#------------------------------------------------------------------------------
#$Date: 2009-12-10 09:06:56 +0200 (Thu, 10 Dec 2009) $
#$Revision: 927 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/2223997.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2223997_Fobs
loop_
_publ_author_name
'Wen, Liyuan'
'Yin, Handong'
'Wang, Chuanhua'
_publ_section_title
;
 Bis(2-amino-4-chlorobenzoato)triphenylantimony(V)
;
_journal_coeditor_code           RZ2373
_journal_issue                   11
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              m1442
_journal_volume                  65
_journal_year                    2009
_space_group_IT_number           43
_symmetry_space_group_name_Hall  'F 2 -2d'
_symmetry_space_group_name_H-M   'F d d 2'
_cell_angle_alpha                90.000
_cell_angle_beta                 90.000
_cell_angle_gamma                90.000
_cell_length_a                   13.0168
_cell_length_b                   20.2982
_cell_length_c                   21.8494
_exptl_crystal_F_000             2784.00
_reflns_d_resolution_high        0.8404
_[local]_cod_data_source_file    rz2373Isup2.hkl
_[local]_cod_data_source_block   I
#BEGIN Tags that were not found in dictionaries:
_shelx_title                     ' 081202g in Fdd2'
_shelx_refln_list_code           4
_shelx_f_calc_maximum            885.39
_shelx_f_squared_multiplier      1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, z'
'x+1/4, -y+1/4, z+1/4'
'-x+1/4, y+1/4, z+1/4'
'x, y+1/2, z+1/2'
'-x, -y+1/2, z+1/2'
'x+1/4, -y+3/4, z+3/4'
'-x+1/4, y+3/4, z+3/4'
'x+1/2, y, z+1/2'
'-x+1/2, -y, z+1/2'
'x+3/4, -y+1/4, z+3/4'
'-x+3/4, y+1/4, z+3/4'
'x+1/2, y+1/2, z'
'-x+1/2, -y+1/2, z'
'x+3/4, -y+3/4, z+1/4'
'-x+3/4, y+3/4, z+1/4'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
3 1 -25 1708.01 1561.35 552.64 o
1 3 -25 1651.82 2072.42 352.91 o
3 3 -25 1986.18 2092.83 261.39 o
4 0 -24 5818.19 6516.85 521.11 o
2 2 -24 4668.03 4758.72 306.29 o
4 2 -24 2.61 -198.29 132.19 o
2 4 -24 53.45 96.11 198.23 o
4 4 -24 4379.59 4588.06 321.59 o
4 6 -24 97.86 -47.43 156.81 o
1 1 -23 5576.38 5894.31 322.66 o
3 1 -23 3226.01 2574.92 261.63 o
5 1 -23 3074.72 2919.03 466.67 o
7 1 -23 2999.71 3132.90 325.73 o
1 3 -23 6174.14 5710.41 449.02 o
3 3 -23 2546.22 2564.88 269.90 o
5 3 -23 3279.98 3740.48 298.91 o
1 5 -23 3113.39 2115.22 330.39 o
3 5 -23 2701.39 3238.44 281.09 o
5 5 -23 3805.25 3553.10 308.90 o
3 7 -23 2910.23 3305.48 314.77 o
5 7 -23 2652.26 2396.04 420.49 o
2 0 -22 9871.94 9075.83 542.13 o
6 0 -22 10133.41 9545.88 626.23 o
