#------------------------------------------------------------------------------ #$Date: 2016-04-03 04:21:12 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181161 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/40/2224077.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2224077_Fobs loop_ _publ_author_name 'Znovjyak, Kateryna O.' 'Ovchynnikov, Vladimir A.' 'Sliva, Tetyana Yu.' 'Shishkina, Svitlana V.' 'Amirkhanov, Vladimir M.' _publ_section_title ; N-{Bis[methyl(phenyl)amino]phosphoryl}-2,2,2-trichloroacetamide ; _journal_coeditor_code XU2626 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2812 _journal_volume 65 _journal_year 2009 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 93.345 _cell_angle_gamma 90.000 _cell_length_a 12.8226 _cell_length_b 19.5161 _cell_length_c 15.1132 _exptl_crystal_F_000 1728.00 _reflns_d_resolution_high 0.7696 _cod_data_source_file xu2626Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' k9 in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 408.91 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 25006.07 24337.12 127.11 o 4 0 0 2663.26 2620.63 96.98 o 6 0 0 17618.86 17548.98 159.61 o 8 0 0 5453.74 5533.19 165.57 o 10 0 0 48.84 121.00 57.69 o 12 0 0 9074.66 8645.92 402.15 o 14 0 0 1095.60 870.36 125.33 o 16 0 0 54.31 159.49 117.41 o 2 1 0 164.64 192.20 26.73 o 3 1 0 3606.55 3395.96 75.45 o 5 1 0 10554.46 9722.63 105.31 o 6 1 0 776.20 583.49 54.53 o 7 1 0 3433.14 3277.60 83.10 o 8 1 0 87.21 144.29 39.34 o 9 1 0 256.34 204.02 46.48 o 10 1 0 645.55 624.72 59.52 o 11 1 0 898.54 829.91 68.25 o 12 1 0 417.28 506.76 84.57 o 13 1 0 1094.36 1133.61 122.55 o 14 1 0 4144.05 3995.73 166.57 o 15 1 0 175.81 138.94 80.29 o 16 1 0 141.54 132.84 96.29 o 1 2 0 42.01 80.10 31.21 o 2 2 0 12.66 58.78 22.95 o 3 2 0 164.91 204.06 33.67 o 4 2 0 7533.34 7801.71 110.76 o 5 2 0 189.72 244.97 38.79 o 7 2 0 47.20 71.27 24.08 o 8 2 0 63.36 90.81 31.30 o 9 2 0 2155.24 1896.91 69.94 o 10 2 0 1704.91 1785.14 108.76 o 11 2 0 1227.87 1491.14 106.35 o 12 2 0 162.05 147.32 51.49 o 13 2 0 16.00 97.94 50.44 o 14 2 0 1131.18 1119.63 137.74 o 15 2 0 2681.14 2502.16 159.21 o 16 2 0 4.17 63.80 68.42 o 1 3 0 26969.37 26656.14 100.89 o 2 3 0 166.69 322.71 49.83 o 3 3 0 7195.45 6848.21 104.81 o 4 3 0 776.45 694.02 41.90 o 5 3 0 38.73 52.79 18.90 o 6 3 0 1045.95 1321.23 