#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/40/2224066.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2224066_Fobs loop_ _publ_author_name 'H\"okelek, Tuncer' 'Dal, Hakan' 'Tercan, Bar\?i\,s' '\"Ozbek, F. Elif' 'Necefo\(glu, Hacali' _publ_section_title ; Tetraaquabis(nicotinamide-\kN^1^)nickel(II) bis(2-fluorobenzoate) ; _journal_coeditor_code XU2610 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1330 _journal_page_last m1331 _journal_volume 65 _journal_year 2009 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 82.115 _cell_angle_beta 77.332 _cell_angle_gamma 63.664 _cell_length_a 7.2529 _cell_length_b 7.3315 _cell_length_c 14.3831 _exptl_crystal_F_000 338.00 _reflns_d_resolution_high 0.7454 _[local]_cod_data_source_file xu2610Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' el5 in P -1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 128.25 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 6394.60 5895.50 96.34 o 2 0 0 434.36 466.50 4.24 o 3 0 0 2.02 3.64 0.20 o 4 0 0 484.96 510.91 5.58 o 5 0 0 325.02 313.71 4.81 o 6 0 0 54.88 57.11 1.63 o 7 0 0 153.89 146.59 4.25 o 8 0 0 56.18 56.31 5.21 o -8 1 0 236.22 240.94 6.00 o -7 1 0 18.33 18.77 2.16 o -6 1 0 31.63 33.52 1.78 o -5 1 0 88.38 83.38 1.95 o -4 1 0 91.46 95.88 3.59 o -3 1 0 845.37 880.72 10.27 o -2 1 0 2250.04 2283.94 29.17 o -1 1 0 884.40 982.40 10.42 o 0 1 0 566.60 564.94 5.18 o 1 1 0 311.30 302.05 3.22 o 2 1 0 363.54 385.39 3.50 o 3 1 0 43.20 38.89 0.58 o 4 1 0 2105.53 2164.84 20.48 o 5 1 0 9.96 9.10 0.53 o 6 1 0 834.15 802.05 12.66 o 7 1 0 110.37 114.04 3.26 o 8 1 0 330.64 326.30 7.45 o -7 2 0 3.43 5.15 0.98 o -6 2 0 26.14 22.16 1.52 o -5 2 0 2.00 2.89 0.60 o -4 2 0 558.25 576.47 8.11 o -3 2 0 34.71 35.80 1.52 o -2 2 0 251.48 240.08 2.81 o -1 2 0 1734.83 1850.00 21.40 o 0 2 0 16447.79 15386.95 237.72 o 1 2 0 9399.96 9023.07 144.39 o 2 2 0 11.52 18.43 0.43 o 3 2 0 49.24 48.88 0.76 o 4 2 0 660.60 652.18 6.41 o 5 2 0 1623.76 1630.79 15.49 o 6 2 0 720.05 721.11 7.87 o 7 2 0 5.19 4.23 0.71 o 8 2 0 31.19 35.04 1.93 o 9 2 0 271.43 277.82 8.82 o -6 3 0 1.46 1.28 0.78 o -5 3 0 111.65 107.09 2.55 o -4 3 0 310.98 304.05 7.87 o -3 3 0 12.11 12.16 1.28 o -2 3 0 913.84 925.58 9.14 o -1 3 0 426.44 445.66 5.04 o 0 3 0 120.04 115.82 1.53 o 1 3 0 90.36 73.70 0.98 o 2 3 0 913.63 880.65 10.24 o 3 3 0 3634.79 3562.50 40.20 o 4 3 0 543.96 508.49 6.28 o 5 3 0 3.77 6.96 0.41 o 6 3 0 1260.48 1231.03 11.96 o 7 3 0 0.86 0.82 0.54 o 8 3 0 387.70 389.20 7.98 o 9 3 0 199.18 213.69 7.21 o -6 4 0 46.07 47.14 2.43 o -5 4 0 48.84 48.71 1.96 o -4 4 0 14.20 10.59 0.97 o -3 4 0 311.67 315.01 5.33 o -2 4 0 16.52 18.39 0.78 o -1 4 0 232.22 229.63 2.92 o 0 4 0 3321.74 3459.33 30.84 o 1 4 0 2423.91 2484.87 22.34 o 2 4 0 748.42 751.35 8.82 o 3 4 0 383.49 371.40 4.79 o 4 4 0 16.77 15.18 0.66 o 5 4 0 274.80 257.92 2.93 o 6 4 0 678.32 682.57 6.96 o 7 4 0 786.01 786.00 9.76 o 8 4 0 20.98 21.36 1.46 o -5 5 0 6.30 4.62 1.41 o -4 5 0 20.65 20.94 1.37 o -3 5 0 61.02 57.06 1.91 o -2 5 0 430.19 425.25 6.81 o -1 5 0 652.47 640.14 8.19 o 0 5 0 26.71 29.77 1.00 o 1 5 0 1191.43 1177.59 11.02 o 2 5 0 36.00 39.38 0.97 o 3 5 0 201.66 175.55 2.38 o 4 5 0 604.69 576.74 7.25 o 5 5 0 12.83 14.31 0.76 o 6 5 0 132.42 131.47 2.15 o 7 5 0 31.03 32.42 1.19 o 8 5 0 429.42 425.79 11.70 o -4 6 0 4.28 5.61 1.60 o -3 6 0 99.73 94.04 4.36 o -2 6 0 303.62 295.63 5.42 o -1 6 0 99.70 96.51 2.96 o 0 6 0 22.49 23.98 1.26 o 1 6 0 226.82 208.29 2.88 o 2 6 0 210.69 212.31 2.90 o 3 6 0 384.03 383.95 4.11 o 4 6 0 33.43 32.00 1.01 o 5 6 0 385.67 372.28 7.77 o 6 6 0 1157.02 1138.46 12.54 o 7 6 0 454.76 449.81 11.64 o 8 6 0 156.07 154.48 3.85 o 9 6 0 4.26 4.33 1.60 o -3 7 0 92.59 93.30 4.33 o -2 7 0 218.74 207.58 5.31 o -1 7 0 323.73 315.21 6.89 o 0 7 0 2.75 3.90 1.00 o 1 7 0 24.42 25.70 0.96 o 2 7 0 307.95 308.92 4.04 o 3 7 0 162.95 156.79 2.47 o 4 7 0 139.71 128.69 1.96 o 5 7 0 221.65 211.87 3.09 o 6 7 0 55.92 51.61 1.40 o 7 7 0 69.71 69.81 2.10 o 8 7 0 18.92 19.21 2.00 o -1 8 0 32.36 31.12 2.16 o 0 8 0 1.50 0.11 0.95 o 1 8 0 3.63 2.59 0.87 o 2 8 0 69.08 71.88 1.93 o 3 8 0 316.72 322.44 4.88 o 4 8 0 33.00 30.79 1.44 o 5 8 0 18.71 17.16 0.99 o 6 8 0 434.23 421.32 6.50 o 7 8 0 346.31 335.90 13.35 o 8 8 0 95.02 91.98 3.12 o 1 9 0 93.98 103.37 3.74 o 2 9 0 