#------------------------------------------------------------------------------ #$Date: 2010-01-22 14:33:52 +0200 (Fri, 22 Jan 2010) $ #$Revision: 960 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2224441.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2224441_Fobs loop_ _publ_author_name 'Chopra, Deepak' 'Choudhury, A. R.' 'Venugopala, K. N.' 'Govender, Thavendran' 'Kruger, Hendrik G.' 'Maguire, Glenn E. M.' 'Guru Row, T. N.' _publ_section_title ; 3-(2-Amino-1,3-thiazol-4-yl)-6-chloro-2H-chromen-2-one ; _journal_coeditor_code SJ2672 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3111 _journal_volume 65 _journal_year 2009 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 98.156 _cell_angle_gamma 90.000 _cell_length_a 12.4940 _cell_length_b 7.3498 _cell_length_c 25.0128 _exptl_crystal_F_000 1136.00 _reflns_d_resolution_high 0.8300 _[local]_cod_data_source_file sj2672Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' vg4_m in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 315.93 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 61.63 35.16 6.14 o 2 0 0 41386.34 44970.39 194.68 o 3 0 0 1839.10 2084.87 35.00 o 4 0 0 88.14 74.50 19.24 o 5 0 0 2313.15 2396.48 44.77 o 6 0 0 2520.73 2498.49 50.45 o 7 0 0 134.85 131.75 26.03 o 8 0 0 146.48 122.04 26.63 o 9 0 0 4.90 39.80 30.54 o 10 0 0 3.96 -11.50 35.08 o 11 0 0 5.06 0.11 36.92 o 12 0 0 211.50 228.16 45.61 o 13 0 0 88.31 130.34 44.07 o 14 0 0 64.87 61.34 59.44 o 1 1 0 107.07 100.32 6.62 o 2 1 0 708.47 690.46 14.73 o 3 1 0 439.05 406.83 21.86 o 4 1 0 11.36 28.42 12.21 o 5 1 0 283.69 288.38 16.88 o 6 1 0 685.87 661.43 23.14 o 7 1 0 347.77 369.18 21.45 o 8 1 0 183.17 180.15 21.16 o 9 1 0 52.48 61.22 21.11 o 10 1 0 0.07 -21.53 24.56 o 11 1 0 19.30 12.90 25.81 o 12 1 0 348.37 329.32 40.95 o 13 1 0 0.88 6.03 28.04 o 14 1 0 29.28 15.20 44.29 o 0 2 0 507.81 382.14 16.50 o 1 2 0 26892.68 28284.61 116.96 o 2 2 0 126.54 97.51 12.04 o 3 2 0 5847.37 5736.30 42.75 o 4 2 0 725.70 837.27 20.86 o 5 2 0 4042.60 4234.08 43.99 o 6 2 0 2.98 -12.98 14.42 o 7 2 0 17.50 26.62 17.37 o 8 2 0 198.79 207.42 21.31 o 9 2 0 723.03 702.56 30.34 o 10 2 0 78.08 58.94 25.05 o 11 2 0 63.91 41.68 40.52 o 12 2 0 72.65 63.10 29.29 o 13 2 0 6.40 47.60 30.81 o 14 2 0 421.46 455.05 45.96 o 1 3 0 596.24 590.69 16.28 o 2 3 0 8.33 -5.13 10.83 o 3 3 0 4.16 10.86 