#------------------------------------------------------------------------------ #$Date: 2010-01-22 14:33:52 +0200 (Fri, 22 Jan 2010) $ #$Revision: 960 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2224195.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2224195_Fobs loop_ _publ_author_name 'Hou, Hong-Bo' 'Liu, Yi-Ming' 'Yang, Luan-Fang' _publ_section_title ; 1-(3-Pyridyl)pyrrolidine-2,5-dione ; _journal_coeditor_code FB2172 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3054 _journal_volume 65 _journal_year 2009 _space_group_IT_number 33 _symmetry_space_group_name_Hall 'P 2c -2n' _symmetry_space_group_name_H-M 'P n a 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 12.1368 _cell_length_b 10.8382 _cell_length_c 6.8308 _exptl_crystal_F_000 368.00 _reflns_d_resolution_high 0.8409 _[local]_cod_data_source_file fb2172Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ZZZ in Pna2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 72.53 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z+1/2' 'x+1/2, -y+1/2, z' '-x+1/2, y+1/2, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2556.86 2557.75 67.14 o 4 0 0 4381.69 4379.60 114.76 o 6 0 0 27.11 23.75 2.92 o 8 0 0 39.57 41.34 3.54 o 10 0 0 15.72 17.95 3.02 o 12 0 0 2.25 1.11 2.36 o 14 0 0 1.80 0.68 2.95 o 1 1 0 947.91 936.37 26.01 o 2 1 0 1079.32 1103.62 21.03 o 3 1 0 2067.32 2036.33 48.68 o 4 1 0 32.75 31.49 1.51 o 5 1 0 14.70 18.47 1.35 o 6 1 0 20.89 21.47 1.60 o 7 1 0 305.31 298.60 9.73 o 8 1 0 109.24 123.11 7.82 o 9 1 0 10.13 8.54 1.49 o 10 1 0 1.00 -0.10 1.05 o 11 1 0 33.36 36.03 3.96 o 12 1 0 0.75 -0.70 1.50 o 13 1 0 11.71 10.29 3.51 o 14 1 0 9.63 19.13 3.62 o 0 2 0 136.21 137.43 4.55 o 1 2 0 2488.03 2259.00 128.55 o 2 2 0 1465.57 1396.24 24.54 o 3 2 0 2162.25 2153.19 62.83 o 4 2 0 11.46 17.83 8.76 o 5 2 0 169.15 176.41 12.41 o 6 2 0 146.83 146.36 4.44 o 7 2 0 331.56 314.84 8.38 o 8 2 0 0.04 0.50 0.75 o 9 2 0 2.72 1.83 1.43 o 10 2 0 295.38 292.05 15.58 o 11 2 0 39.37 36.07 3.52 o 12 2 0 0.18 -0.60 1.57 o 13 2 0 1.50 1.15 2.67 o 14 2 0 9.36 8.43 3.79 o 1 3 0 2775.92 2540.91 42.43 o 2 3 0 2069.71 2086.25 58.00 o 3 3 0 5.20 4.82 0.72 o 4 3 0 2.76 2.75 0.71 o 5 3 0 0.89 1.14 0.61 o 6 3 0 0.07 1.79 0.96 o 7 3 0 65.96 68.06 3.10 o 8 3 0 226.87 214.84 14.98 o 9 3 0 3.10 2.23 1.31 o 10 3 0 0.02 0.08 1.15 o 11 3 0 1.48 -0.05 1.31 o 12 3 0 0.08 -1.15 1.27 o 13 3 0 5.39 2.03 2.09 o 14 3 0 0.55 -2.31 2.47 o 0 4 0 1067.94 1051.65 46.35 o 1 4 0 53.75 48.12 1.81 o 2 4 0 13.97 14.40 1.18 o 3 4 0 72.86 73.84 2.37 o 4 4 0 17.36 21.63 1.62 o 5 4 0 6.97 6.77 1.06 o 6 4 0 38.38 37.49 2.24 o 7 4 0 102.04 100.12 6.88 o 8 4 0 459.93 453.48 23.11 o 9 4 0 24.95 22.70 2.74 o 10 4 0 52.85 53.39 3.87 o 11 4 0 28.98 30.85 3.47 o 12 4 0 13.06 8.79 2.52 o 13 4 0 3.78 1.62 2.10 o 1 5 0 529.41 513.53 10.92 o 2 5 0 