#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/43/2224309.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2224309_Fobs loop_ _publ_author_name 'Peitz, Stephan' 'Peulecke, Normen' 'M\"uller, Bernd H.' 'Spannenberg, Anke' 'Rosenthal, Uwe' _publ_section_title ; Bis[N,N'-bis(2,6-diisopropylphenyl)ethane-1,2-diimine]-1\k^2^N,N';2\k^2^N,N'-tri-\m-trichlorido-1:2\k^6^Cl:Cl-chlorido-1\kCl-tetrahydrofuran-2\kO-dichromium(II) dichloromethane 4.5-solvate ; _journal_coeditor_code IM2155 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1574 _journal_volume 65 _journal_year 2009 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 105.160 _cell_angle_gamma 90.000 _cell_length_a 18.2545 _cell_length_b 15.4111 _cell_length_c 27.3121 _exptl_crystal_F_000 3028.00 _reflns_d_resolution_high 0.8255 _[local]_cod_data_source_file im2155Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ks765m in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 372.63 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 62300.04 67342.65 1129.30 o 3 0 0 13952.14 11129.92 185.04 o 4 0 0 44581.39 57711.81 406.06 o 5 0 0 26768.99 27364.62 606.53 o 6 0 0 17757.72 20099.00 400.73 o 7 0 0 1544.48 968.78 98.37 o 8 0 0 13936.52 13820.85 148.68 o 9 0 0 12.61 134.94 98.36 o 10 0 0 33702.18 34013.91 453.24 o 11 0 0 9298.71 8903.72 122.63 o 12 0 0 7055.27 7688.84 144.20 o 13 0 0 12254.69 12324.51 256.69 o 14 0 0 9361.20 8991.64 177.82 o 15 0 0 7566.76 7352.95 110.63 o 16 0 0 9580.00 9992.42 292.73 o 17 0 0 54.20 74.98 118.77 o 18 0 0 1326.30 1441.11 127.40 o 19 0 0 65.10 68.15 116.46 o 20 0 0 206.44 295.26 122.20 o 21 0 0 69.88 156.59 127.36 o 1 1 0 71242.66 56582.77 570.04 o 2 1 0 21878.09 19098.30 283.04 o 3 1 0 9548.38 8565.86 117.09 o 4 1 0 22283.65 20612.60 291.65 o 5 1 0 36911.99 43714.81 235.65 o 6 1 0 1823.04 1830.03 69.75 o 7 1 0 7605.87 7894.84 101.46 o 8 1 0 2374.52 2545.50 76.40 o 9 1 0 3511.58 3285.06 74.29 o 10 1 0 7387.03 7904.59 101.91 o 11 1 0 39.05 50.69 71.27 o 12 1 0 9192.01 8407.92 85.14 o 13 1 0 1516.19 1526.84 78.81 o 14 1 0 4281.02 4322.74 83.12 o 15 1 0 270.60 151.23 100.15 o 16 1 0 1372.11 1187.75 83.85 o 17 1 0 130.01 186.50 72.10 o 18 1 0 171.33 92.46 78.26 o 19 1 0 48.53 121.03 86.44 o 20 1 0 15.65 -9.42 91.43 o 21 1 0 106.29 43.52 83.49 o 0 2 0 20358.19 11434.90 214.11 o 1 2 0 3500.25 6537.69 120.35 o 2 2 0 153.40 132.56 64.81 o 3 2 0 556.34 310.86 76.43 o 4 2 0 97294.75 111484.91 1273.14 o 5 2 0 27064.27 26408.71 205.79 o 6 2 0 