#------------------------------------------------------------------------------ #$Date: 2016-04-03 04:22:38 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181163 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/42/2224254.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2224254_Fobs loop_ _publ_author_name 'Comerlato, Nadia M.' 'Tiekink, Edward R. T.' 'Wardell, James L.' 'Wardell, Solange M. S. V.' _publ_section_title ; (Dimethyl sulfoxide-\kO)diphenyl(3-thioxo-3H-1,2-dithiole-4,5-dithiolato-\k^2^S^4^,S^5^)tin(IV) ; _journal_coeditor_code HB5220 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1592 _journal_page_last m1593 _journal_volume 65 _journal_year 2009 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 96.892 _cell_angle_gamma 90.000 _cell_length_a 11.1420 _cell_length_b 15.7237 _cell_length_c 11.9646 _exptl_crystal_F_000 1088.00 _reflns_d_resolution_high 0.7696 _cod_data_source_file hb5220Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 2009src0472 in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 403.64 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 21.50 9.44 17.17 o 4 0 0 41397.69 37200.47 1453.28 o 6 0 0 14358.30 12730.95 393.66 o 8 0 0 17283.56 16452.32 535.22 o 10 0 0 248.55 313.57 43.15 o 12 0 0 1833.33 1981.95 128.28 o 14 0 0 1824.66 1900.42 249.20 o 2 1 0 14893.76 13962.33 497.32 o 3 1 0 1749.61 1525.52 43.45 o 4 1 0 1727.93 1482.04 49.40 o 5 1 0 2208.34 1833.25 48.74 o 6 1 0 1.89 13.96 13.53 o 7 1 0 0.39 15.47 17.57 o 8 1 0 1481.16 1571.74 85.91 o 9 1 0 794.38 661.02 34.81 o 10 1 0 2922.68 3185.49 94.09 o 11 1 0 5729.05 5920.94 286.72 o 12 1 0 381.92 439.90 41.64 o 13 1 0 464.29 402.77 77.77 o 14 1 0 92.40 121.03 84.59 o 2 2 0 10979.02 10260.87 233.27 o 3 2 0 73.65 85.29 9.32 o 4 2 0 2787.25 2605.50 61.30 o 5 2 0 10235.09 8866.76 186.42 o 6 2 0 9729.75 9119.93 201.35 o 7 2 0 8183.91 8203.56 178.01 o 8 2 0 1072.76 1107.55 39.86 o 9 2 0 396.88 365.82 22.84 o 10 2 0 2.19 24.11 18.07 o 11 2 0 111.52 108.74 26.67 o 12 2 0 1366.62 1184.02 57.99 o 13 2 0 4561.84 5127.74 270.95 o 14 2 0 294.95 330.16 110.19 o 1 3 0 117.76 120.56 7.19 o 2 3 0 44311.17 40556.50 866.07 o 3 3 0 890.19 829.98 27.14 o 4 3 0 7921.73 6725.36 147.80 o 5 3 0 1110.68 970.76 31.70 o 6 3 0 1137.67 1140.81 35.00 o 7 3 0 1829.29 1731.03 44.84 o 8 3 0 15.70 42.44 12.66 o 9 3 0 95.09 114.27 15.13 o 10 3 0 6207.35 6022.70 131.80 o 11 3 0 936.00 941.05 47.45 o 12 3 0 1561.67 1411.35 111.37 o 13 3 0 0.41 2.66 58.04 o 14 3 0 227.28 197.70 