#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/45/2224517.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2224517_Fobs loop_ _publ_author_name 'Xu, Ying-Ming' 'Gao, Shan' 'Ng, Seik Weng' _publ_section_title ; Bis(4-hydroxypyridinium) sulfate monohydrate ; _journal_coeditor_code XU2675 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3146 _journal_volume 65 _journal_year 2009 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 102.557 _cell_angle_gamma 90.000 _cell_length_a 7.1404 _cell_length_b 19.9797 _cell_length_c 9.5148 _exptl_crystal_F_000 640.00 _reflns_d_resolution_high 0.7712 _[local]_cod_data_source_file xu2675Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P21/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 237.78 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 3098.89 3136.08 37.18 o 4 0 0 914.14 885.97 10.42 o 6 0 0 371.03 432.95 7.36 o 8 0 0 240.23 252.62 6.15 o 1 1 0 4796.78 5127.26 43.15 o 2 1 0 21036.72 20306.98 245.60 o 3 1 0 305.40 292.89 3.41 o 4 1 0 1041.03 1078.09 9.17 o 5 1 0 710.74 717.86 7.33 o 6 1 0 168.88 177.86 3.47 o 7 1 0 93.45 95.64 3.18 o 8 1 0 44.30 43.18 2.71 o 9 1 0 0.42 -0.53 1.87 o 1 2 0 2117.90 2330.47 22.11 o 2 2 0 194.34 208.90 2.07 o 3 2 0 83.13 65.06 1.59 o 4 2 0 1258.05 1232.18 10.37 o 5 2 0 129.22 129.24 2.56 o 6 2 0 420.80 425.13 5.55 o 7 2 0 27.06 29.50 3.44 o 8 2 0 93.37 100.07 3.58 o 9 2 0 62.93 59.72 5.18 o 1 3 0 456.57 488.38 13.67 o 2 3 0 6041.22 6161.05 65.43 o 3 3 0 135.90 114.26 2.44 o 4 3 0 50.32 40.62 1.29 o 5 3 0 242.63 234.98 3.09 o 6 3 0 1325.51 1330.91 12.64 o 7 3 0 1.50 1.54 1.50 o 8 3 0 0.01 -0.06 1.96 o 0 4 0 6577.48 6447.51 84.16 o 1 4 0 3090.13 3150.79 24.86 o 2 4 0 139.58 137.34 1.25 o 3 4 0 8.20 19.09 1.26 o 4 4 0 526.25 524.87 5.68 o 5 4 0 172.37 182.73 4.21 o 6 4 0 9.34 11.99 1.91 o 7 4 0 176.51 178.85 3.86 o 8 4 0 13.79 14.36 2.54 o 1 5 0 104.17 81.02 1.61 o 2 5 0 444.23 328.83 5.03 o 3 5 0 160.48 129.01 1.38 o 4 5 0 87.52 96.11 1.65 o 5 5 0 78.31 81.24 2.36 o 6 5 0 452.18 459.57 6.02 o 7 5 0 6.29 5.44 1.04 o 8 5 0 29.35 29.60 1.63 o 0 6 0 12627.33 11742.97 196.09 o 1 6 0 809.24 819.36 10.70 o 2 6 0 1111.49 1133.39 30.57 o 3 6 0 0.19 1.44 0.44 o 4 6 0 224.21 227.56 2.38 o 5 6 0 68.98 80.16 2.19 o 