#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/42/2224250.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2224250_Fobs loop_ _publ_author_name 'Muramulla, Savitha' 'Arman, Hadi D.' 'Zhao, Cong-Gui' 'Tiekink, Edward R. T.' _publ_section_title ; 1-[3,5-Bis(trifluoromethyl)phenyl]-3-[(5-ethenyl-1-azabicyclo[2.2.2]octan-2-yl)(6-methoxyquinolin-4-yl)methyl]thiourea--L-proline--methanol (1/1/1) ; _journal_coeditor_code HB5216 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3070 _journal_volume 65 _journal_year 2009 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 11.5970 _cell_length_b 13.0440 _cell_length_c 23.9070 _exptl_crystal_F_000 1552.00 _reflns_d_resolution_high 0.7698 _[local]_cod_data_source_file hb5216Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' cd0305a in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 241.33 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 842.75 601.27 13.52 o 4 0 0 10867.03 10270.95 106.75 o 6 0 0 37.08 24.41 8.60 o 8 0 0 3.28 27.77 15.31 o 10 0 0 11821.92 13673.27 377.21 o 12 0 0 16.07 26.18 7.17 o 14 0 0 411.60 458.43 49.49 o 1 1 0 878.74 725.38 24.03 o 2 1 0 1673.44 1607.54 18.00 o 3 1 0 5449.16 5400.97 55.83 o 4 1 0 60.00 40.51 5.28 o 5 1 0 103.77 92.38 7.18 o 6 1 0 382.45 353.18 17.39 o 7 1 0 820.77 605.36 39.92 o 8 1 0 1096.33 715.12 174.34 o 9 1 0 1334.32 966.66 318.55 o 10 1 0 974.63 1156.36 49.26 o 11 1 0 1424.48 1578.83 40.36 o 12 1 0 89.82 94.10 8.57 o 13 1 0 55.43 44.83 6.69 o 14 1 0 89.53 87.43 8.79 o 15 1 0 62.87 62.97 9.43 o 0 2 0 199.34 189.59 12.56 o 1 2 0 24113.30 23834.55 780.88 o 2 2 0 3448.54 3203.92 55.73 o 3 2 0 1350.48 1244.40 16.58 o 4 2 0 61.03 17.74 5.89 o 5 2 0 81.45 61.07 6.82 o 6 2 0 319.23 327.01 12.75 o 7 2 0 168.15 157.29 14.68 o 8 2 0 333.39 363.14 22.33 o 9 2 0 1603.68 1702.47 44.71 o 10 2 0 11.32 29.63 6.75 o 11 2 0 170.95 198.58 20.19 o 12 2 0 40.19 26.98 7.82 o 13 2 0 356.68 409.85 27.45 o 14 2 0 43.12 44.74 6.91 o 1 3 0 7.89 139.38 13.18 o 2 3 0 1480.63 1239.54 30.06 o 3 3 0 1480.42 1184.55 18.00 o 4 3 0 3460.17 3699.60 32.15 o 5 3 0 724.64 494.39 14.88 o 6 3 0 3019.63 2981.56 37.71 o 7 3 0 831.84 798.83 28.27 o 8 3 0 619.36 606.17 21.69 o 9 3 0 1470.04 1499.64 45.72 o 10 3 0 138.89 105.54 12.86 o 11 3 0 26.47 24.15 10.90 o 12 3 