#------------------------------------------------------------------------------ #$Date: 2010-01-22 14:33:52 +0200 (Fri, 22 Jan 2010) $ #$Revision: 960 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2224140.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2224140_Fobs loop_ _publ_author_name 'Zhang, Zheyu' _publ_section_title ; catena-Poly[[[aquasilver(I)]-\m-1,1'-(butane-1,4-diyl)di-1H-imidazole-\k^2^N^3^:N^3'^] hemi(biphenyl-4,4'-dicarboxylate) dihydrate] ; _journal_coeditor_code CI2938 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1519 _journal_page_last m1520 _journal_volume 65 _journal_year 2009 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 80.190 _cell_angle_beta 68.898 _cell_angle_gamma 74.775 _cell_length_a 9.7685 _cell_length_b 10.0659 _cell_length_c 10.9224 _exptl_crystal_F_000 482.00 _reflns_d_resolution_high 0.8206 _[local]_cod_data_source_file ci2938Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' p-1 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 185.65 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 6543.76 6323.91 73.63 o 2 0 0 61.87 63.42 1.04 o 3 0 0 951.38 901.46 10.46 o 4 0 0 614.98 630.44 6.64 o 5 0 0 68.50 73.86 1.52 o 6 0 0 26.13 25.81 1.56 o 7 0 0 474.45 438.95 7.45 o 8 0 0 406.46 395.28 7.27 o 9 0 0 243.08 236.62 8.87 o -10 1 0 2.38 3.02 1.71 o -9 1 0 130.31 113.90 6.07 o -8 1 0 538.16 552.32 14.34 o -7 1 0 1317.86 1315.55 17.31 o -6 1 0 1002.55 996.42 13.33 o -5 1 0 2337.70 2389.04 22.68 o -4 1 0 6257.44 6330.36 57.17 o -3 1 0 525.42 505.16 5.42 o -2 1 0 1324.61 1397.13 22.05 o -1 1 0 4.27 -1.65 1.65 o 0 1 0 2.20 4.88 0.30 o 1 1 0 188.54 183.90 2.46 o 2 1 0 971.53 939.54 8.97 o 3 1 0 4079.89 4138.86 37.67 o 4 1 0 2485.21 2481.66 23.10 o 5 1 0 4105.03 4132.06 37.94 o 6 1 0 3772.40 3874.23 44.70 o 7 1 0 597.54 578.69 9.59 o 8 1 0 106.31 102.56 3.30 o 9 1 0 48.09 55.22 2.91 o 10 1 0 317.80 292.71 10.48 o 11 1 0 60.68 64.18 5.05 o -10 2 0 197.67 211.26 9.04 o -9 2 0 464.13 450.18 13.30 o -8 2 0 383.64 374.11 11.25 o -7 2 0 321.41 294.86 9.22 o -6 2 0 6.89 6.81 1.00 o -5 2 0 673.45 707.42 7.79 o -4 2 0 29.15 26.17 3.29 o -3 2 0 6980.20 7022.00 77.55 o -2 2 0 22339.31 21193.76 392.61 o -1 2 0 15786.50 15939.08 242.67 o 0 2 0 17.51 12.88 0.82 o 1 2 