96.79 o 1 4 0 37739.32 35258.81 697.61 o 2 4 0 1269.58 1227.28 27.60 o 3 4 0 34.29 28.23 6.59 o 4 4 0 3435.95 3062.99 72.37 o 5 4 0 5882.58 5618.18 189.98 o 6 4 0 1653.67 1540.89 39.25 o 7 4 0 21116.21 20907.10 367.35 o 8 4 0 11723.52 11833.83 216.76 o 9 4 0 549.36 514.95 26.85 o 10 4 0 400.16 216.09 38.94 o 11 4 0 482.84 466.93 96.82 o 12 4 0 751.69 797.42 87.87 o 13 4 0 1841.78 1924.29 136.23 o 14 4 0 437.35 332.72 121.21 o 1 5 0 6800.05 7159.40 179.72 o 2 5 0 19.39 24.21 6.08 o 3 5 0 3899.87 3919.20 109.46 o 4 5 0 8832.22 8447.75 225.18 o 5 5 0 1899.15 1741.99 48.79 o 6 5 0 944.41 867.49 31.70 o 7 5 0 107.88 179.02 23.95 o 8 5 0 3929.58 3915.18 96.64 o 9 5 0 479.17 490.11 29.77 o 10 5 0 1732.90 1992.01 93.42 o 11 5 0 3388.37 3875.82 172.62 o 12 5 0 230.29 135.32 59.65 o 13 5 0 199.35 112.21 60.97 o 0 6 0 77471.96 75515.15 2717.20 o 1 6 0 2426.41 2485.09 64.27 o 2 6 0 23455.39 23371.92 427.10 o 3 6 0 255.48 288.57 17.43 o 4 6 0 10646.55 10352.79 217.21 o 5 6 0 42.69 59.12 10.37 o 6 6 0 30901.44 30688.94 633.98 o 7 6 0 222.27 265.56 25.12 o 8 6 0 2543.72 2601.64 67.40 o 9 6 0 1758.57 1695.76 56.14 o 10 6 0 31.39 45.98 41.83 o 11 6 0 576.39 553.35 64.21 o 12 6 0 1871.15 1907.22 136.89 o 13 6 0 89.28 82.34 59.14 o 1 7 0 2351.20 2263.19 56.10 o 2 7 0 8141.74 8145.54 189.95 o 3 7 0 3158.63 2958.88 61.49 o 4 7 0 381.79 367.84 15.38 o 5 7 0 13219.43 13336.50 267.63 o 6 7 0 293.65 258.22 21.03 o 7 7 0 4777.42 4660.52 116.38 o 8 7 0 49.52 39.83 19.47 o 9 7 0 5613.97 5769.22 169.19 o 10 7 0 94.83 121.37 38.71 o 11 7 0 7460.55 7784.19 360.41 o 12 7 0 9.46 20.12 57.37 o 13 7 0 92.34 127.54 130.71 o 0 8 0 2606.90 2693.45 126.16 o 1 8 0 9127.13 9356.79 217.66 o 2 8 0 841.20 735.11 29.02 o 3 8 0 1235.71 1271.38 31.98 o 4 8 0 1013.80 927.80 36.09 o 5 8 0 1924.07 1921.85 56.10 o 6 8 0 9109.67 9322.62 210.98 o 7 8 0 11237.37 11704.15 279.96 o 8 8 0 79.33 188.00 35.29 o 9 8 0 2165.04 2204.18 82.35 o 10 8 0 1916.02 1742.78 88.65 o 11 8 0 297.82 220.15 59.73 o 12 8 0 645.63 834.09 109.30 o 13 8 0 1636.32 1166.28 145.94 o 1 9 0 4921.03 5226.48 132.39 o 2 9 0 1178.97 1204.06 36.73 o 3 9 0 1714.15 1738.68 54.17 o 4 9 0 14122.24 15354.12 307.61 o 5 9 0 734.34 735.71 34.11 o 6 9 0 68.02 67.80 19.35 o 7 9 0 1272.75 1208.41 46.04 o 8 9 0 2642.72 2835.75 93.01 o 9 9 0 7.97 201.93 44.46 o 10 9 0 3799.27 3797.74 159.87 o 11 9 0 2041.68 2269.38 136.47 o 12 9 0 304.41 324.98 91.15 o 0 10 0 2387.88 2794.65 320.89 o 1 10 0 20035.04 20776.64 509.15 o 2 10 0 2626.53 2570.16 68.63 o 3 10 