#------------------------------------------------------------------------------
#$Date: 2010-01-22 14:33:52 +0200 (Fri, 22 Jan 2010) $
#$Revision: 960 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/2224510.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2224510_Fobs
loop_
_publ_author_name
'Ou, Guang-Chuan'
'Zhou, Qiang'
'Ng, Seik Weng'
_publ_section_title
;
[4-Carboxyimidazole-5-carboxylato(2--)-\k^2^N^1^,O^5^](5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane-\k^4^N,N',N'',N''')nickel(II)
monohydrate
;
_journal_coeditor_code XU2666
_journal_issue 12
_journal_name_full 'Acta Crystallographica Section E'
_journal_page_first m1556
_journal_volume 65
_journal_year 2009
_space_group_IT_number 14
_symmetry_space_group_name_Hall '-P 2ybc'
_symmetry_space_group_name_H-M 'P 1 21/c 1'
_cell_angle_alpha 90.000
_cell_angle_beta 103.675
_cell_angle_gamma 90.000
_cell_length_a 10.4070
_cell_length_b 12.7806
_cell_length_c 19.0947
_exptl_crystal_F_000 1104.00
_reflns_d_resolution_high 0.8409
_[local]_cod_data_source_file xu2666Isup2.hkl
_[local]_cod_data_source_block I
#BEGIN Tags that were not found in dictionaries:
_shelx_title ' P21/c'
_shelx_refln_list_code 4
_shelx_f_calc_maximum 286.19
_shelx_f_squared_multiplier 1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
1 0 0 2871.72 3724.20 68.89 o
2 0 0 66799.44 79321.53 1194.93 o
3 0 0 6422.20 8148.42 152.27 o
4 0 0 1366.53 1341.06 53.20 o
5 0 0 11208.79 10995.02 150.49 o
6 0 0 12505.73 13728.16 186.94 o
7 0 0 1075.72 973.38 92.16 o
8 0 0 5886.16 6119.19 113.41 o
9 0 0 65.39 90.71 59.17 o
10 0 0 232.74 217.91 75.45 o
11 0 0 986.66 1060.23 120.12 o
12 0 0 276.74 306.15 99.83 o
1 1 0 2521.16 1924.22 38.58 o
2 1 0 1479.96 1741.16 38.24 o
3 1 0 404.07 400.27 16.06 o
4 1 0 1366.81 1568.21 31.88 o
5 1 0 290.48 340.00 28.30 o
6 1 0 250.36 309.50 37.55 o
7 1 0 2619.87 2520.07 54.04 o
8 1 0 149.39 105.92 22.24 o
9 1 0 1189.72 1193.33 111.43 o
10 1 0 163.43 145.18 49.42 o
11 1 0 86.74 43.96 62.03 o
0 2 0 33031.19 39453.74 724.37 o
1 2 0 776.50 765.54 14.99 o
2 2 0 2801.06 3257.43 40.79 o
3 2 0 27.40 13.48 12.52 o
4 2 0 93.53 57.12 13.13 o
5 2 0 2417.30 2155.08 41.42 o
6 2 0 69.65 78.96 18.40 o
7 2 0 4039.66 3907.78 67.53 o
8 2 0 822.03 893.74 51.75 o
9 2 0 74.41 26.19 30.85 o
10 2 0 219.58 240.19 54.01 o
11 2 0 1069.74 1018.98 70.01 o
1 3 0 5058.44 6401.95 71.65 o
2 3 0 3135.81 3310.45 43.08 o