4.64 4.44 0.88 o 3 5 0 5.44 6.37 0.99 o 4 5 0 67.86 64.21 2.60 o 5 5 0 44.47 42.67 2.20 o 6 5 0 0.34 0.25 0.70 o 7 5 0 9.57 11.27 2.00 o 8 5 0 49.57 44.98 2.95 o 9 5 0 95.72 92.00 9.17 o 10 5 0 136.08 137.13 6.50 o 11 5 0 2.61 2.23 1.78 o 12 5 0 0.02 0.83 1.74 o 13 5 0 9.06 7.81 3.36 o 0 6 0 5.36 3.88 1.15 o 1 6 0 186.70 181.47 7.73 o 2 6 0 1.71 2.27 0.86 o 3 6 0 305.16 301.10 9.53 o 4 6 0 85.72 92.17 3.41 o 5 6 0 65.72 67.13 3.75 o 6 6 0 5.30 6.91 1.58 o 7 6 0 18.14 20.28 2.35 o 8 6 0 56.03 54.65 3.38 o 9 6 0 7.50 4.05 1.89 o 10 6 0 8.65 6.48 2.11 o 11 6 0 17.54 18.10 3.15 o 12 6 0 0.01 -0.96 1.98 o 1 7 0 259.53 249.73 6.28 o 2 7 0 0.09 -0.26 0.73 o 3 7 0 42.41 44.23 4.42 o 4 7 0 1.02 -0.44 0.86 o 5 7 0 468.73 460.92 13.08 o 6 7 0 64.64 63.96 3.60 o 7 7 0 153.93 154.98 9.88 o 8 7 0 84.28 84.73 5.58 o 9 7 0 2.99 4.01 2.10 o 10 7 0 10.41 10.96 2.71 o 11 7 0 5.22 10.20 3.88 o 12 7 0 1.01 3.97 4.54 o 0 8 0 669.61 633.83 23.87 o 1 8 0 103.08 93.78 7.30 o 2 8 0 199.80 205.40 5.82 o 3 8 0 4.05 7.91 1.62 o 4 8 0 81.15 77.27 3.79 o 5 8 0 147.41 150.67 7.32 o 6 8 0 23.87 29.73 3.26 o 7 8 0 20.21 23.33 2.76 o 8 8 0 39.00 41.85 3.76 o 9 8 0 1.75 1.35 2.31 o 10 8 0 4.90 3.88 3.04 o 1 9 0 42.30 48.39 4.81 o 2 9 0 99.94 92.39 7.39 o 3 9 0 62.10 54.38 8.79 o 4 9 0 0.02 0.20 1.44 o 5 9 0 1.73 0.83 1.61 o 6 9 0 2.78 3.33 1.83 o 7 9 0 3.33 4.06 2.68 o 8 9 0 9.45 11.09 3.91 o 9 9 0 15.25 18.56 4.29 o 0 10 0 136.81 139.69 7.80 o 1 10 0 10.27 9.89 2.59 o 2 10 0 10.93 10.69 2.22 o 3 10 0 8.26 6.32 2.36 o 4 10 0 2.09 0.52 1.77 o 5 10 0 0.87 -1.23 2.26 o 6 10 0 61.60 68.87 6.38 o 7 10 0 3.64 5.45 2.98 o 8 10 0 0.04 0.70 2.68 o 9 10 0 0.94 1.14 6.00 o 1 11 0 0.07 2.35 2.84 o 2 11 0 7.80 7.43 3.40 o 3 11 0 3.14 2.95 2.99 o 4 11 0 4.72 8.92 3.40 o 5 11 0 1.62 1.04 2.67 o 6 11 0 0.10 -1.45 2.66 o 7 11 0 4.13 4.79 4.60 o 0 12 0 2.16 -1.22 7.44 o 1 12 0 0.04 2.03 4.58 o 2 12 0 0.16 1.10 4.27 o 3 12 0 9.48 14.09 4.80 o 4 12 0 3.37 4.15 3.68 o 5 12 0 9.62 9.43 5.93 o 2 0 1 3076.07 3288.84 56.14 o 4 0 1 5260.73 5729.62 163.62 o 6 0 1 404.84 403.21 9.31 o 8 0 1 87.28 85.70 3.52 o 10 0 1 5.05 2.80 1.56 o 12 0 1 129.85 139.44 11.46 o 14 0 1 18.81 14.06 4.51 o 0 1 1 2869.91 2912.65 115.37 o 1 1 1 2637.57 2730.90 68.11 o 2 1 1 2840.95 2932.24 56.09 o 3 1 1 3997.17 4123.82 82.47 o 4 1 1 721.65 741.62 11.05 o 5 1 1 212.61 202.95 3.58 o 6 1 1 492.22 492.01 7.44 o 7 1 1 357.43 361.91 6.26 o 8 1 1 0.92 2.19 0.76 o 9 1 1 3.95 4.05 0.93 o 10 1 1 16.37 17.19 1.65 o 11 1 1 9.87 8.07 1.39 o 12 1 1 9.80 9.07 1.69 o 13 1 1 9.72 8.07 1.92 o 14 1 1 3.33 1.93 2.70 o 1 2 1 2681.10 2561.63 76.72 o 2 2 1 1460.15 1395.14 21.24 o 3 2 1 427.40 426.93 6.72 o 4 2 1 16.29 13.93 1.31 o 5 2 1 68.63 69.44 1.83 o 6 2 1 409.96 429.51 7.08 o 7 2 1 11.03 9.81 1.03 o 8 2 1 45.13 50.17 2.11 o 9 2 1 76.05 71.53 2.63 o 10 2 1 