833.14 1482.53 69.99 o 7 2 0 990.53 905.94 71.99 o 8 2 0 19139.81 19475.66 183.36 o 9 2 0 1896.19 2098.95 72.19 o 10 2 0 1779.57 1724.40 74.72 o 11 2 0 4733.87 4791.07 104.35 o 12 2 0 604.02 613.41 66.77 o 13 2 0 154.86 202.25 71.25 o 14 2 0 1673.02 1564.54 76.00 o 15 2 0 1967.60 1879.51 79.21 o 16 2 0 6304.48 6009.94 119.74 o 17 2 0 8.58 -50.75 84.50 o 18 2 0 3557.07 3366.22 86.38 o 19 2 0 123.62 124.76 92.03 o 20 2 0 465.22 524.34 93.01 o 21 2 0 214.01 334.35 109.71 o 1 3 0 471.17 978.38 72.35 o 2 3 0 100.84 195.64 67.25 o 3 3 0 24895.19 31168.30 278.08 o 4 3 0 27560.27 26864.32 266.88 o 5 3 0 17910.55 17509.38 119.03 o 6 3 0 5444.49 6396.78 105.37 o 7 3 0 18762.44 18865.86 126.20 o 8 3 0 1452.28 1621.12 132.21 o 9 3 0 3393.95 3322.81 75.08 o 10 3 0 427.53 589.48 73.67 o 11 3 0 918.98 920.71 62.47 o 12 3 0 897.90 879.06 67.12 o 13 3 0 2071.17 1873.48 79.52 o 14 3 0 600.41 573.31 73.92 o 15 3 0 2170.32 2252.31 72.88 o 16 3 0 4955.25 4859.67 99.98 o 17 3 0 3673.64 3575.11 100.29 o 18 3 0 457.72 443.41 84.71 o 19 3 0 15.83 60.62 88.40 o 20 3 0 98.66 102.20 91.51 o 21 3 0 543.94 599.17 105.10 o 0 4 0 11932.45 14386.18 211.75 o 1 4 0 114.75 273.20 70.35 o 2 4 0 3353.65 3687.03 85.94 o 3 4 0 12.63 296.84 78.17 o 4 4 0 9716.79 11132.62 114.40 o 5 4 0 1014.32 1105.41 70.02 o 6 4 0 895.86 974.55 71.23 o 7 4 0 701.67 975.14 101.61 o 8 4 0 1668.36 1675.54 71.74 o 9 4 0 967.58 1060.23 71.51 o 10 4 0 5040.49 5114.34 85.29 o 11 4 0 1284.70 1562.88 72.86 o 12 4 0 64.67 60.00 74.38 o 13 4 0 255.28 266.73 75.58 o 14 4 0 1620.54 1477.52 70.88 o 15 4 0 4451.00 4219.80 85.85 o 16 4 0 241.13 298.97 74.52 o 17 4 0 274.40 242.09 77.75 o 18 4 0 172.65 182.81 85.07 o 19 4 0 415.42 400.19 77.67 o 20 4 0 346.85 246.29 93.70 o 1 5 0 16998.33 17456.53 176.49 o 2 5 0 2.13 247.38 73.95 o 3 5 0 305.01 179.33 65.73 o 4 5 0 2271.07 2401.70 78.03 o 5 5 0 577.76 652.24 69.25 o 6 5 0 4525.67 4805.71 84.87 o 7 5 0 1695.72 1334.73 67.62 o 8 5 0 2277.27 2678.22 78.28 o 9 5 0 5589.73 5064.85 73.72 o 10 5 0 3978.57 4405.91 79.61 o 11 5 0 2.36 63.47 68.65 o 12 5 0 1253.48 1491.52 98.51 o 13 5 0 5988.90 6199.17 91.77 o 14 5 0 307.53 346.33 71.95 o 15 5 0 733.27 737.94 83.67 o 16 5 0 11.74 75.55 72.37 o 17 5 0 420.03 475.71 82.68 o 18 5 0 109.37 114.29 86.88 o 19 5 0 1.20 29.16 96.00 o 20 5 0 269.01 317.19 95.64 o 0 6 0 1934.71 1930.49 106.75 o 1 6 0 9830.56 10021.18 120.60 o 2 6 0 379.04 894.42 74.65 o 3 6 0 2827.51 3094.49 80.14 o 4 6 0 174.92 328.78 62.29 o 5 6 0 1565.70 