0 5233.55 5143.59 80.83 o 2 2 0 3694.55 3793.98 41.43 o 3 2 0 390.64 351.43 8.31 o 4 2 0 21.36 16.41 0.71 o 5 2 0 8.50 6.20 0.55 o 6 2 0 36.45 30.20 1.88 o 7 2 0 66.95 64.89 5.78 o 8 2 0 108.54 99.09 3.31 o 9 2 0 867.18 859.86 13.21 o 10 2 0 168.10 167.28 4.85 o 11 2 0 177.71 196.57 8.92 o -9 3 0 44.85 46.27 4.14 o -8 3 0 319.29 353.10 11.17 o -7 3 0 758.92 757.72 17.71 o -6 3 0 410.00 419.49 11.15 o -5 3 0 174.60 180.89 2.94 o -4 3 0 3064.25 3136.67 29.20 o -3 3 0 3006.75 3207.46 35.29 o -2 3 0 3158.66 3326.85 36.40 o -1 3 0 13.70 17.59 1.04 o 0 3 0 95.85 99.38 2.53 o 1 3 0 47.95 43.82 1.63 o 2 3 0 1279.13 1327.16 21.23 o 3 3 0 2269.78 2252.33 25.21 o 4 3 0 1819.40 1748.82 20.03 o 5 3 0 4748.13 4990.13 54.52 o 6 3 0 2130.40 2040.72 25.01 o 7 3 0 887.63 854.51 12.42 o 8 3 0 1255.78 1243.89 17.21 o 9 3 0 193.08 177.83 4.84 o 10 3 0 39.85 37.80 2.46 o 11 3 0 4.16 4.04 2.08 o -9 4 0 36.70 30.40 3.74 o -8 4 0 63.89 64.11 4.53 o -7 4 0 3.86 3.74 1.81 o -6 4 0 39.64 21.72 2.68 o -5 4 0 92.49 99.00 6.48 o -4 4 0 2939.25 2984.32 33.36 o -3 4 0 1502.68 1605.45 18.58 o -2 4 0 223.10 215.54 3.52 o -1 4 0 3321.30 3440.38 52.05 o 0 4 0 4151.84 4302.86 64.75 o 1 4 0 1497.00 1386.04 22.17 o 2 4 0 6191.91 6485.04 97.18 o 3 4 0 2184.37 2310.40 36.41 o 4 4 0 119.41 110.11 3.67 o 5 4 0 10.43 14.14 1.51 o 6 4 0 248.58 239.27 6.56 o 7 4 0 151.80 149.45 5.25 o 8 4 0 69.18 59.43 3.49 o 9 4 0 389.03 356.47 9.76 o 10 4 0 689.26 689.53 15.73 o 11 4 0 338.01 330.28 10.06 o -8 5 0 46.30 55.98 4.46 o -7 5 0 83.73 95.50 5.35 o -6 5 0 662.59 679.74 16.45 o -5 5 0 3730.79 3702.61 60.49 o -4 5 0 831.28 839.20 16.37 o -3 5 0 520.28 525.01 7.32 o -2 5 0 682.35 660.53 8.76 o -1 5 0 53.40 42.98 1.83 o 0 5 0 285.31 378.22 7.46 o 1 5 0 352.96 345.05 7.13 o 2 5 0 3868.76 4172.21 63.71 o 3 5 0 2321.52 2372.06 37.65 o 4 5 0 1837.78 1774.56 29.33 o 5 5 0 2918.57 2860.37 45.73 o 6 5 0 1444.82 1543.09 26.83 o 7 5 0 1162.54 1159.77 21.63 o 8 5 0 203.32 201.30 6.76 o 9 5 0 219.11 216.31 7.46 o 10 5 0 279.83 271.05 8.87 o -8 6 0 28.12 25.47 3.57 o -7 6 0 19.92 13.60 2.58 o -6 6 0 23.43 18.90 2.63 o -5 6 0 397.31 389.91 9.83 o -4 6 0 21.98 20.73 2.13 o -3 6 0 566.46 605.33 13.18 o -2 6 0 2328.77 2469.08 28.44 o -1 6 0 2486.67 2758.78 42.88 o 0 6 0 2511.80 