#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/40/2224026.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2224026_Fobs loop_ _publ_author_name 'Dang, Yan-Qiu' _publ_section_title ; Bis{2-(5-hydroxy-2-[1-(hydroxyimino)ethyl]phenolato-\k^2^O^1^,N}nickel(II) N,N-dimethylformamide disolvate ; _journal_coeditor_code TK2537 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1305 _journal_volume 65 _journal_year 2009 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 99.129 _cell_angle_gamma 90.000 _cell_length_a 13.2905 _cell_length_b 5.8649 _cell_length_c 15.9345 _exptl_crystal_F_000 564.00 _reflns_d_resolution_high 0.8107 _[local]_cod_data_source_file tk2537Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' test in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 163.34 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 10265.55 9661.68 169.15 o 3 0 0 5.20 6.86 1.09 o 4 0 0 713.19 794.60 15.85 o 5 0 0 770.71 749.45 15.57 o 6 0 0 3.86 7.87 1.60 o 7 0 0 313.78 368.29 9.95 o 8 0 0 2834.25 2759.69 51.52 o 9 0 0 302.61 303.43 9.78 o 10 0 0 306.68 310.97 10.46 o 11 0 0 607.23 565.04 15.69 o 12 0 0 123.76 137.97 7.39 o 13 0 0 244.40 243.38 10.49 o 14 0 0 278.08 262.34 11.20 o 15 0 0 15.73 16.89 4.27 o 16 0 0 113.88 119.58 8.68 o 1 1 0 2312.16 2347.05 29.11 o 2 1 0 1397.75 1391.68 14.67 o 3 1 0 187.27 199.50 3.12 o 4 1 0 798.04 774.35 9.16 o 5 1 0 464.94 466.50 6.37 o 6 1 0 7.18 9.79 3.94 o 7 1 0 2652.05 2830.08 37.01 o 8 1 0 114.91 123.57 4.05 o 9 1 0 40.32 50.46 2.97 o 10 1 0 4.89 7.82 2.20 o 11 1 0 0.26 -1.62 1.62 o 12 1 0 72.72 64.05 3.85 o 13 1 0 69.35 67.61 4.15 o 14 1 0 11.30 10.06 2.57 o 15 1 0 11.30 12.14 2.91 o 16 1 0 1.28 6.49 2.83 o 0 2 0 19.31 22.72 1.27 o 1 2 0 5329.33 5206.61 45.45 o 2 2 0 1978.92 1957.99 20.78 o 3 2 0 295.53 250.26 4.02 o 4 2 0 1328.93 1260.46 14.35 o 5 2 0 280.55 240.06 4.27 o 6 2 0 141.12 123.24 3.08 o 7 2 0 1676.91 1607.21 18.70 o 8 2 0 704.19 712.03 12.25 o 9 2 0 3836.40 3857.80 50.68 o 10 2 0 1746.51 1762.04 50.45 o 11 2 0 231.16 221.30 6.66 o 12 2 0 68.18 61.04 3.92 o 13 2 0 1.62 0.90 2.65 o 14 2 0 9.43 8.27 2.56 o 15 2 0 73.63 68.65 8.61 o 1 3 0 50.56 49.20 1.57 o 2 3 0 1067.81 1099.27 11.10 o 3 3 0 295.00 345.67 5.50 o 4 3 0 19.83 20.20 1.47 o 