6 6 0 69.34 70.72 2.60 o 7 6 0 214.51 200.83 3.44 o 8 6 0 181.37 176.56 4.81 o 1 7 0 2551.86 2626.36 18.45 o 2 7 0 149.59 141.94 1.52 o 3 7 0 107.78 117.27 1.20 o 4 7 0 0.51 0.29 0.57 o 5 7 0 1402.07 1376.26 11.83 o 6 7 0 11.83 10.47 0.88 o 7 7 0 1.08 0.31 0.74 o 8 7 0 42.45 39.76 5.86 o 0 8 0 2324.32 2373.35 26.14 o 1 8 0 2050.86 2505.58 20.57 o 2 8 0 64.24 68.49 0.88 o 3 8 0 367.43 341.81 4.29 o 4 8 0 658.75 670.35 5.38 o 5 8 0 22.61 25.37 1.20 o 6 8 0 118.83 117.96 2.20 o 7 8 0 107.39 111.28 2.74 o 8 8 0 73.04 71.51 3.31 o 1 9 0 467.21 468.10 3.74 o 2 9 0 1040.81 1170.15 11.40 o 3 9 0 856.00 859.96 7.26 o 4 9 0 980.01 1072.66 8.80 o 5 9 0 95.31 85.44 2.25 o 6 9 0 43.25 44.72 2.75 o 7 9 0 3.62 3.00 0.73 o 8 9 0 194.28 194.31 5.98 o 0 10 0 2125.48 2152.87 24.64 o 1 10 0 1239.26 1241.02 9.46 o 2 10 0 380.09 407.98 4.24 o 3 10 0 9.76 7.09 0.96 o 4 10 0 131.44 143.34 2.55 o 5 10 0 7.53 6.57 0.87 o 6 10 0 31.72 29.67 1.30 o 7 10 0 34.18 37.96 2.75 o 8 10 0 4.21 4.46 2.06 o 1 11 0 145.57 187.22 1.94 o 2 11 0 20.24 32.05 0.81 o 3 11 0 290.74 282.78 3.72 o 4 11 0 261.51 263.58 3.18 o 5 11 0 9.00 9.72 1.31 o 6 11 0 480.64 479.93 7.01 o 7 11 0 182.87 186.93 4.57 o 8 11 0 116.78 117.05 4.34 o 0 12 0 1.45 17.53 10.56 o 1 12 0 265.42 292.02 2.69 o 2 12 0 304.05 300.28 3.17 o 3 12 0 0.53 1.27 0.49 o 4 12 0 61.29 55.85 1.70 o 5 12 0 243.15 243.59 3.51 o 6 12 0 0.13 0.90 1.17 o 7 12 0 37.80 38.46 2.38 o 8 12 0 55.42 56.62 2.74 o 1 13 0 1418.28 1424.28 11.54 o 2 13 0 213.47 194.99 2.03 o 3 13 0 178.92 162.41 1.74 o 4 13 0 22.92 26.69 1.57 o 5 13 0 91.71 87.97 2.60 o 6 13 0 49.49 47.04 2.00 o 7 13 0 60.75 61.02 2.99 o 0 14 0 5455.69 5431.42 185.02 o 1 14 0 121.13 100.37 1.68 o 2 14 0 246.96 230.77 2.56 o 3 14 0 595.41 574.72 8.02 o 4 14 0 346.53 331.11 4.61 o 5 14 0 113.71 114.10 2.42 o 6 14 0 5.56 5.92 1.53 o 7 14 0 2.52 2.96 1.49 o 1 15 0 1.77 1.02 0.59 o 2 15 0 1612.58 1566.97 13.18 o 3 15 0 20.93 20.86 0.81 o 4 15 0 23.84 21.67 1.39 o 5 15 0 109.51 108.94 2.88 o 6 15 0 11.19 13.44 1.78 o 7 15 0 4.55 4.89 1.87 o 0 16 0 54.72 49.83 2.05 o 1 16 0 265.22 264.34 2.78 o 2 16 0 3.63 3.45 1.06 o 3 16 0 346.76 336.46 3.34 o 4 16 0 58.12 59.21 2.02 o 5 16 0 49.55 46.93 2.09 o 6 16 0 155.30 159.50 3.17 o 7 16 0 2.09 2.61 