0 31.41 43.99 7.86 o 13 3 0 114.38 142.44 17.84 o 14 3 0 151.91 156.20 13.81 o 0 4 0 8161.14 8143.52 94.01 o 1 4 0 1348.84 1181.06 13.29 o 2 4 0 2396.44 2317.46 113.31 o 3 4 0 2731.96 2269.26 68.02 o 4 4 0 278.71 288.40 20.47 o 5 4 0 287.46 288.08 13.76 o 6 4 0 2.02 13.34 4.06 o 7 4 0 51.28 41.21 6.14 o 8 4 0 1556.83 1442.91 30.61 o 9 4 0 56.86 57.45 20.71 o 10 4 0 7.38 6.38 4.91 o 11 4 0 11.36 23.18 6.39 o 12 4 0 258.18 238.99 35.47 o 13 4 0 18.27 31.04 11.89 o 14 4 0 101.61 159.46 19.82 o 1 5 0 218.99 138.02 10.00 o 2 5 0 16.23 18.96 6.61 o 3 5 0 4743.34 4809.98 206.93 o 4 5 0 34.01 59.22 9.45 o 5 5 0 2495.89 2599.00 55.42 o 6 5 0 297.30 315.79 17.96 o 7 5 0 1.60 18.32 6.65 o 8 5 0 749.72 633.20 46.06 o 9 5 0 1369.63 1476.26 50.72 o 10 5 0 331.26 253.03 21.90 o 11 5 0 364.69 426.57 44.65 o 12 5 0 127.93 81.17 15.66 o 13 5 0 201.18 269.49 27.44 o 14 5 0 40.70 65.05 17.44 o 0 6 0 41787.85 44961.57 745.37 o 1 6 0 4262.36 4057.07 35.33 o 2 6 0 3993.83 3975.79 64.09 o 3 6 0 0.86 5.99 11.24 o 4 6 0 0.81 10.58 5.76 o 5 6 0 145.69 175.03 15.32 o 6 6 0 49.58 75.75 10.15 o 7 6 0 55.52 25.23 6.69 o 8 6 0 676.81 537.13 47.69 o 9 6 0 68.36 62.28 9.62 o 10 6 0 407.88 340.22 50.79 o 11 6 0 61.23 42.18 13.72 o 12 6 0 220.95 185.50 30.37 o 13 6 0 189.78 183.68 24.51 o 14 6 0 285.86 353.72 47.22 o 1 7 0 3231.93 3481.53 53.83 o 2 7 0 2836.93 3173.34 90.95 o 3 7 0 341.71 410.83 73.31 o 4 7 0 1198.28 1152.23 38.22 o 5 7 0 449.41 480.81 29.80 o 6 7 0 1516.27 1610.32 66.67 o 7 7 0 76.50 90.87 13.30 o 8 7 0 92.73 88.53 12.55 o 9 7 0 908.27 852.33 31.05 o 10 7 0 97.16 86.56 9.90 o 11 7 0 966.73 1055.71 22.96 o 12 7 0 144.37 105.49 21.65 o 13 7 0 79.46 123.06 38.49 o 0 8 0 220.52 157.49 18.32 o 1 8 0 274.85 227.00 18.23 o 2 8 0 359.07 348.41 34.29 o 3 8 0 424.08 376.26 31.15 o 4 8 0 343.54 387.86 28.00 o 5 8 0 2161.04 2093.84 81.85 o 6 8 0 183.90 154.79 28.94 o 7 8 0 27.12 18.53 6.72 o 8 8 0 511.91 530.25 35.87 o 9 8 0 361.88 369.66 27.38 o 10 8 0 138.74 142.09 22.25 o 11 8 0 122.49 100.45 16.29 o 12 8 0 3.52 23.63 25.91 o 13 8 0 53.45 77.12 20.10 o 1 9 0 105.47 62.50 23.56 o 2 9 0 91.25 85.15 22.98 o 3 9 0 723.12 786.08 40.19 o 4 9 0 2799.04 3058.02 73.99 o 5 9 0 801.31 878.40 58.75 o 6 9 0 1013.09 1264.00 61.48 o 7 9 0 85.97 85.28 10.90 o 8 9 0 17.39 25.26 