#------------------------------------------------------------------------------ #$Date: 2016-04-03 04:24:24 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181165 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/44/2224488.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2224488_Fobs loop_ _publ_author_name 'Anuradha, N.' 'Thiruvalluvar, A.' 'Pandiarajan, K.' 'Chitra, S.' 'Butcher, R. J.' _publ_section_title ; 5-Acetyl-4-(4-methoxyphenyl)-6-methyl-3,4-dihydropyrimidine-2(1H)-thione ; _journal_coeditor_code WN2363 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3036 _journal_volume 65 _journal_year 2009 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 100.901 _cell_angle_gamma 90.000 _cell_length_a 12.0415 _cell_length_b 6.2219 _cell_length_c 18.0192 _exptl_crystal_F_000 584.00 _reflns_d_resolution_high 0.8018 _cod_data_source_file wn2363Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' dc-3 in P 21/n Z=4 C14H16N2O2S1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 143.16 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1644.19 1749.81 5.67 o 4 0 0 1845.63 1893.54 35.21 o 6 0 0 2574.28 2687.79 13.22 o 8 0 0 801.63 730.05 13.56 o 10 0 0 694.67 665.48 11.03 o 12 0 0 114.11 118.71 2.58 o 14 0 0 558.50 551.38 5.26 o 1 1 0 2480.50 2518.55 26.10 o 2 1 0 2445.95 2576.51 63.03 o 3 1 0 367.76 352.44 11.74 o 4 1 0 2186.63 2346.27 38.65 o 5 1 0 2707.43 2803.56 41.58 o 6 1 0 27.55 33.35 1.86 o 7 1 0 41.32 51.12 8.09 o 8 1 0 361.52 414.60 10.12 o 9 1 0 771.87 724.60 9.31 o 10 1 0 806.42 774.59 10.95 o 11 1 0 5.24 5.58 1.26 o 12 1 0 92.62 95.27 2.63 o 13 1 0 78.73 80.43 2.07 o 14 1 0 3.25 4.05 1.82 o 0 2 0 160.52 121.23 2.36 o 1 2 0 57.73 77.18 2.21 o 2 2 0 1611.14 1882.68 98.74 o 3 2 0 63.12 87.46 1.87 o 4 2 0 89.01 82.86 1.94 o 5 2 0 536.39 675.05 6.33 o 6 2 0 77.99 107.25 2.39 o 7 2 0 203.08 209.90 5.45 o 8 2 0 17.61 17.27 0.84 o 9 2 0 0.04 1.23 0.75 o 10 2 0 437.15 407.73 5.29 o 11 2 0 216.50 215.63 2.36 o 12 2 0 22.05 46.40 25.90 o 13 2 0 69.01 66.57 2.43 o 14 2 0 146.28 168.96 2.63 o 1 3 0 644.93 681.00 5.39 o 2 3 0 2980.15 2977.30 11.55 o 3 3 0 21.37 30.76 1.96 o 4 3 0 95.26 110.56 3.20 o 5 3 0 41.00 48.23 2.50 o 6 3 0 146.64 136.95 5.26 o 7 3 0 0.33 0.96 0.88 o 8 3 0 564.03 527.07 4.38 o 9 3 0 5.85 4.25 1.16 o 10 3 0 397.77 353.37 3.05 o 11 3 0 33.29 33.78 