58.38 o 7 3 0 165.43 164.04 36.27 o 9 3 0 4855.17 4407.28 106.34 o 10 3 0 145.75 180.88 37.81 o 11 3 0 3425.80 3512.64 115.64 o 12 3 0 135.24 156.11 44.54 o 13 3 0 219.38 189.28 54.83 o 14 3 0 893.86 769.28 123.65 o 15 3 0 1557.86 1280.40 133.18 o 16 3 0 0.46 159.74 102.32 o 0 4 0 162891.19 159683.77 1278.87 o 2 4 0 15886.20 17423.20 171.00 o 3 4 0 307.05 507.28 59.60 o 4 4 0 5219.86 5254.43 120.70 o 5 4 0 267.21 329.96 35.38 o 6 4 0 13738.48 15237.58 188.84 o 7 4 0 93.11 115.53 26.93 o 8 4 0 239.08 203.28 35.17 o 9 4 0 651.57 631.63 67.06 o 10 4 0 118.08 119.02 48.41 o 11 4 0 2257.38 1974.31 88.62 o 12 4 0 2409.59 2507.24 109.39 o 13 4 0 287.36 318.23 62.09 o 14 4 0 289.55 199.15 86.50 o 15 4 0 1647.89 1448.85 142.16 o 16 4 0 6.09 97.83 90.04 o 1 5 0 11603.66 12851.08 148.81 o 2 5 0 647.65 610.63 45.05 o 3 5 0 2107.79 1947.43 161.51 o 4 5 0 1253.65 1320.77 74.85 o 5 5 0 1275.05 1358.59 73.32 o 6 5 0 652.84 801.08 70.21 o 7 5 0 2339.25 2024.96 65.16 o 8 5 0 93.87 81.64 24.52 o 9 5 0 1329.97 1061.95 93.17 o 10 5 0 70.78 101.33 41.09 o 11 5 0 2083.53 1872.04 88.54 o 12 5 0 2646.17 2486.26 157.04 o 13 5 0 1231.82 1218.23 112.84 o 14 5 0 483.48 459.36 108.89 o 15 5 0 343.44 276.87 89.42 o 16 5 0 188.96 199.87 121.73 o 0 6 0 12948.65 13988.41 176.10 o 2 6 0 39316.54 41821.52 156.09 o 3 6 0 1138.49 1166.02 69.59 o 4 6 0 33330.52 34906.88 135.80 o 5 6 0 661.30 817.97 87.59 o 6 6 0 882.81 772.82 85.57 o 8 6 0 5712.31 5633.49 122.98 o 9 6 0 178.63 278.42 61.97 o 10 6 0 438.80 376.02 75.11 o 11 6 0 473.33 479.84 86.45 o 12 6 0 0.02 111.18 44.06 o 13 6 0 2494.74 2404.05 114.95 o 14 6 0 1577.06 1473.62 118.44 o 15 6 0 53.30 169.95 66.65 o 1 7 0 10264.49 10437.78 115.27 o 2 7 0 1653.67 1383.48 57.13 o 3 7 0 21940.61 21595.08 159.07 o 4 7 0 462.59 477.04 69.07 o 5 7 0 14114.97 13518.35 218.07 o 6 7 0 60.00 144.76 90.81 o 8 7 0 488.47 493.15 76.37 o 9 7 0 477.13 552.58 78.32 o 10 7 0 821.08 817.60 86.59 o 11 7 0 283.57 300.91 78.73 o 12 7 0 492.45 428.42 72.56 o 13 7 0 16.51 148.03 53.19 o 14 7 0 217.35 288.41 75.64 o 15 7 0 210.53 153.90 83.90 o 0 8 0 563.43 340.64 81.80 o 1 8 0 554.77 789.52 61.66 o 2 8 0 8269.96 8978.75 105.93 o 3 8 0 9.07 77.15 28.18 o 5 8 0 732.17 641.90 43.34 o 6 8 0 1944.66 2190.60 106.73 o 7 8 0 271.66 242.73 61.10 o 8 8 0 28.48 73.30 40.57 o 9 8 0 70.08 124.84 44.18 o 10 8 0 5104.68 