34.67 30.68 2.15 o 11 2 1 26.47 27.76 2.38 o 12 2 1 10.58 11.33 1.81 o 13 2 1 7.46 4.83 1.71 o 14 2 1 13.35 8.57 4.02 o 0 3 1 890.42 869.41 16.07 o 1 3 1 202.19 189.75 3.31 o 2 3 1 305.95 294.38 4.81 o 3 3 1 1158.28 1155.51 19.99 o 4 3 1 1161.83 1194.03 16.51 o 5 3 1 52.52 54.97 1.50 o 6 3 1 204.11 200.80 5.15 o 7 3 1 26.01 25.26 1.47 o 8 3 1 227.89 228.63 9.58 o 9 3 1 5.85 4.46 0.99 o 10 3 1 25.74 26.92 2.11 o 11 3 1 50.58 54.11 3.50 o 12 3 1 16.19 17.49 2.19 o 13 3 1 0.85 0.23 1.64 o 1 4 1 39.18 42.38 1.18 o 2 4 1 817.23 774.13 20.82 o 3 4 1 26.02 29.34 1.15 o 4 4 1 1391.39 1437.72 40.04 o 5 4 1 79.97 79.22 2.65 o 6 4 1 9.53 10.38 1.25 o 7 4 1 65.73 65.76 2.28 o 8 4 1 62.22 64.77 2.39 o 9 4 1 25.22 23.43 1.97 o 10 4 1 71.93 72.32 3.20 o 11 4 1 11.74 12.43 1.87 o 12 4 1 5.88 5.60 1.93 o 13 4 1 4.53 3.57 2.33 o 0 5 1 389.34 393.23 8.81 o 1 5 1 8.18 7.06 0.65 o 2 5 1 380.17 374.87 9.39 o 3 5 1 120.89 117.10 2.49 o 4 5 1 472.10 469.67 7.50 o 5 5 1 67.34 69.10 2.27 o 6 5 1 17.16 16.99 1.37 o 7 5 1 14.07 16.68 1.45 o 8 5 1 5.65 6.30 1.18 o 9 5 1 2.93 2.89 1.08 o 10 5 1 16.01 14.11 1.98 o 11 5 1 0.22 0.22 1.37 o 12 5 1 8.23 7.53 2.09 o 13 5 1 2.90 2.22 2.91 o 1 6 1 106.56 111.92 2.98 o 2 6 1 205.11 205.49 3.76 o 3 6 1 22.92 21.00 1.24 o 4 6 1 60.27 61.31 2.11 o 5 6 1 9.40 10.58 1.12 o 6 6 1 52.06 53.24 2.08 o 7 6 1 219.35 219.66 5.09 o 8 6 1 93.85 90.09 3.30 o 9 6 1 22.99 27.02 2.50 o 10 6 1 12.24 16.06 2.14 o 11 6 1 39.69 45.02 3.60 o 12 6 1 6.34 4.82 2.27 o 0 7 1 235.64 223.82 9.47 o 1 7 1 38.14 44.13 2.16 o 2 7 1 71.15 75.60 2.32 o 3 7 1 92.21 91.59 2.40 o 4 7 1 20.37 22.32 1.58 o 5 7 1 127.13 137.83 3.42 o 6 7 1 38.22 42.65 2.08 o 7 7 1 179.92 175.50 5.45 o 8 7 1 27.63 32.03 2.66 o 9 7 1 11.73 10.89 1.90 o 10 7 1 2.72 1.55 1.51 o 11 7 1 10.15 10.90 2.34 o 1 8 1 34.94 38.45 2.55 o 2 8 1 1.45 1.03 0.72 o 3 8 1 21.53 24.61 1.74 o 4 8 1 82.79 84.22 3.49 o 5 8 1 105.50 109.47 3.67 o 6 8 1 23.56 23.45 2.26 o 7 8 1 22.85 27.21 2.38 o 8 8 1 9.03 9.48 1.78 o 9 8 1 15.12 14.45 2.19 o 10 8 1 10.45 10.34 2.11 o 11 8 1 11.36 9.19 4.45 o 0 9 1 132.16 135.77 6.44 o 1 9 1 81.56 78.81 2.80 o 2 9 1 15.80 17.13 1.81 o 3 9 1 50.75 53.65 2.59 o 4 9 1 86.00 89.60 4.59 o 5 9 1 62.87 66.04 3.33 o 6 9 1 30.99 32.62 3.18 o 7 9 1 1.93 2.35 1.52 o 8 9 1 29.56 35.19 3.21 o 9 9 1 2.11 2.33 1.76 o 10 9 1 6.13 7.30 3.64 o 1 10 1 20.80 15.84 3.27 o 2 10 1 41.39 41.69 3.11 o 3 10 1 9.50 8.24 1.73 o 4 10 1 30.24 27.73 2.63 o 5 10 1 0.12 0.51 1.45 o 6 10 1 7.69 6.13 2.43 o 7 10 1 14.83 22.31 2.65 o 8 10 1 5.01 4.37 1.92 o 0 11 1 3.58 3.82 2.79 o 1 11 1 35.71 34.05 3.46 o 2 11 1 2.21 2.94 1.81 o 3 11 1 43.60 48.30 7.11 o 4 11 1 12.23 14.36 2.73 o 5 11 1 5.77 7.25 2.38 o 6 11 1 2.43 1.92 2.01 o 7 11 1 1.93 3.81 4.22 o 1 12 1 2.65 3.76 2.32 o 2 12 1 1.14 3.00 2.18 o 3 12 1 14.64 17.03 3.53 o 4 12 1 