#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/45/2224508.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2224508_Fobs loop_ _publ_author_name 'He, Long' 'Qin, Hong-Mei' 'Chen, Lian-Mei' _publ_section_title ; 3-(3-Bromophenyl)-N-phenyloxirane-2-carboxamide ; _journal_coeditor_code XU2663 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3000 _journal_volume 65 _journal_year 2009 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _cell_angle_alpha 90.000 _cell_angle_beta 94.405 _cell_angle_gamma 90.000 _cell_length_a 5.5124 _cell_length_b 11.1975 _cell_length_c 21.3298 _exptl_crystal_F_000 640.00 _reflns_d_resolution_high 0.8501 _[local]_cod_data_source_file xu2663Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 090916-4 in P2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 171.50 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 -13 0 4.87 3.96 1.86 o 0 -12 0 465.03 415.40 16.41 o 1 -12 0 110.58 113.10 3.87 o 2 -12 0 47.37 48.94 2.79 o 1 -11 0 180.94 182.56 17.41 o 2 -11 0 7.40 7.06 1.96 o 3 -11 0 139.98 156.46 4.24 o 0 -10 0 331.52 350.16 12.43 o 1 -10 0 313.17 344.65 12.39 o 2 -10 0 113.59 122.06 3.89 o 3 -10 0 408.70 451.46 7.00 o 4 -10 0 8.67 10.31 2.07 o 1 -9 0 13.33 11.64 1.63 o 2 -9 0 0.17 -1.47 2.28 o 3 -9 0 191.08 182.21 4.19 o 4 -9 0 173.22 176.31 4.49 o 0 -8 0 1605.88 1650.39 19.10 o 1 -8 0 232.47 254.81 20.30 o 2 -8 0 94.69 100.34 3.62 o 3 -8 0 169.88 169.76 3.74 o 4 -8 0 19.85 23.42 2.44 o 5 -8 0 68.90 68.06 3.65 o 1 -7 0 376.28 383.24 13.68 o 2 -7 0 515.87 416.84 10.74 o 3 -7 0 357.76 367.73 10.11 o 4 -7 0 58.70 61.81 2.30 o 5 -7 0 24.28 26.62 3.09 o 0 -6 0 905.46 853.46 23.16 o 1 -6 0 3100.88 3021.45 76.68 o 2 -6 0 254.56 238.74 14.37 o 3 -6 0 835.63 845.98 30.96 o 4 -6 0 107.51 113.50 3.01 o 5 -6 0 6.69 16.35 2.21 o 1 -5 0 280.80 311.67 9.14 o 2 -5 0 843.19 830.05 21.76 o 3 -5 0 243.74 223.67 9.05 o 4 -5 0 282.28 262.51 4.27 o 5 -5 0 18.81 21.80 2.22 o 0 -4 0 14042.96 12315.64 707.10 o 1 -4 0 528.18 477.35 14.52 o 2 -4 0 314.63 310.45 17.73 o 3 -4 0 243.51 229.49 6.85 o 4 -4 0 161.09 170.51 9.73 o 5 -4 0 345.53 372.42 11.73 o 6 -4 0 9.54 5.69 1.39 o 1 -3 0 62.82 60.50 2.87 o 2 -3 0 1119.77 1086.74 27.31 o 3 -3 0 2103.37 2287.90 22.61 o 4 -3 0 400.16 401.71 12.08 o 5 -3 0 154.40 162.94 4.07 o 6 -3 0 49.97 47.70 2.46 o 0 -2 0 193.53 160.90 2.66 o 1 -2 0 3833.58 3836.18 173.74 o 2 -2 0 415.50 373.49 5.07 o 3 -2 0 3156.37 3216.30 39.16 o 4 -2 0 447.76 405.92 12.34 o 5 -2 0 128.24 140.49 5.60 o 6 -2 0 257.28 287.00 7.58 o 1 -1 0 4033.10 3567.04 59.06 o 2 -1 0 1769.88 1664.78 29.03 o 3 -1 0 1331.61 1283.24 15.81 o 4 -1 0 843.81 824.60 21.39 o 5 -1 0 258.14 273.36 9.03 o 6 -1 0 122.34 123.36 5.05 o 1 0 0 66.14 64.10 2.42 o 2 0 0 4360.37 4290.57 20.03 o 3 0 0 219.90 186.84 2.94 o 4 0 0 19.58 46.56 3.47 o 5 0 0 883.85 964.80 15.38 o 6 0 0 8.46 6.12 3.15 o 1 1 0 4269.14 3943.92 110.24 o 2 1 0 1901.80 1736.40 12.78 o 3 1 0 1438.73 1420.04 20.69 o 4 1 0 838.73 829.81 13.15 o 5 1 0 219.08 227.89 6.62 o 6 1 0 124.16 114.01 5.97 o 0 2 0 204.44 181.44 3.22 o 1 2 0 4129.56 4242.65 115.77 o 2 2 0 409.05 365.71 2.94 o 3 2 0 3209.28 3304.55 23.47 o 4 2 0 434.87 394.25 6.80 o 5 2 0 135.49 141.90 4.34 o 6 2 0 246.57 282.91 10.02 o 1 3 0 66.76 59.85 2.49 o 2 3 0 1014.27 906.84 5.39 o 3 3 0 2075.65 2150.32 24.48 o 4 3 0 432.37 422.87 10.99 o 5 3 0 172.68 177.43 6.38 o 6 3 0 47.00 44.47 2.81 o 0 4 0 14124.29 12611.60 72.30 o 1 4 0 539.60 460.27 21.81 o 2 4 0 324.94 310.74 11.02 o 3 4 0 239.66 211.03 3.60 o 4 4 0 153.37 136.70 8.16 o 5 4 0 329.40 338.79 8.66 o 6 4 0 13.31 7.56 1.92 o 1 5 0 327.96 357.66 15.80 o 2 5 0 808.74 842.46 12.55 o 3 5 0 255.13 246.77 3.61 o 4 5 0 248.77 226.33 4.76 o 5 5 0 22.93 22.23 3.10 o 0 6 0 895.00 842.90 30.00 o 1 6 0 3117.79 2999.42 118.80 o 2 6 0 247.27 236.60 4.78 o 3 6 0 820.44 864.80 18.09 o 4 6 0 123.10 122.91 3.71 o 5 6 0 9.85 13.15 2.71 o 1 7 0 367.87 323.54 10.49 o 2 7 0 477.42 432.44 10.76 o 3 7 0 370.76 384.22 10.66 o 4 7 0 60.15 59.58 3.30 o 5 7 0 29.23 25.81 4.28 o 1 8 0 254.15 244.75 13.10 o 2 8 0 106.83 114.13 6.86 o 3 8 0 170.59 167.87 4.53 o 5 8 0 69.69 66.29 5.50 o 1 9 0 10.88 10.06 5.10 o 2 9 0 2.34 2.11 2.20 o 3 9 0 186.69 180.91 5.06 o 1 10 0 357.61 289.82 16.01 o 2 10 0 108.54 109.32 6.53 o -1 -13 1 7.19 7.27 1.50 o 0 -13 1 75.14 71.36 4.44 o -2 -12 1 34.38 39.54 2.96 o -1 -12 1 36.59 33.06 2.47 o 0 -12 1 4.32 2.73 3.85 o 1 -12 1 18.89 18.27 2.25 o 2 -12 1 23.01 26.27 2.38 o -3 -11 1 60.52 64.90 3.14 o -2 -11 1 145.06 145.34 4.41 o -1 -11 1 331.02 