5034.00 172.33 o 11 8 0 1830.34 1972.59 110.55 o 12 8 0 643.50 690.01 103.78 o 13 8 0 108.85 206.61 53.29 o 14 8 0 18.12 165.90 69.91 o 15 8 0 174.67 293.02 83.87 o 1 9 0 2674.97 2251.52 80.20 o 2 9 0 1.37 52.62 24.35 o 3 9 0 2642.11 2325.96 82.52 o 4 9 0 4.01 113.14 42.79 o 5 9 0 507.79 535.43 81.36 o 6 9 0 131.94 192.78 57.20 o 7 9 0 1.90 52.03 32.24 o 8 9 0 27.66 82.50 47.73 o 10 9 0 31.09 163.34 60.64 o 11 9 0 809.85 1125.12 106.28 o 12 9 0 186.98 278.03 75.14 o 13 9 0 1334.02 1418.88 109.30 o 14 9 0 14.77 165.95 69.99 o 15 9 0 19.59 134.92 85.51 o 0 10 0 650.70 413.05 80.48 o 1 10 0 204.59 415.45 76.17 o 2 10 0 6257.11 6544.26 104.91 o 3 10 0 55.47 108.85 33.71 o 6 10 0 2876.72 3119.23 152.31 o 7 10 0 34.95 111.03 41.79 o 8 10 0 203.61 101.00 47.25 o 9 10 0 117.77 190.97 59.14 o 10 10 0 99.94 150.92 53.35 o 11 10 0 665.38 618.44 82.36 o 12 10 0 1194.53 1194.86 104.85 o 13 10 0 491.23 446.19 109.26 o 14 10 0 186.97 211.19 84.28 o 15 10 0 133.55 85.94 63.01 o 1 11 0 438.09 478.06 64.51 o 2 11 0 28.87 78.16 32.86 o 3 11 0 3438.02 3026.51 101.95 o 4 11 0 375.66 373.20 58.78 o 5 11 0 2433.28 2421.67 122.03 o 6 11 0 2.28 101.09 51.23 o 7 11 0 769.83 733.53 94.21 o 8 11 0 9.17 82.36 47.02 o 9 11 0 49.36 105.54 52.74 o 10 11 0 515.43 329.75 64.89 o 11 11 0 219.38 188.25 68.90 o 12 11 0 178.90 194.67 71.03 o 14 11 0 111.52 164.56 83.36 o 1 12 0 177.51 108.66 40.76 o 2 12 0 2655.93 2440.41 89.00 o 3 12 0 2359.17 2784.89 97.10 o 5 12 0 39.37 171.96 74.97 o 6 12 0 2532.21 2563.68 115.43 o 8 12 0 1091.90 955.90 111.31 o 9 12 0 84.19 121.08 54.27 o 10 12 0 726.92 783.81 92.44 o 11 12 0 33.86 138.01 52.57 o 12 12 0 190.62 157.53 67.15 o 13 12 0 596.70 545.33 119.72 o 14 12 0 1.64 120.26 68.23 o 2 13 0 294.88 318.23 64.57 o 3 13 0 26463.06 26142.48 229.34 o 4 13 0 513.90 526.13 65.57 o 5 13 0 1669.62 1990.51 125.07 o 6 13 0 14.25 160.25 72.48 o 8 13 0 195.25 292.98 81.25 o 9 13 0 624.00 726.24 96.59 o 10 13 0 455.14 442.38 75.81 o 11 13 0 304.84 243.61 68.28 o 12 13 0 91.80 155.25 62.76 o 13 13 0 522.55 319.32 134.35 o 14 13 0 50.77 187.30 106.73 o 0 14 0 1361.06 1374.93 111.00 o 1 14 0 342.36 278.45 59.32 o 2 14 0 21005.73 20675.23 317.18 o 4 14 0 787.11 1032.83 84.29 o 6 14 0 277.75 236.11 52.69 o 7 14 0 41.61 218.80 75.69 o 8 14 0 1554.92 1366.96 102.65 o 9 14 0 16.14 123.78 49.54 o 10 14 0 3035.44 