1.19 -0.38 2.36 o 0 0 2 1144.14 1118.26 26.26 o 2 0 2 375.67 349.73 7.59 o 4 0 2 150.10 147.08 5.22 o 6 0 2 214.82 235.44 6.21 o 8 0 2 126.45 133.16 4.72 o 10 0 2 28.91 33.80 6.92 o 12 0 2 63.08 69.31 5.18 o 1 1 2 197.23 185.35 4.29 o 2 1 2 948.12 900.16 15.56 o 3 1 2 701.29 689.82 22.31 o 4 1 2 202.26 205.35 3.65 o 5 1 2 220.88 221.93 3.74 o 6 1 2 178.66 182.93 5.83 o 7 1 2 49.30 44.95 1.67 o 8 1 2 168.13 168.10 3.88 o 9 1 2 67.99 70.25 2.56 o 10 1 2 40.25 43.95 2.06 o 11 1 2 24.25 22.74 2.16 o 12 1 2 112.99 105.84 4.49 o 13 1 2 6.61 10.11 2.73 o 0 2 2 68.34 69.84 4.22 o 1 2 2 145.51 147.64 3.06 o 2 2 2 310.54 304.88 6.40 o 3 2 2 601.98 607.87 14.19 o 4 2 2 302.74 300.78 5.22 o 5 2 2 97.14 103.02 2.41 o 6 2 2 471.10 473.01 10.48 o 7 2 2 55.57 55.01 2.54 o 8 2 2 69.10 70.09 3.75 o 9 2 2 2.93 3.42 0.95 o 10 2 2 25.94 26.84 2.11 o 11 2 2 6.15 6.48 1.66 o 12 2 2 2.66 3.04 1.68 o 13 2 2 0.62 -0.62 1.58 o 1 3 2 357.41 373.60 6.23 o 2 3 2 1440.87 1447.53 18.79 o 3 3 2 660.93 650.85 11.69 o 4 3 2 680.82 694.84 11.85 o 5 3 2 406.47 436.30 9.78 o 6 3 2 44.38 46.65 1.84 o 7 3 2 283.81 281.07 5.35 o 8 3 2 50.87 49.00 1.97 o 9 3 2 5.66 5.54 1.24 o 10 3 2 73.74 78.30 3.44 o 11 3 2 39.62 36.50 3.32 o 12 3 2 10.17 8.86 2.15 o 13 3 2 0.13 0.65 1.92 o 0 4 2 1441.56 1481.27 49.19 o 1 4 2 495.51 487.30 6.83 o 2 4 2 303.91 313.75 6.30 o 3 4 2 97.15 92.80 2.06 o 4 4 2 167.12 170.71 3.54 o 5 4 2 169.29 169.68 4.62 o 6 4 2 45.95 44.73 2.17 o 7 4 2 14.03 14.88 1.60 o 8 4 2 25.35 31.64 2.20 o 9 4 2 40.24 42.09 2.68 o 10 4 2 5.52 8.42 1.67 o 11 4 2 0.97 0.30 1.45 o 12 4 2 3.96 2.70 1.81 o 13 4 2 4.85 2.46 2.91 o 1 5 2 202.50 211.04 3.71 o 2 5 2 725.67 738.57 11.54 o 3 5 2 7.04 6.47 0.75 o 4 5 2 103.72 99.34 2.52 o 5 5 2 63.96 61.88 2.43 o 6 5 2 58.25 58.26 2.58 o 7 5 2 70.75 76.65 4.26 o 8 5 2 83.12 82.61 3.29 o 9 5 2 0.14 0.55 1.10 o 10 5 2 39.61 40.58 3.08 o 11 5 2 15.69 13.71 2.18 o 12 5 2 6.85 8.44 2.33 o 0 6 2 39.70 45.81 2.36 o 1 6 2 22.46 25.03 1.74 o 2 6 2 16.37 15.25 1.24 o 3 6 2 183.64 185.06 4.25 o 4 6 2 158.44 165.69 4.22 o 5 6 2 71.69 69.64 3.09 o 6 6 2 42.92 45.97 3.63 o 7 6 2 40.13 36.07 3.59 o 8 6 2 25.20 25.65 3.08 o 9 6 2 10.28 7.23 1.69 o 10 6 2 18.87 22.10 2.53 o 11 6 2 29.82 39.13 3.36 o 1 7 2 31.83 34.18 1.96 o 2 7 2 14.53 14.19 1.58 o 3 7 2 27.53 29.12 2.59 o 4 7 2 45.84 49.32 2.52 o 5 7 2 29.18 27.91 3.21 o 6 7 2 19.55 16.09 1.79 o 7 7 2 3.85 3.22 1.33 o 8 7 2 20.68 23.36 3.64 o 9 7 2 37.46 35.61 5.07 o 10 7 2 4.95 6.08 1.89 o 11 7 2 23.95 25.97 3.27 o 0 8 2 62.55 59.61 3.49 o 1 8 2 8.34 8.65 1.44 o 2 8 2 12.13 13.06 1.67 o 3 8 2 37.76 40.16 3.83 o 4 8 2 31.71 35.72 4.63 o 5 8 2 33.02 30.93 2.35 o 6 8 2 22.18 22.70 2.31 o 7 8 2 136.32 138.18 5.76 o 8 8 2 10.05 13.33 2.34 o 9 8 2 6.34 5.26 1.83 o 10 8 2 10.16 8.60 2.38 o 1 9 2 61.41 62.17 3.17 o 2 9 2 1.41 1.16 