2599.47 40.65 o 1 6 0 2040.81 2102.27 33.59 o 2 6 0 370.69 352.85 7.78 o 3 6 0 61.38 49.42 2.58 o 4 6 0 119.71 101.14 3.89 o 5 6 0 0.81 1.29 0.87 o 6 6 0 447.15 449.02 10.53 o 7 6 0 269.50 255.67 7.70 o 8 6 0 521.08 487.44 12.06 o 9 6 0 403.37 395.14 10.90 o 10 6 0 71.49 87.37 4.95 o -7 7 0 430.44 448.10 13.72 o -6 7 0 254.68 215.00 8.30 o -5 7 0 742.61 765.13 16.57 o -4 7 0 381.87 376.31 10.03 o -3 7 0 91.42 91.76 4.38 o -2 7 0 41.88 36.80 1.66 o -1 7 0 2.64 3.05 0.71 o 0 7 0 3.81 3.32 0.92 o 1 7 0 403.87 397.74 8.65 o 2 7 0 388.32 361.08 8.30 o 3 7 0 1184.05 1192.82 21.18 o 4 7 0 1480.24 1545.47 26.75 o 5 7 0 1611.70 1731.58 29.97 o 6 7 0 199.71 196.02 6.47 o 7 7 0 863.53 905.96 18.53 o 8 7 0 843.56 798.60 17.29 o 9 7 0 242.19 224.51 7.98 o 10 7 0 99.22 103.72 5.57 o -6 8 0 99.72 99.58 5.72 o -5 8 0 8.60 11.05 2.11 o -4 8 0 99.50 100.57 4.98 o -3 8 0 193.11 208.83 7.36 o -2 8 0 331.01 357.38 10.11 o -1 8 0 746.96 781.25 11.11 o 0 8 0 644.83 662.80 13.01 o 1 8 0 644.00 622.25 12.53 o 2 8 0 93.91 106.47 4.14 o 3 8 0 833.22 829.56 16.18 o 4 8 0 17.71 16.00 1.91 o 5 8 0 539.06 574.31 12.91 o 6 8 0 0.45 2.23 1.24 o 7 8 0 8.00 11.87 2.06 o 8 8 0 190.57 197.16 7.31 o 9 8 0 226.04 222.82 8.25 o -4 9 0 124.33 133.57 6.22 o -3 9 0 253.81 243.93 8.62 o -2 9 0 11.98 9.04 1.96 o -1 9 0 5.76 2.06 1.24 o 0 9 0 102.09 83.57 2.85 o 1 9 0 100.27 109.19 4.29 o 2 9 0 38.04 37.65 2.68 o 3 9 0 66.04 66.07 3.52 o 4 9 0 1143.90 1148.58 21.77 o 5 9 0 1450.71 1470.46 27.08 o 6 9 0 1126.53 1103.79 21.95 o 7 9 0 504.68 481.47 12.39 o 8 9 0 101.74 107.06 5.45 o 9 9 0 176.31 189.36 7.75 o -4 10 0 2.24 0.79 1.49 o -3 10 0 212.70 216.56 8.52 o -2 10 0 73.34 79.67 5.00 o -1 10 0 38.97 51.67 4.01 o 1 10 0 592.58 617.32 13.35 o 2 10 0 577.48 594.58 13.20 o 3 10 0 101.98 101.89 4.63 o 4 10 0 76.66 70.55 4.06 o 5 10 0 61.20 53.21 3.54 o 6 10 0 6.67 7.36 1.83 o 7 10 0 86.16 74.74 4.46 o 8 10 0 22.38 24.50 3.02 o -2 11 0 21.02 19.72 3.02 o -1 11 0 11.78 8.35 2.16 o 0 11 0 6.92 7.83 2.06 o 1 11 0 6.49 5.67 1.61 o 2 11 0 326.87 340.74 9.44 o 3 11 0 311.75 331.94 9.54 o 4 11 0 367.22 378.37 10.60 o 5 11 0 383.24 418.03 11.52 o 6 11 0 225.83 224.19 8.08 o 2 12 0 236.27 226.59 9.14 o 3 12 0 217.31 219.33 8.89 o -6 -11 1 186.28 186.94 5.22 o -5 -11 1 132.60 