1772.40 72.10 o 6 6 0 8827.27 8835.35 96.34 o 7 6 0 1666.41 1756.65 74.46 o 8 6 0 3587.51 3553.86 80.53 o 9 6 0 1921.95 2242.25 70.67 o 10 6 0 3708.82 3806.00 76.07 o 11 6 0 10137.10 9918.86 160.03 o 12 6 0 1.76 66.69 77.37 o 13 6 0 4732.70 4784.85 86.12 o 14 6 0 349.36 349.63 84.79 o 15 6 0 1862.93 1811.59 78.75 o 16 6 0 11.62 58.63 81.34 o 17 6 0 30.38 93.99 83.37 o 18 6 0 6.32 76.96 79.00 o 19 6 0 196.51 263.43 84.02 o 20 6 0 367.21 399.65 98.16 o 1 7 0 9980.51 8724.80 96.66 o 2 7 0 5.15 87.06 63.03 o 3 7 0 2.86 219.50 64.32 o 4 7 0 12710.70 13241.78 139.03 o 5 7 0 108.19 117.39 70.42 o 6 7 0 427.73 483.44 72.24 o 7 7 0 319.10 425.76 67.64 o 8 7 0 1012.49 1197.89 67.19 o 9 7 0 4000.52 3652.86 88.32 o 10 7 0 1412.84 1583.71 70.89 o 11 7 0 1.78 57.61 71.63 o 12 7 0 10013.96 9893.65 152.27 o 13 7 0 940.08 832.10 71.13 o 14 7 0 8560.78 8009.19 215.45 o 15 7 0 4.47 88.73 84.43 o 16 7 0 1666.19 1589.08 90.41 o 17 7 0 32.72 111.47 89.27 o 18 7 0 33.39 62.76 85.52 o 19 7 0 110.49 182.58 89.87 o 0 8 0 11908.51 11739.56 195.00 o 1 8 0 945.54 1153.27 71.23 o 2 8 0 55852.13 56452.36 473.47 o 3 8 0 74.90 144.65 70.81 o 4 8 0 744.91 872.82 68.68 o 5 8 0 2809.34 2607.30 77.95 o 6 8 0 19.91 22.75 71.69 o 7 8 0 257.25 308.17 68.35 o 8 8 0 9312.14 9846.32 95.20 o 9 8 0 1688.31 1586.94 77.31 o 10 8 0 157.76 153.84 67.08 o 11 8 0 39.83 51.13 69.26 o 12 8 0 586.02 682.84 86.26 o 13 8 0 4076.55 4339.39 90.49 o 14 8 0 1557.58 1495.50 74.77 o 15 8 0 1024.02 964.11 82.36 o 16 8 0 67.48 63.97 88.54 o 17 8 0 185.21 267.04 83.71 o 18 8 0 68.77 69.53 91.50 o 19 8 0 171.44 318.25 102.11 o 1 9 0 13830.80 12533.58 112.05 o 2 9 0 2884.42 2897.22 70.44 o 3 9 0 1041.08 919.21 61.97 o 4 9 0 28.63 122.86 68.19 o 5 9 0 263.18 291.80 68.10 o 6 9 0 1484.47 1674.99 77.12 o 7 9 0 838.59 786.60 72.23 o 8 9 0 328.65 278.85 67.54 o 9 9 0 31.49 18.31 75.54 o 10 9 0 1826.16 2127.05 77.93 o 11 9 0 1387.87 1396.83 81.99 o 12 9 0 7.18 69.20 86.22 o 13 9 0 1425.89 1495.52 87.25 o 14 9 0 713.85 734.27 101.68 o 15 9 0 247.90 269.21 84.46 o 16 9 0 181.99 170.00 79.64 o 17 9 0 114.61 206.01 103.31 o 18 9 0 600.35 566.84 90.71 o 0 10 0 6306.88 6814.94 125.72 o 1 10 0 458.05 555.69 63.63 o 2 10 0 23163.99 24473.58 236.75 o 3 10 0 3270.77 2954.20 74.32 o 4 10 0 43.42 142.60 78.53 o 5 10 0 1417.80 1364.07 73.32 o 6 10 0 2733.35 2366.65 73.15 o 7 10 0 816.35 1028.17 78.20 o 8 10 0 28.91 148.43 68.87 o 9 10 0 1332.74 1209.70 76.35 o 10 10 0 399.74 398.70 80.69 o 11 10 0 2860.55 3019.79 