13.13 o 4 3 0 178.22 203.00 20.84 o 5 3 0 1586.51 1493.74 30.46 o 6 3 0 331.93 296.67 21.37 o 7 3 0 480.44 507.76 25.56 o 8 3 0 614.59 561.21 27.69 o 9 3 0 32.68 16.03 20.72 o 10 3 0 103.43 67.13 23.11 o 11 3 0 60.85 74.94 24.36 o 12 3 0 194.57 144.75 38.54 o 13 3 0 2.03 -36.21 36.21 o 14 3 0 74.03 129.85 51.45 o 0 4 0 129.19 182.78 18.70 o 1 4 0 8.18 9.90 10.20 o 2 4 0 866.13 779.87 21.91 o 3 4 0 1565.96 1409.46 28.49 o 4 4 0 3121.52 3051.22 44.39 o 5 4 0 110.14 145.19 18.76 o 6 4 0 636.05 673.09 27.56 o 7 4 0 0.67 1.75 27.78 o 8 4 0 1003.70 990.31 51.52 o 9 4 0 1744.94 1755.36 53.41 o 10 4 0 80.87 65.13 26.67 o 11 4 0 3250.89 3172.69 106.66 o 12 4 0 35.08 24.25 38.99 o 13 4 0 11.59 28.26 53.03 o 1 5 0 94.42 106.12 16.04 o 2 5 0 211.85 226.28 21.01 o 3 5 0 0.11 18.73 17.59 o 4 5 0 257.56 284.55 23.92 o 5 5 0 14.36 8.14 21.10 o 6 5 0 0.88 -18.17 21.38 o 7 5 0 122.43 108.15 23.69 o 8 5 0 123.75 132.01 24.73 o 9 5 0 29.87 34.36 25.02 o 10 5 0 19.06 80.79 34.92 o 11 5 0 45.06 67.74 29.10 o 12 5 0 1.53 27.12 37.79 o 0 6 0 0.42 -1.78 27.60 o 1 6 0 18.04 6.99 19.33 o 2 6 0 203.45 195.03 26.05 o 3 6 0 513.20 520.92 32.81 o 4 6 0 27.89 64.88 25.46 o 5 6 0 63.14 131.15 25.92 o 6 6 0 31.62 3.66 24.47 o 7 6 0 2.27 0.32 25.25 o 8 6 0 188.70 160.52 34.96 o 9 6 0 30.47 95.83 74.78 o 10 6 0 193.88 232.41 34.88 o 1 7 0 7.99 19.28 25.59 o 2 7 0 17.51 35.61 26.73 o 3 7 0 203.73 258.44 34.16 o 4 7 0 78.62 232.39 144.18 o 5 7 0 19.79 79.57 60.99 o 6 7 0 73.56 71.86 49.75 o 7 7 0 1.21 -17.67 28.42 o 8 7 0 0.02 -26.62 52.26 o 9 7 0 26.97 100.62 53.57 o 0 8 0 94.03 125.07 59.11 o 1 8 0 46.09 47.16 52.32 o 2 8 0 0.65 -16.44 44.44 o 3 8 0 2.97 -20.76 32.56 o 4 8 0 0.41 54.04 34.79 o 5 8 0 267.39 412.95 130.35 o 6 8 0 11.31 72.30 64.40 o -14 1 1 64.16 95.39 31.73 o -13 1 1 594.02 632.33 52.40 o -12 1 1 6.08 -7.88 26.63 o -11 1 1 130.22 126.67 28.62 o -10 1 1 1019.48 966.47 82.17 o -9 1 1 285.68 270.00 24.45 o -8 1 1 4335.90 4305.09 52.86 o -7 1 1 6173.37 6212.13 58.24 o -6 1 1 164.44 187.56 17.76 o -5 1 1 3591.88 3667.01 38.19 o -4 1 1 0.93 6.52 11.63 o -3 1 1 1684.31 1709.45 22.70 o -2 1 1 10663.57 11377.56 50.95 o -1 1 1 344.86 327.22 7.65 o 0 1 1 128.81 134.66 5.22 o 1 1 1 68.02 81.40 6.97 o 2 1 1 2764.63 2858.84 25.33 o 3 1 1 135.05 143.69 14.51 o 4 1 1 0.53 8.20 12.70 o 5 1 1 88.84 106.21 14.84 o 6 1 1 1234.47 