1.24 o 12 3 0 512.54 484.80 3.36 o 13 3 0 72.13 69.00 2.02 o 0 4 0 160.61 182.82 5.22 o 1 4 0 1324.96 1309.46 15.07 o 2 4 0 87.98 110.28 3.11 o 3 4 0 1367.27 1316.73 17.91 o 4 4 0 205.31 177.36 2.65 o 5 4 0 907.91 882.96 27.52 o 6 4 0 91.34 101.30 2.15 o 7 4 0 267.72 259.66 7.69 o 8 4 0 262.91 216.02 2.91 o 9 4 0 80.12 75.28 1.79 o 10 4 0 5.48 6.49 1.12 o 11 4 0 99.52 106.15 4.76 o 12 4 0 6.65 6.34 0.92 o 1 5 0 1.78 1.92 1.14 o 2 5 0 2031.15 1804.41 48.16 o 3 5 0 486.24 453.13 18.01 o 4 5 0 0.07 1.21 1.42 o 5 5 0 1361.91 1202.31 7.69 o 6 5 0 9.05 5.06 1.42 o 7 5 0 57.90 50.42 1.68 o 8 5 0 588.29 516.89 6.17 o 9 5 0 715.57 720.18 10.32 o 10 5 0 45.73 47.57 1.21 o 11 5 0 27.48 28.05 0.91 o 0 6 0 1395.41 1286.49 8.09 o 1 6 0 694.99 599.54 11.53 o 2 6 0 260.70 253.62 10.93 o 3 6 0 51.80 39.66 2.02 o 4 6 0 119.00 107.24 2.63 o 5 6 0 165.85 155.40 2.83 o 6 6 0 290.54 293.82 23.47 o 7 6 0 184.10 174.62 2.24 o 8 6 0 329.19 357.81 2.38 o 9 6 0 5.95 9.91 0.63 o 1 7 0 20.27 21.55 0.86 o 2 7 0 117.72 132.33 2.23 o 3 7 0 13.43 17.40 1.21 o 4 7 0 290.95 348.23 3.24 o 5 7 0 241.91 279.56 14.77 o 6 7 0 87.98 110.88 2.23 o -13 0 1 454.21 449.81 6.07 o -11 0 1 1.62 2.55 1.62 o -9 0 1 1473.31 1432.55 28.23 o -7 0 1 443.82 432.16 6.03 o -5 0 1 1248.97 1250.15 34.50 o -3 0 1 3410.87 3945.11 20.13 o 1 0 1 6.73 7.28 0.81 o 3 0 1 8334.25 8118.32 115.13 o 5 0 1 110.21 79.84 4.35 o 7 0 1 3.93 -1.01 3.24 o 9 0 1 29.84 33.59 2.23 o 11 0 1 885.59 799.88 5.78 o 13 0 1 623.62 615.85 16.39 o -14 1 1 99.28 150.35 24.18 o -13 1 1 4.62 4.72 1.75 o -12 1 1 225.37 198.85 3.28 o -11 1 1 509.71 443.93 6.78 o -10 1 1 51.66 53.05 1.15 o -9 1 1 58.13 69.86 1.16 o -8 1 1 2136.18 2123.98 21.45 o -7 1 1 587.94 651.90 12.04 o -6 1 1 715.50 809.42 5.53 o -5 1 1 21.89 13.42 1.18 o -4 1 1 223.88 197.63 2.50 o -3 1 1 1393.89 1416.34 4.88 o -2 1 1 1167.91 1267.67 6.54 o -1 1 1 456.60 471.46 5.26 o 0 1 1 9246.95 8276.45 108.76 o 1 1 1 408.13 416.38 3.10 o 2 1 1 3273.10 3236.58 16.59 o 3 1 1 20496.04 20171.87 114.66 o 4 1 1 86.08 114.62 2.14 o 5 1 1 2193.47 2540.66 41.88 o 6 1 1 14.14 5.61 1.02 o 7 1 1 1621.96 1825.30 12.06 o 8 1 1 1.71 4.45 4.65 o 9 1 1 877.13 809.36 7.93 o 10 1 1 19.77 11.40 0.91 o 11 1 1 104.78 94.40 2.43 o 12 1 1 76.59 69.89 1.69 o 13 1 1 3.50 3.64 1.35 o 14 1 1 7.44 4.86 1.82 o -14 2 1 13.35 16.59 1.62 o -13 2 1 22.73 