89.71 o 12 10 0 127.46 145.24 83.63 o 13 10 0 2180.28 2119.07 103.45 o 14 10 0 9.91 -0.19 93.62 o 15 10 0 210.27 352.90 86.58 o 16 10 0 335.76 285.58 96.13 o 17 10 0 841.10 788.87 91.34 o 18 10 0 135.52 223.98 104.07 o 1 11 0 3613.81 3166.84 79.57 o 2 11 0 2210.37 1922.40 84.27 o 3 11 0 1486.62 1448.26 78.45 o 4 11 0 994.90 1202.49 85.62 o 5 11 0 104.15 128.48 71.28 o 6 11 0 2291.26 2075.16 82.43 o 7 11 0 1105.66 1285.73 81.01 o 8 11 0 118.52 103.42 75.04 o 9 11 0 141.17 140.17 75.82 o 10 11 0 2794.12 2802.80 100.86 o 11 11 0 1118.54 1114.93 86.79 o 12 11 0 4402.21 3857.54 112.56 o 13 11 0 695.78 851.89 78.00 o 14 11 0 1857.17 1964.46 83.09 o 15 11 0 88.57 47.27 100.91 o 16 11 0 391.19 491.27 93.40 o 17 11 0 31.81 89.21 92.11 o 0 12 0 195.94 287.26 110.24 o 1 12 0 1060.11 831.38 84.30 o 2 12 0 2032.06 1781.40 73.50 o 3 12 0 67.50 137.35 83.09 o 4 12 0 2291.90 2221.52 98.06 o 5 12 0 213.19 237.09 85.18 o 6 12 0 944.53 1065.02 81.42 o 7 12 0 74.11 68.38 85.23 o 8 12 0 673.79 580.14 78.46 o 9 12 0 96.51 143.20 83.62 o 10 12 0 4.12 36.56 96.86 o 11 12 0 1104.10 1301.06 93.50 o 12 12 0 1502.19 1486.39 91.85 o 13 12 0 1820.56 2027.03 90.98 o 14 12 0 52.49 124.24 89.91 o 15 12 0 1041.55 1139.27 100.78 o 16 12 0 16.84 51.51 88.36 o 1 13 0 9.07 95.22 79.49 o 2 13 0 402.40 423.03 86.65 o 3 13 0 136.65 183.19 80.60 o 4 13 0 914.12 844.81 82.84 o 5 13 0 2005.77 1841.52 90.91 o 6 13 0 0.81 55.99 94.61 o 7 13 0 337.24 274.04 79.25 o 8 13 0 120.87 290.58 91.98 o 9 13 0 185.75 159.85 92.92 o 10 13 0 324.62 342.05 96.26 o 11 13 0 2.04 -10.91 97.37 o 12 13 0 4.60 69.11 88.65 o 13 13 0 174.01 181.54 90.12 o 14 13 0 252.49 278.56 94.58 o 15 13 0 88.18 155.42 97.27 o 0 14 0 1572.48 1751.19 139.05 o 1 14 0 662.24 654.37 83.43 o 2 14 0 348.25 417.68 83.95 o 3 14 0 483.58 544.59 84.44 o 4 14 0 638.61 728.75 92.47 o 5 14 0 2081.99 1951.74 85.34 o 6 14 0 408.52 386.30 82.58 o 7 14 0 362.96 514.41 88.18 o 8 14 0 11.16 67.65 82.93 o 9 14 0 1768.45 1789.81 93.54 o 10 14 0 167.79 191.55 88.11 o 11 14 0 2220.16 2406.83 93.87 o 12 14 0 131.37 180.85 97.51 o 13 14 0 910.34 969.86 97.58 o 14 14 0 10.39 25.76 97.65 o 1 15 0 462.82 407.88 75.22 o 2 15 0 0.51 187.43 86.88 o 3 15 0 61.01 49.24 77.61 o 4 15 0 794.23 876.31 81.52 o 5 15 0 0.32 -26.29 84.21 o 6 15 0 1109.63 1237.74 93.45 o 7 15 0 368.38 311.73 91.84 o 8 15 0 944.33 1069.91 96.78 o 9 15 0 93.19 180.34 89.49 o 10 15 0 423.38 342.68 86.93 o 11 15 0 300.79 245.48 102.08 o 12 15 0 1538.36 1527.19 105.33 o 0 