#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/43/2224313.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2224313_Fobs loop_ _publ_author_name 'de Lima, Geraldo M.' 'Wardell, Solange M. S. V.' 'Wardell, James L.' 'Tiekink, Edward R. T.' _publ_section_title ; Bis(2-ethoxycarbonylethyl-\k^2^C^1^,O)(2-thioxo-1,3-dithiole-4,5-dithiolato-\k^2^S^4^,S^5^)tin(IV) ; _journal_coeditor_code IM2162 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1635 _journal_page_last m1636 _journal_volume 65 _journal_year 2009 _space_group_IT_number 33 _symmetry_space_group_name_Hall 'P 2c -2n' _symmetry_space_group_name_H-M 'P n a 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 12.1224 _cell_length_b 13.3825 _cell_length_c 11.9228 _exptl_crystal_F_000 1032.00 _reflns_d_resolution_high 0.7703 _[local]_cod_data_source_file im2162Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 2009src0472 in New: Pna21' _shelx_refln_list_code 4 _shelx_f_calc_maximum 372.23 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z+1/2' '-x+1/2, y+1/2, z+1/2' 'x+1/2, -y+1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 -13 926.10 816.20 171.85 o 2 1 -13 3879.47 3625.61 492.49 o 3 1 -13 87.75 -65.95 43.97 o 4 1 -13 1358.63 1118.39 172.10 o 5 1 -13 306.59 188.89 83.95 o 2 2 -13 107.32 111.47 89.18 o 3 2 -13 1786.24 1491.88 241.39 o 4 2 -13 932.17 1032.10 172.06 o 5 2 -13 661.39 504.35 126.11 o 1 3 -13 356.02 223.33 89.32 o 2 3 -13 194.27 199.13 110.64 o 3 3 -13 511.68 305.42 109.09 o 4 3 -13 91.26 21.43 107.12 o 1 4 -13 1183.18 903.74 176.36 o 2 4 -13 9.21 -109.33 87.48 o 3 4 -13 641.80 453.55 129.59 o 4 4 -13 199.20 84.99 84.99 o 1 5 -13 36.67 0.00 65.05 o 2 5 -13 996.29 667.56 193.83 o 3 5 -13 197.18 340.73 127.78 o 0 0 -12 2540.16 2548.26 242.78 o 2 0 -12 786.27 690.85 119.12 o 6 0 -12 775.80 648.52 129.72 o 1 1 -12 948.05 965.60 77.97 o 2 1 -12 59.82 52.34 39.59 o 3 1 -12 126.87 102.78 70.06 o 4 1 -12 916.65 822.41 96.87 o 5 1 -12 87.59 88.96 47.17 o 6 1 -12 519.36 429.71 118.21 o 7 1 -12 30.23 62.97 62.97 o 0 2 -12 1560.40 1509.31 191.70 o 1 2 -12 196.87 162.79 51.59 o 2 2 -12 786.86 756.38 84.97 o 3 2 -12 1115.13 1190.72 98.93 o 4 2 -12 495.81 379.49 64.52 o 5 2 -12 1901.27 1484.08 144.06 o 6 2 -12 135.81 89.76 52.02 o 7 2 -12 1243.57 