19.02 2.02 o -12 2 1 2.15 1.90 1.42 o -11 2 1 88.90 73.54 1.63 o -10 2 1 497.87 453.43 2.87 o -9 2 1 291.10 288.78 3.60 o -8 2 1 0.70 1.01 0.65 o -7 2 1 162.86 204.16 5.87 o -6 2 1 1305.07 1429.99 10.62 o -5 2 1 904.62 1126.56 7.32 o -4 2 1 17.02 19.61 1.30 o -3 2 1 41.08 33.86 1.11 o -2 2 1 309.72 356.47 7.89 o -1 2 1 14.43 20.70 1.34 o 0 2 1 6844.51 7189.58 14.41 o 1 2 1 470.26 485.06 5.21 o 2 2 1 151.65 150.31 6.27 o 3 2 1 1970.44 2241.68 14.16 o 4 2 1 617.43 618.40 4.57 o 5 2 1 15.56 7.89 1.32 o 6 2 1 10.55 8.99 1.38 o 7 2 1 41.82 54.13 2.11 o 8 2 1 1302.88 1328.05 6.42 o 9 2 1 618.74 614.48 5.66 o 10 2 1 311.31 272.07 2.98 o 11 2 1 214.80 179.66 2.37 o 12 2 1 245.18 258.89 9.51 o 13 2 1 238.57 232.49 3.44 o -13 3 1 20.58 26.71 1.82 o -12 3 1 47.71 45.43 1.57 o -11 3 1 1600.65 1465.89 9.51 o -10 3 1 326.65 281.62 3.95 o -9 3 1 8.59 8.17 1.05 o -8 3 1 229.19 204.50 2.73 o -7 3 1 142.57 140.90 4.99 o -6 3 1 7.06 11.10 1.99 o -5 3 1 254.77 214.08 3.98 o -4 3 1 466.96 525.64 13.35 o -3 3 1 526.82 523.96 17.70 o -2 3 1 75.58 99.77 3.44 o -1 3 1 9.22 20.24 1.25 o 0 3 1 117.12 146.81 2.80 o 1 3 1 287.87 356.12 5.72 o 2 3 1 1087.15 1246.49 8.91 o 3 3 1 2378.78 2310.85 15.07 o 4 3 1 0.13 1.75 1.47 o 5 3 1 157.71 170.87 3.95 o 6 3 1 209.63 216.47 5.87 o 7 3 1 4.58 4.80 1.00 o 8 3 1 1.69 1.99 1.07 o 9 3 1 190.90 205.56 3.34 o 10 3 1 275.82 270.41 2.71 o 11 3 1 187.73 177.09 2.21 o 12 3 1 64.09 67.12 1.72 o 13 3 1 159.10 180.49 2.63 o -12 4 1 5.16 2.90 0.92 o -11 4 1 128.21 124.94 1.84 o -10 4 1 174.11 174.65 2.19 o -9 4 1 126.45 118.51 2.09 o -8 4 1 1.87 0.33 1.22 o -7 4 1 56.63 49.98 2.02 o -6 4 1 1644.36 1629.94 77.50 o -5 4 1 1.59 8.02 2.53 o -4 4 1 117.78 121.61 3.04 o -3 4 1 97.87 98.68 4.00 o -2 4 1 24.37 33.53 6.27 o -1 4 1 388.38 351.98 7.79 o 0 4 1 386.01 369.99 5.34 o 1 4 1 2.36 3.31 1.72 o 2 4 1 197.39 171.37 6.20 o 3 4 1 143.71 158.03 6.98 o 4 4 1 3.49 3.84 1.10 o 5 4 1 383.29 372.80 3.76 o 6 4 1 129.06 117.68 2.33 o 7 4 1 1.01 2.90 1.11 o 8 4 1 4.31 3.29 1.12 o 9 4 1 2.44 2.66 1.12 o 10 4 1 19.78 19.79 1.12 o 11 4 1 2.13 2.02 1.32 o -11 5 1 24.93 18.32 0.86 o -10 5 1 21.04 23.50 1.07 o -9 5 1 41.92 39.99 1.31 o -8 5 1 161.22 176.15 2.58 o -7 5 1 192.33 183.16 2.72 o -6 5 1 254.61 237.55 3.64 o -5 5 1 0.05 0.00 1.42 o -4 5 1 194.98 164.50 3.24 o -3 5 1 8.16 8.90 1.62 o -2 5 1 29.02 27.34 