3128.73 160.92 o 11 14 0 435.41 277.98 74.04 o 12 14 0 105.61 185.52 88.61 o 13 14 0 1641.75 1270.24 196.57 o 2 15 0 202.65 232.80 46.14 o 3 15 0 370.21 561.79 70.98 o 5 15 0 228.93 267.44 57.58 o 6 15 0 1.23 140.58 56.96 o 7 15 0 136.16 174.10 56.07 o 8 15 0 57.51 128.84 56.72 o 9 15 0 65.12 134.30 59.12 o 10 15 0 532.50 456.42 107.46 o 11 15 0 161.04 265.07 105.82 o 13 15 0 482.47 248.50 130.32 o 0 16 0 549.18 602.15 103.69 o 1 16 0 685.34 734.06 78.60 o 2 16 0 8367.67 8166.72 218.14 o 3 16 0 604.17 840.82 81.26 o 4 16 0 285.97 262.98 56.05 o 6 16 0 32.31 206.08 99.33 o 7 16 0 596.53 678.29 99.02 o 8 16 0 754.43 680.45 96.62 o 9 16 0 139.83 169.04 73.27 o 10 16 0 240.70 271.84 97.56 o 11 16 0 1028.62 824.07 132.08 o 2 17 0 599.31 677.94 119.74 o 3 17 0 5490.11 5460.56 218.83 o 4 17 0 97.90 186.87 51.20 o 7 17 0 167.06 311.51 79.97 o 8 17 0 390.74 364.70 93.95 o 9 17 0 936.52 710.37 113.08 o 10 17 0 397.48 248.35 86.96 o 11 17 0 6.73 167.95 116.13 o 12 17 0 1780.11 1771.80 203.02 o 0 18 0 153.89 397.58 92.47 o 3 18 0 468.20 416.84 78.91 o 4 18 0 180.55 266.91 60.89 o 5 18 0 1384.62 1646.26 110.83 o 6 18 0 21.82 154.68 72.96 o 7 18 0 0.31 139.61 89.43 o 8 18 0 169.60 142.52 63.14 o 9 18 0 512.13 379.09 105.34 o 10 18 0 645.04 543.80 110.50 o 11 18 0 7.33 68.45 71.36 o 1 19 0 383.37 352.53 63.46 o 2 19 0 117.13 202.60 51.55 o 3 19 0 235.60 188.13 54.07 o 4 19 0 47.57 173.56 53.94 o 5 19 0 2745.09 2795.19 147.60 o 6 19 0 420.31 482.48 96.02 o 7 19 0 493.54 458.35 104.30 o 8 19 0 108.93 186.55 83.44 o 9 19 0 953.75 793.71 131.51 o 10 19 0 923.55 556.82 130.38 o 11 19 0 1047.81 875.80 167.47 o 0 20 0 2635.98 3083.85 221.37 o 1 20 0 92.95 226.42 69.88 o 2 20 0 3798.79 4075.65 183.17 o 3 20 0 133.11 165.46 55.97 o 4 20 0 1383.55 1501.61 128.13 o 5 20 0 107.16 165.77 58.11 o 6 20 0 1487.23 1574.00 133.12 o 7 20 0 8.30 104.23 67.88 o 8 20 0 1.77 82.66 53.52 o 9 20 0 1024.13 897.83 174.34 o 10 20 0 252.34 139.34 117.58 o 1 21 0 423.18 434.08 124.92 o 2 21 0 106.85 172.35 72.90 o 3 21 0 219.16 161.46 79.25 o 4 21 0 170.23 254.45 82.55 o 5 21 0 231.89 225.01 75.44 o 6 21 0 78.80 176.53 76.71 o 7 21 0 13.30 95.59 75.02 o 8 21 0 0.84 128.94 87.41 o 9 21 0 1432.19 1018.83 142.77 o 0 22 0 970.35 622.83 184.56 o 1 22 0 75.83 167.23 76.84 o 2 22 0 3.14 73.76 63.28 o 3 22 0 35.96 154.82 80.09 o 4 22 0 115.28 