819.79 147.16 o 1 3 -12 4819.92 5133.50 333.72 o 2 3 -12 20.32 -23.41 46.83 o 3 3 -12 3160.14 3353.38 210.19 o 4 3 -12 380.13 353.00 64.36 o 5 3 -12 2766.48 2600.15 217.93 o 6 3 -12 234.52 127.59 75.81 o 7 3 -12 20.06 126.47 105.39 o 0 4 -12 3353.56 3094.45 325.88 o 1 4 -12 278.97 239.84 72.51 o 2 4 -12 1860.35 1845.66 161.61 o 3 4 -12 814.40 866.50 114.05 o 4 4 -12 573.72 516.07 112.21 o 5 4 -12 842.70 857.84 110.01 o 1 5 -12 764.01 740.36 80.54 o 2 5 -12 561.57 475.60 90.60 o 3 5 -12 313.68 246.52 112.06 o 4 5 -12 1596.54 1634.17 176.73 o 0 6 -12 3737.43 3263.77 380.18 o 1 6 -12 42.23 -19.12 53.55 o 2 6 -12 909.98 798.62 133.12 o 3 6 -12 46.76 21.97 87.87 o 1 7 -12 379.81 305.72 109.19 o 3 7 -12 76.62 86.09 86.09 o 0 8 -12 851.34 556.43 128.42 o 1 8 -12 349.99 235.07 106.86 o 2 0 -11 3123.81 3233.73 187.34 o 4 0 -11 1280.18 1430.30 145.50 o 6 0 -11 2466.01 2472.99 229.08 o 8 0 -11 1131.73 1013.58 107.87 o 0 1 -11 3061.99 3219.48 217.72 o 1 1 -11 704.24 582.76 51.10 o 2 1 -11 5289.09 5660.39 230.51 o 3 1 -11 197.07 188.53 29.22 o 4 1 -11 2208.32 2141.58 125.89 o 5 1 -11 638.74 612.85 94.31 o 6 1 -11 363.29 326.07 55.01 o 7 1 -11 1080.96 1001.37 78.66 o 8 1 -11 67.17 43.14 43.14 o 1 2 -11 3289.40 3226.67 148.18 o 2 2 -11 326.02 366.98 46.05 o 3 2 -11 3697.48 3736.57 168.95 o 4 2 -11 1091.25 957.83 143.85 o 5 2 -11 646.82 643.27 73.70 o 6 2 -11 2459.40 2276.67 153.54 o 7 2 -11 542.52 481.76 69.61 o 8 2 -11 598.91 583.64 108.10 o 0 3 -11 174.88 164.00 53.52 o 1 3 -11 1141.21 1030.20 57.06 o 2 3 -11 35.76 34.89 29.33 o 3 3 -11 1367.62 1260.50 88.83 o 4 3 -11 40.47 -4.83 40.23 o 5 3 -11 2959.69 2947.93 199.93 o 6 3 -11 46.50 22.93 32.43 o 7 3 -11 1493.60 1266.59 123.08 o 8 3 -11 130.12 195.13 65.05 o 1 4 -11 1616.38 1707.83 89.65 o 2 4 -11 39.20 126.37 43.81 o 3 4 -11 1145.85 1150.92 87.54 o 4 4 -11 480.82 496.64 89.41 o 5 4 -11 613.40 566.47 72.97 o 6 4 -11 1663.45 1580.68 130.54 o 7 4 -11 464.79 313.49 89.57 o 8 4 -11 769.00 369.12 108.57 o 0 5 -11 1179.36 1123.14 143.42 o 1 5 -11 176.99 83.46 59.52 o 2 5 -11 2787.13 2940.77 145.05 o 3 5 -11 155.00 129.15 34.54 o 4 5 -11 1387.03 1297.66 107.49 o 5 5 -11 193.06 148.65 66.87 o 6 5 -11 1061.99 889.63 111.22 o 1 6 -11 161.63 101.10 58.34 o 2 6 -11 983.41 970.29 89.14 o 3 6 -11 187.84 