#------------------------------------------------------------------------------ #$Date: 2016-04-03 04:25:15 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181166 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/45/2224511.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2224511_Fobs loop_ _publ_author_name 'H\"okelek, Tuncer' 'Y\?ilmaz, Filiz' 'Tercan, Bar\?i\,s' '\"Ozbek, F. Elif' 'Necefo\(glu, Hacali' _publ_section_title ; Bis(\m-2-fluorobenzoato-1:2\k^2^O:O')(2-fluorobenzoato-1\k^2^O,O')(2-fluorobenzoato-2\kO)dinicotinamide-1\kN^1^,2\kN^1^-dizinc(II)--2-fluorobenzoic acid (1/1) ; _journal_coeditor_code XU2668 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1608 _journal_page_last m1609 _journal_volume 65 _journal_year 2009 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 92.929 _cell_angle_gamma 90.000 _cell_length_a 12.5143 _cell_length_b 16.7106 _cell_length_c 20.6673 _exptl_crystal_F_000 2176.00 _reflns_d_resolution_high 0.7495 _cod_data_source_file xu2668Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' el3 in P 21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 726.04 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 986.49 962.52 18.38 o 2 0 0 3511.25 4721.29 51.98 o 3 0 0 589.13 417.71 36.78 o 4 0 0 18758.50 20140.23 201.87 o 5 0 0 1134.34 1133.57 28.88 o 6 0 0 2192.16 1822.23 42.83 o 7 0 0 18.48 29.64 21.71 o 8 0 0 1052.11 936.33 40.91 o 9 0 0 4823.79 4724.75 92.10 o 10 0 0 2857.44 2702.02 74.69 o 11 0 0 8.20 39.03 33.31 o 12 0 0 18060.16 17135.68 293.25 o 13 0 0 11980.69 12396.59 300.86 o 14 0 0 3264.57 3775.51 165.55 o 15 0 0 825.66 987.00 109.59 o 16 0 0 782.58 671.61 148.57 o 1 1 0 11852.35 13199.46 115.80 o 2 1 0 76447.09 74180.58 471.27 o 3 1 0 2.70 -19.74 19.74 o 4 1 0 9551.84 8503.49 64.92 o 5 1 0 162.51 148.78 11.83 o 6 1 0 10798.91 12293.48 94.05 o 7 1 0 12385.26 13172.83 122.75 o 8 1 0 11.22 3.19 16.83 o 9 1 0 175.49 246.47 23.41 o 10 1 0 11018.55 10704.57 121.65 o 11 1 0 218.75 196.96 30.42 o 12 1 0 4428.41 4475.19 92.00 o 13 1 0 825.22 1005.47 79.33 o 14 1 0 2605.70 2553.04 101.39 o 15 1 0 136.51 231.29 61.62 o 16 1 0 2052.23 2319.10 193.09 o 0 2 0 188.22 180.41 15.92 o 1 2 0 3443.30 3671.17 48.16 o 2 2 0 9033.61 8514.44 80.95 o 3 2 0 18073.01 16726.18 109.23 o 4 2 0 3184.78 3019.15 29.73 o 5 2 0 2756.42 2531.78 30.45 o 6 2 0 