0 2 -22 24618.52 22780.82 865.01 o
2 2 -22 13.29 -98.35 115.62 o
4 2 -22 6310.28 7104.07 364.12 o
6 2 -22 90.43 -195.11 130.07 o
8 2 -22 5753.95 6636.99 560.15 o
2 4 -22 8465.29 8422.56 375.27 o
4 4 -22 305.84 71.60 145.13 o
6 4 -22 8363.12 9112.43 441.63 o
2 6 -22 1179.89 1116.11 209.69 o
4 6 -22 6429.44 6330.42 353.97 o
6 6 -22 90.49 -52.00 157.31 o
4 8 -22 98.94 -19.97 150.26 o
6 8 -22 3284.51 4144.43 479.43 o
4 10 -22 5952.71 5737.44 494.83 o
1 1 -21 9559.79 8931.61 363.70 o
3 1 -21 3782.54 2895.97 231.63 o
5 1 -21 5470.84 5876.35 341.07 o
7 1 -21 3973.70 4078.31 305.81 o
9 1 -21 1713.85 1289.68 253.80 o
1 3 -21 7297.85 7139.49 331.92 o
3 3 -21 4643.41 4547.41 299.97 o
5 3 -21 4787.82 4686.38 308.09 o
7 3 -21 3742.67 3399.02 301.04 o
1 5 -21 5549.22 4794.30 282.16 o
3 5 -21 3225.03 3326.68 255.92 o
5 5 -21 4715.79 4575.67 328.13 o
7 5 -21 3380.25 3328.07 316.39 o
3 7 -21 1960.07 1885.60 236.91 o
5 7 -21 3132.59 2746.81 356.67 o
7 7 -21 3938.50 3986.80 313.25 o
3 9 -21 3149.05 3366.93 385.95 o
5 9 -21 2362.93 2207.00 278.21 o
7 9 -21 2670.42 3332.90 339.66 o
3 11 -21 4072.93 4365.59 424.24 o
5 11 -21 2388.30 2622.06 418.99 o
0 0 -20 37862.26 35936.91 1102.29 o
4 0 -20 6602.08 7594.36 503.84 o
8 0 -20 5214.77 5464.12 487.32 o
2 2 -20 6831.91 6843.63 320.96 o
4 2 -20 584.82 158.55 140.69 o
6 2 -20 19219.66 18159.00 596.25 o
8 2 -20 25.76 -102.93 144.42 o
0 4 -20 21969.56 24197.25 1122.18 o
2 4 -20 360.04 149.37 124.63 o
4 4 -20 8729.08 8180.98 377.24 o
6 4 -20 47.82 -188.14 125.43 o
8 4 -20 6205.88 6430.91 378.03 o
2 6 -20 12663.24 13102.34 459.27 o
4 6 -20 96.26 53.48 136.74 o
6 6 -20 8498.89 8637.03 441.89 o
8 6 -20 186.84 3.28 142.53 o
2 8 -20 1045.02 530.12 241.03 o
4 8 -20 11638.15 12420.15 589.06 o
6 8 -20 242.42 0.35 131.86 o
8 8 -20 4371.12 4077.03 314.03 o
2 10 -20 10272.20 10693.22 604.45 o
4 10 -20 814.11 387.45 233.52 o
6 10 -20 2994.42 3034.34 477.56 o
4 12 -20 5924.39 5005.34 464.04 o
6 12 -20 148.17 28.53 201.23 o
4 14 -20 30.11 -187.72 204.24 o
1 1 -19 14640.17 14590.52 308.75 o
3 1 -19 6803.15 5929.69 301.49 o
5 1 -19 6763.28 6382.04 343.99 o
7 1 -19 8407.29 8953.89 417.94 o
9 1 -19 4170.82 3742.78 298.87 o
1 3 -19 3902.43 3414.17 187.62 o
3 3 -19 6010.26 5856.02 305.79 o
5 3 -19 17787.24 17502.17 560.57 o
7 3 -19 8734.39 7676.38 392.62 o
9 3 -19 1738.67 1639.84 261.88 o
1 5 -19 13808.13 14006.40 571.04 o
3 5 -19 4551.78 4629.31 278.47 o
5 5 -19 5658.77 5658.22 491.45 o
7 5 -19 4347.48 4135.24 299.37 o
9 5 -19 2871.48 3459.80 304.58 o
1 7 -19 4694.12 4915.23 384.45 o