91.93 57.46 o 4 6 -11 449.96 476.20 90.72 o 5 6 -11 6.00 89.13 66.85 o 0 7 -11 2666.39 2880.46 274.48 o 1 7 -11 184.19 130.41 54.77 o 2 7 -11 1930.59 1918.33 135.80 o 3 7 -11 155.34 179.95 89.97 o 4 7 -11 1566.35 1510.38 133.31 o 1 8 -11 3190.99 3059.47 268.14 o 2 8 -11 398.00 333.42 88.91 o 3 8 -11 3053.77 2712.50 220.62 o 0 0 -10 2247.46 2608.42 217.45 o 2 0 -10 369.19 429.37 56.70 o 4 0 -10 5460.20 5769.51 325.84 o 6 0 -10 73.81 121.14 72.68 o 8 0 -10 920.02 1000.42 113.71 o 1 1 -10 2623.66 2830.25 103.64 o 2 1 -10 648.09 647.24 45.25 o 3 1 -10 296.49 346.78 53.35 o 4 1 -10 562.49 622.92 61.64 o 5 1 -10 349.05 355.12 42.23 o 6 1 -10 1678.97 1630.03 120.04 o 7 1 -10 87.42 117.46 33.22 o 8 1 -10 2867.19 2623.49 184.61 o 9 1 -10 176.89 44.12 66.18 o 0 2 -10 1214.48 1160.28 84.30 o 1 2 -10 892.83 875.35 51.17 o 2 2 -10 482.11 499.96 39.77 o 3 2 -10 3384.95 3450.59 130.27 o 4 2 -10 1177.47 1242.70 56.22 o 5 2 -10 4215.95 4219.02 167.28 o 6 2 -10 333.49 325.64 84.32 o 7 2 -10 3095.06 3033.76 180.80 o 8 2 -10 247.12 234.34 54.67 o 9 2 -10 2001.14 1836.14 265.53 o 1 3 -10 7267.81 7831.77 265.93 o 2 3 -10 293.41 243.81 34.29 o 3 3 -10 5915.52 6185.97 219.11 o 4 3 -10 156.07 190.61 29.88 o 5 3 -10 2041.36 1790.61 95.18 o 6 3 -10 544.21 526.82 93.58 o 7 3 -10 124.01 46.71 46.71 o 8 3 -10 179.09 125.23 48.30 o 9 3 -10 32.38 66.52 66.52 o 0 4 -10 5700.94 6181.11 319.54 o 1 4 -10 517.85 459.49 41.41 o 2 4 -10 2884.17 3030.98 126.12 o 3 4 -10 1656.03 1633.78 85.52 o 4 4 -10 2116.12 2194.51 94.04 o 5 4 -10 2096.98 2081.62 125.51 o 6 4 -10 471.44 421.69 51.06 o 7 4 -10 2244.57 2257.06 181.42 o 8 4 -10 62.24 0.00 45.85 o 9 4 -10 1194.51 908.51 199.45 o 1 5 -10 2120.47 2061.45 103.65 o 2 5 -10 898.15 891.61 66.83 o 3 5 -10 1.97 6.29 25.15 o 4 5 -10 2111.77 2186.47 136.56 o 5 5 -10 166.72 212.96 55.65 o 7 5 -10 9.92 -22.63 45.28 o 8 5 -10 3374.85 2809.46 388.43 o 9 5 -10 30.48 0.00 66.15 o 0 6 -10 6229.76 6543.19 680.75 o 1 6 -10 0.16 27.90 30.02 o 2 6 -10 2173.56 2256.46 105.33 o 3 6 -10 17.86 38.93 36.29 o 4 6 -10 4208.55 4410.98 291.14 o 5 6 -10 232.94 245.16 68.45 o 6 6 -10 365.48 329.13 49.71 o 7 6 -10 194.36 70.24 70.24 o 1 7 -10 1161.58 1232.41 91.59 o 2 7 -10 367.39 333.69 50.31 o 3 7 -10 339.23 234.78 70.43 o 4 7 -10 3044.75 