0 359.85 394.90 22.85 o 4 10 0 4.12 11.05 11.34 o 5 10 0 3408.57 3700.98 101.62 o 6 10 0 4886.56 5128.88 142.08 o 7 10 0 9512.25 9956.14 251.94 o 8 10 0 1790.52 1841.99 73.43 o 9 10 0 3919.52 3881.68 145.45 o 10 10 0 191.82 136.11 38.77 o 11 10 0 705.11 629.74 178.42 o 12 10 0 141.55 194.28 89.59 o 1 11 0 2.02 2.48 11.91 o 2 11 0 3241.65 3339.61 76.07 o 3 11 0 3305.93 3501.98 98.24 o 4 11 0 4889.07 5115.11 129.27 o 5 11 0 3659.53 3947.73 104.28 o 6 11 0 1159.74 1205.74 54.60 o 7 11 0 789.86 782.72 34.54 o 8 11 0 1914.12 1972.07 78.80 o 9 11 0 2380.44 2463.96 100.04 o 10 11 0 1969.90 1879.44 151.61 o 11 11 0 1108.57 1379.57 308.90 o 12 11 0 1676.18 1725.92 165.08 o 0 12 0 4955.69 5565.43 454.28 o 1 12 0 2437.50 2550.01 61.60 o 2 12 0 4965.90 5170.58 163.28 o 3 12 0 932.08 949.90 40.59 o 4 12 0 1460.34 1486.24 58.16 o 5 12 0 1585.65 1553.17 47.96 o 6 12 0 12304.78 13735.61 350.18 o 7 12 0 259.60 377.25 58.44 o 8 12 0 757.02 690.60 44.96 o 9 12 0 50.04 -8.68 42.33 o 10 12 0 1442.57 1381.17 114.29 o 11 12 0 0.34 -25.93 79.21 o 1 13 0 128.69 118.36 28.60 o 2 13 0 414.43 409.50 32.87 o 3 13 0 4529.64 5083.77 123.21 o 4 13 0 1224.49 1238.77 55.64 o 5 13 0 7097.88 8049.70 269.12 o 6 13 0 927.36 972.85 38.19 o 7 13 0 1843.51 1807.34 68.42 o 8 13 0 1612.51 1570.12 103.79 o 9 13 0 2394.27 2421.45 162.21 o 10 13 0 165.12 119.86 70.88 o 11 13 0 5571.98 5494.97 401.17 o 0 14 0 9531.21 10030.56 528.72 o 1 14 0 3902.93 4219.44 163.33 o 2 14 0 449.03 455.44 32.18 o 3 14 0 745.06 691.83 41.91 o 4 14 0 2081.62 2391.23 84.63 o 5 14 0 236.15 192.04 40.47 o 6 14 0 1463.47 1441.51 73.84 o 7 14 0 5203.38 5547.79 247.22 o 8 14 0 248.92 132.03 58.87 o 9 14 0 1883.15 1884.87 134.58 o 10 14 0 58.64 126.41 66.52 o 1 15 0 2909.87 3117.55 126.90 o 2 15 0 4790.55 5015.56 126.21 o 3 15 0 326.51 366.51 35.27 o 4 15 0 6472.37 7183.16 231.36 o 5 15 0 34.88 45.66 37.46 o 6 15 0 1.79 56.36 33.50 o 7 15 0 12.57 -1.19 57.18 o 8 15 0 1630.86 1781.35 190.49 o 9 15 0 92.64 81.61 71.28 o 0 16 0 282.88 334.62 73.17 o 1 16 0 5454.12 6125.94 228.40 o 2 16 0 8.67 28.26 13.42 o 3 16 0 2.68 36.48 23.71 o 4 16 0 157.21 182.60 35.83 o 5 16 0 2714.11 2739.78 146.94 o 6 16 0 510.72 701.49 112.89 o 7 16 0 969.77 1044.16 98.89 o 8 16 0 10.38 25.98 92.14 o 1 17 0 803.68 933.58 71.22 o 2 17 0 6493.90 7413.86 291.08 o 3 17 0 1942.14 1830.10 74.24 o 4 17 0 1309.12 1151.11 87.68 o 5 17 0 391.54 336.28 51.55 o 6 17 0 1584.22 1679.89 138.29 o 7 17 0 120.24 61.25 65.50 o 0 18 0 6460.16 7621.84 455.83 o 1 18 0 586.96 