#------------------------------------------------------------------------------ #$Date: 2010-01-22 14:33:52 +0200 (Fri, 22 Jan 2010) $ #$Revision: 960 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2224132.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2224132_Fobs loop_ _publ_author_name 'Li, Yang' 'Shi, Qi' 'Slawin, Alexandra M. Z.' 'Woollins, J. Derek' 'Dong, Jinxiang' _publ_section_title ; Tris(ethylenediamine)zinc(II) hexafluoridosilicate ; _journal_coeditor_code BT5123 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1522 _journal_volume 65 _journal_year 2009 _space_group_IT_number 182 _symmetry_space_group_name_Hall 'P 6c 2c' _symmetry_space_group_name_H-M 'P 63 2 2' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 120.000 _cell_length_a 9.1920 _cell_length_b 9.1920 _cell_length_c 9.7550 _exptl_crystal_F_000 400.00 _reflns_d_resolution_high 0.7732 _[local]_cod_data_source_file bt5123Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P63_fs in P6(3) P6322' _shelx_refln_list_code 4 _shelx_f_calc_maximum 96.75 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x-y, x, z+1/2' '-y, x-y, z' '-x, -y, z+1/2' '-x+y, -x, z' 'y, -x+y, z+1/2' '-y, -x, -z+1/2' 'x-y, -y, -z' 'x, x-y, -z+1/2' 'y, x, -z' '-x+y, y, -z+1/2' '-x, -x+y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status -1 2 0 6077.48 5923.60 133.14 o 0 2 0 5171.12 5171.74 117.73 o -1 3 0 165.98 135.73 1.60 o 0 3 0 197.89 144.08 4.45 o -2 4 0 1545.80 1442.29 20.70 o -1 4 0 188.81 168.88 2.26 o 0 4 0 1423.67 1473.26 30.42 o -2 5 0 8.22 11.79 0.70 o -1 5 0 3925.36 3897.92 63.62 o 0 5 0 2704.77 2792.89 79.70 o -3 6 0 419.30 393.70 8.23 o -2 6 0 586.08 602.82 9.02 o -1 6 0 2092.33 2076.04 31.51 o 0 6 0 9361.44 9915.91 576.59 o -3 7 0 577.32 574.72 9.57 o -2 7 0 1662.41 1699.85 29.97 o -1 7 0 649.02 670.37 14.48 o 0 7 0 35.55 35.75 6.24 o -4 8 0 871.90 840.67 41.55 o -3 8 0 42.06 37.90 2.56 o -2 8 0 666.40 643.27 10.37 o -1 8 0 1631.63 1707.20 47.77 o 0 8 0 772.86 824.05 58.39 o -4 9 0 38.83 25.76 5.43 o -3 9 0 581.49 606.50 12.66 o -2 9 0 327.84 341.56 10.52 o -1 9 0 223.84 217.41 8.58 o 0 9 0 408.65 448.10 37.99 o -5 10 0 1053.97 1041.05 76.12 o -4 10 0 197.02 183.61 12.87 o -3 10 0 218.33 191.74 10.99 o -2 10 0 485.58 484.08 22.85 o -1 10 0 57.39 45.54 6.57 o 0 10 0 192.39 165.25 23.41 