218.50 246.52 14.59 o 7 2 0 7128.46 7629.39 70.26 o 8 2 0 1542.42 1535.97 35.51 o 9 2 0 1398.87 1459.51 38.12 o 10 2 0 10293.88 9828.37 109.41 o 11 2 0 651.10 576.03 36.87 o 12 2 0 1634.37 1585.87 64.99 o 13 2 0 740.92 694.81 63.42 o 14 2 0 1188.97 1213.14 81.95 o 15 2 0 3.47 163.06 58.79 o 16 2 0 2492.55 2715.08 167.73 o 1 3 0 1632.17 1483.36 30.08 o 2 3 0 23023.86 23383.29 241.33 o 3 3 0 1066.63 816.37 16.95 o 4 3 0 3146.26 2845.20 29.37 o 5 3 0 100.38 62.35 11.17 o 6 3 0 129.16 201.71 12.59 o 7 3 0 55.12 88.63 13.68 o 8 3 0 356.37 358.94 22.04 o 9 3 0 2565.26 2445.16 46.45 o 10 3 0 199.47 181.92 28.19 o 11 3 0 139.17 97.41 33.47 o 12 3 0 358.48 407.18 52.99 o 13 3 0 194.31 94.61 48.50 o 14 3 0 220.42 208.33 57.06 o 15 3 0 1.72 -11.30 79.65 o 16 3 0 18.35 119.68 71.23 o 0 4 0 46024.68 50331.25 868.30 o 1 4 0 31.22 -2.65 32.93 o 2 4 0 82893.30 83581.81 902.82 o 3 4 0 190.28 203.25 32.90 o 4 4 0 18134.63 18579.74 148.44 o 5 4 0 7992.82 7683.09 69.10 o 6 4 0 11063.76 12176.07 108.96 o 7 4 0 1515.74 1509.59 30.53 o 8 4 0 683.12 714.75 26.01 o 9 4 0 2805.47 2782.55 54.85 o 10 4 0 1620.35 1655.76 49.50 o 11 4 0 8020.42 8217.14 134.56 o 12 4 0 43.47 104.54 45.37 o 13 4 0 432.00 352.90 53.70 o 14 4 0 1570.25 1544.24 97.99 o 15 4 0 212.44 293.03 96.50 o 16 4 0 1296.58 1384.97 88.71 o 1 5 0 12297.78 12949.71 177.67 o 2 5 0 23935.65 23794.37 274.55 o 3 5 0 1775.11 2258.44 43.05 o 4 5 0 18020.13 18865.06 174.78 o 5 5 0 10221.02 10159.07 92.83 o 6 5 0 1657.99 1776.95 30.22 o 7 5 0 1650.65 1249.76 30.05 o 8 5 0 7544.25 7685.70 86.65 o 9 5 0 279.95 258.94 38.26 o 10 5 0 170.32 201.99 33.62 o 11 5 0 607.87 645.84 52.32 o 12 5 0 827.75 983.91 62.03 o 13 5 0 8.23 42.33 47.42 o 14 5 0 91.00 73.36 50.92 o 15 5 0 130.50 294.96 101.10 o 16 5 0 7.88 58.14 87.60 o 0 6 0 48324.18 49938.54 873.84 o 1 6 0 10588.95 10045.66 146.42 o 2 6 0 90830.98 90765.17 984.41 o 3 6 0 962.71 870.06 42.96 o 4 6 0 1480.28 1385.10 34.62 o 5 6 0 343.18 450.66 24.23 o 6 6 0 22618.54 22501.70 200.90 o 7 6 0 2913.97 2907.59 45.69 o 8 6 0 15385.25 14480.61 149.49 o 9 6 0 1295.18 1494.56 49.04 o 10 6 0 3544.70 3192.34 75.64 o 11 6 0 1430.12 1381.98 64.87 o 12 6 0 563.68 698.85 59.74 o 13 6 0 1375.20 1515.43 123.31 o 14 6 0 1576.24 1533.57 221.35 o 15 6 0 2058.18 2164.92 254.70 o 16 6 0 3103.99 2759.21 286.53 o 1 7 0 29719.80 29123.99 