1.31 o 3 9 2 10.67 8.45 1.82 o 4 9 2 60.46 52.07 8.50 o 5 9 2 8.77 5.98 1.84 o 6 9 2 3.48 3.53 1.58 o 7 9 2 9.88 11.25 2.13 o 8 9 2 8.33 4.82 1.88 o 9 9 2 8.25 8.76 2.54 o 0 10 2 11.57 12.82 5.50 o 1 10 2 62.70 64.30 4.60 o 2 10 2 21.41 19.49 2.43 o 3 10 2 157.65 166.20 7.29 o 4 10 2 5.01 5.65 1.94 o 5 10 2 8.08 7.44 2.33 o 6 10 2 27.53 20.56 3.03 o 7 10 2 1.50 0.69 1.96 o 8 10 2 0.88 1.44 3.19 o 1 11 2 9.97 10.67 2.35 o 2 11 2 20.20 17.86 2.57 o 3 11 2 39.04 36.24 3.80 o 4 11 2 2.29 2.01 2.16 o 5 11 2 7.04 6.35 2.68 o 6 11 2 15.15 17.06 4.56 o 0 12 2 13.76 14.48 4.38 o 1 12 2 5.45 8.16 3.25 o 2 12 2 0.83 3.30 2.83 o 3 12 2 14.63 11.79 5.05 o 2 0 3 15.45 13.78 1.18 o 4 0 3 155.46 140.12 4.16 o 6 0 3 121.68 130.43 4.93 o 8 0 3 77.74 73.33 3.75 o 10 0 3 85.06 82.03 5.00 o 12 0 3 55.70 42.94 5.40 o 0 1 3 2331.11 2401.54 121.13 o 1 1 3 34.45 39.40 1.37 o 2 1 3 391.00 359.49 29.53 o 3 1 3 84.86 83.18 5.06 o 4 1 3 28.02 27.85 1.19 o 5 1 3 22.40 22.22 1.24 o 6 1 3 538.71 521.80 16.26 o 7 1 3 73.70 73.16 2.33 o 8 1 3 38.89 40.08 5.13 o 9 1 3 47.03 49.59 2.54 o 10 1 3 22.36 25.21 3.28 o 11 1 3 59.83 55.59 2.81 o 12 1 3 6.39 6.34 2.05 o 13 1 3 24.54 33.00 6.77 o 1 2 3 25.11 24.34 1.23 o 2 2 3 109.85 100.37 8.62 o 3 2 3 55.55 58.61 2.17 o 4 2 3 19.98 19.72 1.11 o 5 2 3 145.04 146.98 4.01 o 6 2 3 19.45 18.61 1.46 o 7 2 3 123.88 126.17 3.47 o 8 2 3 168.46 165.09 4.52 o 9 2 3 31.86 31.51 4.93 o 10 2 3 7.99 9.80 1.63 o 11 2 3 11.74 12.96 2.01 o 12 2 3 0.62 0.83 1.42 o 13 2 3 7.90 8.33 6.78 o 0 3 3 22.83 20.55 1.81 o 1 3 3 30.89 33.58 1.28 o 2 3 3 73.11 79.12 2.16 o 3 3 3 287.12 294.18 5.85 o 4 3 3 2.67 2.23 0.67 o 5 3 3 190.51 191.81 4.57 o 6 3 3 6.91 6.76 1.09 o 7 3 3 45.01 42.17 2.12 o 8 3 3 33.55 34.43 2.42 o 9 3 3 52.08 54.46 3.45 o 10 3 3 49.44 46.73 6.23 o 11 3 3 35.44 36.47 3.26 o 12 3 3 0.85 1.26 1.71 o 1 4 3 205.26 201.27 4.27 o 2 4 3 118.58 124.11 3.19 o 3 4 3 263.18 270.81 5.42 o 4 4 3 274.19 268.48 6.78 o 5 4 3 4.17 2.73 0.87 o 6 4 3 38.71 37.69 2.22 o 7 4 3 0.89 0.70 0.89 o 8 4 3 79.82 83.07 3.14 o 9 4 3 35.95 37.68 2.44 o 10 4 3 100.00 99.92 9.23 o 11 4 3 27.86 26.13 4.35 o 12 4 3 15.73 11.57 2.95 o 0 5 3 327.80 322.83 8.18 o 1 5 3 27.71 29.25 1.81 o 2 5 3 82.06 78.57 2.54 o 3 5 3 30.98 36.12 1.89 o 4 5 3 49.55 45.74 2.65 o 5 5 3 16.72 16.92 2.11 o 6 5 3 19.83 18.44 2.14 o 7 5 3 0.47 -0.15 0.98 o 8 5 3 67.31 68.50 3.17 o 9 5 3 0.80 -1.07 1.08 o 10 5 3 72.37 70.55 6.55 o 11 5 3 6.92 8.97 2.17 o 12 5 3 2.02 2.17 2.87 o 1 6 3 291.25 286.54 5.82 o 2 6 3 87.45 80.56 4.47 o 3 6 3 6.39 5.79 1.26 o 4 6 3 70.23 72.19 3.16 o 5 6 3 47.63 44.80 3.45 o 6 6 3 0.69 -0.27 1.01 o 7 6 3 34.43 34.23 4.17 o 8 6 3 39.97 34.82 4.43 o 9 6 3 1.89 2.40 1.43 o 10 6 3 2.12 4.29 1.69 o 11 6 3 0.53 0.76 1.71 o 0 7 3 92.97 86.81 3.92 o 1 7 3 38.23 36.86 2.31 o 2 7 3 10.09 9.56 1.56 o 3 