#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/42/2224215.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2224215_Fobs loop_ _publ_author_name 'Wang, De-Cai' 'Xu, Wei' 'Wu, Wen-Yuan' _publ_section_title ; 5-Methylisoxazole-4-carboxylic acid ; _journal_coeditor_code FL2281 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3140 _journal_volume 65 _journal_year 2009 _space_group_IT_number 62 _symmetry_space_group_name_Hall '-P 2ac 2n' _symmetry_space_group_name_H-M 'P n m a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 7.2540 _cell_length_b 6.4700 _cell_length_c 12.2730 _exptl_crystal_F_000 260.00 _reflns_d_resolution_high 0.8323 _[local]_cod_data_source_file fl2281Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' X in Pnma' _shelx_refln_list_code 4 _shelx_f_calc_maximum 166.64 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z+1/2' '-x, y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' '-x-1/2, y-1/2, z-1/2' 'x, -y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2867.00 2315.22 77.57 o 4 0 0 1327.99 1210.77 19.78 o 6 0 0 167.37 157.97 1.82 o 8 0 0 57.49 57.65 1.43 o 2 1 0 84.46 73.81 4.69 o 4 1 0 158.70 158.71 1.87 o 6 1 0 56.04 47.06 1.05 o 8 1 0 19.94 24.70 1.51 o 0 2 0 27768.71 29061.89 122.71 o 2 2 0 1743.70 1596.12 16.08 o 4 2 0 691.24 788.84 37.82 o 6 2 0 124.30 127.16 2.54 o 8 2 0 44.90 46.08 1.37 o 2 3 0 29.29 36.80 1.56 o 4 3 0 60.53 63.19 2.40 o 6 3 0 20.16 23.99 1.75 o 8 3 0 10.83 15.81 0.86 o 0 4 0 4060.24 3995.39 46.40 o 2 4 0 335.20 310.74 2.97 o 4 4 0 145.77 157.18 2.89 o 6 4 0 58.11 57.13 3.72 o 2 5 0 7.94 8.31 0.53 o 4 5 0 18.51 16.04 1.10 o 6 5 0 3.33 4.63 0.59 o 0 6 0 530.23 526.10 5.03 o 2 6 0 30.15 29.79 0.95 o 4 6 0 21.16 20.98 1.48 o 2 7 0 1.53 0.84 0.78 o 1 0 1 88.17 76.34 1.31 o 2 0 1 45.72 37.84 0.46 o 3 0 1 28.63 29.17 1.73 o 4 0 1 71.70 57.91 2.59 o 5 0 1 84.33 91.83 3.13 o 6 0 1 50.14 52.19 1.11 o 7 0 1 39.79 31.88 1.62 o 8 0 1 45.53 43.34 1.72 o 0 1 1 0.04 4.68 0.22 o 1 1 1 1446.43 1454.93 77.15 o 2 1 1 1189.88 1224.78 71.81 o 3 1 1 619.40 705.15 46.58 o 4 1 1 43.63 43.30 3.29 o 5 1 1 0.40 0.40 0.27 o 6 1 1 35.54 33.47 1.91 o 7 1 1 18.31 21.03 2.99 o 8 1 1 7.29 9.96 0.75 o 1 2 1 