o -5 11 0 230.73 226.25 19.25 o -4 11 0 294.23 260.52 15.32 o -3 11 0 9.94 6.39 6.31 o -2 11 0 11.27 7.65 6.58 o 0 1 1 399.48 345.12 1.93 o -1 2 1 185.67 156.48 0.90 o 0 2 1 1417.68 1393.88 11.80 o -2 3 1 1788.24 1755.01 17.26 o -1 3 1 1759.75 1750.66 23.87 o 0 3 1 68.56 63.43 1.52 o -3 4 1 1682.30 1673.80 14.24 o -2 4 1 15.51 19.68 0.70 o -1 4 1 1669.06 1697.96 24.29 o 0 4 1 769.16 764.30 11.85 o -4 5 1 290.59 301.79 4.79 o -3 5 1 1337.24 1374.15 14.80 o -2 5 1 1484.13 1526.50 19.33 o -1 5 1 289.92 302.23 3.85 o 0 5 1 1405.72 1480.94 25.20 o -5 6 1 224.08 229.27 4.67 o -4 6 1 125.17 107.51 2.50 o -3 6 1 494.22 509.68 6.02 o -2 6 1 122.82 110.73 3.14 o -1 6 1 278.68 275.76 5.01 o 0 6 1 2.17 2.28 1.48 o -6 7 1 44.21 43.66 2.74 o -5 7 1 234.48 244.80 6.06 o -4 7 1 421.31 423.68 6.38 o -3 7 1 462.82 444.37 12.12 o -2 7 1 234.16 242.12 5.42 o -1 7 1 81.64 69.97 3.76 o 0 7 1 25.21 29.96 4.02 o -7 8 1 111.29 114.65 4.62 o -6 8 1 64.63 53.16 3.20 o -5 8 1 229.99 233.94 6.32 o -4 8 1 64.82 59.99 2.44 o -3 8 1 254.27 258.87 6.66 o -2 8 1 23.70 15.54 3.35 o -1 8 1 111.34 110.18 6.94 o 0 8 1 64.19 56.73 4.23 o -8 9 1 122.00 115.86 6.42 o -7 9 1 278.14 303.54 11.73 o -6 9 1 81.40 63.37 4.45 o -5 9 1 428.76 441.43 15.85 o -4 9 1 375.12 374.63 10.21 o -3 9 1 81.67 69.83 5.22 o -2 9 1 286.38 302.03 16.00 o -1 9 1 147.64 145.98 6.02 o 0 9 1 39.21 21.81 3.87 o -9 10 1 127.79 124.71 11.81 o -8 10 1 18.13 22.73 4.55 o -7 10 1 131.74 137.35 7.03 o -6 10 1 210.60 234.08 13.29 o -5 10 1 45.64 48.15 3.57 o -4 10 1 198.87 199.76 11.51 o -3 10 1 109.41 100.73 9.49 o -2 10 1 18.16 11.67 5.41 o -1 10 1 131.92 129.16 9.61 o 0 10 1 186.98 191.78 31.71 o -9 11 1 130.19 89.59 13.36 o -8 11 1 79.06 89.01 9.53 o -7 11 1 33.68 15.68 6.41 o -6 11 1 217.25 203.76 17.91 o -5 11 1 215.38 196.77 17.78 o -4 11 1 33.82 20.89 6.47 o -3 11 1 64.57 41.94 7.74 o -2 11 1 171.66 148.28 10.31 o 0 1 2 1377.60 1405.37 13.08 o -1 2 2 4877.11 4806.08 64.00 o 0 2 2 2271.10 2258.46 23.03 o -2 3 2 5235.21 5405.91 91.97 o -1 3 2 5598.35 5628.82 85.13 o 0 3 2 2549.60 2379.50 29.75 o -3 4 2 2254.29 2272.71 25.08 o -2 4 2 4554.88 4396.48 67.98 o -1 4 2 2034.36 1984.77 25.61 o 0 4 2 1166.79 1122.49 11.63 o -4 5 2 2338.22 2258.02 26.29 o -3 5 2 1491.98 1537.47 19.16 o -2 5 2 1685.32 1696.00 19.83 o -1 5 2 2415.23 2386.30 