703.44 70.45 o 2 18 0 739.16 670.75 69.64 o 3 18 0 230.08 195.89 25.80 o 4 18 0 1276.42 1293.27 88.62 o 5 18 0 980.80 936.28 90.30 o 6 18 0 1507.20 1412.95 132.43 o 1 19 0 577.87 401.98 73.55 o 2 19 0 157.90 132.22 59.59 o 3 19 0 2318.67 2180.69 141.65 o 4 19 0 109.44 161.42 91.95 o 5 19 0 1254.09 1100.84 114.47 o 0 20 0 2337.75 2578.32 259.87 o 1 20 0 229.10 226.47 68.62 o 2 20 0 1920.07 1989.76 204.36 o -13 0 1 1872.09 1726.47 228.94 o -11 0 1 93.96 42.19 73.88 o -9 0 1 294.72 272.71 33.46 o -7 0 1 13.71 35.12 17.32 o -5 0 1 16300.32 14423.84 408.85 o -3 0 1 58.45 50.94 11.93 o 3 0 1 1286.52 1434.24 74.72 o 5 0 1 3250.34 3340.42 154.72 o 7 0 1 37470.78 36765.86 1113.20 o 9 0 1 2412.32 2433.46 102.93 o 11 0 1 5094.00 5284.88 376.52 o 13 0 1 4885.43 5071.17 257.70 o -14 1 1 658.30 432.85 124.11 o -13 1 1 25.84 77.58 70.81 o -12 1 1 1054.74 1073.91 83.03 o -11 1 1 680.68 758.82 50.05 o -10 1 1 10802.81 11113.91 269.90 o -9 1 1 5.61 75.62 21.12 o -8 1 1 8245.40 7911.80 232.86 o -7 1 1 321.49 234.74 20.24 o -6 1 1 669.72 788.73 25.58 o -5 1 1 771.12 730.24 29.87 o -4 1 1 35943.10 31200.10 586.38 o -3 1 1 2837.25 2370.01 54.72 o -2 1 1 41123.83 33222.06 769.97 o 2 1 1 16585.47 15409.30 457.02 o 3 1 1 243.69 245.65 13.06 o 4 1 1 6069.62 5373.31 173.68 o 5 1 1 46.33 -4.58 16.59 o 6 1 1 6129.26 5398.17 175.34 o 7 1 1 8149.40 8581.44 202.73 o 8 1 1 5547.13 5346.57 192.97 o 9 1 1 3037.71 2894.19 86.62 o 10 1 1 2715.43 2656.09 163.58 o 11 1 1 2144.63 2258.13 99.18 o 12 1 1 4381.46 4498.63 148.82 o 13 1 1 101.79 64.45 43.46 o 14 1 1 110.97 6.66 100.08 o -14 2 1 789.81 936.66 131.55 o -13 2 1 531.70 631.96 71.90 o -12 2 1 135.50 192.71 29.40 o -11 2 1 159.80 223.72 24.24 o -10 2 1 654.42 662.18 40.51 o -9 2 1 392.89 349.09 36.13 o -8 2 1 4553.82 4373.95 101.08 o -7 2 1 1313.97 1189.63 32.72 o -6 2 1 28972.29 25416.75 491.37 o -5 2 1 3260.93 2828.10 59.11 o -4 2 1 5877.06 4957.90 122.57 o -3 2 1 335.77 288.08 14.04 o -2 2 1 20224.48 18493.52 427.45 o -1 2 1 11184.81 10705.35 317.06 o 0 2 1 51189.99 30002.20 2933.47 o 1 2 1 6486.46 6109.24 241.10 o 2 2 1 7453.66 7213.10 174.69 o 3 2 1 445.09 425.11 27.76 o 4 2 1 7640.47 7067.96 224.39 o 5 2 1 1368.77 1241.17 45.86 o 6 2 1 2636.96 2398.19 78.59 o 7 2 1 4419.92 4250.56 101.51 o 8 2 1 2723.49 2687.17 70.75 o 9 2 1 899.55 871.75 44.90 o 10 2 1 788.75 704.10 52.98 o 11 2 1 16.82 3.77 25.36 o 12 2 1 1519.41 1543.19 66.90 o 13 2 1 994.94 923.19 76.44 o 14 2 1 296.21 247.13 129.27 o -14 3 1 191.16 157.74 72.93 o -13 3 1 