3 3 0 580.45 605.17 20.11 o
4 3 0 1876.23 2349.28 50.28 o
5 3 0 467.17 245.96 133.00 o
6 3 0 2181.77 2278.34 75.45 o
7 3 0 1951.71 1747.44 59.03 o
8 3 0 66.16 49.89 44.33 o
9 3 0 436.62 397.46 52.69 o
10 3 0 425.66 401.63 60.72 o
11 3 0 286.93 223.89 62.85 o
0 4 0 1449.25 1732.48 36.96 o
1 4 0 390.05 432.25 17.08 o
2 4 0 439.32 478.35 35.54 o
3 4 0 56.44 34.93 12.90 o
4 4 0 455.76 531.78 23.30 o
5 4 0 54.93 37.55 26.68 o
6 4 0 12.04 -14.68 24.99 o
7 4 0 1073.08 1071.53 49.70 o
8 4 0 1013.53 1046.51 80.40 o
9 4 0 124.80 142.38 65.05 o
10 4 0 966.66 940.36 90.63 o
11 4 0 259.03 218.72 61.26 o
1 5 0 3867.23 3399.19 48.99 o
2 5 0 1773.98 1955.60 31.80 o
3 5 0 2206.06 2598.21 55.09 o
4 5 0 5197.47 5336.39 71.83 o
5 5 0 1196.63 1123.84 39.70 o
6 5 0 1574.95 1562.66 82.36 o
7 5 0 938.72 1005.52 66.71 o
8 5 0 142.50 166.70 40.46 o
9 5 0 1313.13 1277.51 64.12 o
10 5 0 771.36 874.54 72.15 o
11 5 0 487.74 537.79 110.06 o
0 6 0 326.05 339.25 73.96 o
1 6 0 12.67 3.44 12.77 o
2 6 0 803.00 725.93 44.73 o
3 6 0 43.17 20.74 15.29 o
4 6 0 333.33 334.30 22.52 o
5 6 0 32.52 39.51 21.23 o
6 6 0 77.04 70.94 37.68 o
7 6 0 5.32 -17.91 31.91 o
8 6 0 280.92 344.25 47.12 o
9 6 0 0.55 -17.90 44.21 o
10 6 0 57.10 42.71 82.61 o
11 6 0 49.85 4.26 96.76 o
1 7 0 1380.90 1139.28 28.67 o
2 7 0 2369.90 2170.81 39.06 o
3 7 0 537.33 554.99 24.61 o
4 7 0 13424.46 13277.24 148.08 o
5 7 0 0.71 21.59 21.26 o
6 7 0 2338.17 2217.24 56.13 o
7 7 0 10.51 -7.79 30.87 o
8 7 0 58.42 -24.46 44.42 o
9 7 0 1251.68 1545.24 189.69 o
10 7 0 1207.61 1206.98 79.09 o
0 8 0 1156.16 1003.77 42.58 o
1 8 0 3208.12 3160.22 49.17 o
2 8 0 11.15 5.68 18.73 o
3 8 0 6499.09 6549.97 79.12 o
4 8 0 11.49 -11.71 21.81 o
5 8 0 2962.98 2748.14 60.98 o
6 8 0 252.09 274.81 36.71 o
7 8 0 187.35 185.60 49.51 o
8 8 0 1166.78 1197.49 69.38 o
9 8 0 94.25 34.33 56.60 o
10 8 0 408.63 371.73 74.30 o
1 9 0 944.87 810.04 30.78 o
2 9 0 7.65 -12.46 21.01 o
3 9 0 228.11 253.45 32.62 o
4 9 0 82.78 168.12 26.89 o
5 9 0 71.52 -7.39 39.84 o
6 9 0 129.37 84.23 45.21 o
7 9 0 2.83 -52.95 45.85 o
8 9 0 19.69 -17.03 54.02 o
9 9 0 173.57 264.68 68.41 o
0 10 0 640.79 639.83 46.33 o
1 10 0 688.26 673.62 32.58 o
2 10 0 9.83 -20.07 24.49 o
3 10 0 183.06 240.00 30.18 o
4 10 0 6.46 2.68 41.57 o
5 10 0 243.05 207.04 50.68 o
6 10 0 330.04 372.81 57.85 o
7 10 0 848.22 923.40 154.27 o
8 10 0 778.92 1012.95 89.18 o
9 10 0 37.68 20.90 67.43 o
1 11 0 381.27 390.43 41.61 o