6.29 o 9 9 0 25.96 22.20 7.30 o 10 9 0 26.06 31.68 9.72 o 11 9 0 421.13 427.88 81.26 o 12 9 0 4.90 28.57 10.54 o 0 10 0 270.28 253.52 28.89 o 1 10 0 594.22 638.12 33.37 o 2 10 0 1006.36 1123.92 40.14 o 3 10 0 755.15 845.41 47.45 o 4 10 0 666.91 625.04 45.73 o 5 10 0 25.26 24.15 7.38 o 6 10 0 0.09 -3.88 5.94 o 7 10 0 616.85 716.59 41.75 o 8 10 0 30.50 27.56 7.01 o 9 10 0 104.27 132.12 20.97 o 10 10 0 133.45 100.08 12.29 o 11 10 0 7.47 8.57 3.59 o 12 10 0 38.70 61.35 18.28 o 1 11 0 78.26 42.64 8.83 o 2 11 0 329.25 297.03 21.21 o 3 11 0 822.59 885.03 43.64 o 4 11 0 12.34 12.41 5.97 o 5 11 0 180.57 161.09 17.69 o 6 11 0 8.00 29.98 8.61 o 7 11 0 57.16 40.55 10.29 o 8 11 0 90.83 87.46 16.54 o 9 11 0 55.22 75.60 10.91 o 10 11 0 16.24 23.35 7.25 o 11 11 0 487.64 329.13 82.95 o 0 12 0 169.94 145.69 24.92 o 1 12 0 580.16 557.44 32.45 o 2 12 0 30.30 35.59 7.94 o 3 12 0 17.37 12.83 10.44 o 4 12 0 15.57 33.08 11.98 o 5 12 0 566.31 556.14 37.04 o 6 12 0 78.10 79.13 13.17 o 7 12 0 30.54 35.39 8.65 o 8 12 0 18.07 41.74 9.55 o 9 12 0 6.25 24.86 14.21 o 10 12 0 114.29 115.52 15.50 o 1 13 0 267.31 287.43 21.52 o 2 13 0 0.10 12.19 10.48 o 3 13 0 5.38 21.73 8.62 o 4 13 0 265.76 313.71 35.79 o 5 13 0 330.47 366.31 27.96 o 6 13 0 6.10 11.77 7.30 o 7 13 0 32.40 44.35 9.16 o 8 13 0 63.15 75.33 12.52 o 9 13 0 8.99 30.22 9.17 o 0 14 0 900.75 1020.05 88.94 o 1 14 0 162.97 131.79 30.71 o 2 14 0 12.22 12.61 5.43 o 3 14 0 23.18 57.30 11.31 o 4 14 0 253.54 348.32 27.98 o 5 14 0 447.39 510.36 36.17 o 6 14 0 69.01 59.41 10.53 o 7 14 0 313.28 270.96 23.85 o 8 14 0 353.89 380.18 38.23 o 1 15 0 17.88 0.67 8.01 o 2 15 0 2.36 36.03 13.31 o 3 15 0 22.51 25.17 13.60 o 4 15 0 79.58 70.93 13.56 o 5 15 0 8.89 9.59 10.94 o 6 15 0 562.49 620.68 58.17 o 7 15 0 0.51 14.14 14.39 o 0 16 0 2.21 42.86 23.49 o 1 16 0 0.35 6.38 11.78 o 2 16 0 4.48 50.99 23.60 o 3 16 0 90.00 103.69 14.50 o 4 16 0 257.95 262.68 29.59 o 2 0 1 33398.63 31089.08 124.31 o 3 0 1 12146.72 12374.87 36.43 o 4 0 1 1251.31 1354.10 17.77 o 5 0 1 438.90 376.57 29.45 o 6 0 1 315.79 494.31 18.93 o 7 0 1 0.03 19.29 4.10 o 9 0 1 306.46 271.15 20.51 o 10 0 1 139.89 155.06 14.55 o 11 0 1 37.27 39.21 10.09 o 12 0 1 33.48 28.81 8.01 o 13 0 1 10.80 18.94 10.14 o 14 0 1 595.97 604.38 62.37 o 15 0 1 86.32 91.41 9.66 o -15 1 1 