25.11 23.77 1.56 o 3 9 0 45.00 46.30 2.46 o 4 9 0 75.91 73.93 2.39 o 5 9 0 32.04 31.53 1.48 o 6 9 0 155.61 153.61 3.39 o 7 9 0 221.30 209.69 7.37 o -6 -9 1 307.21 304.10 5.31 o -5 -9 1 49.84 55.91 1.94 o -4 -9 1 107.41 105.81 3.29 o -3 -9 1 76.39 71.19 2.33 o -2 -9 1 30.37 25.35 1.50 o -1 -9 1 50.41 53.89 2.77 o -8 -8 1 85.31 80.96 4.17 o -7 -8 1 98.33 103.14 5.23 o -6 -8 1 15.53 17.61 2.27 o -5 -8 1 21.60 19.62 1.17 o -4 -8 1 114.08 112.29 2.97 o -3 -8 1 206.11 204.46 3.55 o -2 -8 1 49.01 50.54 1.60 o -1 -8 1 120.43 107.32 3.42 o 0 -8 1 11.98 9.33 1.39 o 1 -8 1 51.99 51.18 2.62 o -8 -7 1 1.14 0.19 0.89 o -7 -7 1 611.14 602.03 10.91 o -6 -7 1 1048.54 1009.33 14.13 o -5 -7 1 707.02 679.36 7.78 o -4 -7 1 56.06 57.58 1.25 o -3 -7 1 224.27 216.70 3.11 o -2 -7 1 16.22 18.22 0.86 o -1 -7 1 0.81 1.55 0.48 o 0 -7 1 194.70 191.83 7.29 o 1 -7 1 66.45 65.32 2.62 o 2 -7 1 136.20 142.14 5.21 o 3 -7 1 2.71 3.21 1.44 o -9 -6 1 33.23 30.78 2.56 o -8 -6 1 146.40 147.33 5.85 o -7 -6 1 96.72 96.51 2.16 o -6 -6 1 260.97 258.80 3.92 o -5 -6 1 367.86 358.27 5.00 o -4 -6 1 73.74 73.85 1.48 o -3 -6 1 106.73 105.08 2.04 o -2 -6 1 96.72 89.15 1.64 o -1 -6 1 250.64 268.24 3.47 o 0 -6 1 498.39 491.59 7.45 o 1 -6 1 75.70 77.31 3.22 o 2 -6 1 476.63 477.62 7.73 o 3 -6 1 27.90 28.03 1.53 o 4 -6 1 188.26 181.05 5.61 o -8 -5 1 2.45 3.79 0.96 o -7 -5 1 1012.23 986.46 13.83 o -6 -5 1 1748.11 1719.38 18.30 o -5 -5 1 717.24 704.20 7.93 o -4 -5 1 447.34 425.57 6.22 o -3 -5 1 88.32 81.27 1.37 o -2 -5 1 41.73 42.20 1.14 o -1 -5 1 595.11 587.89 5.81 o 0 -5 1 1094.88 1060.45 10.01 o 1 -5 1 182.21 180.69 2.97 o 2 -5 1 194.78 185.62 3.65 o 3 -5 1 117.59 112.54 2.78 o 4 -5 1 7.55 7.11 1.34 o 5 -5 1 139.00 143.32 4.87 o -8 -4 1 54.30 56.59 2.89 o -7 -4 1 504.29 498.02 6.58 o -6 -4 1 726.74 704.28 9.60 o -5 -4 1 357.31 347.63 4.42 o -4 -4 1 16.65 23.41 0.93 o -3 -4 1 142.63 144.61 3.21 o -2 -4 1 2219.77 2136.61 23.89 o -1 -4 1 582.48 661.93 6.32 o 0 -4 1 317.95 411.17 3.89 o 1 -4 1 75.05 82.57 1.63 o 2 -4 1 248.71 259.94 3.34 o 3 -4 1 309.61 310.99 5.24 o 4 -4 1 157.98 146.61 3.21 o 5 -4 1 22.59 20.03 1.87 o -9 -3 1 176.12 182.92 6.57 o -8 -3 1 20.63 21.96 2.08 o -7 -3 1 121.61 120.33 2.71 o -6 -3 1 1603.69 1579.90 15.22 o -5 -3 1 361.94 356.18 4.69 o -4 -3 1 230.59 232.75 2.59 o -3 -3 1 741.22 744.73 12.17 o -2 -3 1 1055.24 1007.26 11.66 o -1 -3 1 1250.70 1230.48 12.44 o 0 -3 1 728.02 680.25 6.64 o 1 -3 1 84.26 89.95 1.26 o 2 -3 1 780.82 821.17 10.45 o 3 -3 1 57.64 61.57 1.65 o 4 -3 1 287.21 278.21 4.77 o 5 -3 1 815.95 798.63 11.70 o 6 -3 1 369.15 362.76 6.46 o -9 -2 1 87.54 84.16 4.33 o -8 -2 1 36.13 34.37 2.40 o -7 -2 1 25.14 23.69 1.82 o -6 -2 1 1977.85 1979.57 22.85 o -5 -2 1 1467.43 1456.55 13.94 o -4 -2 1 399.71 375.57 3.90 o -3 -2 1 75.43 91.37 2.60 o -2 -2 1 5345.18 5183.62 57.57 o -1 -2 1 1.36 2.54 0.27 o 0 -2 1 8880.26 8953.41 75.69 o 1 -2 1 9.82 22.12 0.41 o 2 -2 1 1086.30 1093.43 16.13 o 3 -2 1 1800.14 1866.48 38.69 o 4 -2 1 278.90 287.54 4.38 o 5 -2 1 10.90 13.07 0.81 o 6 -2 1 45.81 45.25 2.00 o 7 -2 1 0.77 0.34 0.92 o -8 -1 1 62.81 61.12 2.60 o -7 -1 1 338.42 338.35 5.51 o -6 -1 1 270.91 275.09 5.21 o -5 -1 1 190.11 206.11 2.37 o -4 -1 1 959.79 1031.34 9.26 o -3 -1 1 128.85 115.70 1.29 o -2 -1 1 239.23 270.50 3.01 o -1 -1 1 1141.41 1078.83 9.53 o 0 -1 1 1251.91 1343.87 12.17 o 1 -1 1 176.24 182.45 1.69 o 2 -1 1 3700.34 3857.66 44.85 o 3 -1 1 2455.08 2619.47 23.18 o 4 -1 1 175.68 187.23 3.01 o 5 -1 1 643.77 631.01 8.87 o 6 -1 1 788.19 751.02 13.68 o 7 -1 1 143.29 130.04 3.69 o 8 -1 1 1.83 2.65 1.84 o -8 0 1 281.79 267.39 7.61 o -7 0 1 131.60 127.22 5.85 o -6 0 1 1013.92 993.08 13.60 o -5 0 1 998.07 995.87 13.49 o -4 0 1 38.25 28.72 0.62 o -3 0 1 315.61 349.98 3.35 o -2 0 1 294.91 323.49 3.01 o -1 0 1 1744.92 1858.75 13.90 o 0 0 1 1007.31 909.09 10.99 o 1 0 1 1170.64 1146.33 13.01 o 2 0 1 134.73 152.07 2.30 o 3 0 1 1133.39 1180.89 12.25 o 4 0 1 424.06 451.69 4.96 o 5 0 1 31.18 31.77 1.12 o 6 0 1 200.89 194.81 4.84 o 7 0 1 225.06 218.52 5.11 o 8 0 1 8.91 7.12 1.23 o -8 1 1 78.80 83.45 3.22 o -7 1 1 76.84 75.67 2.81 o -6 1 1 111.65 103.23 3.18 o -5 1 1 200.00 189.94 3.36 o -4 1 1 77.83 81.30 1.77 o -3 1 1 1710.15 1747.00 22.59 o -2 1 1 682.14 661.10 8.80 o -1 1 1 2445.36 2548.07 24.53 o 0 1 1 8.19 9.07 0.30 o 