335.28 21.45 o 0 -11 1 47.90 47.30 3.85 o 1 -11 1 328.60 368.80 8.92 o 2 -11 1 24.70 21.45 2.32 o 3 -11 1 18.07 25.02 2.21 o -4 -10 1 54.22 48.68 3.31 o -3 -10 1 40.10 47.30 2.93 o -2 -10 1 168.77 180.40 6.03 o -1 -10 1 38.70 41.47 2.65 o 0 -10 1 227.83 226.05 4.83 o 1 -10 1 21.92 22.47 2.34 o 2 -10 1 299.28 318.55 8.39 o 3 -10 1 113.43 123.43 4.01 o 4 -10 1 0.51 0.38 1.83 o -4 -9 1 32.70 31.34 2.47 o -3 -9 1 19.70 20.39 2.29 o -2 -9 1 276.18 279.65 7.86 o -1 -9 1 324.31 336.98 5.54 o 0 -9 1 1008.40 1029.79 62.65 o 1 -9 1 59.21 59.56 2.31 o 2 -9 1 400.46 418.32 7.68 o 3 -9 1 120.83 110.24 4.58 o 4 -9 1 57.56 55.37 2.97 o -5 -8 1 16.62 15.72 2.44 o -4 -8 1 83.25 96.51 4.15 o -3 -8 1 390.19 419.65 8.93 o -2 -8 1 149.16 162.54 5.01 o -1 -8 1 701.65 742.48 31.90 o 0 -8 1 30.65 28.34 2.21 o 1 -8 1 95.56 92.28 13.53 o 2 -8 1 172.99 173.47 4.33 o 3 -8 1 284.83 283.41 11.18 o 4 -8 1 81.05 90.55 3.40 o 5 -8 1 5.18 6.14 1.69 o -5 -7 1 7.53 8.12 2.02 o -4 -7 1 312.12 315.98 6.78 o -3 -7 1 348.29 339.14 7.24 o -2 -7 1 695.22 702.18 12.94 o -1 -7 1 949.26 944.65 9.24 o 0 -7 1 19.14 24.39 2.65 o 1 -7 1 1722.82 1752.68 29.17 o 2 -7 1 149.42 130.37 5.43 o 3 -7 1 1134.04 1119.62 23.14 o 4 -7 1 154.45 149.22 6.95 o 5 -7 1 22.61 19.91 2.60 o -5 -6 1 53.75 59.49 3.14 o -4 -6 1 42.15 53.74 2.44 o -3 -6 1 567.08 594.78 11.86 o -2 -6 1 2705.91 2765.58 51.55 o -1 -6 1 88.07 82.81 2.57 o 0 -6 1 600.50 694.64 26.97 o 1 -6 1 164.66 169.82 2.96 o 2 -6 1 26.77 28.68 5.20 o 3 -6 1 616.14 534.11 11.77 o 4 -6 1 417.52 430.76 11.58 o 5 -6 1 92.37 95.72 3.59 o -5 -5 1 278.17 268.83 6.17 o -4 -5 1 82.91 85.99 2.69 o -3 -5 1 1334.78 1425.33 20.07 o -2 -5 1 2093.55 2102.62 42.20 o -1 -5 1 2722.45 2845.92 18.41 o 0 -5 1 6132.93 5969.00 96.18 o 1 -5 1 51.06 49.03 1.58 o 2 -5 1 2182.76 1998.03 73.33 o 3 -5 1 453.94 425.73 14.25 o 4 -5 1 88.20 92.99 3.10 o 5 -5 1 87.14 84.05 3.29 o -6 -4 1 14.32 13.49 1.47 o -5 -4 1 63.48 77.75 3.79 o -4 -4 1 265.58 276.36 6.76 o -3 -4 1 1186.33 1340.81 38.02 o -2 -4 1 632.94 640.51 12.83 o -1 -4 1 1004.00 975.59 15.35 o 0 -4 1 7.14 6.39 0.69 o 1 -4 1 342.64 358.99 17.98 o 2 -4 1 742.30 739.14 20.60 o 3 -4 1 1053.72 1157.82 20.44 o 4 -4 1 451.26 471.79 13.45 o 5 -4 1 53.11 57.55 3.11 o 6 -4 1 50.88 46.16 2.10 o -6 -3 1 179.93 