3 7 -19 6059.43 5932.37 318.30 o
5 7 -19 7968.93 7163.58 586.43 o
7 7 -19 6945.27 6190.77 362.31 o
9 7 -19 1784.98 1951.21 266.84 o
1 9 -19 6174.59 6582.93 447.52 o
3 9 -19 5812.40 5736.69 444.52 o
5 9 -19 5493.63 5582.27 334.37 o
7 9 -19 3472.58 4079.19 339.40 o
3 11 -19 4392.53 4531.53 425.00 o
5 11 -19 5354.72 4851.41 449.77 o
7 11 -19 2689.56 2307.44 401.72 o
3 13 -19 5053.23 5682.63 473.05 o
5 13 -19 3334.39 3639.49 471.55 o
3 15 -19 3773.01 3848.99 411.48 o
2 0 -18 10461.69 10499.89 349.13 o
6 0 -18 19411.49 16554.55 766.64 o
10 0 -18 9116.09 9334.13 629.23 o
0 2 -18 36149.34 35859.43 1049.35 o
2 2 -18 1658.42 1637.58 184.48 o
4 2 -18 22769.62 22820.46 619.97 o
6 2 -18 1133.95 790.95 207.62 o
8 2 -18 9836.63 10479.69 450.32 o
10 2 -18 0.66 -168.12 137.26 o
2 4 -18 19861.81 18967.07 531.74 o
4 4 -18 424.65 166.75 132.42 o
6 4 -18 25273.59 26231.60 710.87 o
8 4 -18 260.56 130.60 147.22 o
10 4 -18 2678.77 2510.09 351.03 o
0 6 -18 29401.18 30829.45 960.37 o
2 6 -18 1789.40 1893.04 204.70 o
4 6 -18 17473.48 16602.78 529.25 o
6 6 -18 246.91 -4.06 138.18 o
8 6 -18 8416.35 8637.32 684.42 o
10 6 -18 46.88 35.62 153.62 o
2 8 -18 15981.30 17409.80 734.36 o
4 8 -18 1418.09 1198.33 203.88 o
6 8 -18 11342.00 10775.08 447.86 o
8 8 -18 854.04 905.61 209.61 o
2 10 -18 1420.90 1027.20 259.80 o
4 10 -18 11981.72 12454.77 667.53 o
6 10 -18 87.05 -167.39 122.64 o
8 10 -18 7070.58 7039.31 396.24 o
2 12 -18 7856.71 8924.16 543.63 o
4 12 -18 985.08 859.75 270.32 o
6 12 -18 5702.21 6187.21 506.09 o
8 12 -18 86.20 303.35 256.05 o
2 14 -18 190.00 185.47 206.49 o
4 14 -18 6272.17 5639.83 481.31 o
6 14 -18 80.83 373.94 244.03 o
4 16 -18 56.29 -159.94 186.97 o
1 1 -17 13596.35 13221.28 275.23 o
3 1 -17 5045.94 4748.47 254.05 o
5 1 -17 14791.19 14769.12 487.10 o
7 1 -17 13030.83 12898.90 478.81 o
9 1 -17 3964.87 3451.54 290.28 o
11 1 -17 3929.31 3593.90 331.69 o
1 3 -17 19565.91 20305.02 358.44 o
3 3 -17 11482.06 10894.24 386.40 o
5 3 -17 4970.40 4585.79 277.53 o
7 3 -17 3180.63 3089.66 252.69 o
9 3 -17 3606.13 3879.87 287.11 o
11 3 -17 3023.30 3414.79 309.12 o
1 5 -17 1605.79 1647.46 142.27 o
3 5 -17 12572.25 12200.59 421.31 o
5 5 -17 9960.97 9004.33 377.76 o
7 5 -17 4436.92 4125.04 279.54 o
9 5 -17 3918.77 3996.57 292.66 o
11 5 -17 2330.22 2717.99 295.67 o
1 7 -17 18844.01 19502.49 732.85 o
3 7 -17 9879.34 9802.13 383.03 o
5 7 -17 2903.57 3114.52 242.05 o
7 7 -17 1275.09 1049.76 194.00 o
9 7 -17 3088.86 2921.24 219.75 o
1 9 -17 4845.68 5099.95 376.19 o
3 9 -17 4748.05 4262.72 373.19 o
5 9 -17 5960.95 5816.02 321.93 o