33.45 o 0 5 2 917.75 929.55 10.71 o -5 6 2 715.01 708.21 8.00 o -4 6 2 747.51 764.39 9.29 o -3 6 2 1772.21 1789.35 22.30 o -2 6 2 781.31 817.07 9.72 o -1 6 2 738.51 737.48 9.06 o 0 6 2 3194.31 3130.68 64.70 o -6 7 2 369.36 355.26 7.11 o -5 7 2 1502.17 1486.45 30.02 o -4 7 2 734.48 716.34 8.12 o -3 7 2 671.88 658.17 14.35 o -2 7 2 1539.74 1580.37 25.94 o -1 7 2 350.07 339.63 6.30 o 0 7 2 187.11 176.27 5.96 o -7 8 2 1297.26 1414.51 44.60 o -6 8 2 398.50 397.94 11.93 o -5 8 2 414.52 405.32 8.97 o -4 8 2 1368.43 1398.84 20.76 o -3 8 2 468.39 459.88 8.15 o -2 8 2 402.36 399.96 9.03 o -1 8 2 1321.04 1438.48 44.10 o 0 8 2 278.78 285.47 10.41 o -8 9 2 311.07 308.85 10.99 o -7 9 2 415.86 463.71 17.69 o -6 9 2 882.77 952.52 25.97 o -5 9 2 251.61 254.08 10.06 o -4 9 2 200.46 203.93 8.91 o -3 9 2 803.51 828.73 20.14 o -2 9 2 376.55 373.90 16.45 o -1 9 2 344.48 336.85 11.37 o 0 9 2 453.74 475.48 17.37 o -9 10 2 90.36 72.80 17.12 o -8 10 2 537.00 535.25 21.79 o -7 10 2 172.04 166.84 9.93 o -6 10 2 169.32 169.21 10.11 o -5 10 2 725.17 746.11 23.21 o -4 10 2 174.00 186.85 11.60 o -3 10 2 174.07 154.99 8.90 o -2 10 2 564.39 588.66 24.87 o -1 10 2 96.76 91.96 10.87 o 0 10 2 112.63 129.04 28.17 o -9 11 2 65.36 32.61 11.50 o -8 11 2 87.05 84.63 16.04 o -7 11 2 392.26 385.33 24.43 o -6 11 2 211.88 118.18 20.73 o -4 11 2 371.75 343.53 18.16 o -3 11 2 70.51 47.54 8.21 o -2 11 2 89.87 48.49 8.22 o 0 1 3 449.68 462.69 4.22 o -1 2 3 18.95 19.81 0.70 o 0 2 3 1375.07 1373.68 15.71 o -2 3 3 966.56 985.33 10.30 o -1 3 3 1026.00 1015.73 8.39 o 0 3 3 70.00 69.21 1.35 o -3 4 3 481.03 463.14 5.00 o -2 4 3 615.87 566.91 9.32 o -1 4 3 399.51 374.89 4.76 o 0 4 3 10.57 4.04 0.63 o -4 5 3 463.93 480.07 5.86 o -3 5 3 660.68 670.30 8.82 o -2 5 3 838.97 864.92 9.65 o -1 5 3 463.89 477.63 6.09 o 0 5 3 64.15 56.74 1.90 o -5 6 3 184.73 182.17 2.49 o -4 6 3 148.17 137.90 2.33 o -3 6 3 541.04 550.68 7.03 o -2 6 3 125.61 116.34 2.66 o -1 6 3 216.71 215.70 4.24 o 0 6 3 0.93 1.80 0.86 o -6 7 3 396.14 387.15 6.21 o -5 7 3 12.79 9.94 1.44 o -4 7 3 413.56 441.20 6.60 o -3 7 3 444.61 474.51 6.99 o -2 7 3 12.87 7.88 1.51 o -1 7 3 434.98 435.02 9.31 o 0 7 3 318.54 322.34 6.93 o -7 8 3 79.98 81.09 4.32 o -6 8 3 383.27 388.96 11.48 o -5 8 3 113.39 111.11 3.41 o -4 8 3 223.77 228.74 4.78 o -3 8 3 155.05 152.50 3.83 o -2 8 3 