58.64 60.66 0.95 o 2 2 1 20.02 30.34 1.54 o 3 2 1 11.97 14.46 0.48 o 4 2 1 36.27 31.18 2.86 o 5 2 1 58.94 65.73 8.15 o 6 2 1 31.91 34.00 1.81 o 7 2 1 25.59 24.21 1.70 o 8 2 1 29.33 30.09 3.10 o 0 3 1 18.51 21.23 0.70 o 1 3 1 305.93 317.81 7.09 o 2 3 1 165.52 183.24 2.82 o 3 3 1 205.38 208.46 7.33 o 4 3 1 14.23 17.84 0.67 o 5 3 1 0.00 -0.22 0.38 o 6 3 1 28.84 27.95 2.99 o 7 3 1 12.07 15.11 2.37 o 8 3 1 3.61 6.89 2.75 o 1 4 1 26.85 27.44 0.69 o 2 4 1 3.99 7.41 0.42 o 3 4 1 2.33 2.43 0.73 o 4 4 1 3.84 4.53 0.46 o 5 4 1 21.87 21.38 1.70 o 6 4 1 10.50 9.44 0.75 o 7 4 1 6.99 8.11 0.94 o 0 5 1 2.80 1.40 0.54 o 1 5 1 63.47 59.75 1.75 o 2 5 1 14.29 13.99 1.00 o 3 5 1 37.00 35.52 0.97 o 4 5 1 3.89 3.96 0.49 o 5 5 1 0.49 1.12 1.70 o 6 5 1 14.27 12.63 1.16 o 1 6 1 8.69 8.51 0.83 o 2 6 1 0.68 1.05 0.46 o 3 6 1 0.72 0.38 0.45 o 4 6 1 0.01 0.78 0.46 o 5 6 1 4.84 4.71 0.67 o 0 7 1 0.53 0.59 0.65 o 1 7 1 15.58 13.29 1.27 o 2 7 1 1.25 -0.53 0.55 o 3 7 1 5.10 5.17 0.67 o 0 0 2 7817.56 7774.77 40.30 o 1 0 2 53.97 62.08 0.50 o 2 0 2 1281.90 1222.93 12.17 o 3 0 2 1053.00 1088.33 50.38 o 4 0 2 12.93 24.65 0.59 o 5 0 2 188.32 196.92 10.90 o 6 0 2 157.44 137.77 5.17 o 7 0 2 2.94 1.02 0.42 o 8 0 2 74.34 78.66 3.51 o 1 1 2 1035.35 939.42 14.19 o 2 1 2 239.17 223.86 10.61 o 3 1 2 506.11 512.25 32.19 o 4 1 2 14.48 13.41 0.47 o 5 1 2 504.66 505.46 31.44 o 6 1 2 25.19 20.94 1.37 o 7 1 2 104.30 95.16 6.61 o 8 1 2 4.28 7.01 0.70 o 0 2 2 4435.78 4631.98 38.18 o 1 2 2 7.82 6.74 0.65 o 2 2 2 532.79 530.35 50.66 o 3 2 2 524.15 595.38 43.08 o 4 2 2 19.63 24.97 2.37 o 5 2 2 124.36 137.53 14.49 o 6 2 2 119.37 116.59 16.78 o 7 2 2 4.61 2.47 0.51 o 8 2 2 52.25 59.47 6.58 o 1 3 2 246.87 252.33 1.68 o 2 3 2 60.34 45.39 0.80 o 3 3 2 130.55 119.29 5.01 o 4 3 2 12.92 12.40 0.55 o 5 3 2 214.75 214.16 19.90 o 6 3 2 6.93 6.97 0.61 o 7 3 2 45.87 49.71 5.82 o 0 4 2 1041.59 1040.54 5.62 o 1 4 2 0.01 0.30 0.27 o 2 4 2 85.92 88.06 1.26 o 3 4 2 106.64 110.39 2.00 o 4 4 2 15.45 13.27 0.67 o 5 4 2 42.87 40.13 3.42 o 6 4 2 54.33 57.88 7.28 o 7 4 2 5.98 5.09 0.97 o 1 5 2 25.14 24.73 0.80 o 2 5 2 5.29 4.81 1.24 o 3 5 2 11.91 10.68 0.61 o 4 5 2 7.11 7.49 1.56 o 5 5 2 52.56 49.05 3.37 o 6 5 2 0.33 0.51 0.59 o 0 6 