129.75 4.25 o -4 -11 1 43.72 40.62 2.38 o -3 -11 1 119.03 114.82 7.06 o -2 -11 1 13.97 14.54 2.68 o -1 -11 1 0.25 0.47 1.24 o 0 -11 1 82.05 84.20 5.28 o 1 -11 1 96.35 111.35 6.27 o 2 -11 1 91.83 83.38 5.40 o -7 -10 1 47.90 52.99 3.84 o -6 -10 1 8.55 6.91 1.86 o -5 -10 1 90.25 89.75 4.68 o -4 -10 1 465.44 462.43 8.50 o -3 -10 1 691.66 708.73 15.75 o -2 -10 1 3.80 7.51 1.23 o -1 -10 1 305.24 310.57 10.06 o 0 -10 1 411.44 432.00 12.53 o 1 -10 1 119.35 139.59 6.59 o 2 -10 1 230.95 222.85 8.69 o 3 -10 1 103.11 101.42 5.75 o 4 -10 1 39.89 44.37 4.09 o -8 -9 1 417.45 437.97 12.36 o -7 -9 1 482.15 499.53 12.98 o -6 -9 1 328.52 324.88 9.51 o -5 -9 1 775.48 769.24 16.55 o -4 -9 1 431.55 424.71 10.65 o -3 -9 1 0.97 1.93 1.02 o -2 -9 1 52.77 46.05 2.20 o -1 -9 1 1.01 1.04 0.71 o 0 -9 1 10.32 9.69 2.01 o 1 -9 1 456.42 456.65 12.44 o 2 -9 1 493.35 495.83 13.33 o 3 -9 1 447.66 463.85 12.86 o 4 -9 1 222.32 241.45 8.77 o -9 -8 1 16.44 14.42 2.65 o -8 -8 1 2.56 0.57 1.36 o -7 -8 1 24.94 25.07 2.77 o -6 -8 1 355.79 347.30 9.69 o -5 -8 1 3.45 4.06 1.34 o -4 -8 1 1.42 2.87 1.16 o -3 -8 1 1656.37 1717.22 29.55 o -2 -8 1 2708.44 2853.70 45.93 o -1 -8 1 1227.44 1283.93 22.44 o 0 -8 1 391.88 407.85 8.36 o 1 -8 1 761.77 775.29 17.19 o 2 -8 1 807.87 796.44 17.66 o 3 -8 1 78.92 77.07 4.36 o 4 -8 1 0.56 0.84 1.16 o 5 -8 1 2.94 1.91 1.34 o -9 -7 1 190.37 196.07 7.65 o -8 -7 1 496.97 494.94 12.78 o -7 -7 1 2222.81 2307.46 39.83 o -6 -7 1 1472.48 1429.27 26.26 o -5 -7 1 1073.80 1105.40 20.81 o -4 -7 1 105.30 101.99 4.19 o -3 -7 1 259.86 243.38 6.64 o -2 -7 1 96.63 81.47 3.37 o -1 -7 1 151.04 153.51 4.63 o 0 -7 1 269.38 246.73 4.67 o 1 -7 1 572.15 577.08 8.47 o 2 -7 1 1173.22 1227.52 23.76 o 3 -7 1 870.98 930.24 19.25 o 4 -7 1 366.65 386.27 10.43 o 5 -7 1 401.67 393.63 10.60 o 7 -7 1 220.19 193.25 8.22 o -10 -6 1 163.61 165.01 7.08 o -9 -6 1 293.00 286.12 9.31 o -8 -6 1 5.67 2.75 1.59 o -7 -6 1 24.31 23.66 2.53 o -6 -6 1 9.12 8.45 1.63 o -5 -6 1 427.87 423.90 9.96 o -4 -6 1 2575.23 2735.04 44.07 o -3 -6 1 1494.07 1456.69 24.82 o -2 -6 1 1675.79 1718.01 28.29 o -1 -6 1 4364.32 4393.33 67.16 o 0 -6 1 2929.49 3057.23 47.26 o 1 -6 1 2017.46 2156.67 25.04 o 2 -6 1 11.89 10.59 0.89 o 3 -6 1 81.11 77.66 3.79 o 4 -6 1 1.67 3.99 1.34 o 5 -6 1 4.51 