7 9 -17 6969.42 7307.28 377.76 o
9 9 -17 4101.77 3923.83 265.53 o
1 11 -17 4964.42 5199.81 392.71 o
3 11 -17 6749.02 6797.68 480.56 o
5 11 -17 3970.60 3904.55 399.47 o
7 11 -17 4402.96 4626.90 455.78 o
9 11 -17 2725.22 3154.44 321.97 o
1 13 -17 5901.28 6980.14 471.55 o
3 13 -17 5215.94 5239.61 435.51 o
5 13 -17 2312.61 1977.06 352.16 o
7 13 -17 1322.49 931.84 292.09 o
3 15 -17 1769.33 1364.34 298.85 o
5 15 -17 2145.60 2519.94 399.47 o
3 17 -17 1720.19 1554.31 346.90 o
0 0 -16 19208.35 17630.56 630.74 o
4 0 -16 11738.58 11926.91 573.67 o
8 0 -16 15430.52 14617.29 722.34 o
12 0 -16 7753.42 8421.07 607.46 o
2 2 -16 23397.06 23459.79 445.56 o
4 2 -16 1229.13 1026.05 165.53 o
6 2 -16 6088.15 6184.45 314.69 o
8 2 -16 242.97 137.11 136.40 o
10 2 -16 11567.77 11372.90 474.67 o
12 2 -16 56.10 -190.37 136.46 o
0 4 -16 49520.05 52381.05 967.67 o
2 4 -16 3358.10 3090.24 156.00 o
4 4 -16 12778.04 12414.96 418.61 o
6 4 -16 56.53 -87.77 103.74 o
8 4 -16 9402.09 10209.37 326.63 o
10 4 -16 200.30 -122.73 120.25 o
2 6 -16 30976.05 32483.58 727.59 o
4 6 -16 809.34 858.29 152.37 o
6 6 -16 8478.50 7928.55 360.93 o
8 6 -16 82.57 -28.20 86.83 o
10 6 -16 5873.36 5813.25 287.94 o
0 8 -16 21547.79 20959.19 732.85 o
2 8 -16 357.67 458.03 187.72 o
4 8 -16 9580.08 10217.40 395.45 o
6 8 -16 1378.50 1169.93 193.51 o
8 8 -16 5890.66 6043.07 363.70 o
10 8 -16 105.86 45.98 119.53 o
2 10 -16 7127.50 7282.74 454.28 o
4 10 -16 136.71 -5.26 167.45 o
6 10 -16 5936.34 6202.76 338.17 o
8 10 -16 46.21 38.35 105.28 o
10 10 -16 7702.97 8247.43 343.52 o
0 12 -16 8354.60 7734.77 452.78 o
2 12 -16 626.20 596.20 207.99 o
4 12 -16 5352.06 4900.96 433.26 o
6 12 -16 523.42 741.87 260.55 o
8 12 -16 3987.27 3953.36 445.27 o
2 14 -16 8320.55 8007.34 518.10 o
4 14 -16 349.48 331.14 218.50 o
6 14 -16 3073.46 2598.78 407.73 o
8 14 -16 3.90 -192.22 220.01 o
2 16 -16 5.65 -147.92 144.92 o
4 16 -16 4913.73 5000.83 463.29 o
6 16 -16 15.77 -137.41 214.00 o
1 1 -15 30639.99 31522.29 453.58 o
3 1 -15 6184.46 6189.24 235.62 o
5 1 -15 4508.54 3819.14 240.22 o
7 1 -15 11199.31 11233.48 423.15 o
9 1 -15 10216.10 10043.20 502.34 o
11 1 -15 4735.63 4634.85 316.28 o
1 3 -15 11367.48 11170.82 238.84 o
3 3 -15 13130.73 13626.71 413.84 o
5 3 -15 9945.60 10236.33 379.09 o
7 3 -15 6101.76 5598.57 252.03 o
9 3 -15 5525.29 5405.70 315.88 o
11 3 -15 4212.81 3507.85 283.52 o
1 5 -15 19260.66 19127.51 386.17 o
3 5 -15 14859.84 14982.62 448.12 o
5 5 -15 6211.82 6096.74 297.75 o
7 5 -15 2220.13 2110.29 167.62 o
9 5 -15 1345.16 1229.61 156.20 o
11 5 -15 2314.77 2117.42 261.53 o