2874.54 278.26 o 5 7 -10 254.35 319.35 68.44 o 1 8 -10 541.35 466.74 93.35 o 2 8 -10 339.37 301.96 92.91 o 3 8 -10 918.56 898.77 115.25 o 4 8 -10 293.22 364.68 68.38 o 2 0 -9 4515.75 5100.35 208.34 o 4 0 -9 1464.38 1453.32 95.19 o 6 0 -9 7453.99 7762.19 385.97 o 8 0 -9 3641.30 3900.93 335.22 o 0 1 -9 4976.59 5215.34 202.18 o 1 1 -9 1321.29 1478.54 59.59 o 2 1 -9 7750.16 8276.03 242.38 o 3 1 -9 66.26 38.64 20.89 o 4 1 -9 3693.94 3761.50 136.25 o 5 1 -9 550.55 623.70 35.90 o 6 1 -9 278.49 255.50 29.84 o 7 1 -9 2772.18 2706.58 108.80 o 8 1 -9 108.18 71.85 33.87 o 9 1 -9 297.26 313.00 49.12 o 1 2 -9 5119.91 5631.27 154.42 o 2 2 -9 866.93 846.19 44.38 o 3 2 -9 6459.52 6860.53 210.81 o 4 2 -9 1321.14 1367.06 66.99 o 5 2 -9 254.16 261.13 28.14 o 6 2 -9 4228.95 4308.82 171.70 o 7 2 -9 198.62 209.75 33.64 o 8 2 -9 1774.19 1691.35 114.99 o 9 2 -9 124.71 209.59 49.13 o 10 2 -9 1423.52 1214.25 134.97 o 0 3 -9 466.30 420.96 59.36 o 1 3 -9 2057.50 2188.69 81.53 o 2 3 -9 65.73 72.20 21.13 o 3 3 -9 1350.49 1509.26 67.93 o 4 3 -9 678.79 658.81 45.12 o 5 3 -9 6508.00 6676.44 232.82 o 6 3 -9 46.76 62.02 20.77 o 7 3 -9 3529.86 3607.32 169.61 o 8 3 -9 556.64 607.52 102.29 o 9 3 -9 3399.49 3396.82 288.61 o 10 3 -9 76.82 44.98 44.98 o 1 4 -9 4221.05 4412.23 140.91 o 2 4 -9 845.87 772.18 66.38 o 3 4 -9 1170.75 1242.59 62.64 o 4 4 -9 593.30 545.09 41.93 o 5 4 -9 456.46 455.53 40.85 o 6 4 -9 1618.84 1622.96 83.73 o 7 4 -9 526.32 579.61 49.86 o 8 4 -9 1160.46 1243.33 110.14 o 9 4 -9 63.69 23.26 46.54 o 10 4 -9 1048.92 627.46 134.47 o 0 5 -9 1575.04 1510.45 88.70 o 1 5 -9 291.82 287.05 34.99 o 2 5 -9 3579.24 3827.13 125.25 o 3 5 -9 252.37 278.02 31.43 o 4 5 -9 2142.81 2151.40 99.74 o 5 5 -9 762.49 828.83 54.57 o 6 5 -9 1692.15 1661.94 94.26 o 7 5 -9 534.32 447.54 57.61 o 8 5 -9 292.57 239.76 71.94 o 9 5 -9 539.00 438.80 92.39 o 10 5 -9 53.18 177.70 88.84 o 1 6 -9 875.29 903.17 57.88 o 2 6 -9 242.83 248.64 34.75 o 3 6 -9 466.57 408.40 38.85 o 4 6 -9 351.51 450.25 52.36 o 5 6 -9 3.59 -16.70 28.92 o 6 6 -9 3362.97 3564.96 251.39 o 7 6 -9 1.35 -23.66 39.14 o 8 6 -9 949.97 615.81 142.13 o 9 6 -9 36.95 113.98 91.17 o 0 7 -9 2991.15 2844.54 165.13 o 1 7 -9 1566.62 1655.03 85.25 o 2 7 -9 2317.24 2383.24 128.89 o 3 7 -9 174.99 138.24 36.78 o 4 7 -9 2097.36 2006.93 