10.33 1.81 o 7 -6 1 318.61 293.89 10.21 o 8 -6 1 280.13 293.45 10.70 o -10 -5 1 439.51 400.61 11.52 o -9 -5 1 769.43 743.53 16.72 o -8 -5 1 1396.41 1356.31 25.59 o -7 -5 1 62.59 72.76 3.91 o -6 -5 1 886.58 937.02 18.13 o -5 -5 1 1362.35 1449.46 25.29 o -4 -5 1 709.39 701.22 13.60 o -3 -5 1 147.86 149.52 4.48 o -2 -5 1 2.88 2.01 0.87 o -1 -5 1 86.02 86.23 2.92 o 0 -5 1 239.77 246.65 4.14 o 1 -5 1 72.50 44.42 2.49 o 2 -5 1 1849.39 2059.50 23.63 o 3 -5 1 643.47 668.54 8.77 o 4 -5 1 1381.73 1411.46 25.54 o 5 -5 1 413.75 421.99 10.16 o 6 -5 1 1661.19 1590.28 30.75 o 7 -5 1 183.04 197.28 7.88 o 8 -5 1 0.12 -1.14 1.14 o 9 -5 1 7.16 11.94 2.82 o -10 -4 1 223.68 215.37 7.78 o -9 -4 1 153.01 141.22 5.95 o -8 -4 1 82.82 77.46 4.11 o -7 -4 1 0.47 0.10 1.04 o -6 -4 1 599.84 607.09 12.83 o -5 -4 1 592.36 550.88 11.44 o -4 -4 1 815.27 742.59 13.97 o -3 -4 1 5082.17 5456.76 82.76 o -2 -4 1 8083.05 8443.69 126.06 o -1 -4 1 6557.59 6789.37 101.42 o 0 -4 1 8968.97 9254.45 141.27 o 1 -4 1 1832.27 1821.25 20.68 o 2 -4 1 292.68 274.92 4.12 o 3 -4 1 36.19 33.50 1.14 o 4 -4 1 9.57 11.19 1.67 o 5 -4 1 316.39 287.08 7.38 o 6 -4 1 540.70 523.87 17.09 o 7 -4 1 383.15 396.47 11.59 o 8 -4 1 240.33 254.38 9.26 o 9 -4 1 197.04 231.37 9.41 o -10 -3 1 70.06 70.43 3.22 o -9 -3 1 150.92 147.34 9.77 o -8 -3 1 514.37 525.33 9.24 o -7 -3 1 2103.39 2142.83 26.90 o -6 -3 1 1386.16 1348.29 23.81 o -5 -3 1 945.28 930.53 17.04 o -4 -3 1 780.08 773.60 14.17 o -3 -3 1 6267.72 6758.60 101.52 o -2 -3 1 67.97 68.82 2.50 o -1 -3 1 28.56 31.56 1.49 o 0 -3 1 604.68 646.42 7.93 o 1 -3 1 5436.20 5789.82 62.84 o 2 -3 1 1181.68 1159.78 13.39 o 3 -3 1 4401.24 4584.53 49.80 o 4 -3 1 8712.24 9115.99 98.89 o 5 -3 1 1881.88 1881.28 23.42 o 6 -3 1 1.18 2.28 0.78 o 7 -3 1 641.48 642.16 15.68 o 8 -3 1 10.51 10.70 2.28 o 9 -3 1 0.45 0.17 1.16 o 10 -3 1 0.16 -1.29 1.29 o -10 -2 1 285.85 268.36 6.55 o -9 -2 1 36.51 36.83 2.29 o -8 -2 1 14.79 14.66 2.03 o -7 -2 1 104.32 93.66 3.12 o -6 -2 1 166.45 147.11 4.41 o -5 -2 1 938.74 900.50 12.28 o -4 -2 1 11341.33 11442.67 377.75 o -3 -2 1 15030.51 14740.76 227.11 o -2 -2 1 10570.73 10240.69 162.50 o -1 -2 1 3150.18 3182.87 48.11 o 0 -2 1 4430.34 4529.93 65.17 o 1 -2 1 917.71 1049.46 11.91 o 2 -2 1 1702.06 1722.55 19.19 o 3 -2 1 588.65 