280.06 94.34 o 5 22 0 168.29 222.13 104.05 o 6 22 0 209.28 179.25 96.22 o 7 22 0 26.67 136.03 80.04 o 8 22 0 662.39 682.27 126.07 o 1 23 0 1030.06 882.63 124.37 o 2 23 0 81.21 105.57 65.27 o 3 23 0 635.19 628.71 128.26 o 4 23 0 8.64 114.25 69.18 o 5 23 0 1230.15 993.36 144.23 o 6 23 0 96.84 101.42 83.28 o 7 23 0 45.73 271.79 155.88 o 0 24 0 211.78 122.35 93.08 o 1 24 0 63.36 81.22 64.71 o 2 24 0 956.06 769.31 132.91 o 3 24 0 0.01 203.39 99.99 o 4 24 0 261.87 205.95 96.58 o 5 24 0 22.54 203.79 90.79 o 1 25 0 449.27 318.57 99.36 o 2 25 0 71.14 103.24 76.46 o -15 0 1 1014.62 1229.27 205.26 o -13 0 1 712.36 869.75 158.63 o -11 0 1 9791.93 10142.52 189.83 o -9 0 1 6701.37 7325.51 300.12 o -7 0 1 42.94 88.46 54.58 o -5 0 1 194.43 164.47 64.51 o -3 0 1 15355.98 14491.43 136.85 o 3 0 1 821.54 715.67 74.39 o 5 0 1 720.13 591.57 79.79 o 7 0 1 466.52 484.48 85.23 o 9 0 1 46.80 72.24 45.37 o 11 0 1 375.64 370.11 73.82 o 13 0 1 626.61 658.75 184.74 o 15 0 1 158.90 90.30 96.66 o -16 1 1 111.19 126.53 98.88 o -15 1 1 203.04 321.69 100.02 o -14 1 1 1075.67 1124.64 123.93 o -13 1 1 2.32 133.01 56.88 o -12 1 1 1049.25 1074.87 124.48 o -11 1 1 896.23 884.90 90.39 o -10 1 1 2138.02 2058.64 81.46 o -9 1 1 6.22 100.88 39.78 o -8 1 1 84.28 107.34 31.65 o -7 1 1 135.28 147.74 35.28 o -6 1 1 560.52 649.49 54.91 o -5 1 1 410.79 343.30 51.64 o -4 1 1 5514.50 4759.03 100.12 o -3 1 1 2569.41 2593.19 92.63 o -2 1 1 13241.34 12518.69 81.52 o 2 1 1 14971.94 15110.25 73.65 o 3 1 1 13.75 49.42 22.58 o 5 1 1 3.15 60.70 25.35 o 6 1 1 2092.51 2179.45 70.43 o 7 1 1 2292.05 2215.19 70.11 o 8 1 1 52.57 86.39 31.99 o 9 1 1 1110.83 1037.17 63.16 o 10 1 1 187.81 196.02 47.75 o 11 1 1 51.97 117.09 38.61 o 12 1 1 53.04 109.13 50.62 o 13 1 1 243.18 292.07 76.69 o 14 1 1 3.30 136.09 89.84 o 15 1 1 1307.02 1199.53 159.20 o 16 1 1 60.94 75.73 74.48 o -16 2 1 117.40 193.40 109.81 o -15 2 1 1692.76 1588.97 144.87 o -14 2 1 89.03 175.02 80.01 o -13 2 1 576.60 616.40 104.81 o -12 2 1 205.12 197.30 57.42 o -11 2 1 712.41 754.39 85.96 o -10 2 1 1339.51 1182.23 77.03 o -9 2 1 14591.55 14428.09 148.55 o -8 2 1 0.96 81.96 30.04 o -7 2 1 3364.72 3304.87 85.72 o -6 2 1 62.76 84.38 30.47 o -5 2 1 17260.48 17979.45 109.22 o -4 2 1 2852.38 2455.29 66.52 o -3 2 1 6488.19 6288.83 119.04 o -2 2 1 20868.84 20628.01 173.99 o 2 2 1 32173.33 32518.15 117.56 