 1 1060.28 1212.06 100.76 o 1 5 1 108.36 70.79 37.32 o 3 5 1 2167.35 2176.00 87.38 o 5 5 1 9704.26 9596.35 215.58 o 7 5 1 3150.76 3268.40 100.54 o 9 5 1 381.57 452.97 48.52 o 11 5 1 4936.61 4668.09 199.21 o 13 5 1 192.92 165.56 64.07 o 15 5 1 299.65 127.57 71.53 o 17 5 1 898.78 804.76 155.04 o 19 5 1 41.04 -51.07 102.09 o 21 5 1 219.26 307.62 129.67 o -22 6 1 537.26 579.25 144.06 o -20 6 1 38.10 -15.43 98.30 o -18 6 1 200.27 139.02 84.75 o -16 6 1 1146.12 1415.55 149.46 o -14 6 1 4.38 -35.79 46.52 o -12 6 1 18.19 49.04 44.51 o -10 6 1 11838.90 11728.07 320.39 o -8 6 1 5391.08 5245.62 141.85 o -6 6 1 5517.61 5746.43 174.69 o -4 6 1 9418.95 9913.21 320.64 o -2 6 1 3634.30 3387.82 175.42 o 0 6 1 8114.88 7573.01 261.54 o 2 6 1 16.21 12.85 39.50 o 4 6 1 622.86 700.95 79.18 o 6 6 1 965.48 903.73 115.64 o 8 6 1 1217.52 1395.18 75.65 o 10 6 1 26.04 -24.43 41.06 o 12 6 1 1482.06 1671.67 200.62 o 14 6 1 1755.40 2059.04 151.19 o 16 6 1 2434.80 2914.66 186.90 o 18 6 1 165.18 103.60 76.19 o 20 6 1 27.89 120.36 113.07 o 22 6 1 20.75 22.05 118.15 o -21 7 1 910.96 1044.00 175.05 o -19 7 1 168.38 52.04 84.42 o -17 7 1 474.41 474.59 120.68 o -15 7 1 891.24 931.72 113.34 o -13 7 1 474.15 222.32 77.28 o -11 7 1 1900.25 2205.47 145.15 o -9 7 1 9017.29 8685.27 215.36 o -7 7 1 19.04 -37.60 37.60 o -5 7 1 3422.95 3102.39 122.32 o -3 7 1 103.49 69.53 50.75 o -1 7 1 116.13 133.09 60.36 o 1 7 1 272.24 152.39 60.69 o 3 7 1 13812.09 13969.77 356.65 o 5 7 1 5476.05 5313.31 174.41 o 7 7 1 5407.70 5075.16 169.01 o 9 7 1 27.54 22.02 53.02 o 11 7 1 145.28 37.12 57.17 o 13 7 1 1044.68 1052.31 136.63 o 15 7 1 281.47 142.91 79.90 o 17 7 1 567.24 544.80 105.58 o 19 7 1 39.26 87.84 110.87 o 21 7 1 60.43 -101.30 101.30 o -20 8 1 5.81 -78.34 78.34 o -18 8 1 451.62 312.69 115.53 o -16 8 1 568.94 410.60 95.43 o -14 8 1 2969.34 3032.78 152.90 o -12 8 1 554.00 542.09 92.03 o -10 8 1 455.12 288.01 95.45 o -8 8 1 3376.96 3159.80 136.45 o -6 8 1 167.05 149.13 55.35 o -4 8 1 1116.07 1271.16 122.47 o -2 8 1 5827.99 5633.83 238.27 o 0 8 1 298.63 236.06 83.43 o 2 8 1 535.94 592.19 91.41 o 4 8 1 2316.61 2217.11 107.47 o 6 8 1 13.11 85.77 53.71 o 8 8 1 9417.72 9134.37 355.91 o 10 8 1 234.82 205.69 68.79 o 12 8 1 9.26 7.61 60.52 o 14 8 1 1802.78 2392.34 169.98 o 16 8 1 286.00 144.69 105.12 o 18 8 1 585.81 626.57 112.56 o 20 8 1 212.70 189.60 124.13 o -19 9 1 371.62 278.47 122.38 o -17 9 1 592.08 697.20 149.70 o -15 9 1 339.98 509.68 122.84 o -13 9 1 1382.78 1753.59 209.13 o -11 9 1 649.12 892.89 141.38 o -9 9 1 1302.77 1549.46 167.76 o -7 9 1 1800.42 2403.27 149.61 o -5 9 1 624.39 647.76 85.47 o -3 9 1 1077.82 1193.36 245.96 o -1 9 1 3653.39 3614.24 245.59 o 1 9 1 426.00 487.10 97.12 o 3 9 1 101.65 123.92 