#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/41/2224111.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2224111_Fobs loop_ _publ_author_name 'Zhang, Yun-Liang' 'Liu, Ti-Lou' 'Sun, Shuang-Jiao' _publ_section_title ; Tetraaquabis[3-(3-pyridyl)-5-(4-pyridyl)-1,2,4-triazolido]nickel(II) dihydrate ; _journal_coeditor_code BG2306 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1590 _journal_volume 65 _journal_year 2009 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 90.700 _cell_angle_beta 104.960 _cell_angle_gamma 96.470 _cell_length_a 8.2240 _cell_length_b 9.1990 _cell_length_c 9.3850 _exptl_crystal_F_000 267.96 _reflns_d_resolution_high 0.8337 _[local]_cod_data_source_file bg2306Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' AA in P1 New: P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 94.80 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 646.82 695.35 19.74 o 3 0 0 102.90 109.59 3.56 o 4 0 0 203.75 128.00 59.33 o 5 0 0 1.39 1.41 1.68 o 6 0 0 26.82 29.68 5.00 o 7 0 0 10.17 16.65 4.90 o 8 0 0 328.91 337.03 28.71 o 9 0 0 10.39 9.67 4.87 o -9 1 0 12.82 11.65 5.44 o -8 1 0 37.01 37.82 3.82 o -7 1 0 440.13 469.70 27.89 o -6 1 0 262.40 311.41 12.63 o -5 1 0 741.00 858.73 26.74 o -4 1 0 100.74 112.81 4.25 o -3 1 0 12.35 17.54 3.46 o -2 1 0 910.76 963.02 17.50 o -1 1 0 329.83 333.20 4.89 o 1 1 0 2613.59 1505.00 155.54 o 2 1 0 222.20 215.21 4.75 o 3 1 0 511.41 529.34 13.42 o 4 1 0 2291.76 2574.32 69.03 o 5 1 0 559.92 626.02 20.89 o 6 1 0 38.89 42.52 3.59 o 7 1 0 0.92 1.61 1.98 o 8 1 0 103.27 106.14 12.79 o 9 1 0 201.46 202.71 21.83 o -9 2 0 13.47 13.70 6.31 o -8 2 0 58.02 64.81 9.33 o -7 2 0 102.16 105.30 10.54 o -6 2 0 93.02 91.29 7.20 o -5 2 0 48.84 57.45 2.99 o -4 2 0 7.01 12.61 1.31 o -3 2 0 1211.70 1318.85 38.11 o -2 2 0 1132.62 1126.58 22.44 o -1 2 0 2931.68 3096.05 45.19 o 0 2 0 439.71 474.13 6.34 o 1 2 0 262.86 300.97 17.51 o 2 2 0 903.15 775.18 118.70 o 3 2 0 1435.29 1150.55 118.80 o 4 2 0 2.30 7.59 2.43 o 5 2 0 29.97 38.59 2.67 o 6 2 0 15.47 11.09 3.44 o 7 2 0 42.30 46.23 4.80 o 8 2 0 5.66 7.82 2.01 o 9 2 0 18.90 20.18 6.82 o -9 3 0 65.90 72.26 12.96 o -8 3 0 66.81 71.39 9.91 o -7 3 0 6.84 11.98 2.19 o -6 3 0 272.38 275.32 11.54 o -5 3 0 532.10 549.52 17.87 o -4 3 0 