2 183.40 175.76 2.98 o 1 6 2 0.21 0.74 0.40 o 2 6 2 8.94 9.29 0.67 o 3 6 2 16.63 14.87 0.82 o 4 6 2 6.11 6.39 0.61 o 5 6 2 10.47 10.00 1.10 o 1 7 2 1.82 1.86 0.81 o 2 7 2 0.25 0.65 0.70 o 3 7 2 0.52 1.15 0.47 o 1 0 3 208.39 220.28 1.70 o 2 0 3 320.07 326.43 5.51 o 3 0 3 76.90 57.28 0.92 o 4 0 3 0.60 0.99 0.21 o 5 0 3 159.39 152.65 10.59 o 6 0 3 146.93 136.47 11.03 o 7 0 3 6.32 6.32 0.58 o 8 0 3 9.18 8.77 0.70 o 0 1 3 305.52 300.32 1.88 o 1 1 3 460.14 461.38 3.38 o 2 1 3 19.47 24.18 0.48 o 3 1 3 1124.77 1221.10 70.28 o 4 1 3 74.35 87.98 5.94 o 5 1 3 296.11 318.19 24.79 o 6 1 3 510.15 504.46 36.12 o 7 1 3 76.11 77.95 5.75 o 8 1 3 11.93 14.75 1.86 o 1 2 3 76.24 70.54 0.80 o 2 2 3 176.08 171.32 9.32 o 3 2 3 32.93 32.68 1.83 o 4 2 3 0.05 0.14 0.32 o 5 2 3 90.35 93.14 7.02 o 6 2 3 105.18 107.36 9.96 o 7 2 3 4.00 3.05 0.62 o 8 2 3 7.61 7.94 0.68 o 0 3 3 26.38 26.84 0.86 o 1 3 3 60.71 49.22 0.80 o 2 3 3 0.19 0.63 0.25 o 3 3 3 418.96 423.85 33.87 o 4 3 3 39.34 40.98 2.08 o 5 3 3 87.68 97.78 8.88 o 6 3 3 275.39 293.77 40.02 o 7 3 3 38.09 44.77 2.51 o 1 4 3 4.67 3.59 0.38 o 2 4 3 39.34 37.25 1.05 o 3 4 3 3.12 4.30 0.65 o 4 4 3 0.06 0.29 0.43 o 5 4 3 18.76 21.27 1.45 o 6 4 3 41.26 44.69 4.98 o 7 4 3 1.08 1.17 0.55 o 0 5 3 7.38 6.41 0.65 o 1 5 3 0.91 0.99 0.36 o 2 5 3 0.58 0.48 0.43 o 3 5 3 84.52 76.50 1.41 o 4 5 3 9.29 9.89 0.65 o 5 5 3 8.41 10.41 0.70 o 6 5 3 93.03 97.64 8.44 o 1 6 3 0.04 0.24 0.40 o 2 6 3 6.14 5.91 0.59 o 3 6 3 0.07 0.16 0.42 o 4 6 3 0.09 -0.32 0.46 o 5 6 3 1.90 1.06 0.61 o 0 7 3 3.27 3.98 0.70 o 1 7 3 0.46 -0.51 0.51 o 2 7 3 0.66 0.64 0.47 o 3 7 3 13.95 13.23 1.48 o 0 0 4 157.48 175.83 1.53 o 1 0 4 329.73 370.48 3.15 o 2 0 4 187.51 224.71 2.21 o 3 0 4 11.58 13.28 0.81 o 4 0 4 2.38 4.26 1.80 o 5 0 4 120.97 116.76 5.84 o 6 0 4 291.61 274.23 6.63 o 7 0 4 131.26 126.97 7.86 o 8 0 4 21.14 19.78 0.95 o 1 1 4 0.35 1.73 0.24 o 2 1 4 0.85 2.88 1.48 o 3 1 4 62.01 69.68 1.51 o 4 1 4 42.52 42.27 3.42 o 5 1 4 270.71 252.79 15.95 o 6 1 4 12.09 13.99 1.00 o 7 1 4 19.14 17.95 2.21 o 8 1 4 6.50 6.65 0.70 o 0 2 4 58.15 65.63 1.13 o 1 2 4 121.03 118.98 3.85 o 2 2 4 66.22 78.56 1.19 o 3 2 4 0.92 1.61 0.28 o 4 2 4 0.55 0.73 0.27 o 5 2 4 89.05 91.61 11.99 o 6 2 4 