105.54 o 5 7 -9 2258.49 2280.74 152.95 o 6 7 -9 595.30 516.82 57.31 o 7 7 -9 1201.00 1181.98 168.89 o 1 8 -9 7887.70 8134.29 552.38 o 2 8 -9 187.65 177.99 69.80 o 3 8 -9 3336.53 3324.83 265.24 o 4 8 -9 413.90 452.75 71.50 o 5 8 -9 673.45 681.57 94.03 o 0 0 -8 14398.61 16050.22 753.65 o 2 0 -8 1182.86 1257.05 62.77 o 4 0 -8 10149.04 10383.62 415.52 o 6 0 -8 3014.76 3277.41 140.06 o 8 0 -8 1118.04 1009.06 132.65 o 10 0 -8 141.62 117.04 46.82 o 1 1 -8 4519.10 4739.64 129.01 o 2 1 -8 1156.55 1203.15 44.28 o 3 1 -8 1248.45 1194.53 46.13 o 4 1 -8 1772.02 1867.15 64.65 o 5 1 -8 787.28 787.60 43.67 o 6 1 -8 3021.37 3089.73 107.90 o 7 1 -8 49.71 70.82 25.75 o 8 1 -8 4951.72 5068.72 199.10 o 9 1 -8 70.60 64.28 27.83 o 10 1 -8 2029.74 2020.23 146.16 o 0 2 -8 2950.90 3075.69 135.16 o 1 2 -8 938.58 1029.55 51.84 o 2 2 -8 1700.60 1733.31 77.74 o 3 2 -8 3785.85 3872.01 118.26 o 4 2 -8 1777.41 1874.93 65.59 o 5 2 -8 4316.95 4489.64 140.74 o 6 2 -8 302.60 327.52 34.82 o 7 2 -8 4016.06 4120.32 148.65 o 8 2 -8 927.94 890.13 57.44 o 9 2 -8 3209.90 3251.57 166.45 o 10 2 -8 669.45 662.47 60.31 o 1 3 -8 12758.57 13351.09 393.14 o 2 3 -8 136.29 167.68 28.94 o 3 3 -8 6571.32 7044.11 205.93 o 4 3 -8 341.45 379.17 32.98 o 5 3 -8 3244.11 3259.19 107.43 o 6 3 -8 40.54 68.60 19.95 o 7 3 -8 315.74 297.79 42.33 o 8 3 -8 143.52 113.90 65.26 o 9 3 -8 356.49 304.57 36.49 o 10 3 -8 17.49 -47.01 70.50 o 0 4 -8 4468.57 4761.66 301.59 o 1 4 -8 394.10 380.68 33.35 o 2 4 -8 1903.91 1918.49 74.04 o 3 4 -8 5314.33 5591.41 153.38 o 4 4 -8 3999.90 4211.42 137.71 o 5 4 -8 3502.22 3676.84 141.82 o 6 4 -8 74.61 88.98 26.02 o 7 4 -8 3659.15 3742.78 155.40 o 8 4 -8 116.82 107.06 31.38 o 9 4 -8 2026.22 2031.26 112.63 o 10 4 -8 339.66 280.32 93.44 o 1 5 -8 3314.79 3319.39 106.92 o 2 5 -8 767.63 804.31 44.26 o 3 5 -8 111.50 139.55 39.44 o 4 5 -8 2859.83 2962.24 132.65 o 5 5 -8 524.73 446.80 39.81 o 6 5 -8 2603.59 2828.62 134.46 o 7 5 -8 2.69 -16.60 28.73 o 8 5 -8 4944.13 5098.40 238.41 o 9 5 -8 106.66 117.29 33.17 o 10 5 -8 1398.18 1131.63 184.80 o 0 6 -8 11777.98 12361.17 638.66 o 1 6 -8 90.15 96.21 22.14 o 2 6 -8 1358.35 1404.79 63.99 o 3 6 -8 13.76 16.30 44.19 o 4 6 -8 6212.50 6304.24 282.97 o 5 6 -8 64.45 78.40 30.16 o 6 6 -8 359.58 352.87 32.09 o 7 6 -8 133.60 106.17 28.28 