78.45 69.43 3.32 o -3 3 0 258.24 242.50 22.93 o -2 3 0 2525.35 2507.23 51.14 o -1 3 0 286.24 265.69 7.20 o 0 3 0 429.35 404.76 27.25 o 1 3 0 1529.73 1866.98 72.88 o 2 3 0 1405.35 1472.75 28.23 o 3 3 0 650.70 721.72 32.24 o 4 3 0 1.28 2.25 1.01 o 5 3 0 5.35 11.55 4.72 o 6 3 0 80.99 86.82 5.61 o 7 3 0 53.47 55.89 4.86 o 8 3 0 138.19 142.13 10.47 o -9 4 0 8.08 10.54 6.04 o -8 4 0 18.16 19.31 5.71 o -7 4 0 6.04 4.05 1.76 o -6 4 0 30.91 31.65 2.84 o -5 4 0 43.99 49.96 3.45 o -4 4 0 897.20 933.35 27.85 o -3 4 0 496.74 473.81 12.03 o -2 4 0 3012.97 3321.35 69.75 o -1 4 0 4210.76 4627.51 106.86 o 0 4 0 682.46 634.62 16.27 o 1 4 0 873.72 967.86 40.16 o 2 4 0 622.16 605.42 26.33 o 3 4 0 486.36 398.65 9.00 o 4 4 0 420.89 439.13 13.24 o 5 4 0 236.63 236.98 9.61 o 6 4 0 544.16 463.48 27.50 o 7 4 0 135.85 134.72 8.78 o 8 4 0 28.71 25.55 4.90 o -8 5 0 96.26 101.21 13.06 o -7 5 0 404.01 426.41 35.22 o -6 5 0 491.88 466.20 18.82 o -5 5 0 22.53 20.26 2.33 o -4 5 0 148.71 156.90 6.16 o -3 5 0 276.68 287.90 9.74 o -2 5 0 158.90 146.98 5.80 o -1 5 0 368.12 390.56 10.90 o 0 5 0 302.65 278.32 13.41 o 1 5 0 22.79 18.00 3.26 o 2 5 0 179.55 160.77 9.37 o 3 5 0 4.25 5.14 1.44 o 4 5 0 92.23 97.65 9.07 o 5 5 0 1.30 2.05 2.12 o 6 5 0 48.70 50.67 7.62 o 7 5 0 263.29 226.89 17.73 o -8 6 0 99.04 100.60 13.20 o -7 6 0 0.93 0.71 2.15 o -6 6 0 0.86 2.38 2.05 o -5 6 0 3.14 7.77 1.58 o -4 6 0 82.28 83.62 5.73 o -3 6 0 284.34 281.16 11.92 o -2 6 0 370.41 385.68 13.42 o -1 6 0 379.37 385.33 27.35 o 0 6 0 1036.46 1172.19 61.52 o 1 6 0 401.95 442.43 26.39 o 2 6 0 430.26 374.13 19.71 o 3 6 0 9.16 11.95 3.56 o 4 6 0 4.17 3.09 2.69 o 5 6 0 20.53 26.09 5.51 o 6 6 0 14.15 13.60 4.94 o 7 6 0 1.07 1.78 2.28 o -8 7 0 34.71 24.65 5.53 o -7 7 0 83.05 77.56 8.27 o -6 7 0 28.30 29.33 4.77 o -5 7 0 150.82 142.56 9.60 o -4 7 0 364.26 385.17 18.61 o -3 7 0 793.97 772.28 28.91 o -2 7 0 5.14 5.92 1.65 o -1 7 0 33.02 39.42 6.04 o 0 7 0 413.30 471.17 32.34 o 1 7 0 899.50 1059.30 66.12 o 2 7 0 75.64 76.96 6.92 o 3 7 0 74.94 70.48 8.19 o 4 7 0 85.58 90.70 9.00 o 5 7 0 352.70 337.50 25.12 o 6 7 0 22.20 23.97 6.25 o -7 8 0 1.53 0.79 1.89 o -6 8 0 76.79 76.90 8.19 o -5 8 0 440.05 419.70 23.23 o -4 8 0 186.38 166.43 9.92 o -3 8 0 219.56 227.50 11.38 o -2 8 0 211.63 240.96 22.36 o -1 8 0 80.65 82.23 8.76 o 0 8 0 65.87 78.14 11.62 o 1 8 0 348.58 426.55 37.91 o 2 8 0 180.59 177.83 16.05 o 3 8 0 78.00 72.09 9.60 o 4 8 0 37.64 25.89 4.60 o 5 8 0 298.40 266.14 22.60 o -6 9 0 68.65 61.56 7.64 o -5 9 0 29.23 26.59 4.67 o -4 9 0 73.96 52.96 5.88 o -3 9 0 7.36 7.69 4.06 o -2 9 0 341.00 311.24 26.96 o -1 9 0 667.16 718.78 54.16 o 0 9 0 325.09 398.58 34.12 o 1 9 0 11.07 16.22 7.19 o 2 9 0 15.86 21.02 6.31 o 3 9 0 30.71 30.25 6.14 o 4 9 0 9.61 8.56 3.46 o -5 10 0 59.99 70.38 13.40 o -4 10 0 32.50 33.21 7.89 o -3 10 0 102.44 95.93 12.86 o -2 10 0 168.75 187.23 20.21 o -1 10 0 97.89 120.78 16.32 o 0 10 0 102.67 130.92 21.09 o 1 10 0 1.91 -0.13 2.65 o 2 10 0 1.03 10.51 4.67 o -1 11 0 100.94 117.52 17.53 o 1 -11 1 140.52 153.12 20.18 o -3 -10 1 59.86 74.61 11.52 o -2 -10 1 123.07 163.90 25.22 o -1 -10 1 367.75 486.45 51.61 o 0 -10 1 454.21 519.63 46.74 o 1 -10 1 177.23 210.34 25.15 o 2 -10 1 335.99 295.56 28.17 o 3 -10 1 27.07 24.34 6.61 o 4 -10 1 3.81 7.79 4.40 o -4 -9 1 12.23 18.50 4.67 o -3 -9 1 17.73 20.62 6.55 o -2 -9 1 58.56 66.42 11.28 o -1 -9 1 50.56 60.91 12.59 o 0 -9 1 109.75 125.55 14.47 o 1 -9 1 53.83 52.52 7.96 o 2 -9 1 20.75 34.12 8.73 o 3 -9 1 376.33 320.17 15.89 o 4 -9 1 234.40 197.57 12.20 o 5 -9 1 86.34 84.17 8.68 o 6 -9 1 3.50 6.88 6.77 o -5 -8 1 59.12 59.67 8.70 o -4 -8 1 160.92 111.31 9.13 o -3 -8 1 360.66 310.43 22.97 o -2 -8 1 567.58 682.18 54.90 o -1 -8 1 506.87 553.51 41.57 o 0 -8 1 163.37 179.01 16.18 o 1 -8 1 355.97 396.26 33.54 o 2 -8 1 58.62 49.39 3.95 o 3 -8 1 5.00 4.18 2.15 o 4 -8 1 13.43 17.59 5.24 o 5 -8 1 35.95 33.97 4.90 o 6 -8 1 0.61 0.72 1.64 o 7 -8 1 0.45 -0.03 2.10 o -6 -7 1 123.48 107.59 11.38 o -5 -7 1 13.49 18.57 4.60 o -4 -7 1 263.97 188.11 12.79 o -3 -7 1 154.96 126.56 11.11 o -2 -7 1 99.69 110.10 13.20 o -1 -7 1 129.79 149.69 13.23 o 0 -7 1 252.16 260.47 17.80 o 1 -7 1 354.25 379.97 20.30 o 2 -7 1 542.11 506.77 19.32 o 3 -7 1 100.52 96.07 6.22 o 4 -7 1 299.95 311.65 15.76 o 5 -7 1 266.65 237.00 14.40 o 6 -7 1 135.61 138.32 10.62 o 7 -7 1 62.94 75.63 8.16 o -7 -6 1 12.15 12.32 4.06 o -6 -6 1 122.02 116.48 10.54 o -5 -6 1 270.86 269.30 21.05 o -4 -6 1 108.30 77.94 6.68 o -3 -6 1 95.03 80.08 7.49 o -2 -6 1 1174.76 1294.82 71.45 o -1 -6 1 903.56 992.65 53.42 o 0 -6 