631.16 7.67 o 4 -2 1 968.07 938.98 9.54 o 5 -2 1 657.68 650.10 7.21 o 6 -2 1 782.40 825.61 9.07 o 7 -2 1 256.05 253.71 8.27 o 8 -2 1 107.79 113.65 5.65 o 9 -2 1 297.86 295.38 10.23 o 10 -2 1 328.01 341.04 11.77 o -10 -1 1 225.39 242.05 9.61 o -9 -1 1 267.44 252.15 6.55 o -8 -1 1 1679.44 1683.52 22.12 o -7 -1 1 1460.43 1400.70 18.50 o -6 -1 1 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146.83 160.25 4.82 o 5 8 10 76.02 74.15 3.27 o 6 8 10 424.28 399.84 8.19 o 7 8 10 95.76 109.52 7.31 o 8 8 10 19.41 21.48 2.04 o 3 9 10 30.19 26.08 2.25 o 4 9 10 6.22 3.51 1.17 o 5 9 10 237.39 240.20 6.26 o 6 9 10 253.18 246.58 6.33 o 7 9 10 104.21 119.62 5.85 o 2 -5 11 9.42 9.81 2.68 o 3 -5 11 34.73 33.34 4.16 o 1 -4 11 964.17 1024.94 22.99 o 2 -4 11 114.95 122.15 6.66 o 3 -4 11 207.58 213.66 9.07 o 4 -4 11 171.43 174.42 8.35 o 5 -4 11 29.86 26.90 3.94 o -1 -3 11 117.53 118.51 5.57 o 1 -3 11 0.54 -0.17 1.49 o 2 -3 11 23.43 22.79 3.22 o 3 -3 11 128.01 139.24 6.94 o 4 -3 11 122.92 125.32 6.71 o 5 -3 11 48.21 52.52 4.73 o 6 -3 11 60.65 61.29 5.05 o -2 -2 11 436.46 471.88 12.83 o -1 -2 11 406.05 441.31 11.92 o 0 -2 11 252.11 267.61 8.40 o 1 -2 11 207.94 226.32 8.08 o 2 -2 11 430.70 442.01 12.51 o 3 -2 11 285.99 274.99 9.66 o 4 -2 11 162.92 163.12 7.46 o 5 -2 11 137.17 157.92 7.56 o 6 -2 11 19.39 16.28 3.15 o 7 -2 11 84.28 86.58 5.82 o -2 -1 11 159.71 162.88 6.94 o -1 -1 11 247.33 278.11 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2 11 113.02 118.61 5.23 o 2 2 11 156.95 165.50 4.41 o 3 2 11 171.71 165.74 4.39 o 4 2 11 55.35 55.27 2.45 o 5 2 11 203.24 203.11 7.88 o 6 2 11 189.55 180.41 7.58 o 7 2 11 81.82 81.23 5.15 o 8 2 11 104.01 97.92 5.77 o 9 2 11 77.27 73.08 5.18 o -2 3 11 128.87 149.94 6.84 o -1 3 11 216.78 211.53 7.98 o 0 3 11 85.00 78.95 4.53 o 1 3 11 12.77 8.50 1.81 o 2 3 11 217.55 199.42 4.94 o 3 3 11 132.42 135.36 4.55 o 4 3 11 7.37 9.24 1.29 o 5 3 11 271.94 270.58 5.81 o 6 3 11 276.49 270.88 9.46 o 7 3 11 103.90 115.96 6.07 o 8 3 11 199.62 192.80 8.10 o 9 3 11 178.75 159.70 7.48 o -1 4 11 0.68 -0.30 0.87 o 0 4 11 218.05 216.53 7.90 o 1 4 11 266.91 275.76 8.79 o 2 4 11 132.95 136.89 6.22 o 3 4 11 305.24 305.42 6.42 o 4 4 11 800.27 775.49 13.30 o 5 4 11 131.63 132.55 3.96 o 6 4 11 86.87 72.68 4.81 o 7 4 11 7.63 