o 3 2 1 1023.74 887.03 53.34 o 4 2 1 494.17 691.05 124.05 o 5 2 1 270.61 183.01 37.39 o 6 2 1 4855.80 5170.26 86.37 o 7 2 1 215.87 222.33 36.70 o 9 2 1 147.62 150.85 35.96 o 10 2 1 1011.85 1091.61 74.38 o 11 2 1 204.67 250.50 45.56 o 12 2 1 1766.94 1722.56 98.24 o 13 2 1 27.86 71.07 59.10 o 14 2 1 1833.75 1661.04 140.87 o 15 2 1 2.31 192.85 100.40 o 16 2 1 75.04 185.76 101.96 o -16 3 1 15.49 190.41 95.55 o -15 3 1 214.41 182.48 87.45 o -14 3 1 1888.60 1886.42 138.33 o -13 3 1 61.43 186.01 63.14 o -12 3 1 20.31 116.76 45.76 o -11 3 1 107.24 93.98 48.57 o -10 3 1 136.31 118.48 55.35 o -9 3 1 227.19 165.81 34.84 o -8 3 1 5379.26 5060.63 114.21 o -6 3 1 567.82 758.25 77.04 o -5 3 1 4237.20 3881.43 66.72 o -4 3 1 762.80 593.02 69.36 o -3 3 1 2462.98 2451.16 91.98 o -2 3 1 30867.81 30179.05 251.81 o -1 3 1 1025.46 1338.56 70.31 o 0 3 1 12823.59 12439.97 74.25 o 1 3 1 140.91 202.04 26.21 o 2 3 1 9268.46 8961.50 90.96 o 3 3 1 1052.87 1043.92 58.39 o 4 3 1 750.81 758.10 45.10 o 5 3 1 13758.09 13397.36 104.96 o 6 3 1 22.42 56.10 21.38 o 7 3 1 9494.12 9340.00 105.98 o 8 3 1 57.82 116.34 34.04 o 9 3 1 315.95 278.12 52.44 o 10 3 1 5.00 70.49 29.85 o 11 3 1 35249.66 37296.86 337.57 o 12 3 1 13.03 120.77 43.60 o 13 3 1 212.52 291.72 73.11 o 14 3 1 59.64 157.15 74.89 o 15 3 1 13.03 96.29 82.45 o 16 3 1 0.00 50.73 62.05 o -16 4 1 52.20 153.68 82.75 o -15 4 1 367.37 319.07 92.39 o -14 4 1 360.23 250.86 66.92 o -13 4 1 254.50 365.92 74.27 o -12 4 1 105.88 141.85 41.77 o -11 4 1 1969.20 2169.53 105.75 o -10 4 1 368.27 314.84 65.08 o -9 4 1 3450.89 3186.95 72.82 o -8 4 1 115.36 141.97 46.06 o -7 4 1 14819.41 15982.75 148.47 o -6 4 1 11.54 40.32 25.24 o -4 4 1 7559.13 6909.21 102.20 o -3 4 1 3882.52 4267.90 134.59 o -2 4 1 3070.40 2745.84 88.19 o -1 4 1 347.23 472.39 41.90 o 0 4 1 9260.56 9157.44 75.23 o 1 4 1 1441.61 1557.29 81.26 o 2 4 1 690.25 729.28 46.62 o 4 4 1 4938.71 5563.33 85.30 o 5 4 1 3718.72 3677.11 76.22 o 6 4 1 9105.95 8807.88 104.39 o 7 4 1 372.58 358.30 36.93 o 8 4 1 0.31 39.82 24.14 o 9 4 1 628.14 590.71 62.63 o 10 4 1 4527.01 4373.09 133.26 o 11 4 1 407.06 555.48 80.57 o 12 4 1 1225.92 1258.25 95.62 o 13 4 1 0.44 71.87 47.29 o 14 4 1 818.15 711.99 110.89 o 15 4 1 15.89 60.63 68.01 o 16 4 1 155.33 176.47 121.01 o -16 5 1 172.37 231.79 92.69 o 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