1.52 o 1 17 0 15.16 13.57 1.05 o 2 17 0 650.37 610.05 7.32 o 3 17 0 911.02 873.88 7.81 o 4 17 0 7.35 8.35 1.26 o 5 17 0 0.06 -0.03 0.94 o 6 17 0 182.51 192.63 3.51 o 0 18 0 1313.61 1195.79 16.91 o 1 18 0 546.67 515.39 4.47 o 2 18 0 327.99 318.91 3.91 o 3 18 0 0.16 0.81 0.53 o 4 18 0 146.00 143.44 2.62 o 5 18 0 29.64 31.09 2.15 o 6 18 0 83.86 81.34 2.60 o 1 19 0 77.61 77.88 1.62 o 2 19 0 33.30 30.81 1.35 o 3 19 0 64.36 56.61 1.28 o 4 19 0 2.37 1.00 1.08 o 5 19 0 34.26 33.32 2.49 o 6 19 0 47.48 50.10 2.95 o 0 20 0 54.89 47.21 2.17 o 1 20 0 40.30 40.71 1.40 o 2 20 0 6.38 4.56 0.85 o 3 20 0 40.23 35.37 1.57 o 4 20 0 532.33 511.44 5.71 o 5 20 0 7.51 4.81 1.68 o 1 21 0 23.14 24.99 2.09 o 2 21 0 258.71 233.86 3.14 o 3 21 0 172.32 167.36 5.27 o 4 21 0 0.04 0.47 1.07 o 5 21 0 63.93 65.05 2.35 o 0 22 0 21.44 25.37 3.95 o 1 22 0 5.31 4.75 0.88 o 2 22 0 26.22 23.54 1.16 o 3 22 0 104.33 110.59 2.78 o 4 22 0 185.82 209.55 3.49 o 1 23 0 82.80 77.50 2.23 o 2 23 0 462.33 502.11 8.28 o 3 23 0 2.96 2.26 1.57 o 4 23 0 70.77 77.89 2.43 o 0 24 0 5.79 7.09 1.34 o 1 24 0 26.04 28.56 1.50 o 2 24 0 17.45 16.77 2.93 o 3 24 0 45.34 41.74 2.23 o 1 25 0 0.07 1.34 0.99 o 2 25 0 95.06 96.04 3.99 o -9 0 1 19.04 21.49 3.38 o -7 0 1 463.90 463.17 8.45 o -5 0 1 697.51 648.75 17.60 o -3 0 1 112.26 84.11 2.28 o -1 0 1 4938.94 5331.00 63.92 o 1 0 1 582.19 604.70 9.32 o 3 0 1 771.04 869.62 19.18 o 5 0 1 1874.26 1893.76 44.56 o 7 0 1 273.46 263.16 5.64 o -9 1 1 11.67 12.69 2.36 o -8 1 1 77.74 73.14 3.01 o -7 1 1 150.07 153.25 3.71 o -6 1 1 1642.75 1659.79 15.74 o -5 1 1 0.04 0.00 0.82 o -4 1 1 74.73 82.01 1.63 o -3 1 1 1418.97 1507.85 11.94 o -2 1 1 1728.75 1834.28 14.30 o -1 1 1 869.07 945.77 5.40 o 1 1 1 1388.52 1495.31 26.93 o 2 1 1 3161.12 3145.77 25.53 o 3 1 1 586.26 546.25 5.52 o 4 1 1 23.50 24.65 1.25 o 5 1 1 226.20 221.29 3.34 o 6 1 1 518.44 516.60 5.64 o 7 1 1 40.67 42.16 2.49 o 8 1 1 0.25 -1.51 1.72 o -9 2 1 2.78 3.16 1.98 o -8 2 1 66.79 72.51 2.98 o -7 2 1 120.16 108.30 2.80 o -6 2 1 374.59 356.43 4.57 o -5 2 1 494.62 496.17 5.32 o -4 2 1 774.88 711.24 6.21 o -3 2 1 179.46 157.33 1.79 o -2 2 1 2642.07 2703.24 21.84 o -1 2 1 2485.11 2642.42 15.99 o 0 2 1 196.12 112.92 1.27 o 1 2 1 9148.91 9085.35 124.99 o 2 2 1 388.05 473.66 4.11 o 