7.38 2.08 o 8 4 11 22.49 26.31 3.34 o 9 4 11 22.69 29.23 3.54 o -1 5 11 19.45 24.99 3.05 o 0 5 11 0.07 0.82 1.19 o 1 5 11 3.57 3.79 1.44 o 2 5 11 8.75 10.36 1.41 o 3 5 11 0.41 1.19 0.80 o 4 5 11 135.64 136.58 4.13 o 5 5 11 261.64 263.25 6.05 o 6 5 11 429.33 416.95 7.98 o 7 5 11 373.11 353.22 11.27 o 8 5 11 144.91 155.64 7.23 o 9 5 11 156.00 156.66 7.36 o 0 6 11 80.71 84.55 4.90 o 1 6 11 117.60 143.31 6.29 o 2 6 11 515.02 501.75 9.17 o 3 6 11 587.50 573.26 10.00 o 4 6 11 60.23 63.08 2.83 o 5 6 11 46.65 42.35 2.46 o 6 6 11 7.92 7.01 1.36 o 7 6 11 2.10 0.79 1.37 o 8 6 11 50.12 54.42 4.29 o 9 6 11 28.16 26.53 3.42 o 1 7 11 4.50 7.65 1.83 o 2 7 11 5.78 7.27 1.27 o 3 7 11 157.62 146.87 4.52 o 4 7 11 212.30 201.77 7.90 o 5 7 11 180.74 171.68 5.03 o 6 7 11 154.95 162.19 4.83 o 7 7 11 17.12 21.54 2.00 o 8 7 11 245.39 253.02 6.19 o 3 8 11 70.78 73.60 4.68 o 4 8 11 144.75 150.85 5.10 o 5 8 11 61.14 59.62 4.07 o 6 8 11 140.41 127.32 4.43 o 7 8 11 86.77 76.43 3.39 o 2 -3 12 76.46 79.49 5.35 o 3 -3 12 133.13 134.24 7.04 o 4 -3 12 288.12 295.26 10.92 o 2 -2 12 198.81 217.15 8.45 o 3 -2 12 131.37 138.33 6.89 o 4 -2 12 13.30 13.30 2.80 o 5 -2 12 7.58 9.17 2.68 o 6 -2 12 1.95 -0.87 1.66 o 0 -1 12 38.28 33.86 3.15 o 2 -1 12 336.08 329.96 10.45 o 3 -1 12 185.70 205.06 8.20 o 4 -1 12 32.01 35.25 3.81 o 5 -1 12 235.37 242.20 9.46 o 6 -1 12 185.45 182.00 8.35 o 7 -1 12 112.45 130.30 7.26 o 0 0 12 249.83 259.73 8.72 o 2 0 12 123.27 125.82 5.97 o 3 0 12 508.06 492.34 13.45 o 4 0 12 23.80 20.29 3.02 o 5 0 12 10.75 10.21 2.60 o 6 0 12 68.52 57.32 4.66 o 7 0 12 0.10 2.03 1.96 o 0 1 12 46.80 42.43 3.52 o 1 1 12 38.94 41.89 3.32 o 2 1 12 176.03 183.35 4.88 o 3 1 12 6.39 7.95 2.18 o 4 1 12 140.38 138.55 6.47 o 5 1 12 409.31 404.38 12.29 o 6 1 12 209.43 218.61 8.82 o 7 1 12 228.54 215.19 8.97 o 8 1 12 126.08 125.02 6.79 o 0 2 12 210.57 224.58 8.20 o 1 2 12 297.96 319.48 9.74 o 2 2 12 562.60 556.41 9.65 o 3 2 12 75.24 80.34 4.95 o 4 2 12 31.61 27.27 3.20 o 5 2 12 0.73 0.10 1.56 o 6 2 12 3.90 3.57 1.83 o 7 2 12 32.67 28.44 3.64 o 8 2 12 193.40 207.02 8.87 o 0 3 12 20.26 23.16 2.95 o 1 3 12 21.06 22.12 2.75 o 2 3 12 215.64 217.37 5.42 o 3 3 12 335.40 325.90 6.85 o 4 3 12 339.53 369.99 13.96 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