1 878.83 862.69 65.18 o 1 -6 1 111.36 107.69 4.99 o 2 -6 1 291.61 301.94 11.82 o 3 -6 1 270.35 281.93 18.77 o 4 -6 1 97.99 107.78 7.13 o 5 -6 1 136.11 145.08 10.37 o 6 -6 1 209.65 197.21 18.27 o 7 -6 1 11.18 21.83 5.34 o 8 -6 1 57.24 45.90 8.73 o -8 -5 1 78.86 70.11 8.39 o -7 -5 1 300.34 256.44 19.61 o -6 -5 1 59.39 62.22 6.38 o -5 -5 1 9.13 10.27 2.65 o -4 -5 1 6.96 7.45 2.08 o -3 -5 1 51.34 51.51 5.14 o -2 -5 1 242.54 234.14 14.37 o -1 -5 1 2224.75 2344.04 104.40 o 0 -5 1 506.87 528.43 22.82 o 1 -5 1 14.27 13.27 1.39 o 2 -5 1 62.17 79.74 4.17 o 3 -5 1 8.83 7.86 1.81 o 4 -5 1 26.39 26.80 4.63 o 5 -5 1 121.75 107.49 5.22 o 6 -5 1 67.48 69.71 8.19 o 7 -5 1 401.68 406.87 31.70 o 8 -5 1 86.37 92.24 12.63 o -8 -4 1 13.22 12.99 4.23 o -7 -4 1 21.35 26.95 3.44 o -6 -4 1 255.17 241.59 10.47 o -5 -4 1 15.15 11.36 1.39 o -4 -4 1 186.72 183.03 6.49 o -3 -4 1 1979.52 2128.67 51.99 o -2 -4 1 809.23 844.85 18.89 o -1 -4 1 397.06 354.33 14.44 o 0 -4 1 16.16 10.76 2.42 o 1 -4 1 256.12 269.94 8.18 o 2 -4 1 1844.96 2038.48 56.57 o 3 -4 1 352.47 364.59 17.66 o 4 -4 1 161.82 150.92 5.51 o 5 -4 1 2.86 4.25 1.23 o 6 -4 1 102.87 108.73 10.34 o 7 -4 1 32.51 31.56 6.38 o 8 -4 1 65.94 74.68 12.73 o -8 -3 1 102.23 99.09 8.12 o -7 -3 1 116.49 121.61 7.95 o -6 -3 1 82.63 78.22 4.93 o -5 -3 1 499.91 476.52 16.15 o -4 -3 1 105.98 71.99 13.46 o -3 -3 1 1461.97 1114.11 24.81 o -2 -3 1 396.64 441.85 25.07 o -1 -3 1 56.37 50.77 5.31 o 0 -3 1 42.54 52.50 1.74 o 1 -3 1 1074.64 1191.70 28.57 o 2 -3 1 2044.67 2170.34 75.99 o 3 -3 1 1785.22 1953.81 110.59 o 4 -3 1 1.32 1.13 0.55 o 5 -3 1 493.84 485.60 17.51 o 6 -3 1 383.35 395.08 28.91 o 7 -3 1 191.57 207.98 20.35 o 8 -3 1 39.47 35.32 7.59 o 9 -3 1 13.45 13.46 5.44 o -9 -2 1 67.02 71.29 11.75 o -8 -2 1 34.53 35.75 4.72 o -7 -2 1 1.14 4.91 1.83 o -6 -2 1 15.30 18.33 2.35 o -5 -2 1 436.60 446.19 21.83 o -4 -2 1 1171.76 1295.92 35.45 o -3 -2 1 1760.78 1620.93 34.62 o -2 -2 1 1054.93 1051.71 31.50 o -1 -2 1 926.50 578.31 103.44 o 0 -2 1 3181.49 3600.28 63.31 o 1 -2 1 2463.70 2625.16 73.57 o 2 -2 1 108.41 127.81 3.39 o 3 -2 1 194.15 203.25 4.88 o 4 -2 1 7.23 9.92 0.82 o 5 -2 1 329.15 332.43 10.60 o 6 -2 1 217.63 212.55 10.39 o 7 -2 1 311.74 343.44 26.73 o 8 -2 1 143.93 160.03 18.67 o 9 -2 1 143.54 135.46 