5 3 0 125.20 113.58 3.11 o 6 3 0 37.19 49.32 2.25 o 7 3 0 0.71 1.83 1.20 o 8 3 0 7.39 8.00 1.56 o 9 3 0 415.39 403.29 8.98 o 10 3 0 1.22 -0.23 1.71 o 11 3 0 260.18 260.10 7.57 o 12 3 0 0.83 0.03 2.08 o 13 3 0 2.98 3.55 2.43 o 14 3 0 1.44 3.21 2.52 o 0 4 0 368.44 349.96 8.93 o 1 4 0 2107.83 2039.84 19.65 o 2 4 0 75.33 74.96 2.24 o 3 4 0 231.80 203.18 3.64 o 4 4 0 49.64 47.94 2.27 o 5 4 0 251.21 254.00 5.23 o 6 4 0 677.46 609.85 9.35 o 7 4 0 137.12 134.91 4.04 o 8 4 0 319.45 302.26 6.36 o 9 4 0 294.95 298.02 6.50 o 10 4 0 267.90 246.33 7.41 o 11 4 0 105.87 121.07 5.53 o 12 4 0 28.38 38.47 9.79 o 13 4 0 16.82 17.79 3.29 o 1 5 0 53.63 60.91 3.89 o 2 5 0 155.01 153.13 4.20 o 3 5 0 80.87 75.36 3.14 o 4 5 0 59.03 50.53 2.67 o 5 5 0 11.70 11.57 1.88 o 6 5 0 28.97 26.41 2.34 o 7 5 0 3.41 2.21 1.84 o 8 5 0 0.85 0.57 1.65 o 9 5 0 7.37 7.20 2.15 o 10 5 0 34.33 40.66 4.38 o 11 5 0 55.27 62.61 4.68 o 0 6 0 475.99 456.51 14.83 o 1 6 0 115.35 116.15 5.20 o 2 6 0 3.62 2.80 2.22 o 3 6 0 25.35 26.78 3.19 o 4 6 0 127.82 122.10 9.66 o 5 6 0 64.13 68.20 5.92 o 6 6 0 88.42 103.22 5.39 o 7 6 0 86.46 89.46 4.10 o 8 6 0 332.32 335.75 7.70 o 9 6 0 84.68 80.47 7.77 o 1 7 0 27.51 27.57 4.29 o 2 7 0 1.55 -2.06 2.36 o 3 7 0 0.02 2.30 2.55 o 4 7 0 13.70 15.37 3.67 o -16 1 1 44.77 49.69 4.42 o -15 1 1 165.52 162.11 6.53 o -14 1 1 135.91 129.69 5.67 o -13 1 1 456.81 452.47 10.45 o -12 1 1 71.63 72.80 5.02 o -11 1 1 346.42 358.30 12.76 o -10 1 1 662.82 632.44 11.67 o -9 1 1 1839.24 1914.93 26.99 o -8 1 1 1835.07 1844.29 61.95 o -7 1 1 1155.87 1130.37 16.58 o -6 1 1 977.09 956.80 11.56 o -5 1 1 94.00 66.36 1.95 o -4 1 1 5108.46 5155.00 52.08 o -3 1 1 203.81 197.72 3.10 o -2 1 1 3335.49 3521.55 30.89 o -1 1 1 497.59 508.34 5.83 o 0 1 1 211.03 162.72 3.81 o 1 1 1 7675.44 7469.57 91.63 o 2 1 1 92.25 111.21 5.25 o 3 1 1 1059.09 1084.59 19.83 o 4 1 1 781.97 780.36 8.97 o 5 1 1 849.42 912.63 10.54 o 6 1 1 2204.52 2353.84 25.02 o 7 1 1 987.75 923.71 11.27 o 8 1 1 998.04 1009.02 12.45 o 9 1 1 884.95 840.69 11.07 o 10 1 1 180.36 186.24 4.33 o 11 1 1 402.45 421.87 9.31 o 12 1 1 71.17 80.78 4.27 o 13 1 1 40.33 42.92 3.50 o 14 1 1 30.04 34.51 3.43 o 15 1 1 194.68 210.42 7.41 o -15 2 1 1.08 5.17 2.62 o -14 2 1 44.85 36.70 3.76 o -13 2 1 8.15 5.04 