332.52 337.91 6.69 o -1 8 3 80.00 74.36 5.61 o 0 8 3 352.58 357.62 11.77 o -8 9 3 112.50 103.39 6.15 o -7 9 3 139.07 144.53 7.65 o -6 9 3 111.24 99.64 5.25 o -5 9 3 181.24 180.64 6.64 o -4 9 3 112.67 108.14 4.74 o -3 9 3 111.54 87.86 3.22 o -2 9 3 141.29 158.27 6.35 o -1 9 3 153.48 150.17 7.08 o 0 9 3 5.63 8.97 3.65 o -9 10 3 13.82 6.30 6.98 o -8 10 3 47.01 37.20 6.55 o -7 10 3 66.55 50.90 6.26 o -6 10 3 14.51 9.08 8.03 o -5 10 3 98.19 89.24 6.69 o -4 10 3 10.79 5.74 3.64 o -3 10 3 45.63 53.33 7.16 o -2 10 3 46.87 60.81 7.77 o -1 10 3 8.61 11.24 5.34 o 0 10 3 8.14 19.93 18.30 o -8 11 3 49.55 59.48 14.96 o -4 11 3 47.68 21.95 7.41 o -3 11 3 31.83 24.31 19.85 o 0 0 4 5651.73 6489.47 332.54 o 0 1 4 43.03 37.37 1.41 o -1 2 4 3144.29 3078.60 51.62 o 0 2 4 418.84 379.06 5.49 o -2 3 4 2073.96 2127.37 33.60 o -1 3 4 2163.71 2239.74 33.13 o 0 3 4 6593.26 6751.13 140.99 o -3 4 4 1344.87 1321.96 18.89 o -2 4 4 6083.22 6112.82 133.08 o -1 4 4 1286.96 1268.58 16.76 o 0 4 4 514.06 509.20 6.16 o -4 5 4 1477.08 1502.18 23.80 o -3 5 4 1567.15 1589.30 24.25 o -2 5 4 1649.03 1705.21 26.09 o -1 5 4 1451.39 1482.37 22.39 o 0 5 4 54.95 51.76 1.92 o -5 6 4 43.25 43.45 2.20 o -4 6 4 622.45 619.34 10.34 o -3 6 4 3899.98 4039.10 97.60 o -2 6 4 607.46 624.39 9.44 o -1 6 4 43.87 47.00 2.03 o 0 6 4 46.40 48.76 2.61 o -6 7 4 133.63 118.10 3.05 o -5 7 4 1284.39 1347.11 24.85 o -4 7 4 404.38 400.80 5.88 o -3 7 4 390.56 395.95 7.32 o -2 7 4 1288.91 1334.87 27.44 o -1 7 4 121.20 119.83 6.60 o 0 7 4 464.82 427.43 8.98 o -7 8 4 664.81 727.86 26.87 o -6 8 4 147.88 146.17 5.64 o -5 8 4 684.10 699.32 14.13 o -4 8 4 1643.69 1828.34 49.95 o -3 8 4 720.26 729.19 14.64 o -2 8 4 136.49 127.45 4.12 o -1 8 4 679.20 729.15 21.22 o 0 8 4 19.34 17.99 4.15 o -8 9 4 176.83 167.48 9.61 o -7 9 4 183.22 172.49 11.57 o -6 9 4 1000.91 1085.69 36.28 o -5 9 4 303.47 288.68 10.13 o -4 9 4 283.66 263.12 9.53 o -3 9 4 978.49 1057.26 31.67 o -2 9 4 174.92 180.19 9.57 o -1 9 4 187.79 176.75 7.64 o 0 9 4 552.18 566.33 22.24 o -9 10 4 163.06 141.18 16.77 o -8 10 4 577.33 667.69 53.13 o -7 10 4 128.12 121.58 10.11 o -6 10 4 128.03 130.01 8.82 o -5 10 4 423.62 421.17 15.89 o -4 10 4 139.88 152.70 11.00 o -3 10 4 131.25 134.71 9.02 o -2 10 4 579.47 628.89 30.64 o -1 10 4 162.26 114.07 16.84 o 0 1 5 1659.77 1659.07 26.71 o -1 2 5 56.72 