376.53 o 2 7 0 85.95 97.57 20.80 o 3 7 0 1449.72 1493.02 46.30 o 4 7 0 3221.02 3624.58 74.60 o 5 7 0 3979.45 3783.68 54.46 o 6 7 0 10.06 -14.19 14.19 o 7 7 0 9824.34 9444.07 90.45 o 8 7 0 16415.69 16073.77 177.22 o 9 7 0 11329.88 10847.72 186.42 o 10 7 0 8.60 36.55 50.70 o 11 7 0 168.63 151.23 82.54 o 12 7 0 691.98 776.15 151.23 o 13 7 0 2095.26 2438.46 252.04 o 14 7 0 1910.42 1883.69 233.47 o 15 7 0 1642.96 1719.20 233.47 o 0 8 0 73.20 113.66 53.06 o 1 8 0 2287.87 2229.43 53.73 o 2 8 0 12.69 53.69 19.31 o 3 8 0 600.26 418.68 30.38 o 4 8 0 6128.49 6104.33 104.35 o 5 8 0 2670.94 2493.11 48.01 o 6 8 0 11.45 18.02 16.14 o 7 8 0 144.18 167.72 21.78 o 8 8 0 1875.49 2043.53 58.44 o 9 8 0 1948.73 1876.25 76.57 o 10 8 0 5662.33 5676.55 215.72 o 11 8 0 3232.28 3484.64 323.68 o 12 8 0 447.71 557.77 102.72 o 13 8 0 210.64 217.55 153.88 o 14 8 0 467.62 419.19 169.80 o 15 8 0 536.65 668.58 201.63 o 1 9 0 1949.52 2125.50 56.06 o 2 9 0 5920.28 6191.37 100.06 o 3 9 0 17189.14 17982.51 230.67 o 4 9 0 2838.13 3016.80 74.00 o 5 9 0 239.73 294.87 35.53 o 6 9 0 1655.34 1737.91 49.17 o 7 9 0 109.39 154.09 29.75 o 8 9 0 1.83 21.88 38.53 o 9 9 0 12.52 25.10 41.43 o 10 9 0 5420.47 5324.56 211.96 o 11 9 0 65.71 47.76 86.30 o 12 9 0 53.99 201.63 137.96 o 13 9 0 72.99 90.20 143.27 o 14 9 0 11.24 5.31 153.88 o 15 9 0 137.50 153.88 175.10 o 0 10 0 2931.43 2893.18 106.49 o 1 10 0 2054.06 1931.93 57.91 o 2 10 0 7158.02 6951.69 111.52 o 3 10 0 116.97 89.49 25.76 o 4 10 0 3929.79 3987.23 85.86 o 5 10 0 947.19 831.70 54.19 o 6 10 0 176.96 198.30 35.90 o 7 10 0 40.32 69.78 33.30 o 8 10 0 2556.61 2562.18 81.99 o 9 10 0 347.68 455.23 70.30 o 10 10 0 535.56 470.13 104.86 o 11 10 0 1448.00 1761.65 206.94 o 12 10 0 116.55 84.90 143.27 o 13 10 0 642.85 599.60 180.41 o 14 10 0 1510.73 1432.67 233.47 o 1 11 0 2978.59 2996.44 73.59 o 2 11 0 886.61 896.58 42.03 o 3 11 0 2885.40 2834.22 70.10 o 4 11 0 18294.44 18164.07 280.31 o 5 11 0 1915.42 1831.36 74.99 o 6 11 0 5135.19 5053.59 126.38 o 7 11 0 3508.02 3484.69 117.65 o 8 11 0 1531.24 1622.25 68.07 o 9 11 0 1170.29 1122.44 78.55 o 10 11 0 1815.55 1820.02 201.63 o 11 11 0 467.17 525.31 153.88 o 12 11 0 1077.59 668.58 180.41 o 13 11 0 6.33 10.61 148.57 o 14 11 0 99.06 63.67 159.19 o 0 12 0 17386.98 16967.73 298.87 o 1 12 0 21.32 1.44 26.77 o 2 12 0 2487.51 2599.63 65.27 o 3 12 0 1281.59 