o 8 6 -8 526.68 445.55 64.40 o 9 6 -8 46.67 71.06 71.06 o 10 6 -8 552.91 318.01 113.58 o 1 7 -8 2693.52 2674.81 114.84 o 2 7 -8 106.15 118.61 34.52 o 3 7 -8 1291.53 1454.43 77.48 o 4 7 -8 2613.69 2719.06 128.83 o 5 7 -8 871.44 754.99 55.20 o 6 7 -8 1833.03 1750.49 100.55 o 7 7 -8 87.94 66.58 31.04 o 8 7 -8 2000.85 2028.74 241.61 o 9 7 -8 253.67 324.78 92.80 o 0 8 -8 1286.51 1156.52 137.72 o 1 8 -8 651.00 817.52 109.04 o 2 8 -8 393.47 396.51 48.22 o 3 8 -8 2324.57 2200.88 160.19 o 4 8 -8 895.17 761.93 81.30 o 5 8 -8 4985.42 5306.59 289.91 o 6 8 -8 160.35 74.29 41.39 o 7 8 -8 1326.13 1295.24 195.54 o 1 9 -8 6078.21 6818.59 639.56 o 2 9 -8 874.92 1008.78 132.76 o 3 9 -8 1035.56 898.81 113.26 o 4 9 -8 392.59 446.35 74.41 o 2 0 -7 6273.59 6789.18 347.73 o 4 0 -7 3103.07 3355.67 135.25 o 6 0 -7 13161.77 13699.60 553.09 o 8 0 -7 3066.56 3099.27 184.13 o 10 0 -7 4084.11 3881.49 463.95 o 0 1 -7 5507.84 5649.97 187.84 o 1 1 -7 5517.87 6299.84 147.97 o 2 1 -7 12613.94 12972.97 308.10 o 3 1 -7 61.08 93.94 21.14 o 4 1 -7 7056.98 7316.06 202.70 o 5 1 -7 4949.40 5178.95 141.39 o 6 1 -7 2008.90 1992.05 67.40 o 7 1 -7 1284.96 1132.16 53.83 o 8 1 -7 430.78 420.31 45.13 o 9 1 -7 2456.71 2646.05 158.33 o 10 1 -7 546.88 527.67 58.63 o 11 1 -7 217.02 117.74 47.09 o 1 2 -7 11303.26 12028.35 278.17 o 2 2 -7 779.61 831.68 35.74 o 3 2 -7 6340.79 6588.49 188.59 o 4 2 -7 1438.05 1394.86 54.05 o 5 2 -7 1600.16 1694.22 63.19 o 6 2 -7 1612.28 1527.64 65.11 o 7 2 -7 742.71 769.27 65.73 o 8 2 -7 104.54 116.92 27.11 o 9 2 -7 237.07 211.87 32.17 o 10 2 -7 1947.03 2164.69 227.16 o 11 2 -7 1161.15 1059.07 117.73 o 0 3 -7 1906.05 1903.64 86.84 o 1 3 -7 4140.17 4212.21 110.11 o 2 3 -7 807.87 853.39 45.38 o 3 3 -7 1132.79 1127.86 49.93 o 4 3 -7 1325.27 1254.47 55.44 o 5 3 -7 8645.22 8968.54 236.73 o 6 3 -7 276.03 313.50 34.89 o 7 3 -7 5475.39 5646.92 249.54 o 8 3 -7 196.45 160.78 20.99 o 9 3 -7 4152.08 4440.68 362.72 o 10 3 -7 203.68 284.85 47.47 o 11 3 -7 1451.28 1381.68 140.59 o 1 4 -7 6059.41 6409.01 153.71 o 2 4 -7 3551.24 3822.73 109.01 o 3 4 -7 5428.06 5472.56 215.24 o 4 4 -7 2589.09 2557.35 84.11 o 5 4 -7 2395.70 2361.42 102.16 o 6 4 -7 3318.53 3454.89 125.66 o 7 4 -7 1086.80 1014.28 69.38 o 8 4 -7 703.69 679.82 47.07 o 9 4 -7 351.36 315.95 42.25 o 10 4 -7 2213.44 2300.12 151.48 o 11 4 -7 404.70 463.70 92.75 o 0 5 -7 8698.93 8767.29 296.63 o 1 5 -7 58.79 39.40 18.65 o 2 5 -7 6012.34 6123.83 160.24 o 3 5 -7 171.98 242.23 31.24 o 4 5 -7 2877.67 2992.43 115.04 o 5 5 -7 1279.73 1235.26 60.22 o 6 5 -7 2330.05 2417.05 105.24 o 7 5 -7 1007.01 984.26 63.35 o 8 5 -7 40.90 24.74 20.13 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5235.52 5569.96 202.62 o 3 11 5 56.27 41.95 20.55 o 4 11 5 1555.78 1505.82 103.72 o 5 11 5 290.62 244.80 24.88 o 6 11 5 591.43 610.20 36.69 o 7 11 5 155.46 150.20 15.43 o 8 11 5 491.20 502.97 60.25 o 9 11 5 40.15 29.11 20.48 o 10 11 5 247.69 242.34 213.97 o 11 11 5 236.76 196.29 77.27 o 1 12 5 413.85 393.65 37.10 o 2 12 5 657.35 576.22 43.36 o 3 12 5 397.50 342.82 28.80 o 4 12 5 522.11 513.29 35.31 o 5 12 5 446.07 444.75 34.92 o 6 12 5 3591.37 3860.77 187.38 o 7 12 5 39.30 48.75 18.62 o 8 12 5 742.29 624.66 58.33 o 9 12 5 118.04 103.32 30.16 o 10 12 5 2445.77 3291.32 486.37 o 0 13 5 1289.04 1213.90 108.87 o 1 13 5 554.73 524.32 46.25 o 2 13 5 853.66 763.92 49.53 o 3 13 5 120.95 147.97 23.31 o 4 13 5 1294.17 1418.17 65.20 o 5 13 5 1749.31 1589.72 96.69 o 6 13 5 110.56 135.16 34.27 o 7 13 5 458.78 541.79 49.80 o 8 13 5 24.94 4.23 19.19 o 9 13 5 814.85 758.92 100.99 o 1 14 5 2537.28 2586.87 177.13 o 2 14 5 163.97 124.48 30.20 o 3 14 5 1420.33 1509.34 84.99 o 4 14 5 19.52 -24.93 31.81 o 5 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12048.40 549.58 o 1 6 8 90.00 103.67 27.62 o 2 6 8 1346.27 1357.20 58.05 o 3 6 8 14.50 20.36 14.50 o 4 6 8 6124.54 6046.67 161.91 o 5 6 8 64.55 86.86 25.11 o 6 6 8 355.99 438.76 27.39 o 7 6 8 132.64 110.09 17.40 o 8 6 8 529.63 507.36 47.35 o 9 6 8 43.63 45.94 17.14 o 10 6 8 539.75 462.90 58.89 o 11 6 8 7.33 31.01 39.96 o 12 6 8 443.16 473.19 45.52 o 1 7 8 2631.74 2616.49 85.05 o 2 7 8 117.45 161.73 23.82 o 3 7 8 1336.77 1450.97 56.32 o 4 7 8 2614.95 2650.95 104.97 o 5 7 8 885.96 814.41 49.37 o 6 7 8 1836.95 1806.80 82.83 o 7 7 8 82.48 45.01 24.30 o 8 7 8 1975.36 2003.01 128.30 o 9 7 8 256.18 282.09 39.59 o 10 7 8 1838.78 1884.29 152.01 o 11 7 8 152.30 108.07 30.70 o 0 8 8 1287.32 1288.60 166.93 o 1 8 8 667.22 634.43 35.94 o 2 8 8 413.98 385.05 30.80 o 3 8 8 2260.97 2220.53 76.48 o 4 8 8 918.46 869.91 45.17 o 5 8 8 5080.95 