1119.85 27.31 o 7 1 1 16.62 18.62 17.26 o 8 1 1 477.79 452.51 24.66 o 9 1 1 633.53 694.64 30.31 o 10 1 1 1257.44 1144.78 41.13 o 11 1 1 15.68 27.35 26.74 o 12 1 1 1200.57 1293.94 57.76 o 13 1 1 30.92 68.32 29.82 o 14 1 1 22.67 23.30 33.37 o -14 2 1 152.54 201.16 39.00 o -13 2 1 125.34 133.81 32.68 o -12 2 1 161.34 130.29 30.74 o -11 2 1 734.46 760.68 48.08 o -10 2 1 131.49 159.05 26.52 o -9 2 1 110.04 133.89 24.02 o -8 2 1 350.82 371.48 24.18 o -7 2 1 15.88 20.96 16.64 o -6 2 1 1.05 5.00 14.95 o -5 2 1 7.33 -12.19 13.12 o -4 2 1 2975.16 3128.08 34.43 o -3 2 1 10083.46 10605.24 59.14 o -2 2 1 8389.71 8761.78 49.03 o -1 2 1 25795.77 28007.28 100.46 o 0 2 1 33851.99 37116.07 122.77 o 1 2 1 44680.99 49381.12 158.06 o 2 2 1 4903.31 5251.93 38.26 o 3 2 1 962.96 869.87 19.70 o 4 2 1 86.09 57.88 13.76 o 5 2 1 6133.11 6988.77 57.56 o 6 2 1 17.88 41.71 16.08 o 7 2 1 283.20 196.25 19.82 o 8 2 1 114.70 95.28 21.47 o 9 2 1 107.75 133.77 23.45 o 10 2 1 51.36 60.05 24.31 o 11 2 1 56.41 51.71 24.01 o 12 2 1 6.72 -3.00 27.45 o 13 2 1 13.80 36.30 36.20 o 14 2 1 7.00 -15.29 67.56 o -14 3 1 45.60 75.06 45.60 o -13 3 1 82.27 52.60 38.61 o -12 3 1 154.52 69.82 36.22 o -11 3 1 101.78 193.19 36.53 o -10 3 1 59.06 66.61 23.36 o -9 3 1 28.97 23.89 22.98 o -8 3 1 1.11 10.72 18.80 o -7 3 1 45.15 40.19 18.60 o -6 3 1 52.16 45.68 15.47 o -5 3 1 125.60 151.45 17.06 o -4 3 1 622.95 596.53 21.16 o -3 3 1 514.52 519.73 18.28 o -2 3 1 23.83 19.75 10.97 o -1 3 1 446.55 450.87 14.42 o 0 3 1 83.01 76.84 9.73 o 1 3 1 2722.25 2771.47 30.37 o 2 3 1 229.60 242.00 14.48 o 3 3 1 1911.22 1798.81 28.62 o 4 3 1 768.53 776.99 22.82 o 5 3 1 498.32 469.74 22.39 o 6 3 1 528.76 510.28 24.59 o 7 3 1 496.51 432.35 23.04 o 8 3 1 207.67 203.65 23.79 o 9 3 1 554.23 536.46 29.92 o 10 3 1 53.95 67.26 22.83 o 11 3 1 136.79 132.56 26.47 o 12 3 1 17.15 16.85 46.97 o 13 3 1 97.54 147.49 45.34 o -13 4 1 1.77 11.77 41.34 o -12 4 1 14.17 32.24 77.36 o -11 4 1 959.89 984.09 96.98 o -10 4 1 1.73 26.54 23.89 o -9 4 1 24.60 25.34 24.06 o -8 4 1 2.48 2.51 21.72 o -7 4 1 278.52 296.62 26.22 o -6 4 1 76.71 85.30 28.43 o -5 4 1 806.18 731.33 25.64 o -4 4 1 3328.18 3371.19 46.05 o -3 4 1 209.02 208.83 17.13 o -2 4 1 1416.69 1353.71 26.06 o -1 4 1 38.33 33.37 11.04 o 0 4 1 3213.58 3276.80 37.05 o 1 4 1 1453.20 1449.41 26.38 o 2 4 1 9.17 38.80 14.07 o 3 4 1 268.42 