1352.38 59.90 o 4 12 0 1118.20 1125.81 57.00 o 5 12 0 802.58 862.01 95.62 o 6 12 0 7358.23 7398.60 236.29 o 7 12 0 226.43 251.63 57.24 o 8 12 0 4115.90 4151.24 102.88 o 9 12 0 1607.56 1814.71 201.63 o 10 12 0 61.93 -68.98 122.04 o 11 12 0 399.89 382.04 153.88 o 12 12 0 2012.13 1804.10 233.47 o 13 12 0 119.85 127.35 164.49 o 14 12 0 194.23 68.98 175.10 o 1 13 0 14456.00 15481.95 217.98 o 2 13 0 5358.92 5120.13 104.86 o 3 13 0 912.44 821.86 52.96 o 4 13 0 1.31 11.67 51.03 o 5 13 0 303.39 217.55 78.79 o 6 13 0 1196.91 1163.65 116.13 o 7 13 0 6683.93 6732.68 298.71 o 8 13 0 1155.88 1069.83 103.47 o 9 13 0 1952.08 1745.73 206.94 o 10 13 0 369.29 275.92 143.27 o 11 13 0 3.44 -127.35 127.35 o 12 13 0 700.20 737.56 191.02 o 0 14 0 221.37 304.67 87.55 o 1 14 0 1959.67 2039.47 73.52 o 2 14 0 1482.59 1613.71 68.39 o 3 14 0 1995.45 2240.83 99.94 o 4 14 0 3609.58 3906.88 217.55 o 5 14 0 1682.43 1527.87 125.65 o 6 14 0 480.64 558.48 167.14 o 7 14 0 404.75 541.23 143.27 o 8 14 0 59.12 47.76 122.04 o 9 14 0 2475.52 2345.33 233.47 o 10 14 0 598.47 748.17 180.41 o 11 14 0 57.08 58.37 143.27 o 12 14 0 372.24 291.84 169.80 o 1 15 0 3949.62 3848.19 114.13 o 2 15 0 4802.55 4730.74 125.99 o 3 15 0 140.16 155.87 74.76 o 4 15 0 4243.08 4398.93 188.37 o 5 15 0 52.85 -71.70 76.85 o 6 15 0 711.41 626.13 148.57 o 7 15 0 39.37 -68.98 122.04 o 8 15 0 601.25 403.27 153.88 o 9 15 0 894.21 971.03 185.72 o 10 15 0 1126.15 1289.40 212.25 o 11 15 0 60.04 68.98 159.19 o 12 15 0 1310.30 1167.36 228.17 o 0 16 0 10.68 2.06 67.22 o 1 16 0 13.97 33.77 41.41 o 2 16 0 2857.32 2838.80 183.85 o 3 16 0 37.28 88.65 76.30 o 4 16 0 14.87 -38.25 80.60 o 5 16 0 527.36 504.09 143.27 o 6 16 0 1272.83 1326.54 191.02 o 7 16 0 0.75 21.22 127.35 o 8 16 0 75.34 84.90 137.96 o 9 16 0 274.13 281.23 159.19 o 10 16 0 12.85 122.04 164.49 o 11 16 0 52.58 84.90 164.49 o 1 17 0 539.52 687.46 70.12 o 2 17 0 1035.97 1182.33 119.89 o 3 17 0 4089.18 3915.89 189.45 o 4 17 0 2097.49 2228.59 217.55 o 5 17 0 207.93 376.74 148.57 o 6 17 0 291.55 275.92 148.57 o 7 17 0 1452.63 1883.69 228.17 o 8 17 0 97.27 -79.59 137.96 o 9 17 0 46.18 95.51 153.88 o 10 17 0 1056.88 689.80 201.63 o 0 18 0 339.46 442.37 98.95 o 1 18 0 142.42 107.32 62.14 o 2 18 0 217.97 182.27 73.92 o 3 18 0 1354.79 1411.44 191.02 o 4 18 0 521.39 461.64 159.19 o 5 18 0 1409.26 1167.36 196.33 o 6 