1.39 -76.39 50.92 o -12 3 1 25.26 73.84 42.62 o -11 3 1 5254.52 5658.60 234.87 o -10 3 1 18.60 370.04 36.01 o -9 3 1 1733.14 1656.52 62.40 o -8 3 1 1259.73 1189.53 86.46 o -7 3 1 2458.42 2393.47 62.98 o -6 3 1 499.21 503.42 23.31 o -5 3 1 2548.23 2436.49 80.25 o -4 3 1 1410.05 1343.80 48.80 o -3 3 1 9834.32 8677.70 181.68 o -2 3 1 4000.48 3698.76 81.47 o -1 3 1 4164.39 4415.70 123.88 o 0 3 1 1932.53 1964.00 51.66 o 1 3 1 5486.22 5896.68 138.39 o 2 3 1 1.88 17.51 6.75 o 3 3 1 61.21 81.45 8.46 o 4 3 1 19.17 37.84 9.25 o 5 3 1 14646.77 13831.38 358.23 o 6 3 1 29.86 48.24 19.17 o 7 3 1 16254.13 16307.64 339.32 o 8 3 1 2114.86 2018.03 57.62 o 9 3 1 6968.89 7067.60 163.07 o 10 3 1 21.74 5.20 28.30 o 11 3 1 8737.87 9266.14 262.84 o 12 3 1 1.91 27.97 26.42 o 13 3 1 974.68 971.23 104.01 o 14 3 1 108.28 60.93 189.06 o -14 4 1 409.47 303.08 66.73 o -13 4 1 267.88 264.94 62.65 o -12 4 1 1192.83 1255.11 100.61 o -11 4 1 377.43 388.14 112.16 o -10 4 1 692.81 728.32 40.34 o -9 4 1 0.31 55.61 27.50 o -8 4 1 1429.63 1261.25 43.58 o -7 4 1 298.13 255.37 23.81 o -6 4 1 14180.80 13166.92 344.68 o -5 4 1 1108.22 1005.88 33.13 o -4 4 1 18046.64 16690.67 395.14 o -3 4 1 2163.08 2242.56 47.00 o -2 4 1 10435.03 10137.06 203.34 o -1 4 1 24740.37 24699.69 528.83 o 0 4 1 72343.27 76268.22 1682.08 o 1 4 1 9376.97 9689.05 215.22 o 2 4 1 5331.27 5344.28 129.67 o 3 4 1 884.65 848.72 23.78 o 4 4 1 4862.19 4445.86 116.65 o 5 4 1 29.47 11.98 10.60 o 6 4 1 16073.51 15167.83 335.86 o 7 4 1 10486.31 10485.20 221.63 o 8 4 1 2812.51 2885.45 90.36 o 9 4 1 587.35 639.30 33.72 o 10 4 1 453.12 435.40 35.12 o 11 4 1 2533.51 2494.94 102.91 o 12 4 1 364.20 450.62 53.92 o 13 4 1 1805.12 1659.49 140.44 o -14 5 1 534.51 239.83 79.73 o -13 5 1 262.20 176.16 67.06 o -12 5 1 444.67 396.56 59.91 o -11 5 1 3196.43 3457.20 182.93 o -10 5 1 7677.45 7859.17 232.44 o -9 5 1 5228.38 5302.62 182.48 o -8 5 1 11374.12 11626.74 285.86 o -7 5 1 715.68 695.06 36.50 o -6 5 1 8.82 30.36 18.14 o -5 5 1 2573.86 2463.35 65.35 o -4 5 1 24890.58 24366.68 509.56 o -3 5 1 6034.45 6069.39 120.46 o -2 5 1 19171.61 18645.09 390.81 o -1 5 1 2921.13 2882.17 63.92 o 0 5 1 7680.15 7875.48 170.87 o 1 5 1 5943.35 5882.90 120.55 o 2 5 1 3405.97 3288.60 75.07 o 3 5 1 8621.56 8543.84 191.30 o 4 5 1 8984.93 8955.49 203.63 o 5 5 1 9377.44 8926.53 189.92 o 6 5 1 3978.03 4051.98 97.69 o 7 5 1 568.08 511.98 34.49 o 8 5 1 3620.10 3630.84 90.34 o 9 5 1 61.62 78.01 16.08 o 10 5 1 1516.82 1401.89 91.97 o 11 5 1 2189.63 2304.11 104.08 o 12 5 1 