168.94 5.05 o -5 -3 1 200.90 215.98 6.50 o -4 -3 1 244.34 270.22 10.10 o -3 -3 1 366.94 378.96 19.67 o -2 -3 1 1904.06 1917.38 38.76 o -1 -3 1 6553.90 6189.83 168.83 o 0 -3 1 2056.33 1791.00 22.23 o 1 -3 1 6238.37 5684.51 229.20 o 2 -3 1 1322.93 1371.89 10.25 o 3 -3 1 1008.92 1099.48 46.86 o 4 -3 1 708.79 733.52 21.78 o 5 -3 1 35.31 39.35 2.39 o 6 -3 1 15.64 21.53 1.78 o -6 -2 1 59.07 72.09 6.71 o -5 -2 1 38.55 36.38 2.87 o -4 -2 1 667.62 773.13 13.29 o -3 -2 1 731.31 713.25 20.95 o -2 -2 1 2111.37 2054.03 27.15 o -1 -2 1 521.23 538.73 13.55 o 0 -2 1 327.03 357.77 20.94 o 1 -2 1 622.80 615.48 16.19 o 2 -2 1 708.69 796.67 16.52 o 3 -2 1 1422.48 1413.03 31.97 o 4 -2 1 698.89 691.47 15.77 o 5 -2 1 351.76 362.57 13.77 o 6 -2 1 9.89 19.73 3.12 o -6 -1 1 40.74 44.21 3.59 o -5 -1 1 376.04 379.68 11.82 o -4 -1 1 140.79 142.73 5.23 o -3 -1 1 504.60 482.24 14.30 o -2 -1 1 2724.35 2645.50 34.86 o -1 -1 1 3218.29 2954.14 13.92 o 0 -1 1 3575.90 2895.47 12.57 o 1 -1 1 3484.09 3382.84 179.00 o 2 -1 1 6138.36 6109.39 93.72 o 3 -1 1 720.37 728.97 13.32 o 4 -1 1 734.34 714.95 16.89 o 5 -1 1 123.06 123.30 5.23 o 6 -1 1 43.19 53.50 3.90 o -6 0 1 0.05 0.26 3.10 o -5 0 1 133.75 186.77 12.38 o -4 0 1 236.61 229.25 6.61 o -3 0 1 616.38 546.16 7.00 o -2 0 1 1379.88 1368.80 23.66 o -1 0 1 6705.37 6238.26 59.04 o 0 0 1 1.31 1.66 0.60 o 1 0 1 6253.71 6586.01 45.37 o 2 0 1 2196.00 2170.31 14.20 o 3 0 1 109.47 129.22 2.74 o 4 0 1 986.45 961.20 12.51 o 5 0 1 2.40 35.44 4.85 o 6 0 1 92.57 91.82 5.62 o -6 1 1 37.97 36.69 4.32 o -5 1 1 381.97 404.68 7.42 o -4 1 1 172.43 165.34 4.58 o -3 1 1 476.80 448.03 8.91 o -2 1 1 2556.96 2428.26 20.98 o -1 1 1 2937.53 2743.66 16.09 o 1 1 1 4149.12 3855.89 139.86 o 2 1 1 6264.20 6023.22 52.59 o 3 1 1 825.86 806.54 8.90 o 4 1 1 715.95 686.13 9.80 o 5 1 1 93.15 93.81 3.65 o 6 1 1 45.27 52.04 4.29 o -6 2 1 60.04 80.66 16.92 o -5 2 1 38.18 39.32 2.68 o -4 2 1 732.22 788.68 23.45 o -3 2 1 742.71 724.98 4.76 o -2 2 1 2137.55 2084.58 16.30 o -1 2 1 516.10 533.81 7.62 o 0 2 1 307.06 339.55 16.63 o 1 2 1 664.72 701.56 11.57 o 2 2 1 791.02 856.11 15.04 o 3 2 1 1468.01 1429.89 10.77 o 4 2 1 672.45 664.19 22.32 o 5 2 1 350.80 356.98 8.03 o 6 2 1 11.88 15.75 2.66 o -6 3 1 170.45 175.85 5.47 o -5 3 1 197.87 196.43 4.65 o -4 3 1 227.93 246.60 4.86 o -3 3 1 413.22 399.35 4.41 o -2 3 1 2016.10 1975.39 17.07 o -1 3 1 6318.84 5849.87 125.29 o 0 3 1 1981.84 1863.39 30.18 o 1 3 1 6549.56 6196.24 197.33 o 2 3 1 1317.87 1251.30 14.48 o 3 3 1 1031.57 1025.63 7.02 o 4 3 1 738.68 696.95 21.58 o 5 3 1 38.97 39.31 2.63 o 6 3 1 14.93 19.13 2.74 o -6 4 1 13.78 13.03 2.25 o -5 4 1 64.77 65.21 5.10 o -4 4 1 279.12 285.14 5.70 o -3 4 1 1211.30 1250.46 16.95 o -2 4 1 634.22 628.45 10.07 o -1 4 1 1122.28 1121.38 26.36 o 0 4 1 5.79 4.86 1.12 o 1 4 1 363.21 364.13 15.86 o 2 4 1 766.87 718.22 5.77 o 3 4 1 1096.82 1114.68 16.42 o 4 4 1 461.04 453.17 5.18 o 5 4 1 42.22 34.38 3.37 o 6 4 1 41.38 35.03 2.39 o -5 5 1 250.15 244.02 7.52 o -4 5 1 99.68 102.01 3.92 o -3 5 1 1308.05 1310.21 13.35 o -2 5 1 2100.73 2135.01 36.01 o -1 5 1 2652.71 2609.56 82.88 o 0 5 1 6040.19 5614.80 191.63 o 1 5 1 95.92 100.42 3.34 o 2 5 1 2129.87 2065.89 19.18 o 3 5 1 441.18 442.35 4.87 o 4 5 1 73.45 75.43 2.69 o 5 5 1 92.49 90.19 4.66 o -5 6 1 55.25 50.29 3.92 o -4 6 1 44.30 63.88 6.89 o -3 6 1 573.57 601.67 7.54 o -2 6 1 2729.72 2740.24 47.74 o -1 6 1 82.19 73.84 2.84 o 0 6 1 592.15 670.75 29.54 o 1 6 1 170.08 171.89 8.88 o 2 6 1 31.70 29.36 2.46 o 3 6 1 629.78 634.09 13.06 o 4 6 1 417.15 409.13 6.24 o 5 6 1 94.89 96.24 6.58 o -5 7 1 7.46 8.40 2.25 o -4 7 1 313.49 290.05 5.33 o -3 7 1 323.17 304.99 5.54 o -2 7 1 732.18 749.31 20.27 o -1 7 1 984.02 878.84 40.66 o 1 7 1 1706.02 1675.96 62.16 o 2 7 1 141.56 135.05 3.63 o 3 7 1 1134.09 1104.50 9.00 o 4 7 1 146.97 143.00 4.82 o 5 7 1 25.13 19.84 3.83 o -5 8 1 17.36 14.34 3.11 o -3 8 1 374.88 375.32 12.38 o -2 8 1 150.41 157.87 5.43 o -1 8 1 693.92 672.52 20.66 o 0 8 1 34.26 37.01 7.88 o 1 8 1 87.83 81.01 4.71 o 2 8 1 177.63 180.06 7.75 o 3 8 1 317.45 312.81 12.27 o 5 8 1 7.46 7.97 3.54 o -3 9 1 23.85 23.10 2.47 o -2 9 1 270.18 270.95 8.35 o -1 9 1 316.68 303.72 16.71 o 0 9 1 1023.76 988.48 145.61 o 1 9 1 55.27 51.94 8.85 o 2 9 1 427.18 427.09 23.97 o 3 9 1 110.20 93.86 3.85 o 0 10 1 240.22 197.44 14.07 o 2 10 1 285.92 287.17 13.17 o 0 -13 2 40.77 30.64 2.88 o -2 -12 2 82.28 92.75 4.08 o -1 -12 2 91.56 91.88 5.09 o 0 -12 2 101.14 101.82 9.54 o 1 -12 2 34.50 37.24 2.34 o 2 -12 2 170.86 186.40 8.73 o -3 -11 2 25.90 25.87 2.32 o -2 -11 2 