7 3 14.11 13.63 2.09 o 4 7 3 28.82 33.38 2.77 o 5 7 3 167.31 162.93 5.21 o 6 7 3 28.38 32.04 3.66 o 7 7 3 30.64 30.47 4.11 o 8 7 3 9.97 8.81 1.84 o 9 7 3 7.92 7.75 2.07 o 10 7 3 19.36 26.51 3.37 o 1 8 3 82.40 78.72 3.87 o 2 8 3 28.99 28.97 3.05 o 3 8 3 80.26 79.98 3.61 o 4 8 3 23.23 27.72 2.67 o 5 8 3 50.51 44.75 4.65 o 6 8 3 16.59 15.03 2.99 o 7 8 3 50.72 50.31 3.81 o 8 8 3 22.29 17.24 2.81 o 9 8 3 0.37 0.48 1.89 o 0 9 3 337.30 324.97 12.06 o 1 9 3 10.29 9.70 2.33 o 2 9 3 16.65 15.01 2.43 o 3 9 3 10.55 9.02 1.95 o 4 9 3 20.51 21.46 2.61 o 5 9 3 12.87 11.30 2.13 o 6 9 3 7.53 9.33 2.21 o 7 9 3 9.71 6.46 2.30 o 8 9 3 3.16 2.12 2.70 o 1 10 3 9.86 9.19 2.08 o 2 10 3 5.78 7.51 1.97 o 3 10 3 27.28 30.09 3.68 o 4 10 3 4.98 3.51 1.98 o 5 10 3 8.39 6.46 2.18 o 6 10 3 8.80 6.43 2.51 o 7 10 3 9.52 7.07 6.79 o 0 11 3 16.32 8.54 5.09 o 1 11 3 5.03 4.94 2.03 o 2 11 3 2.02 0.91 1.96 o 3 11 3 24.53 26.40 3.37 o 4 11 3 1.23 1.04 2.81 o 5 11 3 15.83 19.02 9.17 o 0 0 4 1153.34 1242.79 35.24 o 2 0 4 102.73 97.82 3.59 o 4 0 4 282.26 277.12 7.19 o 6 0 4 402.59 408.84 15.05 o 8 0 4 189.34 180.93 7.66 o 10 0 4 18.26 21.31 3.40 o 12 0 4 14.54 19.41 5.34 o 1 1 4 162.01 159.10 4.84 o 2 1 4 215.51 211.23 5.34 o 3 1 4 1.83 2.16 0.62 o 4 1 4 83.42 75.15 2.98 o 5 1 4 3.24 2.46 0.76 o 6 1 4 116.16 110.88 3.37 o 7 1 4 31.43 28.23 5.04 o 8 1 4 38.12 39.75 2.98 o 9 1 4 43.81 43.36 3.09 o 10 1 4 3.42 3.44 1.53 o 11 1 4 7.84 6.14 1.80 o 12 1 4 0.53 2.06 1.88 o 0 2 4 124.90 92.29 41.12 o 1 2 4 236.19 234.84 8.72 o 2 2 4 53.88 57.04 1.89 o 3 2 4 85.24 87.38 2.94 o 4 2 4 108.19 100.69 6.36 o 5 2 4 60.78 53.61 5.24 o 6 2 4 5.43 6.42 1.13 o 7 2 4 20.48 20.90 1.81 o 8 2 4 92.34 93.36 4.05 o 9 2 4 58.14 57.02 9.80 o 10 2 4 48.61 48.72 4.84 o 11 2 4 4.57 5.04 1.85 o 12 2 4 8.95 9.79 3.17 o 1 3 4 0.55 0.83 0.61 o 2 3 4 3.11 3.61 0.90 o 3 3 4 0.13 0.05 0.65 o 4 3 4 91.84 92.77 3.00 o 5 3 4 58.10 58.76 2.55 o 6 3 4 45.25 54.86 4.03 o 7 3 4 75.34 79.87 4.55 o 8 3 4 0.36 0.45 1.01 o 9 3 4 82.70 77.83 4.88 o 10 3 4 16.98 16.50 5.04 o 11 3 4 7.49 4.78 2.06 o 12 3 4 4.66 2.81 5.97 o 0 4 4 231.86 231.78 13.61 o 1 4 4 81.47 79.70 2.63 o 2 4 4 25.80 25.64 2.13 o 3 4 4 16.99 17.67 1.75 o 4 4 4 29.58 32.70 2.46 o 5 4 4 20.06 22.08 2.08 o 6 4 4 45.87 45.50 2.70 o 7 4 4 17.74 19.03 1.85 o 8 4 4 9.46 9.32 1.50 o 9 4 4 21.15 19.63 3.38 o 10 4 4 12.86 12.71 2.00 o 11 4 4 1.91 1.95 1.56 o 1 5 4 51.33 51.25 2.63 o 2 5 4 52.89 50.36 2.64 o 3 5 4 24.75 27.43 3.78 o 4 5 4 246.80 242.47 7.08 o 5 5 4 9.57 8.47 1.76 o 6 5 4 28.65 29.99 2.82 o 7 5 4 20.16 16.99 2.26 o 8 5 4 9.31 7.24 1.81 o 9 5 4 30.98 25.19 4.41 o 10 5 4 6.98 6.69 1.77 o 11 5 4 3.47 0.70 2.23 o 0 6 4 32.51 35.36 2.93 o 1 6 4 4.70 4.61 1.28 o 2 6 4 81.07 73.11 3.54 o 3 6 4 71.86 66.90 3.15 o 4 6 4 72.37 65.51 3.55 o 5 6 4 7.49 3.72 1.46 o 6 6 4 44.48 47.30 4.14 