252.56 17.92 o 4 4 1 194.37 199.88 18.24 o 5 4 1 305.45 326.87 22.40 o 6 4 1 584.36 528.66 26.38 o 7 4 1 82.64 116.04 23.14 o 8 4 1 0.21 -10.33 21.59 o 9 4 1 8.85 23.13 24.39 o 10 4 1 71.92 83.46 28.84 o 11 4 1 25.99 27.67 27.61 o 12 4 1 18.58 -32.57 39.88 o 13 4 1 3.57 -22.18 41.25 o -12 5 1 85.01 128.50 42.39 o -11 5 1 93.01 93.55 29.33 o -10 5 1 312.37 290.07 35.06 o -9 5 1 2.48 36.64 26.12 o -8 5 1 179.29 213.50 27.17 o -7 5 1 324.14 327.27 28.52 o -6 5 1 0.05 -3.17 21.23 o -5 5 1 739.68 682.36 31.37 o -4 5 1 94.14 112.08 23.54 o -3 5 1 4.67 12.29 18.91 o -2 5 1 147.92 145.67 18.12 o -1 5 1 54.80 36.10 14.64 o 0 5 1 221.27 196.15 18.46 o 1 5 1 1157.04 1169.25 38.02 o 2 5 1 367.10 334.63 22.72 o 3 5 1 765.72 728.42 29.52 o 4 5 1 919.30 907.05 33.09 o 5 5 1 17.55 -11.53 20.48 o 6 5 1 129.27 118.97 27.93 o 7 5 1 344.56 360.34 32.67 o 8 5 1 2.21 19.86 25.58 o 9 5 1 448.56 495.13 39.16 o 10 5 1 214.83 235.74 33.21 o 11 5 1 42.61 35.99 27.91 o 12 5 1 14.74 60.72 42.92 o -11 6 1 1.48 62.27 30.41 o -10 6 1 796.53 843.69 52.13 o -9 6 1 48.96 115.34 51.98 o -8 6 1 49.08 127.44 41.16 o -7 6 1 170.00 185.49 29.66 o -6 6 1 441.22 514.79 35.71 o -5 6 1 172.24 173.31 35.26 o -4 6 1 0.30 30.54 20.93 o -3 6 1 50.21 60.84 23.59 o -2 6 1 39.33 21.16 20.45 o -1 6 1 26.66 37.23 21.66 o 0 6 1 25.11 51.97 22.17 o 1 6 1 0.29 -13.24 20.80 o 2 6 1 0.07 2.35 22.45 o 3 6 1 30.95 33.91 26.68 o 4 6 1 0.02 7.22 43.14 o 5 6 1 2.79 41.37 26.71 o 6 6 1 75.26 89.77 44.21 o 7 6 1 75.70 44.79 27.12 o 8 6 1 9.44 21.97 28.04 o 9 6 1 38.92 113.48 32.36 o 10 6 1 858.16 880.01 52.17 o -9 7 1 9.75 95.39 35.31 o -8 7 1 0.76 -60.58 60.58 o -7 7 1 1.46 -34.34 34.34 o -6 7 1 2.08 38.41 28.22 o -5 7 1 5.13 -17.06 41.51 o -4 7 1 18.70 2.62 25.21 o -3 7 1 146.60 165.07 30.47 o -2 7 1 36.89 53.08 26.27 o -1 7 1 106.39 83.02 23.45 o 0 7 1 40.12 52.66 27.08 o 1 7 1 71.09 74.87 27.00 o 2 7 1 13.34 -23.59 23.59 o 3 7 1 69.49 80.89 28.11 o 4 7 1 6.35 -23.71 31.73 o 5 7 1 43.68 74.88 31.46 o 6 7 1 0.34 21.48 29.18 o 7 7 1 78.33 117.44 64.79 o 8 7 1 30.58 -0.20 37.32 o 9 7 1 0.61 54.00 46.07 o -6 8 1 20.01 53.78 29.88 o -5 8 1 279.46 435.94 119.96 o -4 8 1 91.07 57.59 49.55 o -3 8 1 33.09 -33.08 33.08 o -2 8 1 54.47 127.19 44.75 o -1 8 1 0.51 8.32 51.23 o 0 8 1 0.05 -31.30 39.02 o 1 8 1 0.21 2.95 38.63 o 2 8 1 46.03 25.73 40.50 o 3 8 1 16.30 30.10 