2362.47 2539.40 133.58 o 13 5 1 1600.80 1508.65 146.49 o -13 6 1 1411.58 1475.11 115.83 o -12 6 1 843.92 947.67 81.62 o -11 6 1 343.69 279.70 39.09 o -10 6 1 778.94 631.01 55.20 o -9 6 1 1129.37 1084.35 46.50 o -8 6 1 11.17 -7.57 22.97 o -7 6 1 6728.59 6837.95 212.93 o -6 6 1 521.30 476.02 28.21 o -5 6 1 3712.57 3453.76 88.95 o -4 6 1 1761.08 1752.49 56.91 o -3 6 1 442.43 415.75 20.49 o -2 6 1 103.71 152.25 19.40 o -1 6 1 12512.09 12926.71 239.82 o 0 6 1 5.32 8.72 8.34 o 1 6 1 22120.65 21281.01 451.29 o 2 6 1 84.93 99.29 9.36 o 3 6 1 4649.27 4765.33 103.59 o 4 6 1 704.41 770.05 23.14 o 5 6 1 4744.12 4407.47 91.96 o 6 6 1 1221.60 1199.04 38.96 o 7 6 1 18628.54 18665.70 350.13 o 8 6 1 1973.59 1916.21 53.96 o 9 6 1 1348.59 1275.78 56.11 o 10 6 1 1295.06 1307.24 72.86 o 11 6 1 337.51 285.76 43.61 o 12 6 1 0.01 -54.68 54.90 o 13 6 1 2491.32 2528.87 185.75 o -13 7 1 29.56 -66.48 131.67 o -12 7 1 573.69 665.48 88.45 o -11 7 1 254.36 385.80 46.16 o -10 7 1 6947.33 7532.86 237.63 o -9 7 1 497.39 517.17 52.17 o -8 7 1 992.92 1019.29 45.08 o -7 7 1 2769.58 2685.72 92.02 o -6 7 1 28.76 32.07 15.73 o -5 7 1 876.27 850.08 26.71 o -4 7 1 6971.19 6932.20 143.17 o -3 7 1 1690.23 1600.55 39.41 o -2 7 1 8668.21 8804.08 174.32 o -1 7 1 6.56 22.66 14.63 o 0 7 1 115.46 128.52 7.43 o 1 7 1 1745.52 1868.00 40.13 o 2 7 1 11506.60 11782.25 210.10 o 3 7 1 459.27 567.68 18.38 o 4 7 1 4603.01 4388.14 91.06 o 5 7 1 1707.51 1632.14 48.81 o 6 7 1 2468.91 2359.47 58.41 o 7 7 1 24.70 54.51 20.53 o 8 7 1 653.86 594.74 32.98 o 9 7 1 142.30 165.88 38.20 o 10 7 1 3047.51 3285.89 115.13 o 11 7 1 426.24 466.16 60.08 o 12 7 1 1753.47 1511.99 112.61 o 13 7 1 171.42 216.86 95.46 o -13 8 1 487.97 551.18 133.43 o -12 8 1 1158.54 1148.07 110.40 o -11 8 1 1365.20 1255.69 79.91 o -10 8 1 488.68 423.23 54.23 o -9 8 1 274.48 211.24 32.29 o -8 8 1 6368.85 6328.98 168.86 o -7 8 1 5741.82 5780.20 165.07 o -6 8 1 2684.97 2624.06 80.38 o -5 8 1 5285.55 5458.56 119.77 o -4 8 1 1138.31 1125.18 47.70 o -3 8 1 4488.11 4700.91 92.89 o -2 8 1 1934.60 1895.35 70.25 o -1 8 1 523.64 560.33 26.99 o 0 8 1 26642.50 25953.81 581.92 o 1 8 1 40491.84 40104.47 878.00 o 2 8 1 102.58 63.40 9.12 o 3 8 1 3617.16 3380.56 70.78 o 4 8 1 1378.94 1250.02 36.82 o 5 8 1 2491.05 2536.15 57.59 o 6 8 1 9122.86 9362.82 193.22 o 7 8 1 818.47 889.63 55.45 o 8 8 1 612.63 558.13 36.26 o 9 8 1 1261.76 1120.36 70.39 o 10 8 1 93.65 25.58 36.56 o 11 8 1 518.57 498.89 71.41 o 12 8 1 294.26 259.84 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