o 7 6 4 19.85 18.90 2.39 o 8 6 4 13.37 12.08 2.17 o 9 6 4 2.27 1.82 1.64 o 10 6 4 3.43 1.32 3.14 o 1 7 4 368.41 357.35 10.65 o 2 7 4 105.24 98.01 3.98 o 3 7 4 26.43 28.10 2.49 o 4 7 4 1.89 0.61 1.34 o 5 7 4 32.82 26.59 2.68 o 6 7 4 34.13 33.81 4.58 o 7 7 4 6.21 5.50 1.74 o 8 7 4 2.88 2.25 1.77 o 9 7 4 2.54 2.83 2.63 o 0 8 4 41.53 37.97 4.10 o 1 8 4 35.54 33.00 3.46 o 2 8 4 3.98 6.01 1.60 o 3 8 4 12.90 15.37 2.50 o 4 8 4 40.35 35.79 7.60 o 5 8 4 13.15 10.49 2.12 o 6 8 4 14.32 11.10 2.27 o 7 8 4 7.10 7.16 2.10 o 8 8 4 6.35 9.97 3.14 o 1 9 4 20.71 17.33 2.36 o 2 9 4 50.63 39.05 8.08 o 3 9 4 0.32 1.21 1.41 o 4 9 4 12.67 16.23 2.52 o 5 9 4 5.28 3.52 2.02 o 6 9 4 8.38 5.52 2.14 o 7 9 4 2.23 5.19 5.18 o 0 10 4 9.96 9.74 2.98 o 1 10 4 1.18 0.96 1.94 o 2 10 4 11.09 11.40 2.55 o 3 10 4 11.71 12.16 2.57 o 4 10 4 1.35 2.07 2.70 o 5 10 4 2.16 -1.37 4.24 o 1 11 4 1.39 5.07 7.85 o 2 0 5 32.47 23.84 3.71 o 6 0 5 148.27 148.10 7.98 o 8 0 5 49.27 46.01 4.30 o 10 0 5 0.78 0.96 2.16 o 0 1 5 11.06 8.17 2.59 o 1 1 5 1.12 1.66 0.80 o 2 1 5 15.15 15.91 2.47 o 3 1 5 150.60 102.86 42.26 o 4 1 5 7.23 5.70 1.93 o 5 1 5 35.54 32.40 7.48 o 6 1 5 37.49 38.96 8.32 o 7 1 5 48.49 51.94 10.10 o 8 1 5 5.13 4.80 1.53 o 9 1 5 2.76 1.95 1.38 o 10 1 5 9.79 11.67 2.21 o 11 1 5 5.21 3.97 2.91 o 1 2 5 67.84 74.26 3.09 o 2 2 5 67.38 74.93 3.13 o 3 2 5 161.25 169.53 4.63 o 4 2 5 160.56 169.12 5.64 o 5 2 5 89.94 87.46 4.56 o 6 2 5 133.03 136.82 5.82 o 7 2 5 35.14 23.64 7.68 o 8 2 5 8.23 5.65 1.69 o 9 2 5 2.91 3.60 1.65 o 10 2 5 0.19 0.07 1.52 o 11 2 5 1.72 2.52 2.68 o 0 3 5 43.26 46.58 3.91 o 1 3 5 31.97 33.98 3.11 o 2 3 5 19.13 12.67 4.81 o 3 3 5 58.86 60.24 2.89 o 4 3 5 56.97 57.38 2.76 o 5 3 5 16.14 12.32 2.50 o 6 3 5 39.66 44.03 8.75 o 7 3 5 27.33 20.51 5.18 o 8 3 5 4.34 3.05 1.78 o 9 3 5 5.55 5.03 2.22 o 10 3 5 2.05 2.44 1.99 o 1 4 5 2.31 2.40 0.89 o 2 4 5 329.26 302.60 36.93 o 3 4 5 20.43 20.07 2.76 o 4 4 5 112.44 108.95 4.24 o 5 4 5 31.22 34.46 3.55 o 6 4 5 21.27 19.18 2.17 o 7 4 5 1.70 0.66 1.22 o 8 4 5 20.52 17.99 6.73 o 9 4 5 2.35 1.96 1.64 o 10 4 5 1.26 -3.34 4.96 o 0 5 5 172.44 184.18 8.10 o 1 5 5 13.83 15.39 2.34 o 2 5 5 110.34 115.60 3.98 o 3 5 5 27.48 33.10 4.30 o 4 5 5 5.90 7.08 1.50 o 5 5 5 6.55 6.11 1.52 o 6 5 5 9.61 7.48 1.61 o 7 5 5 0.39 0.13 1.50 o 8 5 5 1.88 2.30 1.92 o 9 5 5 3.41 0.29 2.26 o 1 6 5 80.23 78.01 4.11 o 2 6 5 183.18 193.04 6.15 o 3 6 5 16.48 16.47 2.14 o 4 6 5 2.16 0.89 1.20 o 5 6 5 69.28 70.68 5.67 o 6 6 5 15.13 13.49 2.48 o 7 6 5 8.42 10.11 2.18 o 8 6 5 16.25 12.89 2.35 o 9 6 5 2.26 5.30 3.91 o 0 7 5 31.82 27.11 5.36 o 1 7 5 11.57 11.62 1.91 o 2 7 5 0.51 0.90 1.58 o 3 7 5 3.42 3.45 1.56 o 4 7 5 2.74 2.83 1.55 o 5 7 5 0.26 0.21 1.43 o 6 7 5 27.29 22.45 3.67 o 7 7 5 1.39 0.03 1.83 o 8 7 5 3.29 5.16 3.27 o 1 8 5 12.22 8.14 1.95 o 2 8 5 4.61 4.18 1.79 o 3 8 5 11.75 11.09 