106.38 107.01 3.89 o -1 -11 2 13.84 17.55 3.52 o 0 -11 2 103.29 97.77 5.59 o 1 -11 2 94.96 94.96 8.66 o 2 -11 2 5.67 5.24 1.81 o 3 -11 2 33.54 35.58 2.48 o -4 -10 2 39.91 40.43 2.77 o -3 -10 2 57.93 58.98 3.23 o -2 -10 2 111.41 120.60 4.27 o -1 -10 2 89.58 87.90 3.60 o 0 -10 2 238.56 252.23 5.29 o 1 -10 2 250.77 257.37 7.65 o 2 -10 2 166.13 180.17 4.45 o 3 -10 2 15.35 9.60 2.11 o 4 -10 2 10.63 12.53 2.11 o -4 -9 2 20.13 20.39 2.17 o -3 -9 2 115.35 117.90 5.03 o -2 -9 2 123.37 119.10 4.80 o -1 -9 2 333.94 345.68 10.19 o 0 -9 2 95.73 96.43 3.04 o 1 -9 2 93.14 94.11 3.61 o 2 -9 2 859.59 888.85 11.89 o 3 -9 2 7.93 7.95 1.72 o 4 -9 2 121.40 128.29 4.63 o -5 -8 2 54.98 56.42 3.14 o -4 -8 2 5.96 10.61 1.73 o -3 -8 2 218.76 223.30 4.51 o -2 -8 2 274.02 309.14 11.48 o -1 -8 2 467.92 504.09 17.47 o 0 -8 2 909.42 1019.66 23.52 o 1 -8 2 384.70 367.33 31.82 o 2 -8 2 1019.74 1053.90 18.50 o 3 -8 2 99.04 103.85 3.30 o 4 -8 2 339.76 355.62 9.55 o 5 -8 2 12.49 12.25 1.82 o -5 -7 2 6.50 3.99 2.06 o -4 -7 2 266.39 289.49 7.38 o -3 -7 2 126.72 145.88 2.84 o -2 -7 2 342.23 352.68 9.26 o -1 -7 2 123.72 155.76 4.08 o 0 -7 2 36.53 39.74 2.18 o 1 -7 2 352.15 381.05 9.15 o 2 -7 2 105.69 101.88 4.25 o 3 -7 2 525.49 515.83 8.72 o 4 -7 2 7.45 8.41 1.62 o 5 -7 2 120.94 107.97 6.93 o -5 -6 2 84.92 94.61 3.23 o -4 -6 2 222.37 232.90 3.93 o -3 -6 2 624.94 610.11 14.47 o -2 -6 2 507.40 557.36 10.24 o -1 -6 2 1526.37 1623.88 27.71 o 0 -6 2 217.12 202.87 7.50 o 1 -6 2 4232.39 4537.65 77.89 o 2 -6 2 383.20 354.33 11.14 o 3 -6 2 339.47 297.14 6.88 o 4 -6 2 21.02 24.09 1.62 o 5 -6 2 9.16 13.30 2.17 o -5 -5 2 60.83 64.27 3.04 o -4 -5 2 123.35 128.94 3.76 o -3 -5 2 1333.48 1408.23 19.02 o -2 -5 2 679.08 715.72 8.93 o -1 -5 2 2783.92 2753.08 44.99 o 0 -5 2 1285.62 1399.58 21.21 o 1 -5 2 47.18 54.50 2.32 o 2 -5 2 876.62 968.08 20.64 o 3 -5 2 85.05 83.45 5.44 o 4 -5 2 275.52 282.33 10.43 o 5 -5 2 137.58 130.76 3.81 o -6 -4 2 73.71 76.69 2.37 o -5 -4 2 325.29 350.71 8.97 o -4 -4 2 154.86 187.89 8.27 o -3 -4 2 862.62 904.37 21.03 o -2 -4 2 869.78 961.62 24.85 o -1 -4 2 565.31 555.00 7.65 o 0 -4 2 7765.66 8504.64 87.70 o 1 -4 2 372.95 357.94 6.15 o 2 -4 2 8393.08 9114.33 236.19 o 3 -4 2 4.59 4.51 1.91 o 4 -4 2 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