18 0 1593.00 1820.02 228.17 o 7 18 0 77.85 79.59 148.57 o 8 18 0 172.75 159.19 164.49 o 9 18 0 1204.67 1220.42 222.86 o 1 19 0 4063.62 4167.95 216.98 o 2 19 0 52.96 54.93 95.18 o 3 19 0 582.73 684.50 175.10 o 4 19 0 184.87 196.33 153.88 o 5 19 0 846.76 960.42 196.33 o 6 19 0 6.99 -143.27 143.27 o 7 19 0 4146.91 4282.08 334.29 o 8 19 0 141.59 185.72 169.80 o 0 20 0 20.62 -122.04 122.04 o 1 20 0 110.88 135.59 156.53 o 2 20 0 15.17 -22.79 94.30 o 3 20 0 45.16 50.80 100.47 o 4 20 0 116.50 212.25 164.49 o 5 20 0 67.10 53.06 164.49 o 6 20 0 1797.21 2191.45 270.61 o 7 20 0 3.03 5.31 164.49 o 2 21 0 2777.18 3032.79 200.50 o 3 21 0 129.03 107.18 135.31 o 4 21 0 622.08 711.03 212.25 o 5 21 0 62.63 -84.90 164.49 o -16 1 1 99.85 233.95 98.03 o -15 1 1 1110.69 1220.61 104.93 o -14 1 1 2590.36 2674.39 112.56 o -13 1 1 319.48 362.91 47.43 o -12 1 1 5393.65 5330.00 100.26 o -11 1 1 1315.60 1295.41 47.46 o -10 1 1 4.07 26.72 23.32 o -9 1 1 6423.78 6371.65 75.10 o -8 1 1 3945.61 3866.99 53.20 o -7 1 1 11989.71 12003.80 108.76 o -6 1 1 64.77 99.02 12.96 o -5 1 1 3207.61 3254.56 34.38 o -4 1 1 8978.22 8137.90 64.85 o -3 1 1 254.14 130.48 26.29 o -2 1 1 41721.40 42336.50 270.48 o -1 1 1 55188.29 56642.45 424.66 o 0 1 1 461.12 493.47 16.57 o 1 1 1 32614.44 33813.25 245.25 o 2 1 1 147.21 100.84 6.53 o 3 1 1 781.09 579.20 23.31 o 4 1 1 1109.10 1256.36 20.94 o 5 1 1 2325.37 2176.34 28.96 o 6 1 1 262.43 151.30 13.98 o 7 1 1 15821.99 15840.42 131.30 o 8 1 1 6.18 10.33 17.46 o 9 1 1 13669.82 13571.77 129.20 o 10 1 1 3968.23 3832.20 77.71 o 11 1 1 724.52 679.26 37.83 o 12 1 1 291.87 325.87 39.37 o 13 1 1 5328.22 5148.68 113.38 o 14 1 1 1275.12 1235.50 78.69 o 15 1 1 1762.50 1926.42 95.82 o 16 1 1 198.50 228.25 123.31 o -16 2 1 2.04 44.08 71.67 o -15 2 1 832.60 954.11 121.49 o -14 2 1 3827.18 3595.46 114.27 o -13 2 1 2421.78 2319.97 91.42 o -12 2 1 2857.24 2914.64 75.67 o -11 2 1 505.28 520.16 40.07 o -10 2 1 3443.47 3442.75 57.64 o -9 2 1 1853.64 1736.14 52.82 o -8 2 1 6059.47 6149.53 69.89 o -7 2 1 3077.60 3239.37 40.59 o -6 2 1 1587.65 1865.87 31.18 o -5 2 1 2145.90 2209.59 27.66 o -4 2 1 10264.53 10344.91 76.89 o -3 2 1 6591.49 6453.24 45.38 o -2 2 1 16539.62 17081.67 154.57 o -1 2 1 807.04 776.84 17.85 o 0 2 1 36599.13 36084.95 626.45 o 1 2 1 16071.93 16361.90 168.54 o 2 2 1 18017.12 18154.88 150.64 o 3 2 1 148.72 