1.42 o -1 5 1 36.18 38.57 1.43 o 0 5 1 920.10 829.31 4.78 o 1 5 1 3.18 3.75 1.07 o 2 5 1 2062.65 1851.72 32.48 o 3 5 1 3.85 4.57 1.11 o 4 5 1 949.82 813.46 33.29 o 5 5 1 438.15 395.98 4.45 o 6 5 1 187.10 160.05 3.04 o 7 5 1 148.98 134.58 2.83 o 8 5 1 118.85 129.30 3.44 o 9 5 1 1.17 4.58 0.97 o 10 5 1 411.78 427.28 6.17 o 11 5 1 57.54 53.82 1.42 o -9 6 1 181.94 191.69 3.24 o -8 6 1 190.93 207.50 4.25 o -7 6 1 95.85 88.52 1.83 o -6 6 1 103.57 105.22 2.63 o -5 6 1 237.48 235.73 3.44 o -4 6 1 47.76 44.31 2.02 o -3 6 1 2.24 2.63 1.42 o -2 6 1 3285.82 2800.01 11.94 o -1 6 1 392.46 374.78 11.94 o 0 6 1 157.34 138.73 2.07 o 1 6 1 784.65 700.02 4.20 o 2 6 1 787.69 699.60 17.81 o 3 6 1 7.68 4.06 1.00 o 4 6 1 15.46 12.55 1.42 o 5 6 1 1062.67 1044.29 6.68 o 6 6 1 23.92 22.51 1.22 o 7 6 1 69.26 71.43 2.63 o 8 6 1 225.49 238.36 2.63 o 9 6 1 140.69 181.30 1.82 o -6 7 1 1.95 2.43 1.42 o -5 7 1 192.36 215.73 13.66 o -4 7 1 6.76 5.26 1.21 o -3 7 1 215.45 243.42 3.04 o -2 7 1 155.39 162.08 2.63 o -1 7 1 5.26 6.07 1.01 o 0 7 1 3.52 6.44 0.78 o 1 7 1 5.92 6.65 0.72 o 2 7 1 17.16 14.16 1.01 o 3 7 1 759.05 822.32 4.65 o 4 7 1 43.16 54.03 1.42 o 5 7 1 8.09 4.45 1.62 o 6 7 1 106.78 120.80 2.02 o -14 0 2 0.51 -0.40 2.23 o -12 0 2 29.01 31.36 2.00 o -10 0 2 41.06 40.51 1.93 o -8 0 2 153.31 171.99 5.67 o -6 0 2 1296.92 1324.28 30.45 o -4 0 2 5220.36 5706.75 21.14 o -2 0 2 2473.77 2452.10 53.11 o 0 0 2 7177.77 7130.52 51.80 o 2 0 2 70.89 77.50 1.57 o 4 0 2 1917.35 2045.27 14.97 o 6 0 2 7249.58 7705.78 37.23 o 8 0 2 101.06 141.23 7.28 o 10 0 2 1096.63 1080.03 8.70 o 12 0 2 14.86 13.39 1.64 o -14 1 2 216.61 243.11 11.84 o -13 1 2 277.07 271.09 5.36 o -12 1 2 15.20 12.69 1.42 o -11 1 2 485.20 444.05 3.93 o -10 1 2 171.56 153.50 1.54 o -9 1 2 15.93 18.37 0.80 o -8 1 2 21.50 20.03 2.83 o -7 1 2 1298.78 1407.76 27.31 o -6 1 2 1379.73 1376.36 10.07 o -5 1 2 1.46 1.25 1.13 o -4 1 2 175.43 190.82 1.84 o -3 1 2 2248.15 2362.01 16.49 o -2 1 2 1255.54 1250.67 13.87 o -1 1 2 190.21 221.51 3.34 o 0 1 2 527.66 612.31 24.69 o 1 1 2 382.60 414.20 2.15 o 2 1 2 9968.96 10093.66 65.15 o 3 1 2 10425.56 10249.40 52.10 o 4 1 2 1069.63 1137.90 8.71 o 5 1 2 5527.23 6131.11 54.33 o 6 1 2 767.61 886.12 15.38 o 7 1 2 103.14 97.18 3.90 o 8 1 2 133.88 149.06 2.97 o 9 1 2 405.95 376.15 3.72 o 10 1 2 266.52 211.16 1.87 o 11 1 2 104.03 112.76 1.82 