30.75 o 4 8 1 35.72 76.20 36.53 o 5 8 1 0.28 34.04 43.49 o 6 8 1 111.05 164.01 38.14 o -14 0 2 5.39 4.74 51.50 o -13 0 2 200.42 203.18 46.69 o -12 0 2 142.74 126.13 41.63 o -11 0 2 98.18 89.51 36.97 o -10 0 2 1077.15 940.95 58.69 o -9 0 2 1475.52 1432.23 50.42 o -8 0 2 170.63 196.24 28.66 o -7 0 2 301.47 334.75 29.44 o -6 0 2 8.46 -20.76 20.76 o -5 0 2 9.89 -5.52 17.76 o -4 0 2 5.27 -0.42 17.51 o -3 0 2 79.29 59.44 17.61 o -2 0 2 17902.98 18408.43 114.12 o -1 0 2 1177.59 1240.25 19.13 o 0 0 2 12.69 21.04 3.89 o 1 0 2 3680.21 3939.37 32.43 o 2 0 2 12605.02 13901.13 97.12 o 3 0 2 0.11 -17.87 17.87 o 4 0 2 99813.02 108413.55 441.29 o 5 0 2 229.17 416.03 27.14 o 6 0 2 7.00 -21.72 21.72 o 7 0 2 345.55 614.00 38.87 o 8 0 2 727.49 678.79 38.98 o 9 0 2 651.51 600.18 40.76 o 10 0 2 2672.84 2512.58 85.26 o 11 0 2 289.73 235.68 44.12 o 12 0 2 7.64 59.59 36.58 o 13 0 2 18.50 52.50 116.32 o 14 0 2 4.91 -20.75 40.21 o -14 1 2 4.87 -10.87 28.95 o -13 1 2 3.87 -1.66 28.01 o -12 1 2 11.32 15.71 27.31 o -11 1 2 172.17 201.35 30.55 o -10 1 2 544.93 527.61 36.33 o -9 1 2 773.30 758.31 31.77 o -8 1 2 780.42 810.04 27.44 o -7 1 2 2639.56 2831.97 40.12 o -6 1 2 734.76 684.31 22.18 o -5 1 2 0.31 -12.54 12.54 o -4 1 2 1038.70 974.81 19.41 o -3 1 2 194.67 185.64 12.36 o -2 1 2 7048.30 7372.32 38.93 o -1 1 2 831.79 770.38 13.07 o 0 1 2 295.53 238.64 6.57 o 1 1 2 917.96 867.44 12.44 o 2 1 2 1622.03 1617.22 21.05 o 3 1 2 0.24 14.31 13.02 o 4 1 2 321.15 322.92 16.39 o 5 1 2 174.10 177.47 15.79 o 6 1 2 133.91 119.33 17.79 o 7 1 2 644.75 712.15 26.07 o 8 1 2 371.56 385.77 24.40 o 9 1 2 413.17 434.60 26.88 o 10 1 2 648.09 632.21 39.98 o 11 1 2 192.81 209.59 27.61 o 12 1 2 274.42 313.74 33.67 o 13 1 2 17.33 19.43 43.11 o 14 1 2 29.27 59.54 44.68 o -14 2 2 170.51 152.06 33.93 o -13 2 2 59.97 118.05 33.18 o -12 2 2 490.89 479.80 37.70 o -11 2 2 65.87 49.22 26.39 o -10 2 2 2804.70 2720.58 62.15 o -9 2 2 197.41 175.20 24.03 o -8 2 2 13.18 10.42 18.15 o -7 2 2 13.92 26.13 16.04 o -6 2 2 456.29 473.42 20.69 o -5 2 2 635.25 638.21 20.44 o -4 2 2 133.12 114.72 12.81 o -3 2 2 485.61 453.87 15.65 o -2 2 2 2.20 5.73 9.87 o -1 2 2 43716.52 48238.16 241.50 o 0 2 2 182.84 122.08 10.62 o 1 2 2 90891.49 98936.79 278.95 o 2 2 2 166.35 164.18 13.14 o 3 2 2 79.47 49.02 13.13 o 4 2 2 531.37 474.91 20.99 o 5 2 2 16871.90 18392.91 98.03 o 6 2 2 