57.32 1.67 o 0 2 5 2851.88 2964.46 53.89 o -2 3 5 113.75 115.59 2.51 o -1 3 5 181.39 186.02 2.44 o 0 3 5 14.49 14.69 1.30 o -3 4 5 47.05 45.35 1.41 o -2 4 5 138.43 136.83 2.84 o -1 4 5 10.62 10.45 1.42 o 0 4 5 88.92 77.99 2.41 o -4 5 5 26.15 22.29 2.32 o -3 5 5 55.36 50.30 1.98 o -2 5 5 24.09 25.18 1.99 o -1 5 5 26.11 23.70 1.88 o 0 5 5 14.93 18.45 1.55 o -5 6 5 361.85 380.47 7.11 o -4 6 5 326.01 336.42 6.09 o -3 6 5 138.85 129.69 2.86 o -2 6 5 321.82 326.50 6.34 o -1 6 5 316.35 331.58 8.05 o 0 6 5 2.31 1.63 1.37 o -6 7 5 867.41 926.19 22.04 o -5 7 5 117.50 102.11 4.30 o -4 7 5 88.31 97.14 4.72 o -3 7 5 70.02 75.18 3.86 o -2 7 5 117.59 102.19 4.36 o -1 7 5 853.31 908.27 20.72 o 0 7 5 735.42 824.79 21.44 o -7 8 5 48.07 55.69 9.74 o -6 8 5 519.67 532.07 20.49 o -5 8 5 54.37 68.79 7.20 o -4 8 5 10.95 12.39 2.46 o -3 8 5 64.76 73.32 3.41 o -2 8 5 538.96 573.41 17.13 o -1 8 5 48.15 48.87 3.89 o 0 8 5 609.73 597.72 22.66 o -8 9 5 41.63 44.44 6.93 o -7 9 5 30.88 26.84 4.50 o -6 9 5 32.67 29.32 4.46 o -5 9 5 0.89 3.40 3.41 o -4 9 5 14.65 18.23 3.11 o -3 9 5 32.79 34.82 3.50 o -2 9 5 13.85 8.84 3.35 o -1 9 5 49.75 44.05 5.89 o 0 9 5 21.32 28.22 16.92 o -8 10 5 1.31 3.91 8.81 o -7 10 5 21.57 27.89 11.26 o -6 10 5 6.64 12.82 6.45 o -4 10 5 25.41 32.98 13.13 o -3 10 5 30.88 30.59 7.21 o -2 10 5 1.30 7.29 5.93 o 0 0 6 456.03 528.05 18.09 o 0 1 6 332.54 330.03 5.23 o -1 2 6 2356.40 2335.27 46.61 o 0 2 6 182.13 164.54 3.21 o -2 3 6 1496.79 1459.54 25.60 o -1 3 6 1361.09 1364.42 25.04 o 0 3 6 4262.21 4233.28 107.83 o -3 4 6 1311.12 1309.41 25.54 o -2 4 6 2047.29 2047.51 43.10 o -1 4 6 1405.24 1414.24 25.77 o 0 4 6 264.68 265.09 5.85 o -4 5 6 1945.26 2035.97 41.24 o -3 5 6 1513.83 1504.17 27.43 o -2 5 6 1448.45 1447.12 28.80 o -1 5 6 1886.27 1953.04 43.33 o 0 5 6 91.39 90.47 3.10 o -5 6 6 122.04 112.59 2.62 o -4 6 6 244.22 230.07 5.70 o -3 6 6 2186.05 2313.53 59.24 o -2 6 6 221.19 203.45 5.51 o -1 6 6 105.10 98.26 4.45 o 0 6 6 61.41 72.21 5.44 o -6 7 6 201.27 188.92 7.35 o -5 7 6 1083.26 1140.21 30.16 o -4 7 6 245.86 226.63 7.95 o -3 7 6 281.96 293.95 7.34 o -2 7 6 1070.24 1143.19 33.64 o -1 7 6 205.77 210.89 6.97 o 0 7 6 339.99 348.10 10.87 o -7 8 6 379.97 387.11 15.09 o -6 8 6 93.91 96.22 5.65 o -5 8 6 294.40 288.73 12.15 o -4 8 6 863.37 962.21 26.33 o -3 8 6 284.08 277.90 8.53 o -2 8 6 82.12 85.45 4.59 o -1 8 6 378.79 383.96 16.78 o 0 8 6 61.88 68.15 7.51 o -8 9 6 101.56 69.40 12.22 o -7 9 6 88.67 81.05 7.70 o -6 9 6 867.97 929.24 42.46 o -5 9 6 547.98 590.75 23.09 o -4 9 6 576.83 582.18 20.83 o -3 9 6 908.80 986.67 43.26 o -2 9 6 112.60 100.60 7.39 o -1 9 6 82.51 75.56 10.26 o 0 9 6 653.52 617.28 43.26 o -7 10 6 100.29 75.23 13.96 o -6 10 6 119.49 108.37 14.55 o -4 10 6 123.42 95.97 18.19 o -3 10 6 101.10 98.96 22.40 o 0 1 7 704.53 745.23 20.99 o -1 2 7 3.07 4.12 2.33 o 0 2 7 747.66 747.78 21.84 o -2 3 7 20.11 31.34 5.73 o -1 3 7 4.31 11.66 2.41 o 0 3 7 94.69 102.74 4.99 o -3 4 7 70.28 73.64 4.86 o -2 4 7 146.92 148.38 5.44 o -1 4 7 99.66 100.32 5.37 o 0 4 7 803.08 845.30 18.74 o -4 5 7 164.71 146.81 5.32 o -3 5 7 295.68 271.02 10.09 o -2 5 7 197.78 194.02 6.80 o -1 5 7 164.16 157.88 7.12 o 0 5 7 186.05 191.74 5.89 o -5 6 7 275.47 291.48 8.80 o -4 6 7 422.22 437.26 14.06 o -3 6 7 323.24 306.26 9.49 o -2 6 7 436.35 441.60 12.42 o -1 6 7 239.12 233.87 8.43 o 0 6 7 0.57 1.17 2.50 o -6 7 7 190.61 188.25 7.23 o -5 7 7 26.33 22.12 3.77 o -4 7 7 20.99 16.85 2.67 o -3 7 7 2.43 3.85 2.85 o -2 7 7 26.19 16.81 3.45 o -1 7 7 165.98 161.34 7.11 o 0 7 7 155.69 144.49 8.52 o -7 8 7 31.68 39.93 10.01 o -6 8 7 112.90 118.39 9.22 o -5 8 7 110.10 108.63 6.54 o -4 8 7 71.33 90.75 5.40 o -3 8 7 87.56 89.16 5.12 o -2 8 7 146.21 134.11 9.02 o -1 8 7 31.73 19.85 6.84 o 0 8 7 52.26 34.53 7.65 o -8 9 7 37.56 20.83 12.20 o -7 9 7 10.07 14.20 9.06 o -6 9 7 137.27 128.68 16.42 o -5 9 7 100.41 105.21 15.68 o -4 9 7 146.10 131.64 10.84 o -3 9 7 137.84 126.65 25.57 o -2 9 7 0.60 0.55 5.98 o -1 9 7 21.29 6.82 7.57 o 0 0 8 4647.48 5037.03 621.25 o 0 1 8 1140.89 1137.53 38.27 o -1 2 8 2133.71 2144.79 83.92 o 0 2 8 270.56 280.53 9.90 o -2 3 8 407.43 392.60 12.08 o -1 3 8 334.20 315.62 11.20 o 0 3 8 1203.55 1224.03 43.33 o -3 4 8 507.27 508.75 17.16 o -2 4 8 264.13 293.03 10.34 o -1 4 8 563.97 570.31 19.42 o 0 4 8 199.46 202.71 7.31 o -4 5 8 1733.65 1823.19 59.05 o -3 5 8 689.09 691.26 19.57 o -2 5 8 622.10 628.65 21.59 o -1 5 8 1735.71 1760.66 54.99 o 0 5 8 358.72 370.15 11.88 o -5 6 8 378.01 361.08 13.79 o -4 6 8 78.15 73.61 4.44 o -3 6 8 539.51 539.83 18.67 o -2 6 8 89.74 96.10 5.46 o -1 6 8 373.07 374.36 12.61 o 0 6 8 1110.37 1197.29 41.19 o -6 7 8 358.97 350.66 14.23 o -5 7 8 858.36 915.63 33.12 o -4 7 8 112.42 106.03 6.44 o -3 7 8 129.25 109.99 5.90 o -2 7 8 852.89 893.21 30.47 o -1 7 8 363.45 366.54 13.46 o 0 7 8 186.54 149.33 9.50 o -7 8 8 431.17 407.87 37.51 o -6 8 8 122.09 110.49 10.39 o -5 8 8 121.95 124.92 12.98 o -4 8 8 298.67 315.04 17.34 o -3 8 8 91.67 84.36 7.94 o -2 8 8 129.98 110.30 9.05 o -1 8 8 424.92 399.01 33.17 o -6 9 8 467.44 465.68 43.04 o -5 9 8 359.85 365.39 33.34 o -4 9 8 384.02 305.77 39.17 o -3 9 8 481.95 461.24 64.99 o 0 1 9 37.70 55.16 6.43 o -1 2 9 40.40 35.21 4.31 o 0 2 9 69.55 69.08 4.94 o -2 3 9 164.58 157.81 6.87 o -1 3 9 110.38 105.67 8.12 o 0 3 9 29.25 27.03 4.27 o -3 4 9 249.41 257.44 11.82 o -2 4 9 270.78 255.24 11.03 o -1 4 9 295.14 306.89 12.53 o 0 4 9 553.33 558.79 21.70 o -4 5 9 29.19 26.42 4.15 o -3 5 9 220.12 222.74 8.63 o -2 5 9 204.94 206.19 8.72 o -1 5 9 29.11 14.80 4.17 o 0 5 9 161.83 151.69 7.81 o -5 6 9 60.30 49.66 6.13 o -4 6 9 176.04 167.04 9.11 o -3 6 9 12.66 13.87 3.67 o -2 6 9 186.68 183.96 9.60 o -1 6 9 84.14 89.53 7.89 o 0 6 9 1.22 -2.74 4.02 o -6 7 9 1.04 -3.48 8.55 o -5 7 9 5.05 7.11 4.77 o -4 7 9 14.17 13.76 5.83 o -3 7 9 29.21 25.80 5.43 o -2 7 9 5.05 4.13 4.50 o -1 7 9 6.05 9.50 4.84 o 0 7 9 4.32 -1.19 7.90 o -5 8 9 117.70 80.48 20.82 o -4 8 9 59.61 53.99 12.25 o -3 8 9 97.29 87.98 9.70 o -2 8 9 1.21 11.24 9.52 o 0 0 10 4052.45 4341.25 597.78 o 0 1 10 617.81 608.00 24.97 o -1 2 10 1365.12 1367.51 58.51 o 0 2 10 315.70 330.93 16.34 o -2 3 10 204.73 196.91 11.38 o -1 3 10 244.59 232.71 10.93 o 0 3 10 489.14 484.46 21.22 o -3 4 10 156.01 143.81 8.95 o -2 4 10 405.06 453.74 20.33 o -1 4 10 130.01 123.55 9.63 o 0 4 10 179.81 177.58 10.49 o -4 5 10 684.42 660.37 35.52 o -3 5 10 80.72 80.39 7.07 o -2 5 10 87.08 76.04 7.57 o -1 5 10 726.34 723.81 29.66 o 0 5 10 262.34 273.42 14.88 o -5 6 10 256.61 245.02 30.23 o -4 6 10 158.52 136.90 14.48 o -3 6 10 320.45 304.59 19.59 o -2 6 10 179.89 153.28 11.13 o -1 6 10 265.96 243.04 16.42 o 0 6 10 1338.17 1397.30 101.08 o -5 7 10 574.71 570.53 68.93 o -4 7 10 124.48 97.10 19.91 o -3 7 10 107.58 103.23 12.13 o -2 7 10 583.79 573.04 36.37 o 0 1 11 6.38 7.40 4.63 o -1 2 11 6.90 6.68 5.00 o 0 2 11 26.25 24.38 5.40 o -2 3 11 282.91 282.80 15.51 o -1 3 11 268.85 272.90 15.38 o 0 3 11 17.81 20.96 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