3 2 1 117.49 140.86 1.71 o 4 2 1 2678.52 2822.55 39.02 o 5 2 1 0.06 -0.31 1.04 o 6 2 1 577.48 552.52 6.29 o 7 2 1 69.54 60.77 2.65 o 8 2 1 71.00 76.72 3.20 o -9 3 1 4.99 5.55 1.54 o -8 3 1 75.34 73.36 2.73 o -7 3 1 64.00 66.47 2.36 o -6 3 1 7.12 7.68 1.52 o -5 3 1 767.85 749.49 7.43 o -4 3 1 254.35 286.59 3.36 o -3 3 1 1485.35 1388.84 10.92 o -2 3 1 2662.99 2892.46 20.99 o -1 3 1 4399.95 4624.05 42.52 o 0 3 1 50.07 55.87 0.59 o 1 3 1 233.70 239.87 2.15 o 2 3 1 784.26 776.23 6.47 o 3 3 1 3620.26 3696.97 53.10 o 4 3 1 539.66 570.07 5.80 o 5 3 1 539.89 510.93 5.93 o 6 3 1 4.20 4.42 1.52 o 7 3 1 26.33 28.42 2.93 o 8 3 1 30.45 33.94 2.94 o -9 4 1 5.57 6.42 1.87 o -8 4 1 32.25 33.50 1.82 o -7 4 1 3.63 2.94 1.01 o -6 4 1 33.64 29.34 1.98 o -5 4 1 343.10 340.42 5.11 o -4 4 1 318.37 313.63 2.86 o -3 4 1 333.76 335.65 2.47 o -2 4 1 245.63 301.07 2.38 o -1 4 1 4.35 4.78 0.51 o 0 4 1 8573.90 8881.84 109.13 o 1 4 1 1124.36 1103.65 21.81 o 2 4 1 852.93 874.90 10.48 o 3 4 1 2.45 2.14 0.85 o 4 4 1 437.42 398.94 4.71 o 5 4 1 0.13 0.95 1.78 o 6 4 1 102.26 89.95 2.64 o 7 4 1 6.87 6.77 1.74 o 8 4 1 47.51 51.46 2.90 o -9 5 1 48.88 44.79 3.15 o -8 5 1 0.16 0.42 1.01 o -7 5 1 125.20 133.50 2.44 o -6 5 1 398.39 396.83 4.48 o -5 5 1 859.73 812.42 6.92 o -4 5 1 7.63 9.09 1.48 o -3 5 1 1034.35 1118.82 10.57 o -2 5 1 117.05 128.64 1.16 o -1 5 1 2438.63 2538.37 17.41 o 0 5 1 471.19 490.71 4.05 o 1 5 1 4845.78 4951.03 43.25 o 2 5 1 1588.46 1666.44 17.56 o 3 5 1 73.15 57.71 1.39 o 4 5 1 224.05 194.08 2.74 o 5 5 1 783.33 732.97 8.44 o 6 5 1 96.15 100.99 2.74 o 7 5 1 77.81 84.79 3.00 o 8 5 1 44.02 48.88 3.94 o -8 6 1 0.38 -0.26 0.90 o -7 6 1 149.04 151.43 2.54 o -6 6 1 68.46 71.28 2.96 o -5 6 1 104.30 95.93 1.85 o -4 6 1 753.93 812.77 6.78 o -3 6 1 73.94 55.41 0.96 o -2 6 1 328.00 329.34 2.95 o -1 6 1 1014.60 892.10 6.27 o 0 6 1 445.89 455.73 3.31 o 1 6 1 770.15 859.83 8.02 o 2 6 1 3216.10 3558.74 40.32 o 3 6 1 0.37 1.88 0.60 o 4 6 1 180.98 206.18 2.57 o 5 6 1 238.49 238.59 4.09 o 6 6 1 345.68 354.79 5.04 o 7 6 1 442.75 440.41 7.04 o 8 6 1 0.56 0.38 1.85 o -8 7 1 82.24 81.17 2.55 o -7 7 1 2.97 3.11 1.39 o -6 7 1 211.52 204.39 3.02 o -5 7 1 488.25 472.52 4.50 o -4 7 1 958.08 987.39 7.97 o -3 7 1 19.76 16.65 0.84 o -2 7 1 533.87 622.17 