83.67 88.24 9.97 o -14 1 1 26.94 33.30 8.29 o -13 1 1 7.94 17.36 4.76 o -12 1 1 82.32 59.40 8.47 o -11 1 1 277.58 285.42 16.24 o -10 1 1 956.32 1104.07 42.86 o -9 1 1 1808.59 1920.45 57.76 o -8 1 1 13.69 18.87 7.74 o -7 1 1 2287.88 2477.26 41.37 o -6 1 1 163.47 144.18 14.64 o -5 1 1 419.66 283.49 25.98 o -4 1 1 39.92 8.76 3.35 o -3 1 1 2336.93 2385.14 27.09 o -2 1 1 4503.08 4114.71 35.92 o -1 1 1 6423.74 6172.07 116.37 o 1 1 1 6432.30 6253.12 118.47 o 2 1 1 4518.95 4151.50 38.43 o 3 1 1 2371.09 2388.06 29.40 o 4 1 1 41.43 12.70 2.58 o 5 1 1 418.63 308.78 17.16 o 6 1 1 165.33 154.69 12.81 o 7 1 1 2282.00 2368.25 35.08 o 8 1 1 12.38 17.12 5.22 o 9 1 1 1800.02 2013.62 82.46 o 10 1 1 951.13 1065.08 26.97 o 11 1 1 276.91 251.14 16.81 o 12 1 1 83.08 59.65 8.07 o 13 1 1 7.91 32.24 7.85 o 14 1 1 25.63 32.94 6.59 o 15 1 1 86.78 103.50 12.00 o -14 2 1 69.73 50.59 7.72 o -13 2 1 73.77 67.27 9.73 o -12 2 1 47.29 61.47 8.16 o -11 2 1 625.14 649.66 28.58 o -10 2 1 428.28 458.19 26.25 o -9 2 1 392.66 411.53 33.04 o -8 2 1 416.40 456.37 21.90 o -7 2 1 1217.84 1154.47 26.99 o -6 2 1 700.40 738.14 28.92 o -5 2 1 2565.50 3023.87 26.91 o -4 2 1 2730.69 2803.15 24.49 o -3 2 1 2017.10 1853.77 24.09 o -2 2 1 4131.46 4304.34 43.44 o -1 2 1 2187.06 2070.36 26.22 o 0 2 1 6487.60 5699.91 38.65 o 1 2 1 2197.74 2091.07 31.69 o 2 2 1 4148.31 4263.45 50.97 o 3 2 1 2041.42 1843.32 28.92 o 4 2 1 2804.11 2875.13 26.65 o 5 2 1 2547.78 3008.45 54.86 o 6 2 1 722.50 717.38 24.84 o 7 2 1 1222.43 1182.13 23.71 o 8 2 1 418.42 490.66 15.35 o 9 2 1 389.29 378.93 31.67 o 10 2 1 422.14 499.14 29.44 o 11 2 1 620.76 618.22 28.37 o 12 2 1 45.83 27.37 5.77 o 13 2 1 75.82 66.48 7.59 o 14 2 1 69.40 46.52 6.73 o -14 3 1 135.00 146.10 19.40 o -13 3 1 197.73 216.22 15.46 o -12 3 1 223.76 223.66 20.29 o -11 3 1 58.04 49.33 9.70 o -10 3 1 217.70 178.72 14.61 o -9 3 1 89.11 98.37 11.77 o -8 3 1 1138.49 1123.32 53.28 o -7 3 1 493.11 475.79 13.32 o -6 3 1 3952.99 4346.51 84.89 o -5 3 1 1221.74 1154.14 22.76 o -4 3 1 2924.80 3314.75 41.81 o -3 3 1 79.90 62.21 12.35 o -2 3 1 8184.32 7911.45 46.72 o -1 3 1 19606.02 19679.84 111.34 o 0 3 1 22941.73 23417.61 94.29 o 1 3 1 19588.42 19433.33 105.38 o 2 3 1 8232.44 7653.82 105.73 o 3 3 1 70.45 84.57 8.36 o 4 3 1 2901.84 3246.58 36.05 o 5 3 1 1170.11 