o 12 1 2 220.97 199.67 2.73 o 13 1 2 24.20 19.48 1.72 o -14 2 2 10.93 13.56 1.62 o -13 2 2 214.15 204.97 3.84 o -12 2 2 0.25 0.92 1.26 o -11 2 2 54.94 45.92 1.39 o -10 2 2 12.71 14.43 0.95 o -9 2 2 550.04 514.70 8.50 o -8 2 2 15.21 10.57 1.11 o -7 2 2 63.87 56.86 3.84 o -6 2 2 327.42 413.39 4.39 o -5 2 2 2323.89 2614.82 19.42 o -4 2 2 79.00 93.73 1.53 o -3 2 2 220.42 253.18 4.20 o -2 2 2 2517.26 2562.27 15.18 o -1 2 2 4466.72 4256.66 22.76 o 0 2 2 288.14 313.88 2.26 o 1 2 2 94.70 92.79 1.74 o 2 2 2 628.25 663.65 8.70 o 3 2 2 23.54 15.47 1.70 o 4 2 2 7.28 14.80 1.39 o 5 2 2 2490.52 2652.10 12.49 o 6 2 2 77.79 78.87 2.85 o 7 2 2 378.07 394.99 7.06 o 8 2 2 18.52 15.97 0.79 o 9 2 2 179.94 175.03 1.69 o 10 2 2 183.69 189.88 2.32 o 11 2 2 119.48 97.87 1.53 o 12 2 2 1.74 2.08 1.21 o 13 2 2 534.74 545.66 8.40 o -13 3 2 527.11 561.30 5.06 o -12 3 2 496.57 464.99 4.25 o -11 3 2 7.19 7.94 1.21 o -10 3 2 13.85 14.71 1.26 o -9 3 2 18.74 20.22 1.15 o -8 3 2 691.49 683.90 5.14 o -7 3 2 1.69 1.87 0.87 o -6 3 2 806.93 838.75 7.34 o -5 3 2 2.40 3.26 1.55 o -4 3 2 202.59 194.18 3.63 o -3 3 2 10.47 10.18 2.93 o -2 3 2 493.76 605.28 6.06 o -1 3 2 434.42 466.98 4.42 o 0 3 2 832.13 792.94 8.74 o 1 3 2 633.34 717.96 14.37 o 2 3 2 380.31 415.58 4.66 o 3 3 2 159.36 168.63 3.32 o 4 3 2 22.02 16.05 1.57 o 5 3 2 327.21 372.05 6.36 o 6 3 2 24.33 25.75 4.65 o 7 3 2 972.08 980.88 7.08 o 8 3 2 1866.28 2009.17 9.73 o 9 3 2 84.07 88.28 1.48 o 10 3 2 99.06 91.19 1.70 o 11 3 2 150.50 147.99 2.07 o 12 3 2 21.76 14.44 1.14 o -12 4 2 85.04 94.27 1.50 o -11 4 2 7.06 8.05 1.12 o -10 4 2 65.94 62.27 1.60 o -9 4 2 1069.42 1020.92 6.03 o -8 4 2 2198.59 1929.68 66.47 o -7 4 2 105.61 97.33 2.63 o -6 4 2 274.17 278.83 3.84 o -5 4 2 1097.66 1005.23 7.08 o -4 4 2 68.12 53.62 2.02 o -3 4 2 843.94 903.77 30.55 o -2 4 2 1229.21 1239.05 32.68 o -1 4 2 208.44 190.91 6.17 o 0 4 2 84.39 84.73 2.26 o 1 4 2 4.24 3.27 1.69 o 2 4 2 91.06 83.96 4.91 o 3 4 2 93.81 87.59 4.59 o 4 4 2 97.62 89.76 2.33 o 5 4 2 679.86 676.10 17.60 o 6 4 2 1497.58 1419.74 29.95 o 7 4 2 2929.15 2692.69 51.58 o 8 4 2 223.42 211.64 3.52 o 9 4 2 161.59 161.55 2.13 o 10 4 2 105.69 114.73 1.70 o 11 4 2 4.54 2.43 0.86 o -11 5 2 239.46 239.11 6.17 o -10 5 2 85.02 83.56 2.63 o -9 5 2 186.22 207.89 2.28 o -8 5 2 73.37 76.56 1.98 o -7 5 2 363.53 343.43 9.31 o -6 5 2 17.27 13.76 1.62 