4.56 o -1 7 1 950.87 1045.72 7.80 o 0 7 1 218.66 243.69 2.35 o 1 7 1 447.19 483.03 3.51 o 2 7 1 3870.50 4754.96 48.83 o 3 7 1 677.15 695.84 5.59 o 4 7 1 368.51 425.90 4.19 o 5 7 1 13.05 12.54 0.93 o 6 7 1 222.00 211.58 2.49 o 7 7 1 30.18 32.12 1.57 o 8 7 1 414.45 411.35 8.62 o -8 8 1 1.24 1.66 0.88 o -7 8 1 277.75 266.86 3.74 o -6 8 1 274.02 280.32 3.36 o -5 8 1 270.59 253.30 3.30 o -4 8 1 477.27 491.41 4.96 o -3 8 1 418.65 423.31 3.71 o -2 8 1 45.88 44.52 0.85 o -1 8 1 2867.04 3017.27 26.13 o 0 8 1 1833.88 2141.57 17.28 o 1 8 1 1584.17 1674.43 12.78 o 2 8 1 86.86 108.07 1.77 o 3 8 1 267.52 257.52 2.60 o 4 8 1 0.94 1.29 0.97 o 5 8 1 73.36 81.57 1.40 o 6 8 1 611.97 612.80 6.44 o 7 8 1 229.14 226.19 4.83 o 8 8 1 20.09 17.25 2.53 o -8 9 1 30.50 38.33 2.77 o -7 9 1 28.19 30.20 2.22 o -6 9 1 295.83 277.27 3.13 o -5 9 1 156.80 153.77 2.15 o -4 9 1 278.71 287.94 2.78 o -3 9 1 415.74 386.84 3.34 o -2 9 1 16.16 19.89 1.61 o -1 9 1 68.71 52.90 0.85 o 0 9 1 54.42 55.10 1.46 o 1 9 1 773.59 689.37 5.29 o 2 9 1 883.11 920.16 23.56 o 3 9 1 4.63 5.38 1.07 o 4 9 1 5.00 10.12 1.23 o 5 9 1 375.09 365.08 3.96 o 6 9 1 39.91 37.18 2.14 o 7 9 1 77.31 88.74 3.35 o 8 9 1 196.30 203.37 5.22 o -8 10 1 2.49 1.78 2.06 o -7 10 1 149.70 134.40 3.80 o -6 10 1 16.65 18.02 0.95 o -5 10 1 70.99 73.77 1.77 o -4 10 1 10.55 7.24 1.04 o -3 10 1 18.65 22.04 0.95 o -2 10 1 71.06 73.67 1.60 o -1 10 1 1063.37 1188.36 8.14 o 0 10 1 161.46 202.40 2.43 o 1 10 1 432.08 426.17 3.56 o 2 10 1 23.41 24.59 0.55 o 3 10 1 124.41 114.64 2.16 o 4 10 1 388.52 361.86 3.84 o 5 10 1 87.11 84.35 2.55 o 6 10 1 77.81 74.64 2.27 o 7 10 1 0.36 1.30 1.36 o 8 10 1 21.32 27.09 2.33 o -8 11 1 20.89 21.90 2.54 o -7 11 1 98.19 102.67 3.31 o -6 11 1 43.90 42.70 1.50 o -5 11 1 470.70 456.19 4.70 o -4 11 1 205.33 203.31 2.06 o -3 11 1 1.60 1.78 0.71 o -2 11 1 724.03 801.85 9.32 o -1 11 1 1319.32 1390.07 9.88 o 0 11 1 2.34 5.64 0.70 o 1 11 1 3416.20 3749.65 33.49 o 2 11 1 397.14 444.12 3.74 o 3 11 1 694.85 688.90 9.40 o 4 11 1 63.67 55.86 2.09 o 5 11 1 1157.43 1131.34 10.93 o 6 11 1 0.01 0.12 1.34 o 7 11 1 44.81 46.77 2.27 o -8 12 1 10.60 8.11 1.89 o -7 12 1 202.12 211.95 5.45 o -6 12 1 19.25 18.48 1.16 o -5 12 1 160.88 149.45 1.80 o -4 12 1 284.65 268.73 3.30 o -3 12 1 