1109.59 20.98 o 6 3 1 3939.71 4424.17 44.93 o 7 3 1 480.82 480.85 14.41 o 8 3 1 1138.50 1151.39 29.63 o 9 3 1 95.66 81.45 9.13 o 10 3 1 222.66 164.39 13.74 o 11 3 1 58.32 47.55 9.88 o 12 3 1 227.01 254.98 29.14 o 13 3 1 198.93 196.11 18.84 o 14 3 1 133.55 165.15 19.27 o -14 4 1 60.06 45.56 11.55 o -13 4 1 134.20 131.99 22.56 o -12 4 1 238.63 254.85 41.63 o -11 4 1 356.86 340.31 30.84 o -10 4 1 267.48 261.43 20.86 o -9 4 1 1124.85 1127.29 46.06 o -8 4 1 133.41 126.15 10.70 o -7 4 1 590.43 562.99 19.17 o -6 4 1 2818.94 2880.51 36.92 o -5 4 1 202.09 163.26 12.13 o -4 4 1 4511.02 4493.17 58.62 o -3 4 1 3883.05 4085.12 80.40 o -2 4 1 5765.01 5576.40 64.93 o -1 4 1 8129.84 7955.38 77.29 o 0 4 1 5641.13 6133.23 41.87 o 1 4 1 8178.57 8060.73 93.87 o 2 4 1 5747.83 5576.82 64.74 o 3 4 1 3884.87 4003.85 155.97 o 4 4 1 4536.01 4534.47 49.02 o 5 4 1 199.29 195.85 15.48 o 6 4 1 2809.93 2876.61 41.49 o 7 4 1 600.31 560.94 12.28 o 8 4 1 135.64 128.29 10.98 o 9 4 1 1112.54 1112.09 13.24 o 10 4 1 262.60 270.54 19.75 o 11 4 1 360.47 390.81 33.36 o 12 4 1 235.87 263.37 30.83 o 13 4 1 130.89 135.76 23.06 o 14 4 1 62.68 40.65 19.58 o -14 5 1 16.86 22.21 32.16 o -13 5 1 283.09 232.84 31.51 o -12 5 1 78.47 87.74 13.09 o -11 5 1 415.14 360.21 19.34 o -10 5 1 96.78 94.22 12.13 o -9 5 1 857.48 819.36 23.66 o -8 5 1 951.82 955.93 22.12 o -7 5 1 48.22 45.71 5.72 o -6 5 1 997.92 843.65 26.30 o -5 5 1 1098.19 1126.56 39.59 o -4 5 1 998.12 1007.46 80.40 o -3 5 1 2141.80 2274.95 62.20 o -2 5 1 2909.45 3054.01 40.76 o -1 5 1 1892.08 1910.62 27.37 o 0 5 1 1818.21 1990.08 28.31 o 1 5 1 1873.49 1861.13 29.56 o 2 5 1 2931.89 2975.79 71.53 o 3 5 1 2184.10 2356.30 68.60 o 4 5 1 983.02 1111.47 31.01 o 5 5 1 1112.08 1231.43 28.88 o 6 5 1 1001.28 871.42 32.30 o 7 5 1 47.84 61.25 9.62 o 8 5 1 962.87 1011.93 34.19 o 9 5 1 872.20 838.96 33.57 o 10 5 1 100.61 80.39 12.03 o 11 5 1 415.66 490.06 52.79 o 12 5 1 80.57 69.82 17.73 o 13 5 1 286.76 270.31 46.74 o 14 5 1 17.50 64.32 15.87 o -14 6 1 23.98 10.17 25.46 o -13 6 1 99.80 126.98 39.69 o -12 6 1 38.08 54.04 18.95 o -11 6 1 183.07 201.11 25.16 o -10 6 1 12.21 4.60 5.18 o -9 6 1 223.79 174.43 14.64 o -8 6 1 731.53 758.20 43.19 o -7 6 1 346.18 315.29 23.22 o -6 6 1 1043.94 1098.12 40.23 o -5 6 1 68.42 68.32 14.14 o -4 6 1 1016.50 900.78 