16 0 1806.61 1789.12 137.18 o 1 16 0 1184.56 1202.08 87.87 o 2 16 0 281.99 266.86 91.31 o 3 16 0 641.27 507.47 84.41 o 4 16 0 227.32 240.78 92.95 o 5 16 0 326.49 395.54 94.81 o 6 16 0 569.47 633.49 95.87 o 7 16 0 211.20 268.28 91.40 o 8 16 0 178.05 145.17 93.03 o 9 16 0 8.29 61.56 95.85 o 10 16 0 119.81 180.61 91.69 o 1 17 0 3633.45 3676.16 103.22 o 2 17 0 39.64 10.42 91.18 o 3 17 0 585.92 603.78 87.84 o 4 17 0 724.49 716.62 93.75 o 5 17 0 1.65 77.37 89.81 o 6 17 0 44.02 67.79 99.61 o 7 17 0 5.97 64.53 101.41 o 8 17 0 210.14 217.69 97.44 o 0 18 0 5426.04 4960.16 158.03 o 1 18 0 74.49 48.89 90.74 o 2 18 0 2753.49 2794.15 106.91 o 3 18 0 1070.74 1115.71 99.33 o 4 18 0 307.98 435.94 104.12 o 5 18 0 382.32 349.21 91.22 o -21 1 1 1567.59 1547.30 94.36 o -20 1 1 720.01 649.76 87.17 o -19 1 1 1.70 -6.06 86.50 o -18 1 1 564.99 610.28 88.32 o -17 1 1 2356.44 2338.38 89.61 o -16 1 1 1152.78 1080.68 103.19 o -15 1 1 4987.64 4970.82 101.75 o -14 1 1 3875.16 3572.17 75.39 o -13 1 1 932.74 725.07 67.65 o -12 1 1 8298.37 8183.45 85.11 o -11 1 1 3278.64 3289.96 71.10 o -10 1 1 8646.65 8357.65 88.93 o -9 1 1 11172.63 11471.75 165.35 o -8 1 1 901.32 1088.72 65.99 o -7 1 1 20435.40 21707.59 219.80 o -6 1 1 33019.34 32058.83 216.38 o -5 1 1 16370.06 17462.58 170.26 o -4 1 1 543.79 659.59 66.43 o -3 1 1 12712.97 16636.07 154.41 o -2 1 1 22608.64 29154.46 233.98 o -1 1 1 58751.70 56493.32 443.28 o 0 1 1 116.30 123.93 60.57 o 1 1 1 80722.30 96853.52 1429.03 o 2 1 1 7.41 135.11 59.50 o 3 1 1 13423.80 12789.24 127.42 o 4 1 1 52388.66 51775.25 650.48 o 5 1 1 30463.22 31420.55 303.48 o 6 1 1 116.60 131.55 67.02 o 7 1 1 37373.48 36097.33 361.82 o 8 1 1 3.85 73.73 61.00 o 9 1 1 450.03 554.49 64.90 o 10 1 1 3679.40 4115.34 83.03 o 11 1 1 2813.10 2594.49 76.21 o 12 1 1 2507.97 2528.83 72.15 o 13 1 1 2084.70 2159.33 80.93 o 14 1 1 3188.75 3288.78 86.28 o 15 1 1 6274.32 6358.75 186.52 o 16 1 1 431.42 467.45 71.05 o 17 1 1 3668.45 3410.74 80.12 o 18 1 1 24.97 2.90 83.07 o 19 1 1 892.40 982.03 88.63 o 20 1 1 28.74 72.58 88.03 o 21 1 1 2385.94 2123.59 96.06 o -21 2 1 358.28 266.50 102.31 o -20 2 1 1752.08 1581.06 94.34 o -19 2 1 189.77 188.57 82.07 o -18 2 1 46.38 70.58 72.29 o -17 2 1 193.46 229.21 74.68 o -16 2 1 3286.99 3094.21 104.35 o -15 2 1 405.06 427.19 74.54 o -14 2 1 4700.13 4702.39 83.01 o -13 2 1 4829.13 4787.82 74.54 o -12 2 1 126.97 254.67 68.12 o -11 2 1 21689.95 21620.19 164.57 o -10 2 1 2320.26 2089.16 75.85 o -9 2 1 159.34 249.86 57.84 o -8 2 1 5160.02 