2.20 o -12 2 1 2.36 -1.04 1.90 o -11 2 1 170.49 195.62 6.22 o -10 2 1 67.84 74.32 3.87 o -9 2 1 0.62 0.02 1.59 o -8 2 1 275.20 256.54 5.18 o -7 2 1 16.45 19.58 1.58 o -6 2 1 292.49 311.86 5.27 o -5 2 1 403.27 455.73 8.48 o -4 2 1 186.97 235.04 4.02 o -3 2 1 252.60 254.69 4.09 o -2 2 1 1024.41 1057.07 11.95 o -1 2 1 0.01 -0.38 0.38 o 0 2 1 25.61 36.19 0.94 o 1 2 1 420.26 355.99 5.82 o 2 2 1 19.97 11.82 1.03 o 3 2 1 2305.44 2528.99 26.56 o 4 2 1 46.99 46.50 1.78 o 5 2 1 748.81 750.46 9.57 o 6 2 1 20.92 36.78 1.52 o 7 2 1 9.72 12.83 1.69 o 8 2 1 514.47 503.59 9.67 o 9 2 1 1018.68 1071.68 17.14 o 10 2 1 38.85 47.32 3.20 o 11 2 1 1.71 -1.52 1.77 o 12 2 1 60.81 60.71 3.88 o 13 2 1 94.92 95.12 5.08 o 14 2 1 34.43 46.08 3.91 o 15 2 1 1.84 0.94 2.50 o -14 3 1 74.09 74.10 4.83 o -13 3 1 62.66 67.56 4.46 o -12 3 1 471.51 470.15 19.17 o -11 3 1 149.99 141.90 5.66 o -10 3 1 34.91 34.01 4.98 o -9 3 1 28.23 28.69 2.23 o -8 3 1 856.36 825.36 11.55 o -7 3 1 177.02 167.90 4.13 o -6 3 1 625.73 578.94 11.05 o -5 3 1 674.25 721.89 9.73 o -4 3 1 907.98 964.81 12.01 o -3 3 1 2974.12 3159.20 33.42 o -2 3 1 169.52 133.80 3.15 o -1 3 1 2214.41 2190.46 20.34 o 0 3 1 3539.59 3614.60 32.45 o 1 3 1 1436.11 1423.34 13.83 o 2 3 1 4990.33 5113.27 45.11 o 3 3 1 150.19 136.31 3.15 o 4 3 1 10.88 3.35 0.92 o 5 3 1 555.64 517.60 7.66 o 6 3 1 937.39 928.79 12.12 o 7 3 1 529.11 510.51 13.57 o 8 3 1 497.81 525.24 10.33 o 9 3 1 156.08 156.08 12.24 o 10 3 1 1658.46 1675.24 25.45 o 11 3 1 223.32 217.70 6.82 o 12 3 1 68.25 67.64 4.21 o 13 3 1 98.33 99.97 14.22 o 14 3 1 59.96 50.59 4.31 o -13 4 1 16.01 15.53 3.18 o -12 4 1 65.92 70.53 6.35 o -11 4 1 0.65 1.76 2.21 o -10 4 1 45.37 47.33 3.02 o -9 4 1 38.43 35.27 4.02 o -8 4 1 112.09 105.45 4.76 o -7 4 1 65.90 66.42 3.04 o -6 4 1 11.76 8.88 3.05 o -5 4 1 229.75 245.14 5.42 o -4 4 1 332.96 333.46 7.39 o -3 4 1 23.77 24.73 1.79 o -2 4 1 4.83 3.55 1.16 o -1 4 1 50.69 45.56 2.08 o 0 4 1 182.79 172.44 4.27 o 1 4 1 115.90 116.63 2.67 o 2 4 1 14.49 16.09 1.24 o 3 4 1 0.10 -0.12 0.82 o 4 4 1 38.60 37.73 2.08 o 5 4 1 105.70 115.58 3.02 o 6 4 1 53.28 55.99 2.67 o 7 4 1 105.05 103.32 3.68 o 8 4 1 14.33 15.83 2.39 o 9 4 1 15.61 14.26 2.52 o 10 4 1 78.63 79.84 4.40 o 11 4 1 212.79 214.54 9.36 o 12 4 1 1.42 0.08 