417.55 427.16 3.39 o -2 12 1 5.18 7.24 0.84 o -1 12 1 580.72 582.05 4.40 o 0 12 1 3633.00 4095.24 54.33 o 1 12 1 227.06 228.56 2.28 o 2 12 1 8.91 6.75 0.60 o 3 12 1 895.25 875.47 8.64 o 4 12 1 171.75 160.83 2.64 o 5 12 1 431.72 442.02 5.25 o 6 12 1 2.02 3.81 1.40 o 7 12 1 191.62 200.01 4.36 o -7 13 1 0.39 0.98 1.45 o -6 13 1 91.18 89.39 2.45 o -5 13 1 34.76 33.30 1.77 o -4 13 1 220.86 208.19 2.87 o -3 13 1 13.62 9.49 0.98 o -2 13 1 479.68 470.92 4.57 o -1 13 1 140.60 150.30 2.49 o 0 13 1 0.08 -0.67 0.67 o 1 13 1 54.53 60.92 1.27 o 2 13 1 180.00 167.16 3.88 o 3 13 1 90.26 84.83 2.71 o 4 13 1 9.52 11.68 1.17 o 5 13 1 46.03 42.24 1.99 o 6 13 1 56.71 57.50 2.12 o 7 13 1 3.15 2.43 1.73 o -7 14 1 143.02 148.62 3.54 o -6 14 1 64.88 58.39 2.24 o -5 14 1 262.85 260.83 3.77 o -4 14 1 6.48 5.56 1.19 o -3 14 1 105.52 109.95 1.73 o -2 14 1 0.11 0.05 0.59 o -1 14 1 542.84 554.14 7.40 o 0 14 1 45.42 46.56 1.31 o 1 14 1 111.34 121.78 2.14 o 2 14 1 14.93 17.73 0.81 o 3 14 1 400.80 399.73 4.63 o 4 14 1 6.67 6.99 1.11 o 5 14 1 160.15 160.57 2.76 o 6 14 1 61.19 59.74 2.18 o 7 14 1 98.14 96.22 3.01 o -7 15 1 9.54 12.03 1.81 o -6 15 1 368.39 356.87 5.43 o -5 15 1 15.73 13.36 1.59 o -4 15 1 16.00 13.67 1.29 o -3 15 1 140.72 136.48 1.98 o -2 15 1 40.30 47.14 1.98 o -1 15 1 95.83 86.74 1.50 o 0 15 1 48.92 46.82 1.29 o 1 15 1 270.48 263.45 2.84 o 2 15 1 455.84 421.08 3.74 o 3 15 1 112.80 109.98 2.41 o 4 15 1 206.93 199.31 3.72 o 5 15 1 219.63 206.93 3.71 o 6 15 1 154.81 143.74 3.24 o 7 15 1 29.21 30.93 2.37 o -7 16 1 0.04 0.66 1.35 o -6 16 1 74.69 76.61 2.65 o -5 16 1 159.53 158.27 2.90 o -4 16 1 545.28 500.44 5.54 o -3 16 1 18.59 20.21 1.25 o -2 16 1 241.42 245.95 2.79 o -1 16 1 199.68 208.59 2.28 o 0 16 1 470.61 522.81 5.80 o 1 16 1 285.91 290.35 3.16 o 2 16 1 1.03 1.74 0.79 o 3 16 1 62.72 58.22 1.83 o 4 16 1 1173.29 1102.78 14.67 o 5 16 1 0.03 0.34 1.00 o 6 16 1 33.11 30.12 2.10 o -6 17 1 10.81 7.42 2.13 o -5 17 1 76.08 78.69 2.25 o -4 17 1 147.47 154.58 2.70 o -3 17 1 834.27 827.84 7.78 o -2 17 1 814.61 887.75 7.77 o -1 17 1 1711.10 1713.55 13.33 o 0 17 1 639.30 619.83 6.03 o 1 17 1 256.32 284.17 3.42 o 2 17 1 299.74 244.20 2.80 o 3 17 1 582.34 544.30 7.64 o 4 17 1 61.89 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