196.33 196.69 19.58 o 7 2 4 91.01 92.79 7.72 o 8 2 4 13.17 12.49 0.80 o 1 3 4 0.74 0.24 0.35 o 2 3 4 2.89 3.39 0.43 o 3 3 4 12.33 11.91 1.05 o 4 3 4 12.21 12.02 0.57 o 5 3 4 134.67 131.67 5.54 o 6 3 4 3.16 3.44 0.61 o 7 3 4 11.93 10.25 1.43 o 0 4 4 15.06 15.13 0.81 o 1 4 4 18.08 16.71 0.61 o 2 4 4 9.61 12.65 3.20 o 3 4 4 1.80 1.87 0.38 o 4 4 4 0.93 1.41 0.37 o 5 4 4 40.88 44.80 5.09 o 6 4 4 68.36 73.06 9.44 o 7 4 4 33.72 35.50 5.20 o 1 5 4 1.47 0.66 0.46 o 2 5 4 3.04 2.72 0.46 o 3 5 4 0.66 1.26 0.47 o 4 5 4 0.75 0.70 0.51 o 5 5 4 38.70 40.97 2.40 o 6 5 4 0.19 1.41 0.64 o 0 6 4 4.41 5.01 0.81 o 1 6 4 3.22 3.86 0.51 o 2 6 4 2.19 1.52 0.51 o 3 6 4 2.09 2.07 0.47 o 4 6 4 2.09 1.48 0.55 o 5 6 4 12.73 13.78 1.29 o 1 7 4 0.53 -0.16 0.49 o 2 7 4 1.34 1.81 1.13 o 1 0 5 1434.25 1416.53 15.24 o 2 0 5 238.10 268.18 1.70 o 3 0 5 21.71 12.18 0.50 o 4 0 5 19.40 19.31 0.61 o 5 0 5 95.45 85.18 3.83 o 6 0 5 29.16 25.40 1.40 o 7 0 5 2.94 2.91 0.47 o 8 0 5 3.15 4.75 1.13 o 0 1 5 30.45 26.97 0.70 o 1 1 5 17.29 15.07 0.42 o 2 1 5 279.24 307.96 1.85 o 3 1 5 1168.39 1210.24 20.24 o 4 1 5 62.51 65.66 3.89 o 5 1 5 5.80 7.44 0.49 o 6 1 5 282.12 269.88 18.68 o 7 1 5 50.53 58.91 5.04 o 8 1 5 8.39 8.88 0.74 o 1 2 5 764.32 775.68 26.91 o 2 2 5 138.30 147.74 2.82 o 3 2 5 10.88 7.55 0.46 o 4 2 5 17.70 18.39 1.83 o 5 2 5 60.97 56.43 3.37 o 6 2 5 24.53 23.39 2.02 o 7 2 5 1.46 0.50 0.54 o 0 3 5 0.01 -0.27 0.27 o 1 3 5 20.22 25.91 0.65 o 2 3 5 76.57 80.93 2.32 o 3 3 5 459.54 498.48 24.83 o 4 3 5 14.22 14.32 1.10 o 5 3 5 4.26 5.08 1.18 o 6 3 5 149.35 151.88 16.22 o 7 3 5 28.98 34.65 3.77 o 1 4 5 154.46 151.90 2.22 o 2 4 5 41.04 39.42 1.83 o 3 4 5 1.20 1.31 0.36 o 4 4 5 9.77 10.81 0.89 o 5 4 5 17.46 19.10 0.84 o 6 4 5 13.96 16.27 0.86 o 0 5 5 5.58 5.17 0.65 o 1 5 5 6.84 6.85 0.57 o 2 5 5 4.85 4.64 0.49 o 3 5 5 113.40 112.12 7.18 o 4 5 5 0.77 1.16 0.47 o 5 5 5 1.45 1.97 0.57 o 1 6 5 19.44 19.57 0.86 o 2 6 5 9.00 10.64 0.69 o 3 6 5 0.00 -0.35 0.46 o 4 6 5 3.06 2.86 0.61 o 0 7 5 4.20 3.77 0.75 o 1 7 5 1.28 1.29 0.53 o 2 7 5 0.04 0.16 0.49 o 0 0 6 44.67 52.56 1.08 o 1 0 6 6.22 24.62 14.40 o 2 0 6 4.25 4.68 0.30 o 3 0 6 0.83 0.30 0.23 o 4 0 6 41.24 46.65 3.18 o 5 0 6 7.90 6.95 1.27 o 6 0 6 