3.66 o 13 4 1 38.81 47.80 4.32 o -11 5 1 7.06 7.31 4.79 o -10 5 1 149.93 147.86 5.80 o -9 5 1 296.14 296.99 9.90 o -8 5 1 139.31 133.98 6.75 o -7 5 1 272.15 272.57 6.24 o -6 5 1 15.29 11.46 2.22 o -5 5 1 286.15 299.97 6.28 o -4 5 1 42.60 51.59 2.71 o -3 5 1 637.03 623.41 9.62 o -2 5 1 552.48 545.12 8.70 o -1 5 1 514.49 491.56 8.02 o 0 5 1 710.75 676.54 12.44 o 1 5 1 901.27 870.59 14.89 o 2 5 1 353.41 327.20 7.92 o 3 5 1 362.89 350.41 7.61 o 4 5 1 260.55 269.02 5.78 o 5 5 1 201.63 198.95 7.64 o 6 5 1 130.30 125.09 6.87 o 7 5 1 228.02 224.92 5.63 o 8 5 1 117.34 108.87 5.05 o 9 5 1 280.49 287.02 8.44 o 10 5 1 117.62 116.99 9.48 o 11 5 1 161.35 164.59 6.86 o -9 6 1 6.04 9.86 2.48 o -8 6 1 0.03 -1.02 1.89 o -7 6 1 0.01 -0.57 1.81 o -6 6 1 10.84 12.69 2.30 o -5 6 1 11.24 8.72 2.51 o -4 6 1 0.29 0.25 1.99 o -3 6 1 38.69 40.40 3.56 o -2 6 1 51.65 55.30 3.81 o -1 6 1 77.59 82.44 4.56 o 0 6 1 18.22 17.03 2.80 o 1 6 1 273.67 269.82 7.82 o 2 6 1 50.50 49.54 5.80 o 3 6 1 0.14 -2.07 2.07 o 4 6 1 24.07 24.72 3.57 o 5 6 1 21.02 14.93 2.82 o 6 6 1 84.92 77.98 4.67 o 7 6 1 11.72 11.20 2.85 o 8 6 1 2.09 5.62 2.63 o -4 7 1 45.86 40.26 4.08 o -3 7 1 12.50 8.33 3.36 o -2 7 1 23.56 29.34 3.63 o -1 7 1 20.27 25.92 3.67 o 0 7 1 125.92 133.35 9.10 o 1 7 1 97.17 105.95 12.87 o 2 7 1 131.70 121.63 7.14 o 3 7 1 40.45 40.10 4.10 o -16 0 2 100.99 111.38 8.61 o -15 0 2 32.41 27.27 4.85 o -14 0 2 37.65 32.35 4.90 o -13 0 2 167.61 167.93 8.51 o -12 0 2 371.72 373.93 12.52 o -11 0 2 74.68 73.46 5.64 o -10 0 2 961.28 919.01 21.31 o -9 0 2 4.01 15.74 2.72 o -8 0 2 333.45 271.94 8.63 o -6 0 2 1542.62 1586.89 30.40 o -5 0 2 804.40 772.19 11.26 o -4 0 2 159.88 163.80 2.73 o -3 0 2 2185.51 2352.20 26.06 o -1 0 2 9997.23 9699.52 171.46 o 0 0 2 2980.48 2955.47 54.95 o 2 0 2 9202.07 8806.93 108.37 o 3 0 2 1283.89 1277.73 16.77 o 4 0 2 243.97 190.81 5.43 o 5 0 2 6058.56 5996.73 104.29 o 6 0 2 5477.87 5992.28 104.88 o 7 0 2 8735.46 9085.92 157.67 o 8 0 2 29.05 30.90 3.10 o 9 0 2 522.76 545.00 14.32 o 10 0 2 9.37 18.44 3.12 o 11 0 2 477.94 467.58 14.14 o 12 0 2 822.53 758.12 13.83 o 13 0 2 412.60 398.36 9.41 o 14 0 2 144.97 145.71 8.48 o 15 0 2 69.72 89.21 7.36 o -16 1 2 4.48 1.71 2.65 o -15 1 2 1.50 -0.64 2.26 o -14 1 2 61.20 67.90 4.28 o -13 1 2 