2.45 o 4 8 5 1.81 2.61 1.60 o 5 8 5 14.39 10.85 2.33 o 6 8 5 6.12 6.37 2.82 o 7 8 5 3.06 3.22 3.59 o 0 9 5 15.07 14.20 3.60 o 1 9 5 10.68 10.27 2.59 o 2 9 5 0.28 -1.14 1.48 o 3 9 5 1.73 3.10 1.92 o 4 9 5 0.90 -0.03 2.94 o 5 9 5 2.21 -0.93 6.36 o 1 10 5 6.69 12.92 8.46 o 2 10 5 4.44 9.88 8.41 o 0 0 6 111.89 121.11 11.03 o 2 0 6 16.97 20.95 5.60 o 4 0 6 3.62 6.86 4.36 o 6 0 6 8.67 11.69 4.11 o 8 0 6 3.64 -0.77 2.68 o 1 1 6 5.70 4.82 1.75 o 2 1 6 4.55 1.72 1.59 o 3 1 6 1.18 3.20 1.91 o 4 1 6 32.49 34.08 10.19 o 5 1 6 55.17 54.78 12.78 o 6 1 6 77.66 79.72 6.16 o 7 1 6 15.96 21.15 5.82 o 8 1 6 8.65 8.15 2.29 o 9 1 6 0.09 0.50 2.40 o 0 2 6 43.10 28.78 21.05 o 1 2 6 12.93 19.61 3.84 o 2 2 6 26.49 25.47 5.61 o 3 2 6 14.18 14.61 3.95 o 4 2 6 16.09 16.05 6.24 o 5 2 6 7.67 8.25 3.01 o 6 2 6 18.59 20.46 7.19 o 7 2 6 2.05 5.07 2.75 o 8 2 6 4.88 6.90 2.80 o 9 2 6 3.25 3.56 3.39 o 1 3 6 93.85 104.71 8.38 o 2 3 6 95.12 99.03 11.71 o 3 3 6 114.31 118.23 15.81 o 4 3 6 37.93 38.44 11.13 o 5 3 6 20.69 19.90 4.05 o 6 3 6 4.82 3.44 1.68 o 7 3 6 1.73 1.30 1.73 o 8 3 6 5.93 10.80 6.41 o 0 4 6 152.67 169.07 10.88 o 1 4 6 24.25 26.22 3.63 o 2 4 6 9.77 10.87 2.59 o 3 4 6 17.72 21.99 3.89 o 4 4 6 69.15 66.75 11.04 o 5 4 6 12.31 10.89 2.66 o 6 4 6 4.83 2.03 1.80 o 7 4 6 4.86 5.39 2.17 o 8 4 6 0.32 1.83 2.10 o 1 5 6 29.27 29.18 3.22 o 2 5 6 115.91 128.09 7.14 o 3 5 6 1.10 1.47 1.32 o 4 5 6 26.66 25.39 7.24 o 5 5 6 16.25 11.24 4.19 o 6 5 6 9.32 8.43 2.55 o 7 5 6 8.28 9.23 3.46 o 0 6 6 21.48 15.54 3.40 o 1 6 6 4.80 3.40 1.57 o 2 6 6 19.18 19.65 4.87 o 3 6 6 4.82 4.63 1.70 o 4 6 6 7.43 7.32 2.08 o 5 6 6 4.34 5.53 2.05 o 6 6 6 12.76 18.85 3.74 o 1 7 6 13.10 11.08 2.19 o 2 7 6 3.40 4.32 1.87 o 3 7 6 1.40 2.50 1.62 o 4 7 6 1.98 0.76 1.84 o 5 7 6 2.58 0.35 2.50 o 0 8 6 3.37 2.13 2.47 o 1 8 6 3.53 1.65 1.93 o 2 8 6 0.87 0.85 2.39 o 3 8 6 2.30 0.57 2.93 o 2 0 7 0.81 0.81 3.43 o 4 0 7 26.59 44.11 11.97 o 6 0 7 8.56 6.66 4.61 o 0 1 7 45.51 54.26 9.36 o 1 1 7 4.08 6.66 2.70 o 2 1 7 10.06 6.48 2.97 o 3 1 7 12.84 18.81 3.71 o 4 1 7 15.50 22.04 4.28 o 5 1 7 2.71 4.70 2.77 o 6 1 7 20.20 30.06 5.87 o 1 2 7 5.26 1.87 2.97 o 2 2 7 32.96 42.34 12.38 o 3 2 7 1.14 2.62 2.28 o 4 2 7 1.26 4.52 2.26 o 5 2 7 0.07 3.10 2.37 o 6 2 7 13.02 20.34 4.89 o 0 3 7 5.31 5.47 4.44 o 1 3 7 35.14 29.85 15.01 o 2 3 7 1.44 3.26 2.60 o 3 3 7 13.30 13.21 4.11 o 4 3 7 15.37 17.35 7.18 o 5 3 7 10.56 9.39 4.01 o 6 3 7 0.39 -1.25 2.92 o 1 4 7 5.47 4.79 3.57 o 2 4 7 10.31 5.08 2.72 o 3 4 7 7.63 8.29 3.16 o 4 4 7 35.58 39.71 11.52 o 5 4 7 3.36 3.37 3.63 o 0 5 7 33.76 47.37 10.49 o 1 5 7 3.73 -0.51 2.29 o 2 5 7 7.92 8.15 3.40 o 3 5 7 9.93 12.31 4.46 o 4 5 7 8.03 9.94 4.64 o 1 6 7 25.32 25.68 8.17 o 2 6 7 2.69 3.56 5.01 o 2 0 8 4.12 2.74 4.70 o 1 1 8 2.89 2.86 4.73 o 2 1 8 3.57 2.52 5.13 o 0 2 8 5.03 2.82 5.43 o 1 2 8 2.20 3.89 5.10 o