114.94 124.79 3.65 o 7 0 6 1.54 1.28 0.62 o 1 1 6 127.75 137.58 1.92 o 2 1 6 72.85 84.38 2.08 o 3 1 6 12.00 11.48 0.51 o 4 1 6 41.69 47.33 3.53 o 5 1 6 1.39 0.58 0.43 o 6 1 6 9.36 8.30 0.83 o 7 1 6 17.97 17.62 1.37 o 0 2 6 13.37 9.53 0.59 o 1 2 6 0.04 0.55 0.62 o 2 2 6 10.03 13.81 4.25 o 3 2 6 0.05 0.39 0.28 o 4 2 6 25.67 28.53 1.32 o 5 2 6 8.05 6.23 0.75 o 6 2 6 82.02 85.84 8.69 o 7 2 6 1.58 1.24 0.49 o 1 3 6 36.80 31.53 0.80 o 2 3 6 26.45 27.98 0.76 o 3 3 6 3.55 4.09 0.46 o 4 3 6 21.76 21.48 1.43 o 5 3 6 0.28 0.10 0.44 o 6 3 6 2.31 2.50 0.57 o 7 3 6 8.64 10.27 0.75 o 0 4 6 1.51 3.45 0.54 o 1 4 6 1.98 4.02 0.59 o 2 4 6 11.65 11.01 0.97 o 3 4 6 1.52 0.95 0.36 o 4 4 6 7.42 7.81 0.64 o 5 4 6 6.04 6.35 1.27 o 6 4 6 31.12 32.10 2.21 o 1 5 6 3.93 4.12 0.49 o 2 5 6 7.24 7.45 0.57 o 3 5 6 0.51 0.40 0.49 o 4 5 6 6.80 6.77 1.02 o 5 5 6 0.00 -0.29 0.51 o 0 6 6 5.42 5.11 0.86 o 1 6 6 1.74 2.15 0.51 o 2 6 6 5.52 4.99 0.62 o 3 6 6 1.47 0.92 0.53 o 4 6 6 1.74 1.67 0.59 o 1 7 6 0.20 -0.11 0.49 o 1 0 7 757.78 749.23 8.17 o 2 0 7 161.75 142.16 1.42 o 3 0 7 116.13 114.38 3.19 o 4 0 7 499.30 487.83 9.18 o 5 0 7 86.71 86.86 3.78 o 6 0 7 19.61 18.15 0.82 o 7 0 7 18.75 21.60 1.75 o 0 1 7 298.00 344.35 3.00 o 1 1 7 243.01 265.12 1.89 o 2 1 7 81.47 80.62 1.15 o 3 1 7 207.40 236.35 4.91 o 4 1 7 89.43 91.30 1.89 o 5 1 7 28.10 24.73 2.40 o 6 1 7 11.32 18.11 0.82 o 7 1 7 7.98 11.09 0.76 o 1 2 7 423.57 421.68 7.81 o 2 2 7 104.55 105.31 5.19 o 3 2 7 60.82 56.92 1.38 o 4 2 7 323.18 316.21 14.23 o 5 2 7 57.10 57.47 2.99 o 6 2 7 13.21 11.48 0.75 o 7 2 7 12.76 16.08 2.15 o 0 3 7 116.69 131.39 2.22 o 1 3 7 83.21 82.52 1.28 o 2 3 7 17.99 17.25 0.83 o 3 3 7 121.54 129.47 8.24 o 4 3 7 46.35 47.77 2.83 o 5 3 7 13.98 14.37 1.00 o 6 3 7 3.21 5.63 0.78 o 1 4 7 91.49 87.79 2.11 o 2 4 7 32.77 34.27 1.86 o 3 4 7 8.39 7.86 0.59 o 4 4 7 103.47 112.01 3.56 o 5 4 7 18.76 19.78 1.56 o 6 4 7 4.40 4.34 0.92 o 0 5 7 31.78 33.19 1.45 o 1 5 7 18.05 19.11 0.80 o 2 5 7 0.23 0.95 0.41 o 3 5 7 43.96 43.33 1.91 o 4 5 7 16.34 17.65 1.29 o 5 5 7 3.90 4.55 0.67 o 1 6 7 11.16 11.06 0.73 o 2 6 7 6.80 6.17 0.67 o 3 6 7 0.16 1.13 0.53 o 0 0 8 258.82 283.12 2.94 o 1 0 8 97.86 103.94 1.43 o 2 0 8 4.43 5.49 0.40 o 3 0 8 