1 1 1 3126.53 3084.06 42.93 o 2 1 1 993.77 1026.85 10.61 o 3 1 1 440.44 474.85 4.70 o 4 1 1 32.82 37.20 0.64 o 5 1 1 526.73 511.73 5.69 o 6 1 1 1174.43 1173.48 15.66 o 7 1 1 205.02 203.83 4.79 o 8 1 1 69.39 64.03 2.58 o 9 1 1 0.61 -0.48 1.44 o -7 2 1 37.06 36.82 1.98 o -6 2 1 31.80 28.49 1.23 o -5 2 1 619.98 610.60 7.81 o -4 2 1 370.40 368.02 5.57 o -3 2 1 310.76 306.92 4.59 o -2 2 1 1299.24 1396.81 15.95 o -1 2 1 931.17 917.00 16.59 o 0 2 1 898.57 969.32 9.81 o 1 2 1 6637.56 6577.15 48.55 o 2 2 1 1.77 3.73 0.78 o 3 2 1 465.15 489.61 5.51 o 4 2 1 471.89 520.94 5.19 o 5 2 1 841.44 880.77 9.41 o 6 2 1 6.40 6.89 0.55 o 7 2 1 82.36 75.99 3.69 o 8 2 1 17.84 17.85 1.46 o 9 2 1 4.30 4.31 1.19 o -6 3 1 35.24 35.45 1.92 o -5 3 1 5.73 6.21 0.75 o -4 3 1 140.36 140.15 3.37 o -3 3 1 725.48 710.61 8.71 o -2 3 1 22.17 30.67 0.62 o -1 3 1 224.58 224.96 2.61 o 0 3 1 574.86 589.62 5.24 o 1 3 1 166.30 134.95 1.58 o 2 3 1 3350.65 3373.11 33.43 o 3 3 1 1653.24 1637.38 16.77 o 4 3 1 33.00 34.93 0.73 o 5 3 1 248.60 237.64 2.70 o 6 3 1 207.32 206.13 2.47 o 7 3 1 29.34 31.28 1.73 o 8 3 1 72.36 74.65 2.60 o 9 3 1 60.80 66.05 3.45 o -6 4 1 38.93 42.16 3.05 o -5 4 1 32.62 33.23 1.39 o -4 4 1 119.60 111.14 2.78 o -3 4 1 484.62 456.65 7.19 o -2 4 1 1.54 1.18 0.58 o -1 4 1 254.14 235.16 3.43 o 0 4 1 2797.73 2981.78 40.65 o 1 4 1 7051.17 7089.20 78.38 o 2 4 1 453.29 482.06 4.70 o 3 4 1 9.72 16.54 1.10 o 4 4 1 1222.79 1242.50 14.55 o 5 4 1 88.18 90.82 1.71 o 6 4 1 83.37 81.71 1.50 o 7 4 1 1.92 4.47 1.08 o 8 4 1 2.41 3.61 1.02 o 9 4 1 103.50 114.94 4.81 o -5 5 1 27.66 32.38 3.53 o -4 5 1 3.87 3.39 0.91 o -3 5 1 55.79 51.87 1.84 o -2 5 1 18.82 19.57 1.70 o -1 5 1 45.05 45.85 1.29 o 0 5 1 825.54 808.54 12.94 o 1 5 1 1626.69 1626.35 18.53 o 2 5 1 251.13 244.84 2.73 o 3 5 1 19.46 19.30 0.72 o 4 5 1 141.75 129.48 1.98 o 5 5 1 100.61 101.96 2.24 o 6 5 1 26.02 25.50 1.18 o 7 5 1 43.66 44.78 1.35 o 8 5 1 557.45 583.60 9.29 o -4 6 1 33.94 34.31 2.73 o -3 6 1 114.65 110.66 2.97 o -2 6 1 446.40 435.98 7.29 o -1 6 1 101.64 106.13 3.16 o 0 6 1 915.72 901.38 15.38 o 1 6 1 1523.38 1526.50 15.54 o 2 6 1 721.30 727.67 7.89 o 3 6 1 16.76 