1 7 -15 10317.79 10867.23 445.65 o
3 7 -15 6933.87 6531.23 296.00 o
5 7 -15 4297.37 3898.27 249.27 o
7 7 -15 3697.51 3382.93 196.56 o
9 7 -15 4835.23 4683.04 244.95 o
11 7 -15 5553.84 6131.99 289.99 o
1 9 -15 9740.06 10108.22 335.35 o
3 9 -15 7610.83 7144.58 442.27 o
5 9 -15 4605.36 4331.27 268.10 o
7 9 -15 4177.43 3902.11 215.51 o
9 9 -15 5182.08 4884.35 252.19 o
11 9 -15 2289.01 1761.05 414.20 o
1 11 -15 4155.11 3526.86 308.61 o
3 11 -15 10109.45 10197.64 554.15 o
5 11 -15 5147.36 4820.62 414.48 o
7 11 -15 3367.87 3617.26 547.39 o
9 11 -15 3131.55 3100.28 241.41 o
1 13 -15 4146.26 4043.47 356.67 o
3 13 -15 7970.67 8593.02 530.87 o
5 13 -15 4131.38 3911.31 397.21 o
7 13 -15 1289.90 875.52 281.58 o
9 13 -15 2381.38 2270.23 324.75 o
1 15 -15 7259.59 7426.16 486.57 o
3 15 -15 3000.81 3256.55 406.97 o
5 15 -15 1158.14 1117.30 291.34 o
7 15 -15 594.12 421.99 283.83 o
3 17 -15 953.51 400.22 246.29 o
5 17 -15 999.81 952.11 305.61 o
3 19 -15 681.34 430.25 271.07 o
2 0 -14 28119.25 28551.00 588.02 o
6 0 -14 23773.66 23659.34 868.01 o
10 0 -14 14073.99 14205.06 722.34 o
0 2 -14 24467.45 25365.71 554.15 o
2 2 -14 924.73 827.15 96.66 o
4 2 -14 34797.96 33915.14 734.72 o
6 2 -14 2944.37 2689.27 162.13 o
8 2 -14 17142.97 16644.36 402.88 o
10 2 -14 400.52 137.61 140.79 o
12 2 -14 11203.43 11495.68 827.09 o
2 4 -14 43311.25 43704.41 662.26 o
4 4 -14 309.29 156.33 100.59 o
6 4 -14 33301.40 33795.44 607.50 o
8 4 -14 24.48 -17.38 89.65 o
10 4 -14 4132.73 4052.78 220.49 o
12 4 -14 69.11 86.49 157.03 o
0 6 -14 52419.87 54262.77 1356.83 o
2 6 -14 2349.84 2445.46 134.95 o
4 6 -14 30421.80 29844.17 694.68 o
6 6 -14 740.39 470.65 106.38 o
8 6 -14 11921.58 11674.72 348.59 o
10 6 -14 54.86 -39.10 98.65 o
12 6 -14 3467.31 3814.53 297.28 o
2 8 -14 24782.84 22484.58 1640.66 o
4 8 -14 1412.12 1230.31 170.31 o
6 8 -14 10097.27 9664.20 329.11 o
8 8 -14 229.75 23.03 95.38 o
10 8 -14 13485.07 13710.25 413.08 o
12 8 -14 23.33 -105.30 109.74 o
0 10 -14 13638.51 14028.61 569.16 o
2 10 -14 2322.75 2206.07 254.55 o
4 10 -14 17089.63 17088.43 729.85 o
6 10 -14 1394.98 1706.06 212.10 o
8 10 -14 9776.50 8974.23 325.92 o
10 10 -14 214.16 108.78 118.55 o
2 12 -14 8495.93 8289.67 480.56 o
4 12 -14 1202.72 1515.27 290.59 o
6 12 -14 13196.66 13439.92 705.82 o
8 12 -14 185.62 65.96 137.98 o
10 12 -14 5659.25 5720.95 357.13 o
0 14 -14 18141.67 18007.50 730.60 o
2 14 -14 538.07 198.98 174.95 o
4 14 -14 6683.08 6717.33 486.57 o
6 14 -14 4.25 -203.86 135.91 o
8 14 -14 5359.09 5183.05 334.20 o
2 16 -14 9710.16 10464.95 599.20 o