40.20 o -3 6 1 1105.77 1139.80 36.93 o -2 6 1 4059.94 4223.49 35.72 o -1 6 1 1866.28 2013.24 29.31 o 0 6 1 2294.39 2772.65 33.53 o 1 6 1 1899.20 2014.28 38.03 o 2 6 1 4079.98 4206.96 49.36 o 3 6 1 1099.37 1149.17 44.53 o 4 6 1 983.54 908.77 47.07 o 5 6 1 69.87 75.98 12.33 o 6 6 1 1040.28 1082.32 41.11 o 7 6 1 338.50 301.05 26.07 o 8 6 1 720.42 715.76 29.00 o 9 6 1 220.77 202.16 20.02 o 10 6 1 12.73 14.20 6.08 o 11 6 1 188.56 211.93 34.81 o 12 6 1 39.33 65.79 15.00 o 13 6 1 96.78 84.87 17.88 o 14 6 1 25.72 49.90 15.00 o -13 7 1 39.91 55.11 15.24 o -12 7 1 43.46 71.80 45.69 o -11 7 1 25.97 26.61 14.34 o -10 7 1 600.78 520.57 31.75 o -9 7 1 293.37 264.03 26.53 o -8 7 1 577.12 583.95 39.67 o -7 7 1 592.10 659.33 40.59 o -6 7 1 174.34 145.70 15.47 o -5 7 1 116.62 94.54 16.68 o -4 7 1 1420.96 1529.68 46.38 o -3 7 1 3307.96 3394.94 53.69 o -2 7 1 2246.68 2362.59 41.39 o -1 7 1 1186.34 1076.69 33.42 o 0 7 1 806.05 966.27 18.13 o 1 7 1 1177.38 1045.26 28.77 o 2 7 1 2234.86 2472.58 39.58 o 3 7 1 3322.08 3388.89 76.25 o 4 7 1 1438.87 1548.78 55.03 o 5 7 1 109.35 103.38 25.76 o 6 7 1 173.08 149.18 16.43 o 7 7 1 594.99 694.96 35.04 o 8 7 1 589.00 558.86 37.35 o 9 7 1 293.91 261.33 20.89 o 10 7 1 596.17 576.45 32.43 o 11 7 1 25.13 25.34 20.62 o 12 7 1 42.83 39.84 15.09 o 13 7 1 39.69 75.53 18.86 o -13 8 1 79.79 99.15 22.68 o -12 8 1 123.97 106.10 19.30 o -11 8 1 54.64 31.02 9.51 o -10 8 1 184.04 151.07 16.88 o -9 8 1 258.32 291.37 29.55 o -8 8 1 593.13 610.46 31.36 o -7 8 1 248.55 239.77 20.74 o -6 8 1 271.55 298.52 24.32 o -5 8 1 259.32 303.69 38.37 o -4 8 1 202.18 235.55 23.08 o -3 8 1 142.65 157.53 23.09 o -2 8 1 878.13 884.04 31.69 o -1 8 1 91.18 105.28 8.17 o 0 8 1 360.48 365.73 20.47 o 1 8 1 89.23 91.34 11.09 o 2 8 1 892.95 904.71 36.97 o 3 8 1 145.89 200.87 19.45 o 4 8 1 213.26 208.46 21.46 o 5 8 1 254.32 270.23 29.63 o 6 8 1 280.42 287.45 26.57 o 7 8 1 242.61 234.76 16.56 o 8 8 1 587.11 613.40 32.76 o 9 8 1 250.35 254.25 22.53 o 10 8 1 182.40 158.78 23.69 o 11 8 1 55.34 46.28 7.62 o 12 8 1 125.54 117.02 24.24 o 13 8 1 79.79 89.07 62.07 o -12 9 1 13.92 -0.89 6.20 o -11 9 1 7.84 13.91 13.93 o -10 9 1 43.84 33.19 6.87 o -9 9 1 152.97 192.23 25.69 o -8 9 1 56.83 67.87 10.80 o -7 9 1 181.33 150.86 15.97 o -6 9 1 2337.41 2484.27 60.14 o -5 9 1 