o -5 5 2 28.36 26.10 1.82 o -4 5 2 81.78 77.90 2.43 o -3 5 2 2364.08 2096.06 11.13 o -2 5 2 306.07 257.18 4.25 o -1 5 2 33.43 37.31 4.25 o 0 5 2 2.22 1.64 1.12 o 1 5 2 2766.18 2516.96 43.50 o 2 5 2 260.76 233.18 2.67 o 3 5 2 49.39 41.15 1.46 o 4 5 2 1.44 0.82 0.98 o 5 5 2 846.64 796.21 5.67 o 6 5 2 101.56 90.46 10.52 o 7 5 2 2.80 1.25 1.19 o 8 5 2 128.57 124.04 3.04 o 9 5 2 189.32 183.60 6.98 o 10 5 2 39.06 40.21 2.43 o -9 6 2 34.09 39.83 0.92 o -8 6 2 170.01 167.22 2.23 o -7 6 2 30.18 26.97 1.38 o -6 6 2 91.25 81.34 2.43 o -5 6 2 12.22 8.70 1.42 o -4 6 2 1091.76 981.56 7.08 o -3 6 2 75.11 66.77 2.43 o -2 6 2 35.99 30.55 2.02 o -1 6 2 245.59 219.74 3.84 o 0 6 2 130.54 121.17 4.96 o 1 6 2 198.90 192.97 5.97 o 2 6 2 317.52 278.19 3.44 o 3 6 2 72.05 50.36 3.34 o 4 6 2 63.34 73.29 5.97 o 5 6 2 1.88 2.43 1.21 o 6 6 2 200.63 172.00 14.57 o 7 6 2 80.97 81.75 2.43 o 8 6 2 96.11 119.08 3.14 o -6 7 2 115.46 134.11 2.59 o -5 7 2 47.62 59.67 2.83 o -4 7 2 1.18 1.42 1.01 o -3 7 2 413.83 422.49 3.84 o -2 7 2 0.74 0.81 1.21 o -1 7 2 3.53 4.86 1.21 o 0 7 2 210.22 223.39 3.04 o 1 7 2 36.28 37.20 1.21 o 2 7 2 6.70 4.90 0.78 o 3 7 2 784.99 864.81 4.45 o 4 7 2 571.55 698.89 3.84 o 5 7 2 22.03 20.84 1.62 o -13 0 3 436.57 422.49 6.07 o -11 0 3 428.97 386.66 4.36 o -9 0 3 1688.16 1634.08 7.20 o -7 0 3 623.38 654.58 9.51 o -5 0 3 1823.32 1805.90 39.25 o -3 0 3 7682.42 7099.56 19.02 o -1 0 3 3673.79 3805.12 354.40 o 1 0 3 4.38 5.02 0.70 o 3 0 3 33.47 48.76 2.23 o 5 0 3 216.65 172.40 5.67 o 7 0 3 763.74 740.37 13.35 o 9 0 3 621.98 726.00 6.47 o 11 0 3 607.77 499.88 17.81 o 13 0 3 2.61 5.56 1.35 o -14 1 3 48.42 81.39 21.75 o -13 1 3 183.12 182.11 3.05 o -12 1 3 462.47 420.14 4.41 o -11 1 3 701.23 603.44 7.76 o -10 1 3 150.05 149.73 2.55 o -9 1 3 406.36 387.31 3.09 o -8 1 3 173.88 160.14 4.12 o -7 1 3 172.50 203.99 3.33 o -6 1 3 458.78 386.35 28.53 o -5 1 3 51.84 53.40 1.47 o -4 1 3 1367.78 1407.25 24.47 o -3 1 3 1313.89 1362.54 24.01 o -2 1 3 4.53 7.02 0.59 o -1 1 3 2733.13 2580.52 8.38 o 0 1 3 86.75 95.03 3.42 o 1 1 3 6482.58 6289.83 30.75 o 2 1 3 12669.08 13134.02 300.98 o 3 1 3 6.19 9.51 1.26 o 4 1 3 0.66 1.87 1.10 o 5 1 3 349.82 466.55 4.51 o 6 1 3 264.83 228.80 3.61 o 7 1 3 338.28 337.32 8.50 o 8 1 3 1057.22 1113.88 9.35 o 9 1 3 719.37 660.26 4.94 o 10 1 3 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