0.18 -0.03 4.19 o -12 1 2 4.55 3.57 2.01 o -11 1 2 450.82 458.52 9.82 o -10 1 2 908.61 872.03 16.95 o -9 1 2 43.45 50.81 2.93 o -8 1 2 42.32 49.84 2.23 o -7 1 2 96.25 87.62 2.64 o -6 1 2 210.43 196.29 3.75 o -5 1 2 272.42 267.88 4.88 o -4 1 2 2470.18 2629.94 23.77 o -3 1 2 2051.03 2033.54 21.35 o -2 1 2 4918.33 4856.14 49.01 o -1 1 2 5204.01 5263.71 45.77 o 0 1 2 5942.73 6063.97 73.87 o 1 1 2 1818.60 1853.78 23.21 o 2 1 2 55.26 51.74 1.68 o 3 1 2 1694.05 1768.41 20.63 o 4 1 2 1138.38 1117.90 12.39 o 5 1 2 490.26 552.07 7.05 o 7 1 2 2.04 6.59 1.39 o 8 1 2 388.85 380.80 6.09 o 9 1 2 62.68 75.00 2.69 o 10 1 2 20.17 28.99 1.96 o 11 1 2 1.40 2.53 2.16 o 12 1 2 76.50 62.62 8.79 o 13 1 2 3.39 -1.49 6.26 o 14 1 2 13.15 9.79 2.62 o 15 1 2 0.04 -1.94 2.09 o -15 2 2 17.46 19.50 3.28 o -14 2 2 40.14 46.56 3.91 o -13 2 2 35.62 34.29 3.42 o -12 2 2 339.32 327.63 8.46 o -11 2 2 418.35 395.61 9.14 o -10 2 2 356.13 355.35 8.22 o -9 2 2 642.28 638.81 15.89 o -8 2 2 1214.15 1204.43 15.05 o -7 2 2 1137.19 1127.20 13.89 o -6 2 2 290.78 285.02 4.96 o -5 2 2 715.77 689.01 8.93 o -4 2 2 2742.01 2912.61 30.60 o -3 2 2 7118.25 7205.87 62.80 o -2 2 2 2044.43 2013.29 18.55 o -1 2 2 345.28 365.44 4.31 o 0 2 2 113.03 109.03 2.55 o 1 2 2 49.88 52.07 1.28 o 2 2 2 1747.56 1787.22 16.42 o 3 2 2 1090.19 1188.77 11.45 o 4 2 2 1221.94 1256.18 13.96 o 5 2 2 511.29 472.48 11.31 o 6 2 2 727.35 658.94 11.77 o 7 2 2 1505.89 1375.27 19.99 o 8 2 2 1880.16 1853.38 26.25 o 9 2 2 968.20 983.19 16.11 o 10 2 2 453.83 456.20 9.73 o 11 2 2 353.20 350.00 8.61 o 12 2 2 84.95 90.63 7.99 o 13 2 2 127.29 136.85 13.17 o 14 2 2 152.84 156.72 6.45 o 15 2 2 122.45 129.08 6.20 o -14 3 2 3.82 -0.34 2.32 o -13 3 2 0.67 2.44 2.38 o -12 3 2 7.48 3.54 2.32 o -11 3 2 19.81 26.73 3.20 o -10 3 2 23.77 26.82 2.30 o -9 3 2 66.33 66.18 4.89 o -8 3 2 80.45 79.40 3.47 o -7 3 2 26.56 23.88 1.84 o -6 3 2 0.96 0.56 1.41 o -5 3 2 107.04 106.70 3.02 o -4 3 2 316.19 339.08 5.63 o -3 3 2 162.16 157.93 2.71 o -2 3 2 4.47 -0.45 0.46 o -1 3 2 1305.09 1402.72 13.60 o 0 3 2 113.55 138.35 2.20 o 1 3 2 21.26 30.25 1.08 o 2 3 2 893.00 1036.75 10.45 o 3 3 2 230.52 286.63 4.66 o 4 3 2 33.37 43.84 1.66 o 5 3 2 58.64 63.72 2.45 o 6 3 2 0.01 1.54 1.30 o 7 3 2 139.19 143.32 9.08 o 8 3 2 0.00 0.56 