4 16 -14 118.50 -131.40 198.23 o
6 16 -14 3865.56 3843.73 423.49 o
8 16 -14 90.05 -57.70 148.85 o
2 18 -14 257.99 85.60 199.73 o
4 18 -14 5733.11 6295.34 533.87 o
6 18 -14 24.93 -59.32 213.25 o
2 20 -14 2468.70 2325.46 391.21 o
1 1 -13 13814.37 12874.29 302.92 o
3 1 -13 19654.08 19875.76 407.79 o
5 1 -13 22361.82 22190.44 581.93 o
7 1 -13 29111.91 28323.97 529.54 o
9 1 -13 9140.17 8825.75 379.32 o
11 1 -13 3323.30 3187.98 259.40 o
13 1 -13 5070.75 5670.90 357.30 o
1 3 -13 25365.96 25403.08 380.28 o
3 3 -13 30685.03 29777.53 483.79 o
5 3 -13 26970.72 25386.43 614.83 o
7 3 -13 7359.82 6956.57 248.15 o
9 3 -13 8114.90 8400.73 287.47 o
11 3 -13 5310.89 5321.69 318.43 o
13 3 -13 1678.81 1885.44 272.63 o
1 5 -13 19660.88 20325.12 383.08 o
3 5 -13 14471.87 13682.01 292.99 o
5 5 -13 11876.24 10848.06 296.45 o
7 5 -13 16411.97 16161.95 392.73 o
9 5 -13 11300.52 11402.17 346.18 o
11 5 -13 2229.65 2459.61 211.27 o
13 5 -13 1241.40 1417.66 236.48 o
1 7 -13 10899.62 10629.62 315.38 o
3 7 -13 27033.00 26951.97 629.44 o
5 7 -13 16936.50 17144.93 396.55 o
7 7 -13 14093.78 13955.74 372.24 o
9 7 -13 1364.69 1063.75 204.00 o
11 7 -13 1228.48 983.87 203.48 o
1 9 -13 20059.58 19648.28 474.98 o
3 9 -13 5744.88 5410.06 383.70 o
5 9 -13 10803.72 10112.26 603.33 o
7 9 -13 12274.83 12551.02 362.51 o
9 9 -13 5235.99 5043.94 247.70 o
11 9 -13 3987.06 4093.90 267.45 o
1 11 -13 7098.58 7038.85 275.48 o
3 11 -13 6446.30 7013.18 438.51 o
5 11 -13 16353.33 16004.16 734.36 o
7 11 -13 8155.95 7408.60 356.03 o
9 11 -13 6638.65 6430.24 285.96 o
11 11 -13 1951.11 2019.33 216.83 o
1 13 -13 4411.50 3897.60 231.78 o
3 13 -13 12678.41 12529.11 625.48 o
5 13 -13 6370.00 6263.80 467.80 o
7 13 -13 2024.22 1642.41 229.89 o
9 13 -13 3326.53 3592.29 305.23 o
1 15 -13 2961.30 2893.12 314.62 o
3 15 -13 6548.29 6979.39 490.32 o
5 15 -13 5175.36 4710.99 439.26 o
7 15 -13 1862.01 2003.77 242.78 o
9 15 -13 1969.33 1741.72 255.78 o
1 17 -13 3576.98 3721.34 380.69 o
3 17 -13 2697.96 2065.66 347.66 o
5 17 -13 5681.35 5767.47 502.34 o
7 17 -13 1261.09 1227.68 327.38 o
1 19 -13 2138.98 2589.02 369.43 o
3 19 -13 1907.55 1528.78 349.16 o
5 19 -13 1912.10 1357.58 331.89 o
0 0 -12 70739.91 75376.65 1703.74 o
4 0 -12 15841.01 15024.27 590.19 o
8 0 -12 46915.52 47998.50 913.84 o
12 0 -12 8822.90 9995.66 628.48 o
2 2 -12 42860.49 43335.73 636.68 o
4 2 -12 3337.30 3228.99 193.52 o
6 2 -12 57875.64 57899.92 711.98 o
8 2 -12 1842.21 1786.63 225.90 o
10 2 -12 3931.07 4031.23 204.20 o
12 2 -12 372.44 322.02 187.72 o
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