4826.05 79.36 o -7 2 1 3063.53 3914.81 80.84 o -6 2 1 4548.60 5078.05 84.90 o -5 2 1 2099.68 1940.69 75.41 o -4 2 1 17179.29 21087.99 244.79 o -3 2 1 2406.23 1990.80 155.33 o -2 2 1 3524.94 4487.39 100.78 o -1 2 1 963.60 1438.33 81.53 o 0 2 1 24765.34 26694.12 414.02 o 1 2 1 18573.34 17881.92 178.06 o 2 2 1 41.75 77.34 67.98 o 3 2 1 36262.51 41839.96 349.76 o 4 2 1 24262.06 27356.64 158.44 o 5 2 1 14835.33 16071.55 198.20 o 6 2 1 6356.94 6787.67 86.32 o 7 2 1 6937.60 7522.92 82.01 o 8 2 1 2709.35 2678.66 69.73 o 9 2 1 1065.47 1035.37 66.50 o 10 2 1 1915.72 1968.80 75.79 o 11 2 1 7241.98 6746.27 104.64 o 12 2 1 4577.44 4222.11 81.48 o 13 2 1 216.31 224.02 70.65 o 14 2 1 3770.30 3470.33 85.81 o 15 2 1 85.01 160.55 75.62 o 16 2 1 2894.66 2709.96 77.14 o 17 2 1 251.73 237.65 76.64 o 18 2 1 14.96 37.12 80.19 o 19 2 1 5.79 11.78 79.72 o 20 2 1 1008.81 973.39 85.63 o 21 2 1 36.84 88.18 97.65 o -21 3 1 2556.90 2389.67 92.68 o -20 3 1 361.53 319.48 91.98 o -19 3 1 1898.18 1784.07 92.21 o -18 3 1 96.67 139.41 88.86 o -17 3 1 283.24 331.87 100.55 o -16 3 1 248.26 317.63 78.04 o -15 3 1 7.64 51.40 74.15 o -14 3 1 21.45 42.74 65.11 o -13 3 1 744.22 639.49 76.42 o -12 3 1 2372.23 2217.73 77.64 o -11 3 1 1772.51 1647.27 71.13 o -10 3 1 3650.54 3763.88 83.32 o -9 3 1 9282.70 8134.99 91.15 o -8 3 1 36674.36 37037.13 540.00 o -7 3 1 528.50 528.66 73.21 o -6 3 1 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223.43 o -11 0 28 9.11 0.38 208.32 o -10 0 28 113.58 79.66 183.01 o -9 0 28 54.07 86.85 153.08 o -8 0 28 960.18 989.93 158.73 o -7 0 28 354.40 339.09 142.61 o -6 0 28 1616.76 1386.08 143.08 o -5 0 28 940.07 1011.51 139.64 o -4 0 28 31.22 33.71 147.83 o -3 0 28 1.60 108.37 125.47 o -2 0 28 785.57 776.09 129.11 o -1 0 28 1518.61 1802.87 132.16 o 0 0 28 9.11 9.09 127.84 o 1 0 28 38.81 -9.70 136.45 o 2 0 28 34.38 -22.66 128.65 o 3 0 28 93.43 114.52 134.07 o 4 0 28 129.49 115.65 135.67 o 5 0 28 10.17 55.16 138.08 o 6 0 28 221.83 271.58 142.77 o -16 1 28 18.17 43.17 163.77 o -15 1 28 114.70 89.78 160.87 o -14 1 28 3.23 54.50 149.03 o -13 1 28 994.82 1070.00 144.99 o -12 1 28 87.31 66.69 128.38 o -11 1 28 1.50 -9.25 136.86 o -10 1 28 785.16 839.00 129.72 o -9 1 28 83.21 62.31 121.06 o -8 1 28 510.44 621.17 134.18 o -7 1 28 0.66 37.97 107.79 o -6 1 28 1070.10 1072.59 99.69 o -5 1 28 275.62 224.09 98.53 o -4 1 28 950.71 854.15 98.42 o -3 1 28 5.67 21.23 93.26 o -2 1 28 1322.20 1373.56 93.82 o 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