141.25 123.16 18.90 o 7 2 2 7.64 4.89 17.61 o 8 2 2 264.23 257.78 24.16 o 9 2 2 61.19 56.62 22.43 o 10 2 2 1871.36 1778.26 44.54 o 11 2 2 100.72 77.09 25.01 o 12 2 2 50.90 51.80 28.86 o 13 2 2 167.91 190.79 33.88 o 14 2 2 9.49 30.89 43.29 o -14 3 2 3.78 -47.16 70.61 o -13 3 2 35.03 31.81 38.95 o -12 3 2 1.50 47.38 34.68 o -11 3 2 0.34 13.22 31.45 o -10 3 2 1705.67 1634.22 51.75 o -9 3 2 742.57 696.74 33.59 o -8 3 2 779.29 746.34 29.36 o -7 3 2 4450.50 4539.86 54.65 o -6 3 2 1302.30 1316.30 30.60 o -5 3 2 543.66 516.68 21.38 o -4 3 2 11.08 21.44 13.71 o -3 3 2 68.82 75.66 13.80 o -2 3 2 1616.03 1676.05 27.79 o -1 3 2 704.64 641.85 15.23 o 0 3 2 149.77 161.85 11.35 o 1 3 2 26.13 33.10 11.01 o 2 3 2 2357.20 2262.65 29.76 o 3 3 2 3.39 17.93 13.60 o 4 3 2 696.44 773.59 23.46 o 5 3 2 870.79 867.59 26.18 o 6 3 2 14.58 27.00 18.45 o 7 3 2 561.83 544.54 27.26 o 8 3 2 695.35 638.17 29.68 o 9 3 2 335.50 356.43 27.70 o 10 3 2 1535.23 1529.84 45.66 o 11 3 2 64.00 97.54 26.00 o 12 3 2 337.63 330.87 40.23 o 13 3 2 32.53 45.66 40.91 o -13 4 2 3.96 16.94 43.45 o -12 4 2 29.14 30.11 35.24 o -11 4 2 336.53 265.59 40.28 o -10 4 2 1.80 37.14 24.31 o -9 4 2 1383.02 1391.99 48.91 o -8 4 2 1.24 17.26 23.27 o -7 4 2 720.37 717.69 31.55 o -6 4 2 249.80 225.99 23.30 o -5 4 2 4.41 9.80 18.51 o -4 4 2 8302.04 8193.29 76.23 o -3 4 2 259.01 302.89 17.61 o -2 4 2 89.45 84.21 13.98 o -1 4 2 24.41 16.47 10.23 o 0 4 2 684.95 680.53 18.86 o 1 4 2 498.07 471.93 18.25 o 2 4 2 1490.64 1415.37 28.33 o 3 4 2 765.66 742.40 23.41 o 4 4 2 268.55 247.21 19.55 o 5 4 2 2.03 -1.56 17.41 o 6 4 2 10.85 3.52 19.72 o 7 4 2 133.19 153.37 24.38 o 8 4 2 465.19 523.91 33.46 o 9 4 2 122.29 112.83 26.78 o 10 4 2 2.12 48.57 27.34 o 11 4 2 195.47 175.84 34.40 o 12 4 2 245.19 294.99 49.63 o 13 4 2 65.33 117.99 61.45 o -12 5 2 137.36 179.05 44.93 o -11 5 2 119.37 150.63 40.13 o -10 5 2 88.23 123.16 30.08 o -9 5 2 29.19 68.50 35.05 o -8 5 2 11.94 46.66 26.93 o -7 5 2 55.51 50.52 18.79 o -6 5 2 42.92 32.56 21.79 o -5 5 2 8.65 19.67 20.91 o -4 5 2 42.99 63.23 20.44 o -3 5 2 135.50 144.09 21.45 o -2 5 2 3.55 -3.65 13.89 o -1 5 2 41.68 41.65 15.13 o 0 5 2 224.88 235.46 18.75 o 1 5 2 239.18 271.12 20.34 o 2 5 2 224.60 231.68 21.31 o 3 5 2 100.86 111.42 18.91 o 4 5 2 71.03 62.44 21.64 o 5 5 2 150.68 152.17 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