2 11 0 382.35 354.49 78.07 o
3 11 0 38.03 75.09 37.67 o
4 11 0 203.25 205.66 53.75 o
5 11 0 132.12 111.30 78.95 o
6 11 0 324.70 329.45 64.51 o
7 11 0 29.15 111.19 64.33 o
8 11 0 1.25 -47.76 67.11 o
0 12 0 635.53 716.83 61.28 o
1 12 0 90.91 106.29 42.33 o
2 12 0 301.61 298.22 49.41 o
3 12 0 149.59 154.88 53.58 o
4 12 0 44.16 82.92 57.04 o
5 12 0 211.08 225.49 64.55 o
6 12 0 277.23 229.39 69.15 o
7 12 0 1275.88 1263.14 84.89 o
1 13 0 14.57 28.41 63.29 o
2 13 0 316.68 233.62 51.10 o
3 13 0 168.53 159.78 64.88 o
4 13 0 495.80 708.23 75.28 o
5 13 0 40.68 -27.06 65.83 o
6 13 0 3.97 19.97 70.24 o
0 14 0 1133.79 1448.99 125.32 o
1 14 0 154.61 269.26 77.69 o
2 14 0 130.33 182.53 106.65 o
3 14 0 166.11 370.18 115.26 o
4 14 0 30.36 -29.57 71.06 o
1 15 0 1006.20 1365.45 108.09 o
-12 1 1 1049.66 1344.59 118.93 o
-11 1 1 1332.08 1346.36 76.86 o
-10 1 1 89.65 39.38 47.03 o
-9 1 1 991.32 946.61 61.77 o
-8 1 1 881.74 881.99 39.83 o
-7 1 1 3244.84 3211.90 60.49 o
-6 1 1 4997.61 5051.78 73.34 o
-5 1 1 122.23 276.85 19.72 o
-4 1 1 16.53 14.01 20.58 o
-3 1 1 2514.11 2580.19 36.60 o
-2 1 1 255.37 176.83 13.58 o
-1 1 1 36931.86 38033.16 412.77 o
0 1 1 8823.63 7174.36 234.32 o
1 1 1 11570.76 10906.06 108.87 o
2 1 1 129.87 54.27 8.37 o
3 1 1 11296.71 12648.92 165.82 o
4 1 1 900.29 899.09 25.95 o
5 1 1 284.16 314.74 22.76 o
6 1 1 410.41 419.56 28.94 o
7 1 1 5138.53 4916.72 69.01 o
8 1 1 336.71 358.68 29.11 o
9 1 1 9.89 0.23 40.96 o
10 1 1 6.47 13.80 83.59 o
11 1 1 73.93 -4.12 57.52 o
-12 2 1 22.69 64.65 67.56 o
-11 2 1 2.57 51.75 56.66 o
-10 2 1 2773.18 2727.45 88.94 o
-9 2 1 1.77 -58.68 39.12 o
-8 2 1 4134.38 4105.95 96.01 o
-7 2 1 20.97 26.87 20.04 o
-6 2 1 1106.59 1192.51 33.99 o
-5 2 1 3418.12 3529.88 56.90 o
-4 2 1 1556.37 1462.15 30.37 o
-3 2 1 10.01 20.45 12.95 o
-2 2 1 6658.98 7311.26 123.57 o
-1 2 1 646.18 1104.14 22.81 o
0 2 1 11388.85 13387.23 125.81 o
1 2 1 11738.79 14121.22 115.87 o
2 2 1 8637.82 9553.50 95.17 o
3 2 1 6383.13 6858.39 131.21 o
4 2 1 913.49 1084.51 88.03 o
5 2 1 5714.40 5877.07 134.62 o
6 2 1 2000.67 1989.50 44.94 o
7 2 1 1.10 10.87 21.39 o
8 2 1 554.02 512.43 49.13 o
9 2 1 276.40 248.17 36.93 o
10 2 1 248.37 220.07 55.99 o
11 2 1 116.27 164.38 62.43 o
-11 3 1 674.82 663.89 85.47 o
-10 3 1 0.33 -0.80 47.98 o
-9 3 1 210.83 122.52 45.01 o
-8 3 1 61.48 75.61 36.61 o
-7 3 1 401.34 457.80 42.43 o
-6 3 1 70.45 13.24 23.55 o
-5 3 1 11.31 0.60 28.82 o