133.92 20.23 o 4 2 1 9280.89 9017.01 66.32 o 5 2 1 820.55 851.28 18.52 o 6 2 1 1429.16 1492.28 26.43 o 7 2 1 1277.18 1302.92 29.53 o 8 2 1 1036.06 1082.18 31.64 o 9 2 1 7579.65 7195.74 83.03 o 10 2 1 9.18 1.47 23.48 o 11 2 1 691.25 628.61 38.30 o 12 2 1 1882.42 1909.79 72.25 o 13 2 1 392.88 390.12 57.51 o 14 2 1 3159.22 2919.84 108.37 o 15 2 1 531.48 685.70 71.05 o 16 2 1 0.60 146.60 91.14 o -16 3 1 661.01 772.95 80.42 o -15 3 1 359.47 453.23 88.08 o -14 3 1 44.04 124.85 52.61 o -13 3 1 2657.81 2734.12 98.49 o -12 3 1 5785.88 5536.27 125.77 o -11 3 1 5439.66 5319.71 96.15 o -10 3 1 21871.17 21148.16 219.65 o -9 3 1 3378.94 3325.62 52.16 o -8 3 1 3036.74 3069.71 46.14 o -7 3 1 609.73 690.68 20.32 o -6 3 1 18648.69 18170.12 126.21 o -5 3 1 1105.84 861.63 19.02 o -4 3 1 15238.25 14765.05 102.98 o -3 3 1 1689.93 1673.82 20.63 o -2 3 1 73805.13 72100.49 787.00 o -1 3 1 9258.14 8430.89 102.37 o 0 3 1 3034.87 2759.32 92.86 o 1 3 1 15255.94 14887.47 146.01 o 2 3 1 13254.34 13249.26 164.31 o 3 3 1 1993.49 1961.90 32.37 o 4 3 1 19048.63 17163.07 119.38 o 5 3 1 3724.44 3812.56 39.28 o 6 3 1 379.36 454.10 15.95 o 7 3 1 831.12 833.08 22.93 o 8 3 1 5224.35 5235.06 65.23 o 9 3 1 2560.24 2673.29 48.63 o 10 3 1 10638.67 10076.17 120.60 o 11 3 1 4767.85 4801.70 92.42 o 12 3 1 844.68 894.80 62.73 o 13 3 1 926.47 821.72 70.67 o 14 3 1 11.16 32.39 51.87 o 15 3 1 468.01 482.03 69.14 o 16 3 1 756.91 747.62 77.43 o -16 4 1 46.92 133.42 69.84 o -15 4 1 1191.41 1305.30 81.27 o -14 4 1 162.96 216.66 54.60 o -13 4 1 100.65 83.90 48.62 o -12 4 1 6119.68 6060.87 132.02 o -11 4 1 1711.63 1788.05 65.40 o -10 4 1 739.53 697.25 41.49 o -9 4 1 3800.11 3849.22 62.75 o -8 4 1 3.94 -15.52 15.52 o -7 4 1 2.55 1.81 13.01 o -6 4 1 11816.73 11404.42 87.38 o -5 4 1 3983.96 3799.18 41.69 o -4 4 1 2694.36 3126.33 33.61 o -3 4 1 28287.28 28893.06 272.40 o -2 4 1 65284.09 65893.88 716.44 o -1 4 1 13118.07 13548.35 180.15 o 0 4 1 3621.60 3562.45 89.81 o 1 4 1 1458.98 1510.14 35.04 o 2 4 1 4337.90 4219.15 71.59 o 3 4 1 3879.26 3768.89 43.21 o 4 4 1 3795.68 3985.47 45.02 o 5 4 1 9766.07 9488.07 82.68 o 6 4 1 1210.42 1169.65 25.01 o 7 4 1 664.88 629.48 20.53 o 8 4 1 213.88 166.22 20.22 o 9 4 1 6602.70 6220.42 84.61 o 10 4 1 1800.12 1742.98 51.90 o 11 4 1 304.03 292.42 40.85 o 12 4 1 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