16.78 0.67 o 4 6 1 295.83 281.23 3.24 o 5 6 1 877.72 853.94 9.31 o 6 6 1 212.98 201.34 5.81 o 7 6 1 8.07 8.55 0.81 o 8 6 1 8.98 8.95 1.23 o -2 7 1 5.52 7.50 1.44 o -1 7 1 96.76 100.03 3.35 o 0 7 1 193.88 195.45 8.02 o 1 7 1 153.70 153.11 2.78 o 2 7 1 547.58 547.23 6.34 o 3 7 1 11.46 13.10 0.85 o 4 7 1 147.46 136.08 2.04 o 5 7 1 135.48 129.75 2.00 o 6 7 1 10.20 11.28 0.77 o 7 7 1 98.87 100.56 2.22 o 8 7 1 9.87 11.07 1.23 o -1 8 1 19.05 17.88 1.81 o 0 8 1 157.67 156.44 4.47 o 1 8 1 485.54 454.13 9.12 o 2 8 1 322.69 315.13 4.81 o 3 8 1 264.48 269.77 4.30 o 4 8 1 324.93 320.54 4.28 o 5 8 1 49.61 45.13 2.04 o 6 8 1 82.91 81.75 1.99 o 7 8 1 25.57 25.81 1.23 o 8 8 1 18.23 19.84 4.17 o 1 9 1 272.62 266.53 6.54 o 2 9 1 336.93 326.69 7.44 o 3 9 1 29.74 32.96 1.67 o 4 9 1 1.25 0.52 0.77 o 5 9 1 50.67 47.89 1.67 o 6 9 1 6.49 4.02 0.88 o 7 9 1 3.53 2.08 0.84 o -6 -9 2 17.53 14.61 1.37 o -5 -9 2 7.46 7.06 1.44 o -4 -9 2 141.84 148.77 5.77 o -3 -9 2 8.43 8.15 2.24 o -2 -9 2 18.92 22.15 1.46 o -1 -9 2 5.95 10.91 3.06 o -7 -8 2 95.01 96.87 3.73 o -6 -8 2 17.23 16.84 1.20 o -5 -8 2 0.67 0.94 0.71 o -4 -8 2 241.43 229.14 5.04 o -3 -8 2 156.78 147.66 4.46 o -2 -8 2 299.17 309.94 4.78 o -1 -8 2 402.91 379.34 6.33 o 0 -8 2 354.22 337.30 10.02 o 1 -8 2 2.52 2.18 1.19 o -8 -7 2 105.77 101.34 3.23 o -7 -7 2 14.88 16.82 1.18 o -6 -7 2 83.67 78.85 2.22 o -5 -7 2 90.95 89.98 1.97 o -4 -7 2 151.03 145.41 2.82 o -3 -7 2 427.43 411.20 5.02 o -2 -7 2 82.08 82.70 1.69 o -1 -7 2 68.52 59.80 1.45 o 0 -7 2 0.70 1.37 0.70 o 1 -7 2 31.89 33.52 1.89 o 2 -7 2 7.00 8.26 1.13 o -8 -6 2 201.93 195.96 4.64 o -7 -6 2 96.31 96.72 3.55 o -6 -6 2 0.83 0.41 0.54 o -5 -6 2 2.29 3.68 0.54 o -4 -6 2 882.30 877.49 12.37 o -3 -6 2 116.56 114.48 2.19 o -2 -6 2 129.46 115.76 1.92 o -1 -6 2 512.48 513.48 6.94 o 0 -6 2 41.78 41.80 1.12 o 1 -6 2 147.43 150.04 3.28 o 2 -6 2 107.63 103.48 2.76 o 3 -6 2 70.47 75.95 2.40 o 4 -6 2 30.46 30.94 3.37 o -8 -5 2 274.88 274.69 5.72 o -7 -5 2 340.53 337.80 5.79 o -6 -5 2 290.18 291.83 4.47 o -5 -5 2 309.67 311.68 3.94 o -4 -5 2 462.17 445.71 5.26 o -3 -5 2 205.72 207.51 2.66 o -2 -5 2 43.80 39.96 1.09 o -1 -5 2 46.61 51.85 0.97 o 0 -5 2 334.95 318.83 3.23 o 1 -5 2 301.93 293.30 3.43 o 2 -5 2 0.90 1.22 0.63 o 3 -5 2 125.19 127.16 3.00 o 4 -5 2 52.35 53.93 2.00 o 5 -5 2 33.65 33.12 2.73 o -8 -4 2 264.48 268.06 5.50 o -7 -4 2 382.41 381.57 6.07 o -6 -4 2 2.23 2.85 0.52 o -5 -4 2 58.05 58.59 1.22 o -4 -4 2 158.82 170.23 2.35 o -3 -4 2 1412.66 1383.51 16.06 o -2 -4 2 32.57 29.53 0.90 o -1 -4 2 357.44 351.07 3.96 o 0 -4 2 229.22 229.00 2.59 o 1 -4 2 176.98 167.35 2.11 o 2 -4 2 61.50 63.66 1.28 o 3 -4 2 0.87 1.96 0.66 o 4 -4 2 68.39 68.97 2.10 o 5 -4 2 476.42 454.04 12.34 o -8 -3 2 265.24 289.52 8.66 o -7 -3 2 59.44 60.82 1.71 o -6 -3 2 972.88 974.75 9.71 o -5 -3 2 539.92 507.15 6.40 o -4 -3 2 500.86 499.07 5.06 o -3 -3 2 1840.58 1870.39 19.37 o -2 -3 2 477.89 485.00 6.79 o -1 -3 2 94.26 64.70 0.99 o 0 -3 2 1.14 4.04 0.56 o 1 -3 2 1544.63 1534.51 12.39 o 2 -3 2 51.38 59.20 1.00 o 3 -3 2 4.99 4.12 0.58 o 4 -3 2 187.47 191.62 5.77 o 5 -3 2 9.70 11.37 1.41 o 6 -3 2 56.42 55.58 4.57 o -8 -2 2 1.58 3.21 1.60 o -7 -2 2 141.89 146.60 2.95 o -6 -2 2 48.11 48.65 1.23 o -5 -2 2 782.34 798.95 7.92 o -4 -2 2 998.06 1013.25 9.81 o -3 -2 2 109.48 97.37 1.39 o -2 -2 2 357.17 359.87 3.67 o -1 -2 2 287.26 275.75 3.11 o 0 -2 2 2865.03 2945.84 27.15 o 1 -2 2 7.61 2.29 0.17 o 2 -2 2 520.53 504.28 6.16 o 3 -2 2 460.56 466.43 8.31 o 4 -2 2 34.87 35.59 1.42 o 5 -2 2 604.77 615.70 8.76 o 6 -2 2 274.00 261.31 5.74 o 7 -2 2 4.94 6.05 1.19 o -8 -1 2 213.63 219.92 5.43 o -7 -1 2 285.58 290.12 4.91 o -6 -1 2 551.73 561.88 11.11 o -5 -1 2 2700.30 2690.01 27.76 o -4 -1 2 716.58 747.05 7.79 o -3 -1 2 1095.57 1255.46 11.12 o -2 -1 2 42.33 47.27 0.64 o -1 -1 2 94.35 83.04 0.89 o 0 -1 2 1845.80 1902.31 16.86 o 1 -1 2 251.16 261.27 2.10 o 2 -1 2 664.84 724.31 7.06 o 3 -1 2 841.30 863.93 8.42 o 4 -1 2 173.14 175.46 1.95 o 5 -1 2 13.68 16.63 0.82 o 6 -1 2 90.39 91.11 4.41 o 7 -1 2 49.97 47.92 2.40 o 8 -1 2 0.67 0.59 1.00 o -8 0 2 1.02 0.35 1.07 o -7 0 2 125.87 122.47 2.83 o -6 0 2 619.24 608.10 8.83 o -5 0 2 1105.31 1087.91 14.66 o -4 0 2 377.04 378.71 3.75 o -3 0 2 1.87 2.53 0.19 o 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