98.55 93.93 1.39 o 4 0 8 29.16 24.44 1.27 o 5 0 8 16.76 16.45 1.13 o 6 0 8 11.05 15.47 1.08 o 7 0 8 10.85 13.41 0.76 o 1 1 8 61.58 59.12 1.03 o 2 1 8 48.79 53.13 1.32 o 3 1 8 0.02 -0.20 0.32 o 4 1 8 84.39 74.77 2.37 o 5 1 8 13.94 10.92 1.37 o 6 1 8 45.97 43.05 1.20 o 7 1 8 5.18 6.11 0.61 o 0 2 8 160.72 165.42 2.38 o 1 2 8 56.97 58.82 1.05 o 2 2 8 4.42 5.73 0.46 o 3 2 8 79.34 72.37 4.61 o 4 2 8 16.49 17.06 0.76 o 5 2 8 8.95 8.91 0.73 o 6 2 8 8.78 11.01 0.72 o 1 3 8 35.92 33.56 1.43 o 2 3 8 16.02 15.87 1.00 o 3 3 8 0.49 1.05 0.46 o 4 3 8 43.66 44.07 1.97 o 5 3 8 12.02 11.32 1.00 o 6 3 8 20.27 20.80 2.42 o 0 4 8 45.68 42.80 1.56 o 1 4 8 17.97 17.78 0.74 o 2 4 8 4.34 3.71 0.49 o 3 4 8 45.85 44.68 2.02 o 4 4 8 2.76 3.84 0.63 o 5 4 8 1.53 2.41 1.05 o 1 5 8 11.84 10.59 0.74 o 2 5 8 2.35 2.61 0.51 o 3 5 8 0.45 1.10 0.49 o 4 5 8 13.31 13.18 1.10 o 0 6 8 8.47 6.95 0.97 o 1 6 8 4.57 4.78 0.78 o 2 6 8 2.56 2.37 0.57 o 1 0 9 31.64 24.88 0.74 o 2 0 9 58.18 64.43 1.18 o 3 0 9 12.23 9.92 0.67 o 4 0 9 147.64 131.78 6.44 o 5 0 9 1.92 1.27 0.57 o 6 0 9 8.66 9.82 0.70 o 0 1 9 397.05 406.77 3.82 o 1 1 9 22.33 24.45 0.76 o 2 1 9 35.44 30.40 0.86 o 3 1 9 98.64 102.30 1.92 o 4 1 9 264.76 264.03 8.41 o 5 1 9 47.48 47.51 1.94 o 6 1 9 40.63 47.55 4.10 o 1 2 9 17.33 15.12 0.67 o 2 2 9 36.55 35.02 0.97 o 3 2 9 6.78 7.03 0.57 o 4 2 9 109.25 101.70 2.59 o 5 2 9 0.64 -0.08 0.46 o 6 2 9 4.82 6.08 0.64 o 0 3 9 162.69 164.30 2.71 o 1 3 9 8.42 10.17 1.27 o 2 3 9 22.40 20.17 1.94 o 3 3 9 43.04 43.36 3.88 o 4 3 9 127.80 126.20 4.11 o 5 3 9 19.71 21.21 1.75 o 6 3 9 21.35 24.57 4.15 o 1 4 9 3.95 4.03 0.53 o 2 4 9 10.63 10.86 1.10 o 3 4 9 1.28 1.88 1.10 o 4 4 9 46.83 46.07 2.94 o 5 4 9 0.01 0.23 0.49 o 0 5 9 36.06 36.15 1.72 o 1 5 9 1.11 0.48 0.53 o 2 5 9 9.47 9.00 0.94 o 3 5 9 11.07 11.64 0.92 o 4 5 9 35.64 38.60 1.31 o 1 6 9 0.71 0.51 0.57 o 0 0 10 37.04 34.55 1.29 o 1 0 10 40.41 38.74 1.29 o 2 0 10 49.56 42.19 1.03 o 3 0 10 243.65 229.51 3.28 o 4 0 10 0.43 0.83 0.49 o 5 0 10 7.34 8.36 0.75 o 6 0 10 13.12 19.91 1.16 o 1 1 10 336.00 316.32 4.82 o 2 1 10 73.71 70.24 1.32 o 3 1 10 70.94 66.63 2.05 o 4 1 10 83.82 85.09 5.31 o 5 1 10 22.83 15.97 1.13 o 6 1 10 19.56 17.74 0.89 o 0 2 10 27.50 