1827.19 1998.80 57.55 o -4 9 1 1316.02 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24.88 -5.01 13.50 o -2 8 27 49.69 68.71 13.56 o -1 8 27 338.95 345.83 39.52 o 0 8 27 46.80 63.80 16.76 o 1 8 27 342.79 348.27 44.33 o 2 8 27 47.92 25.49 11.66 o 0 0 28 11.56 4.90 13.45 o 1 0 28 4.24 1.79 12.04 o 2 0 28 40.04 31.28 9.18 o 3 0 28 196.96 215.94 23.76 o 4 0 28 155.21 180.84 30.14 o 5 0 28 71.86 95.29 14.22 o 6 0 28 35.05 30.03 9.87 o -6 1 28 30.46 24.30 9.04 o -5 1 28 38.22 59.42 14.41 o -4 1 28 86.22 53.77 11.49 o -3 1 28 154.02 185.24 21.25 o -2 1 28 108.05 122.88 18.34 o -1 1 28 25.17 23.13 13.54 o 0 1 28 0.57 -0.25 14.35 o 1 1 28 27.93 28.59 18.53 o 2 1 28 106.97 90.16 38.01 o 3 1 28 156.46 179.84 33.41 o 4 1 28 88.81 65.44 13.22 o 5 1 28 38.41 64.68 14.98 o 6 1 28 30.03 32.78 14.39 o -6 2 28 125.42 142.41 21.59 o -5 2 28 34.46 23.34 10.40 o -4 2 28 155.08 172.84 31.00 o -3 2 28 15.16 21.80 9.28 o -2 2 28 65.53 61.91 11.39 o -1 2 28 54.60 34.60 7.70 o 0 2 28 8.45 14.06 25.52 o 1 2 28 51.07 41.44 12.62 o 2 2 28 65.39 81.29 18.89 o 3 2 28 15.94 12.77 17.93 o 4 2 28 157.75 155.36 27.08 o 5 2 28 34.10 19.37 15.96 o 6 2 28 123.99 115.36 35.44 o -5 3 28 85.49 85.08 14.32 o -4 3 28 71.67 79.34 13.95 o -3 3 28 365.48 379.12 43.93 o -2 3 28 623.89 606.84 63.20 o -1 3 28 322.21 315.54 30.24 o 0 3 28 334.75 320.45 62.12 o 1 3 28 313.51 275.66 38.49 o 2 3 28 616.33 654.92 92.14 o 3 3 28 370.10 364.56 51.91 o 4 3 28 69.38 68.08 24.60 o 5 3 28 85.13 62.58 23.25 o -5 4 28 8.26 5.48 12.39 o -4 4 28 51.65 52.52 13.01 o -3 4 28 163.43 143.17 20.43 o -2 4 28 135.05 174.55 19.96 o -1 4 28 29.92 41.13 10.27 o 0 4 28 0.05 14.68 8.01 o 1 4 28 32.08 36.84 15.26 o 2 4 28 131.45 149.64 29.68 o 3 4 28 165.81 135.19 25.00 o 4 4 28 52.51 90.85 28.57 o 5 4 28 8.74 5.26 16.92 o -4 5 28 111.60 122.78 22.17 o -3 5 28 127.72 114.27 17.95 o -2 5 28 123.96 112.97 17.48 o -1 5 28 27.65 28.68 10.10 o 0 5 28 679.28 596.23 56.55 o 1 5 28 30.45 39.55 9.39 o 2 5 28 126.42 171.96 20.82 o 3 5 28 124.38 111.33 17.22 o 4 5 28 110.67 81.17 22.95 o -3 6 28 82.13 100.77 15.58 o -2 6 28 151.81 150.58 16.57 o -1 6 28 50.91 69.46 13.81 o 0 6 28 31.89 27.84 9.89 o 1 6 28 48.99 57.48 15.02 o 2 6 28 150.13 149.15 23.26 o 3 6 28 83.90 113.34 23.67 o -1 7 28 20.85 18.74 7.16 o 0 7 28 