-4 3 1 6159.44 6221.29 77.22 o
-3 3 1 985.06 1178.27 26.99 o
-2 3 1 3969.33 4344.35 52.97 o
-1 3 1 1063.11 1368.24 27.05 o
0 3 1 6745.51 7449.42 77.16 o
1 3 1 397.27 357.79 12.56 o
2 3 1 15595.47 16915.28 140.92 o
3 3 1 2646.34 2825.83 40.69 o
4 3 1 6553.61 6584.81 98.74 o
5 3 1 346.37 462.50 30.76 o
6 3 1 486.97 508.98 69.57 o
7 3 1 892.97 861.86 48.55 o
8 3 1 1301.06 1463.89 60.75 o
9 3 1 566.10 621.88 81.08 o
10 3 1 105.71 52.41 52.02 o
11 3 1 793.19 893.61 92.12 o
-11 4 1 393.52 437.45 102.09 o
-10 4 1 3284.39 3039.60 93.74 o
-9 4 1 437.62 380.12 51.48 o
-8 4 1 2618.27 2666.14 77.25 o
-7 4 1 459.05 503.58 47.57 o
-6 4 1 303.46 343.62 34.93 o
-5 4 1 1545.31 1396.61 35.94 o
-4 4 1 2088.31 1719.26 36.22 o
-3 4 1 633.10 499.82 25.61 o
-2 4 1 6214.33 6234.03 87.50 o
-1 4 1 2021.38 2505.92 32.99 o
0 4 1 351.17 346.65 14.05 o
1 4 1 153.38 168.91 11.70 o
2 4 1 953.14 981.43 31.85 o
3 4 1 2136.17 1749.71 29.24 o
4 4 1 2205.27 2440.72 41.68 o
5 4 1 3299.65 3053.49 105.25 o
6 4 1 430.27 391.06 56.52 o
7 4 1 2846.71 2743.42 109.30 o
9 4 1 10.97 -4.43 60.02 o
10 4 1 838.82 895.26 108.27 o
11 4 1 493.81 521.59 104.35 o
-11 5 1 69.83 49.62 57.45 o
-10 5 1 184.82 199.91 53.99 o
-9 5 1 1995.21 1839.55 150.82 o
-8 5 1 144.27 107.99 70.21 o
-7 5 1 402.88 418.32 42.24 o
-6 5 1 0.95 -8.99 26.71 o
-5 5 1 975.35 934.44 34.99 o
-4 5 1 3378.42 3362.72 54.80 o
-3 5 1 35.77 -3.69 13.85 o
-2 5 1 90.04 55.22 24.68 o
-1 5 1 853.12 913.69 67.54 o
0 5 1 1.76 -4.30 10.38 o
1 5 1 1.60 3.07 10.71 o
2 5 1 679.65 692.76 20.13 o
3 5 1 14.87 -5.68 12.22 o
4 5 1 5214.58 4878.96 77.60 o
5 5 1 69.56 57.20 19.00 o
6 5 1 124.82 123.94 29.15 o
7 5 1 375.82 456.09 52.86 o
8 5 1 8.27 19.29 45.14 o
9 5 1 1580.53 1455.05 67.05 o
10 5 1 130.15 73.58 81.67 o
11 5 1 72.34 77.67 89.94 o
-11 6 1 945.44 987.17 124.90 o
-10 6 1 1326.31 1326.01 71.61 o
-9 6 1 103.49 107.80 46.79 o
-8 6 1 515.42 525.43 51.92 o
-7 6 1 1295.28 1181.83 54.26 o
-6 6 1 318.89 410.34 47.73 o
-5 6 1 6178.41 6114.39 85.56 o
-4 6 1 274.45 371.45 30.59 o
-3 6 1 9525.52 9649.57 111.03 o
-2 6 1 5034.16 5016.09 68.95 o
-1 6 1 345.71 432.54 19.79 o
0 6 1 2812.96 2862.18 40.74 o
1 6 1 1255.17 1471.14 35.51 o
2 6 1 6811.11 7145.63 75.62 o
3 6 1 8123.31 7836.66 110.84 o
4 6 1 94.33 109.88 17.75 o
5 6 1 493.23 481.52 26.82 o
6 6 1 1368.35 1250.98 49.08 o
7 6 1 227.31 198.62 32.15 o
8 6 1 3153.37 2973.86 69.21 o
9 6 1 313.86 292.36 58.02 o