1.55 o 9 3 2 24.22 22.46 4.32 o 10 3 2 18.80 21.56 2.71 o 11 3 2 6.74 8.06 2.27 o 12 3 2 3.22 4.75 4.53 o 13 3 2 15.54 13.90 2.85 o 14 3 2 0.84 3.64 2.56 o -13 4 2 206.43 224.20 17.24 o -12 4 2 488.67 501.00 11.79 o -11 4 2 558.84 555.86 10.10 o -10 4 2 169.81 166.94 5.08 o -9 4 2 201.49 201.64 6.14 o -8 4 2 65.95 58.98 2.91 o -7 4 2 377.41 364.03 6.87 o -6 4 2 10.46 7.99 1.63 o -5 4 2 178.62 175.01 4.38 o -4 4 2 474.74 438.93 7.18 o -3 4 2 735.43 693.24 17.07 o -2 4 2 935.69 961.72 12.36 o -1 4 2 973.63 898.55 11.62 o 0 4 2 999.15 906.32 10.08 o 1 4 2 1535.08 1452.18 14.66 o 2 4 2 353.20 345.64 5.95 o 3 4 2 554.54 578.59 8.43 o 4 4 2 537.91 549.63 8.30 o 5 4 2 130.59 141.28 3.85 o 6 4 2 927.09 893.64 12.28 o 7 4 2 78.40 79.86 3.98 o 8 4 2 291.59 278.37 7.39 o 9 4 2 12.28 8.40 2.29 o 10 4 2 3.35 3.30 2.09 o 11 4 2 18.48 17.78 2.98 o 12 4 2 45.34 45.53 4.03 o 13 4 2 46.41 51.16 4.99 o -11 5 2 33.32 33.09 3.01 o -10 5 2 12.88 12.79 2.37 o -9 5 2 69.01 60.91 3.47 o -8 5 2 2.54 2.21 1.76 o -7 5 2 86.56 74.79 3.46 o -6 5 2 21.28 16.49 2.09 o -5 5 2 31.10 28.37 2.29 o -4 5 2 14.43 17.82 2.01 o -3 5 2 46.34 54.58 2.70 o -2 5 2 13.05 14.10 1.76 o -1 5 2 179.76 170.59 4.78 o 0 5 2 70.22 73.52 2.98 o 1 5 2 42.99 33.66 2.78 o 2 5 2 3.34 4.37 1.98 o 3 5 2 16.24 13.89 2.33 o 4 5 2 44.75 46.86 2.62 o 5 5 2 42.38 39.76 2.15 o 6 5 2 19.16 15.65 2.03 o 7 5 2 23.41 27.78 4.94 o 8 5 2 5.65 7.14 2.34 o 9 5 2 0.11 -2.18 2.74 o 10 5 2 34.24 40.07 4.90 o 11 5 2 7.80 7.58 2.76 o -9 6 2 111.49 112.56 4.90 o -8 6 2 64.46 70.64 5.46 o -7 6 2 53.86 52.07 3.35 o -6 6 2 221.12 216.94 5.96 o -5 6 2 85.14 89.43 3.92 o -4 6 2 182.88 177.20 5.20 o -3 6 2 242.11 246.34 7.49 o -2 6 2 704.30 671.23 13.43 o -1 6 2 289.37 294.40 8.19 o 0 6 2 2.46 0.30 2.02 o 1 6 2 12.44 13.22 2.65 o 2 6 2 18.21 20.38 2.84 o 3 6 2 54.85 51.09 3.80 o 4 6 2 1.02 -1.99 1.99 o 5 6 2 89.87 93.05 4.96 o 6 6 2 195.24 188.44 6.77 o 7 6 2 235.46 230.25 7.65 o 8 6 2 103.41 104.16 13.31 o -4 7 2 15.93 13.00 3.21 o -3 7 2 98.15 92.80 5.42 o -2 7 2 105.07 102.33 5.46 o -1 7 2 2.78 1.11 2.60 o 0 7 2 0.68 1.12 2.55 o 1 7 2 5.56 5.75 2.89 o 2 7 2 0.30 0.70 2.60 o 3 7 2 0.07 1.47 2.42 o -16 1 3 53.31 50.57 5.54 o -15 1 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