5.56 30.05 15.61 o 1 7 28 21.86 34.27 10.70 o 1 0 29 215.19 181.82 47.52 o 2 0 29 11.67 17.10 10.96 o 3 0 29 42.41 71.76 19.87 o 4 0 29 12.25 30.38 11.32 o 5 0 29 0.04 28.63 11.12 o -5 1 29 100.38 95.71 16.27 o -4 1 29 5.34 1.85 9.72 o -3 1 29 37.96 41.94 11.42 o -2 1 29 230.70 229.52 19.58 o -1 1 29 1.08 18.19 9.90 o 0 1 29 6.39 37.92 27.88 o 1 1 29 0.80 23.42 12.60 o 2 1 29 229.05 239.98 23.85 o 3 1 29 36.87 54.91 17.01 o 4 1 29 5.06 31.22 14.39 o 5 1 29 99.64 94.27 16.73 o -5 2 29 32.61 22.40 13.73 o -4 2 29 183.46 217.28 23.41 o -3 2 29 131.20 117.48 20.97 o -2 2 29 19.69 28.22 12.18 o -1 2 29 57.00 51.21 12.70 o 0 2 29 17.87 -3.32 10.01 o 1 2 29 57.42 89.55 18.65 o 2 2 29 20.33 24.37 21.28 o 3 2 29 131.04 100.93 18.58 o 4 2 29 187.52 183.13 28.03 o 5 2 29 33.01 18.11 12.78 o -4 3 29 157.76 166.31 32.97 o -3 3 29 79.03 82.52 15.62 o -2 3 29 114.86 82.22 19.18 o -1 3 29 150.53 139.22 34.15 o 0 3 29 92.75 78.57 17.60 o 1 3 29 149.24 122.26 25.46 o 2 3 29 112.71 122.40 26.39 o 3 3 29 81.93 75.82 36.07 o 4 3 29 157.41 182.27 41.42 o -4 4 29 262.78 241.39 25.36 o -3 4 29 10.14 25.04 16.78 o -2 4 29 9.13 43.76 11.97 o -1 4 29 14.64 30.24 14.82 o 0 4 29 16.17 43.87 17.50 o 1 4 29 15.38 36.09 16.46 o 2 4 29 8.91 17.12 30.54 o 3 4 29 9.71 17.56 12.00 o 4 4 29 264.20 273.29 28.71 o -3 5 29 36.96 34.80 10.58 o -2 5 29 10.97 36.41 12.28 o -1 5 29 27.25 28.73 11.35 o 0 5 29 37.44 44.76 16.51 o 1 5 29 27.95 53.83 16.82 o 2 5 29 11.81 20.05 27.46 o 3 5 29 37.57 19.18 11.58 o 0 6 29 35.14 55.28 14.30 o 0 0 30 380.16 315.29 64.55 o 1 0 30 44.56 42.76 16.87 o 2 0 30 539.35 530.39 77.76 o 3 0 30 57.62 73.34 18.49 o -3 1 30 264.12 240.42 28.13 o -2 1 30 566.58 582.36 78.46 o -1 1 30 332.91 314.42 49.62 o 0 1 30 60.19 47.28 14.72 o 1 1 30 342.00 325.54 46.99 o 2 1 30 566.18 512.14 75.63 o 3 1 30 256.09 216.19 41.25 o -3 2 30 53.07 38.29 12.14 o -2 2 30 324.86 290.53 36.63 o -1 2 30 74.08 41.77 13.83 o 0 2 30 39.58 33.43 13.21 o 1 2 30 74.16 74.63 37.30 o 2 2 30 336.67 286.55 43.83 o 3 2 30 52.67 12.60 16.86 o -2 3 30 177.30 152.84 19.43 o -1 3 30 34.98 31.93 14.27 o 0 3 30 170.56 229.48 30.27 o 1 3 30 37.59 61.95 19.84 o 2 3 30 176.10 182.06 31.24 o -1 4 30 6.45 10.38 12.38 o 0 4 30 129.30 187.39 27.93 o 1 4 30 6.30 4.11 9.90 o 0 1 31 3.32 16.21 9.65 o