25.21 1.24 o 1 2 10 29.91 30.84 0.93 o 2 2 10 28.47 25.54 1.19 o 3 2 10 178.69 172.00 5.03 o 4 2 10 0.23 0.59 0.47 o 5 2 10 5.17 6.57 0.64 o 6 2 10 8.05 12.44 1.18 o 1 3 10 149.54 150.15 2.27 o 2 3 10 38.39 43.43 2.16 o 3 3 10 27.80 26.96 1.45 o 4 3 10 38.90 40.29 3.39 o 5 3 10 13.54 11.29 1.56 o 0 4 10 11.19 13.57 1.02 o 1 4 10 12.16 13.72 0.78 o 2 4 10 6.07 6.88 1.10 o 3 4 10 76.05 73.88 3.18 o 4 4 10 0.06 -0.27 0.54 o 1 5 10 36.25 36.85 1.26 o 2 5 10 12.10 14.84 0.89 o 3 5 10 5.17 5.87 0.72 o 1 0 11 17.67 15.56 0.74 o 2 0 11 0.12 0.08 0.40 o 3 0 11 0.86 0.70 0.38 o 4 0 11 19.68 17.89 0.88 o 5 0 11 4.65 4.11 0.61 o 0 1 11 6.13 6.51 0.81 o 1 1 11 48.10 44.26 1.14 o 2 1 11 58.48 60.28 3.75 o 3 1 11 0.75 0.33 0.44 o 4 1 11 3.05 1.81 0.57 o 5 1 11 1.39 1.81 0.59 o 1 2 11 14.37 14.38 1.35 o 2 2 11 0.05 0.57 0.42 o 3 2 11 0.33 0.62 0.46 o 4 2 11 15.05 15.18 0.78 o 5 2 11 3.48 3.98 0.83 o 0 3 11 0.15 0.00 0.54 o 1 3 11 23.12 21.83 1.48 o 2 3 11 30.30 29.45 1.89 o 3 3 11 0.06 -0.49 0.62 o 4 3 11 4.48 3.86 0.70 o 1 4 11 7.60 9.88 0.70 o 2 4 11 0.01 -0.47 0.51 o 3 4 11 0.00 1.08 0.51 o 0 5 11 0.94 -0.70 0.81 o 1 5 11 6.10 6.43 1.00 o 0 0 12 190.79 198.34 3.19 o 1 0 12 0.10 0.15 0.47 o 2 0 12 62.02 66.98 1.45 o 3 0 12 7.50 7.54 1.00 o 4 0 12 4.14 3.30 0.57 o 5 0 12 3.39 3.90 0.59 o 1 1 12 135.74 126.78 1.95 o 2 1 12 28.64 30.47 1.07 o 3 1 12 11.14 9.85 1.02 o 4 1 12 0.02 0.61 0.81 o 0 2 12 131.05 133.56 2.86 o 1 2 12 0.01 0.36 0.54 o 2 2 12 39.32 39.73 1.20 o 3 2 12 7.79 6.20 0.81 o 4 2 12 2.31 2.07 0.59 o 1 3 12 67.14 62.72 3.86 o 2 3 12 18.03 20.34 1.00 o 3 3 12 5.41 5.09 0.97 o 0 4 12 46.64 48.13 1.94 o 1 4 12 0.57 1.12 0.50 o 2 4 12 10.94 12.10 0.84 o 1 0 13 0.74 0.13 0.57 o 2 0 13 1.17 1.63 0.55 o 3 0 13 17.85 17.89 0.93 o 4 0 13 2.30 0.72 0.53 o 0 1 13 1.95 0.86 0.65 o 1 1 13 0.39 0.62 0.44 o 2 1 13 5.89 5.65 0.63 o 3 1 13 37.14 36.80 1.22 o 1 2 13 0.22 0.05 0.70 o 2 2 13 0.57 0.88 1.37 o 3 2 13 11.47 11.49 0.83 o 0 3 13 1.32 0.27 0.70 o 1 3 13 0.82 1.37 0.65 o 2 3 13 4.63 4.82 0.73 o 0 0 14 7.40 5.71 0.86 o 1 0 14 18.47 16.74 1.29 o 2 0 14 17.26 17.73 2.05 o 1 1 14 0.24 0.16 0.46 o 2 1 14 4.70 4.90 0.75 o 0 2 14 5.93 4.04 0.92 o 1 2 14 12.48 11.24 1.59 o