59.63 o 5 9 1 918.74 994.61 104.43 o 7 9 1 642.93 684.12 107.04 o 9 9 1 9.23 42.03 78.60 o 11 9 1 687.31 618.84 208.22 o 13 9 1 22.70 -29.76 66.83 o 15 9 1 412.49 426.11 111.03 o 17 9 1 629.21 579.29 148.46 o 19 9 1 236.68 198.41 105.59 o -18 10 1 254.29 279.56 102.25 o -16 10 1 87.74 163.99 122.70 o -14 10 1 307.18 82.08 215.06 o -12 10 1 752.01 683.19 140.00 o -10 10 1 243.00 372.38 115.58 o -8 10 1 499.58 526.34 152.71 o -6 10 1 1208.57 1916.03 208.89 o -4 10 1 73.08 34.32 87.49 o -2 10 1 379.12 489.68 102.64 o 0 10 1 3405.71 2895.34 169.12 o 2 10 1 718.25 679.99 120.96 o 4 10 1 42.66 -1.91 59.55 o 6 10 1 487.97 517.21 111.24 o 8 10 1 344.50 290.76 104.73 o 10 10 1 2983.47 3119.53 242.62 o 12 10 1 897.02 734.88 148.42 o 14 10 1 45.59 -0.64 97.89 o 16 10 1 410.75 245.19 99.92 o 18 10 1 3.08 -37.58 89.02 o -17 11 1 111.39 163.85 138.38 o -15 11 1 8.39 -26.78 103.99 o -13 11 1 704.69 985.84 175.96 o -11 11 1 220.20 33.06 106.42 o -9 11 1 5.54 -15.56 109.74 o -7 11 1 345.71 459.67 119.18 o -5 11 1 1507.04 2225.61 211.94 o -3 11 1 535.06 714.18 136.23 o -1 11 1 21.72 -19.14 75.71 o 1 11 1 2039.48 2339.53 207.78 o 3 11 1 794.20 809.61 123.27 o 5 11 1 298.37 479.73 92.56 o 7 11 1 45.05 91.95 91.12 o 9 11 1 510.92 371.38 174.16 o 11 11 1 590.98 747.59 149.49 o 13 11 1 220.91 105.26 137.38 o 15 11 1 195.31 34.85 121.66 o 17 11 1 2.48 5.30 125.49 o -16 12 1 253.69 137.55 170.77 o -14 12 1 316.86 39.54 114.58 o -12 12 1 68.10 -77.39 105.37 o -10 12 1 212.35 172.88 132.59 o -8 12 1 87.46 143.67 104.88 o -6 12 1 62.25 111.44 91.72 o -4 12 1 1171.27 1617.08 344.67 o -2 12 1 424.80 560.53 267.92 o 0 12 1 1961.85 2407.96 217.09 o 2 12 1 6.45 33.67 87.89 o 4 12 1 1276.28 1512.47 178.15 o 6 12 1 135.51 38.81 92.25 o 8 12 1 1909.45 1976.90 249.53 o 10 12 1 309.49 120.35 208.88 o 12 12 1 650.56 812.84 168.99 o 14 12 1 329.01 152.80 134.41 o -13 13 1 7.17 -91.95 114.97 o -11 13 1 315.61 350.66 151.61 o -9 13 1 81.03 -26.05 104.98 o -7 13 1 194.65 220.46 128.71 o -5 13 1 1952.89 2815.26 205.82 o -3 13 1 60.99 -67.81 88.99 o -1 13 1 0.85 -37.57 87.86 o 1 13 1 1224.30 1793.19 235.51 o 3 13 1 17.39 0.78 79.30 o 5 13 1 324.92 476.46 142.10 o 7 13 1 282.63 491.75 140.79 o 9 13 1 266.94 12.40 116.27 o 11 13 1 5.23 -68.44 118.28 o 13 13 1 142.94 293.80 150.01 o -10 14 1 34.39 -31.24 117.57 o -8 14 1 51.05 194.14 131.45 o -6 14 1 142.83 14.77 119.72 o -4 14 1 143.39 135.20 95.15 o -2 14 1 660.91 785.65 158.72 o 0 14 1 20.89 -110.47 113.14 o 2 14 1 8.95 -11.28 84.48 o 4 14 1 257.18 114.34 132.25 o 6 14 1 72.52 -96.44 109.41 o 8 14 1 122.11 191.96 138.27 o 10 14 1 20.94 -115.56 115.83 o -7 15 1 132.34 75.06 137.40 o -5 15 1 49.67 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