5297.89 213.66 o 6 8 8 164.18 193.65 26.93 o 7 8 8 1370.96 1337.47 92.83 o 8 8 8 34.44 23.39 18.35 o 9 8 8 2478.56 2611.79 220.84 o 10 8 8 78.48 56.14 33.07 o 11 8 8 578.87 499.62 57.35 o 1 9 8 6173.95 6441.43 227.43 o 2 9 8 883.71 941.03 70.32 o 3 9 8 1047.11 1103.56 50.20 o 4 9 8 400.87 385.95 33.12 o 5 9 8 1940.72 2142.68 93.95 o 6 9 8 100.59 74.47 30.85 o 7 9 8 15.48 11.66 16.46 o 8 9 8 189.05 179.38 36.33 o 9 9 8 20.72 5.46 28.09 o 10 9 8 294.65 318.45 71.59 o 0 10 8 4222.92 4505.03 254.33 o 1 10 8 32.52 15.43 26.05 o 2 10 8 454.49 350.58 33.30 o 3 10 8 521.45 474.02 39.90 o 4 10 8 1771.88 1873.35 138.16 o 5 10 8 518.79 532.55 39.24 o 6 10 8 337.86 238.45 31.47 o 7 10 8 1109.58 1090.55 99.99 o 8 10 8 104.77 130.79 42.45 o 9 10 8 588.23 667.91 64.17 o 1 11 8 199.19 174.00 38.42 o 2 11 8 121.17 124.63 24.98 o 3 11 8 103.52 111.01 28.24 o 4 11 8 1278.22 1328.08 73.42 o 5 11 8 40.20 -19.82 26.91 o 6 11 8 1126.19 1107.95 69.83 o 7 11 8 0.50 27.77 41.00 o 8 11 8 1944.08 2278.41 264.38 o 9 11 8 93.92 72.88 47.22 o 0 12 8 3791.46 4385.86 511.24 o 1 12 8 7.62 -24.49 24.23 o 2 12 8 832.79 892.40 63.44 o 3 12 8 183.36 135.92 37.42 o 4 12 8 2215.27 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1408.61 1495.53 143.32 o 8 0 13 624.93 623.31 205.09 o 0 1 13 5190.11 5213.22 297.69 o 1 1 13 74.08 73.92 31.67 o 2 1 13 3851.17 3953.96 196.05 o 3 1 13 92.99 85.65 20.76 o 4 1 13 1394.97 1297.67 100.66 o 5 1 13 302.01 340.86 37.51 o 6 1 13 228.88 204.03 39.54 o 7 1 13 380.71 364.55 48.97 o 8 1 13 6.77 -1.57 37.25 o 1 2 13 1918.14 1969.68 104.08 o 2 2 13 112.80 146.82 46.47 o 3 2 13 1747.07 1753.61 95.50 o 4 2 13 927.18 873.98 71.78 o 5 2 13 670.83 591.37 50.73 o 6 2 13 1669.59 1529.81 120.15 o 7 2 13 170.12 130.13 30.87 o 8 2 13 678.92 767.02 154.98 o 0 3 13 13.89 27.12 37.63 o 1 3 13 351.00 366.32 45.09 o 2 3 13 191.55 227.83 46.15 o 3 3 13 510.25 515.37 52.01 o 4 3 13 92.53 83.16 34.76 o 5 3 13 1156.05 1085.23 103.83 o 6 3 13 6.26 41.94 40.26 o 7 3 13 1084.99 1028.50 78.85 o 8 3 13 84.00 33.53 34.83 o 1 4 13 1184.36 1149.02 74.62 o 2 4 13 8.55 0.00 23.80 o 3 4 13 645.64 585.67 59.59 o 4 4 13 200.22 269.09 41.23 o 5 4 13 195.67 132.26 33.92 o 6 4 13 735.18 729.24 61.62 o 7 4 13 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