19.61 o -9 -1 1 15.00 24.88 7.42 o -8 -1 1 331.94 324.90 25.75 o -7 -1 1 21.89 19.51 4.03 o -6 -1 1 23.21 20.48 2.21 o -5 -1 1 105.04 112.51 4.81 o -4 -1 1 1581.87 1787.48 67.14 o -3 -1 1 339.04 313.57 30.05 o -2 -1 1 3274.54 3442.66 88.31 o -1 -1 1 21.61 17.80 0.71 o 0 -1 1 2711.59 1572.14 24.75 o 1 -1 1 424.76 495.05 13.94 o 2 -1 1 2.31 4.03 0.29 o 3 -1 1 630.80 737.38 29.11 o 4 -1 1 173.10 153.76 8.90 o 5 -1 1 538.25 615.09 33.98 o 6 -1 1 285.71 336.70 13.05 o 7 -1 1 172.42 162.35 13.50 o 8 -1 1 2.77 10.51 5.27 o 9 -1 1 6.47 5.57 4.94 o -9 0 1 3.41 8.37 2.68 o -8 0 1 0.89 0.74 2.18 o -7 0 1 245.28 227.80 16.69 o -6 0 1 75.16 77.63 7.62 o -5 0 1 37.27 26.66 3.76 o -4 0 1 320.47 308.36 19.78 o -3 0 1 760.61 693.66 15.02 o -2 0 1 678.13 672.68 16.45 o 1 0 1 1009.17 1106.98 19.10 o 2 0 1 91.93 113.36 3.19 o 3 0 1 453.16 488.49 13.41 o 4 0 1 54.54 44.56 3.86 o 5 0 1 0.94 0.54 1.58 o 6 0 1 306.59 340.59 22.20 o 7 0 1 158.52 171.59 16.92 o 8 0 1 94.46 100.40 13.73 o 9 0 1 76.68 75.11 11.48 o -9 1 1 276.76 245.19 14.40 o -8 1 1 26.21 23.77 3.49 o -7 1 1 45.21 44.01 5.66 o -6 1 1 49.70 55.97 4.14 o -5 1 1 912.66 1025.90 40.97 o -4 1 1 209.56 180.68 6.41 o -3 1 1 1000.78 1019.86 33.31 o -2 1 1 1148.71 1187.20 28.74 o 0 1 1 605.42 511.52 88.48 o 1 1 1 3799.24 125.82 3.32 o 2 1 1 63.20 71.14 2.25 o 3 1 1 1085.71 1241.69 32.15 o 4 1 1 34.81 42.25 2.68 o 5 1 1 56.00 53.70 3.98 o 6 1 1 5.41 6.23 2.35 o 7 1 1 231.53 249.62 20.79 o 8 1 1 167.98 171.12 18.67 o 9 1 1 154.60 139.12 18.64 o -9 2 1 12.60 12.09 5.44 o -8 2 1 23.68 21.50 3.13 o -7 2 1 262.73 265.78 12.60 o -6 2 1 731.20 726.63 26.95 o -5 2 1 1555.37 1627.59 49.96 o -4 2 1 2336.57 2599.54 71.05 o -3 2 1 83.84 86.85 5.89 o -2 2 1 255.99 232.63 10.67 o -1 2 1 961.01 1036.06 21.57 o 0 2 1 210.11 226.69 16.25 o 1 2 1 64.98 52.30 4.63 o 2 2 1 136.80 149.58 11.05 o 3 2 1 205.87 211.80 31.61 o 4 2 1 909.91 1049.38 31.81 o 5 2 1 163.56 181.45 8.62 o 6 2 1 153.01 164.11 8.81 o 7 2 1 144.22 160.89 10.11 o 8 2 1 58.62 57.59 9.67 o -9 3 1 2.24 -0.77 2.95 o -8 3 1 46.93 46.35 4.78 o -7 3 1 0.58 4.59 2.57 o -6 3 1 753.36 770.33 28.98 o -5 3 1 187.80 161.91 7.61 o -4 3 1 272.21 318.60 10.62 o -3 3 1 828.06 888.74 19.45 o -2 3 1 1873.10 1854.60 35.32 o -1 3 1 2058.74 2188.50 81.33 o 0 