10 6 1 732.77 809.88 77.47 o
-10 7 1 0.19 -6.65 83.04 o
-9 7 1 1.82 -104.35 69.57 o
-8 7 1 17.40 23.93 41.10 o
-7 7 1 43.86 -52.69 53.63 o
-6 7 1 127.31 132.94 36.67 o
-5 7 1 555.33 553.51 33.71 o
-4 7 1 1044.09 1060.36 41.99 o
-3 7 1 673.19 670.48 26.80 o
-2 7 1 3087.46 3227.98 55.27 o
-1 7 1 35.17 28.89 15.56 o
0 7 1 27.36 3.91 19.95 o
1 7 1 2.71 -3.38 14.59 o
2 7 1 1372.98 1366.81 38.14 o
3 7 1 7.05 6.50 16.74 o
4 7 1 100.42 156.78 21.65 o
5 7 1 31.05 29.53 26.72 o
6 7 1 2.79 -6.56 27.19 o
7 7 1 491.32 511.30 97.19 o
8 7 1 323.95 293.78 54.79 o
9 7 1 8.12 4.43 76.39 o
10 7 1 1.18 11.10 60.66 o
-10 8 1 205.92 358.77 72.73 o
-9 8 1 14.89 21.75 85.55 o
-8 8 1 30.97 -57.03 48.68 o
-7 8 1 145.04 210.65 37.28 o
-6 8 1 110.96 106.90 48.08 o
-5 8 1 1131.11 1081.48 37.43 o
-4 8 1 671.65 695.49 32.25 o
-3 8 1 6660.42 6385.31 78.81 o
-2 8 1 3337.01 3181.92 50.61 o
-1 8 1 1361.16 1284.72 32.74 o
0 8 1 951.90 891.27 28.70 o
1 8 1 1631.62 1560.34 40.34 o
2 8 1 1875.43 1632.18 36.41 o
3 8 1 5465.90 5244.26 68.91 o
4 8 1 88.84 73.72 22.43 o
5 8 1 519.60 593.55 40.23 o
6 8 1 956.26 932.59 58.09 o
7 8 1 28.47 -2.96 50.90 o
8 8 1 464.99 602.40 64.88 o
9 8 1 46.89 35.42 56.61 o
10 8 1 128.45 17.77 81.12 o
-9 9 1 662.28 723.11 78.26 o
-8 9 1 11.50 15.83 55.38 o
-7 9 1 5.90 18.39 49.47 o
-6 9 1 2228.44 2097.97 98.09 o
-5 9 1 65.83 45.62 27.29 o
-4 9 1 6546.17 5859.01 78.99 o
-3 9 1 23.95 28.15 22.88 o
-2 9 1 1786.39 1733.16 40.29 o
-1 9 1 38.69 20.46 21.72 o
0 9 1 280.97 261.37 25.70 o
1 9 1 199.21 197.45 36.30 o
2 9 1 1373.00 1412.81 37.33 o
3 9 1 193.07 177.52 25.92 o
4 9 1 4012.70 3997.42 96.45 o
5 9 1 149.57 29.77 51.45 o
6 9 1 235.16 143.69 46.83 o
7 9 1 1051.10 976.70 68.31 o
8 9 1 266.42 272.41 59.31 o
9 9 1 723.27 835.71 108.19 o
-9 10 1 10.02 54.78 67.88 o
-8 10 1 65.00 71.79 62.93 o
-7 10 1 15.76 -80.62 53.89 o
-6 10 1 101.94 60.93 80.69 o
-5 10 1 195.96 160.41 50.15 o
-4 10 1 179.98 141.32 30.33 o
-3 10 1 325.89 325.59 38.66 o
-2 10 1 13.56 -3.33 25.65 o
-1 10 1 82.33 43.01 25.50 o
0 10 1 66.06 41.84 25.95 o
1 10 1 15.84 64.99 25.82 o
2 10 1 760.67 751.40 35.39 o
3 10 1 75.00 44.79 32.71 o
4 10 1 117.59 126.93 46.09 o
5 10 1 24.45 26.22 45.55 o
6 10 1 20.68 -10.74 51.69 o
7 10 1 228.37 256.95 61.74 o
8 10 1 172.68 142.82 65.21 o
-8 11 1 23.27 -89.77 66.61 o
-7 11 1 807.33 948.06 193.32 o
-6 11 1 832.90 894.57 156.02 o
-5 11 1 348.51 336.88 58.88 o
-4 11 1 1708.93 1656.23 58.78 o
-3 11 1 3.21 -50.51 33.67 o
-2 11 1 405.01 422.97 35.58 o
-1 11 1 941.96 960.76 46.91 o
0 11 1 333.29 375.38 40.83 o
1 11 1 810.23 884.29 48.70 o
2 11 1 53.94 24.40 38.97 o
3 11 1 413.02 468.69 57.88 o
4 11 1 1280.55 1183.18 66.15 o
5 11 1 622.46 480.12 62.76 o
6 11 1 871.94 996.38 107.76 o
7 11 1 1689.60 1653.26 132.27 o
8 11 1 0.00 88.25 71.33 o
-7 12 1 8.46 -51.84 67.38 o
-6 12 1 24.33 -38.03 62.79 o
-5 12 1 201.35 114.20 80.99 o
-4 12 1 0.02 -79.89 53.26 o
-3 12 1 3.77 -8.73 41.71 o
-2 12 1 407.10 420.19 47.98 o
-1 12 1 11.69 -12.63 33.94 o
0 12 1 127.04 169.81 42.34 o
1 12 1 138.27 167.18 42.99 o
2 12 1 461.08 537.66 75.36 o
3 12 1 0.74 -56.04 50.85 o
4 12 1 0.34 -56.45 54.06 o
5 12 1 5.96 -27.53 60.58 o
6 12 1 2.05 88.60 66.13 o
7 12 1 5.58 -90.68 66.82 o
-6 13 1 478.52 647.76 104.14 o
-5 13 1 2.64 -62.40 65.15 o
-4 13 1 1517.83 1567.15 82.88 o
-3 13 1 865.36 1064.92 80.80 o
-2 13 1 241.51 179.01 67.35 o
-1 13 1 1097.46 1111.72 73.26 o
0 13 1 119.51 40.36 67.78 o
1 13 1 360.41 401.46 54.19 o
2 13 1 576.78 578.52 70.79 o
3 13 1 37.48 -17.97 61.03 o
4 13 1 897.63 857.70 82.64 o
5 13 1 153.63 157.40 87.47 o
6 13 1 322.50 445.66 81.02 o
-4 14 1 12.55 -98.13 111.09 o
-3 14 1 99.56 -99.83 106.65 o
-2 14 1 605.56 509.55 81.07 o
-1 14 1 0.10 -29.37 105.16 o
0 14 1 271.97 271.16 76.10 o
1 14 1 0.69 -97.24 67.48 o
2 14 1 441.87 315.87 113.64 o
3 14 1 447.88 568.49 78.92 o
4 14 1 21.52 34.28 72.25 o
-1 15 1 40.82 -34.83 83.01 o
0 15 1 2.08 58.36 83.55 o
1 15 1 1.42 -21.91 116.97 o
-12 0 2 139.16 21.06 90.11 o
-11 0 2 223.44 179.12 80.57 o
-10 0 2 1188.21 1341.74 95.83 o
-9 0 2 854.88 858.86 79.37 o
-8 0 2 7422.57 8061.97 201.88 o
-7 0 2 9078.90 9700.43 145.13 o
-6 0 2 958.42 1093.59 52.73 o
-5 0 2 1224.86 1496.74 62.58 o
-4 0 2 97.48 32.40 23.19 o
-3 0 2 12665.52 15474.72 261.31 o
-2 0 2 26416.79 27852.30 435.40 o
-1 0 2 6.51 163.20 11.25 o
0 0 2 81905.16 83048.59 2246.26 o
1 0 2 3619.91 5270.63 96.14 o
3 0 2 6551.69 7671.24 105.92 o
4 0 2 5797.14 6360.77 97.43 o
5 0 2 7467.06 7537.22 116.51 o
6 0 2 6814.94 6396.28 109.11 o
7 0 2 11.52 -25.31 24.83 o
8 0 2 1149.42 1061.42 51.82 o
9 0 2 113.01 67.10 62.75 o
10 0 2 932.80 1075.32 106.31 o
11 0 2 1777.42 1928.47 123.19 o
-12 1 2 57.68 43.33 68.59 o
-11 1 2 764.80 840.43 77.46 o
-10 1 2 149.12 209.42 51.75 o
-9 1 2 1420.52 1310.03 115.65 o
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