3 1 6.91 10.28 1.06 o 1 3 1 2.26 4.61 0.69 o 2 3 1 905.99 988.56 20.40 o 3 3 1 60.13 54.31 3.32 o 4 3 1 403.26 393.61 20.42 o 5 3 1 54.39 39.76 6.70 o 6 3 1 59.71 62.78 4.52 o 7 3 1 0.56 1.48 4.05 o 8 3 1 2.28 8.59 3.07 o -9 4 1 51.14 53.32 9.23 o -8 4 1 295.86 269.10 14.27 o -7 4 1 23.01 22.63 6.06 o -6 4 1 1.16 5.16 1.59 o -5 4 1 2.27 2.02 1.23 o -4 4 1 1.58 6.96 2.65 o -3 4 1 529.73 519.65 13.08 o -2 4 1 2373.83 2527.13 52.68 o -1 4 1 1040.59 1094.60 42.46 o 0 4 1 73.96 83.49 2.03 o 1 4 1 878.74 1026.49 41.74 o 2 4 1 60.58 37.61 2.82 o 3 4 1 223.73 220.10 6.42 o 4 4 1 3.05 4.00 0.89 o 5 4 1 96.95 91.49 4.67 o 6 4 1 551.25 484.91 28.74 o 7 4 1 323.19 271.92 19.27 o 8 4 1 189.09 169.07 16.65 o -9 5 1 7.10 1.81 3.90 o -8 5 1 119.04 107.22 13.30 o -7 5 1 298.58 277.98 14.42 o -6 5 1 90.52 104.98 9.82 o -5 5 1 147.74 148.29 6.31 o -4 5 1 1312.53 1311.55 35.65 o -3 5 1 1152.47 1179.78 30.33 o -2 5 1 492.67 500.84 12.80 o -1 5 1 35.06 27.57 1.32 o 0 5 1 701.09 787.78 36.80 o 1 5 1 1163.87 1351.90 66.28 o 2 5 1 487.19 508.95 26.83 o 3 5 1 58.92 58.70 6.85 o 4 5 1 187.44 188.01 13.26 o 5 5 1 1.25 3.09 2.32 o 6 5 1 77.46 70.38 7.56 o 7 5 1 111.50 108.02 10.91 o -8 6 1 88.28 104.65 10.28 o -7 6 1 208.25 191.67 9.84 o -6 6 1 243.17 238.29 10.33 o -5 6 1 307.73 307.31 11.93 o -4 6 1 484.38 457.45 14.79 o -3 6 1 1090.50 1090.39 30.53 o -2 6 1 3.84 14.62 10.81 o -1 6 1 58.61 53.60 2.67 o 0 6 1 111.06 114.94 9.10 o 1 6 1 501.20 559.25 33.85 o 2 6 1 139.30 137.71 11.18 o 3 6 1 1.04 3.63 1.68 o 4 6 1 9.27 8.76 3.79 o 5 6 1 497.22 489.74 32.40 o 6 6 1 82.30 99.26 12.93 o 7 6 1 54.67 47.98 9.13 o -8 7 1 0.77 9.28 6.93 o -7 7 1 24.01 25.47 3.29 o -6 7 1 28.69 26.06 3.10 o -5 7 1 57.24 59.05 4.53 o -4 7 1 31.04 26.97 3.52 o -3 7 1 102.65 105.64 6.36 o -2 7 1 299.69 290.48 10.73 o -1 7 1 252.57 285.11 21.99 o 0 7 1 869.87 1117.02 70.11 o 1 7 1 612.44 683.29 45.40 o 2 7 1 17.44 21.83 3.79 o 3 7 1 129.41 99.80 7.62 o 4 7 1 18.06 12.56 4.87 o 5 7 1 7.39 5.44 3.22 o 6 7 1 20.92 22.20 7.09 o -7 8 1 20.68 25.86 5.06 o -6 8 1 193.48 169.17 12.23 o -5 8 1 496.34 450.87 23.05 o -4 8 1 535.31 491.09 23.11 o -3 8 1 1.05 4.27 2.43 o -2 8 1 160.20 169.50 14.07 o -1 8 1 17.03 13.40 4.40 o 0 8 1 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